CN106436362A - Tea-pigment-dyeing-liquid preparing method based on biological processing and bionic dyeing method for cellulosic fibers - Google Patents

Tea-pigment-dyeing-liquid preparing method based on biological processing and bionic dyeing method for cellulosic fibers Download PDF

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CN106436362A
CN106436362A CN201610819874.9A CN201610819874A CN106436362A CN 106436362 A CN106436362 A CN 106436362A CN 201610819874 A CN201610819874 A CN 201610819874A CN 106436362 A CN106436362 A CN 106436362A
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tea
pigment
dyeing
culture
bacterium
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CN106436362B (en
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巩继贤
任燕飞
娄江飞
王富邦
张健飞
李政
李秋瑾
李辉芹
吴洋彬
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Yuyue Home Textile Co Ltd
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Tianjin Polytechnic University
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/653—Nitrogen-free carboxylic acids or their salts
    • D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D06P1/67358—Halides or oxyhalides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D06P1/67375—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341 with sulfur-containing anions
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58—Material containing hydroxyl groups
    • D06P3/60—Natural or regenerated cellulose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02—After-treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02—After-treatment
    • D06P5/10—After-treatment with compounds containing metal

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

The invention relates to a tea-pigment-dyeing-liquid preparing method based on biological processing and a bionic dyeing method for cellulosic fibers. The tea-pigment-dyeing-liquid preparing method includes the steps that (1) flora in extra-strong tea is selected, efficient-using bacterial strains capable of converting tea pigment and functional compounds are screened with the ultraviolet mutagenesis and chemical mutagenesis method, and a tea pigment solution is fermented and prepared with the bacterial strains; (2) a certain amount of citric acid, a certain amount of vitamins, a certain amount of sodium sulfite, a certain amount of sodium hexametaphosphate and a certain amount of penetrating agent are added into the obtained tea pigment solution, the mixture is stirred for 5 min to 20 min at 1,000 rpm to 18,000 rpm, and tea-pigment dyeing liquid is obtained; (3) cotton fabric is soaked and rolled the tea-pigment dyeing liquid, two-time soaking and two-time rolling are carried out, the product is soaked and rolled color fixing liquid after being dried, the liquid rolling rate is 40% to 60%, and then the product is steamed for 1 min to 10 min and finally soaped and washed. By means of the tea-pigment-dyeing-liquid preparing method, combination of the tea natural function product on textiles is achieved, a bonding agent, a cross-linking agent and a mordant are not used in the process, and the tea-pigment-dyeing-liquid preparing method is environmentally friendly and low in cost, and has broad market prospects.

Description

Tea pigment dye liquor based on biological processing is prepared and to cellulose fibre Biomimetic Dyeing Method
Technical field
The present invention relates to a kind of method of fabric finishing processing is and in particular to by the natural colour in TIEGUANYIN stalky tea and tea dust Element and functional compounds are applied to the processing method on cellulose base fiber fabric, belong to dyeing and finishing process technology.
Technical background
Folium Camelliae sinensis are China's special advantage plant resourceses, and the oolong tea with Anxi Tieguanyin Tea as representative is even more well-known at home and abroad. In addition to the coloring matters such as thearubigins, abrownin, theaflavin, in Folium Camelliae sinensis, contain abundant natural function material.At present There are some researches show that the polyphenols in tea have preferable fungistatic effect, contained triterpenoid compound and tannin class chemical combination in tea Thing has stronger characteristic absorption to ultraviolet.
The leftover bits and pieces such as substantial amounts of stalky tea can be produced during Tea Processing, this is the preparation of natural pigment and functional mass Provide good raw material sources.The stalky tea leftover bits and pieces being formed in Tea Processing are developed, therefrom extracts natural function and become Point, for textile processing, the preparation for high-grade function textile provides new method, also for the comprehensive utilization of tea resources Provide new way.
It was noted that containing many natural pigment such as astaxanthins, carotenoid in many organisms, these pigments exist There are stable combination and suitable distribution in organism.The distribution of natural pigment and the mould being combined with ambient substance in organism We are carried out dyeing and finishing and are machined with important inspiration by formula.Distribution in organism for the natural pigment and and ambient can be used for reference Matter binding pattern is so that pigment and functional mass form stable combination and uniform distribution on fabric, for the dye of fabric Whole.
And, natural product institute is depended on to the chemical products with oil as raw material unduly using not only facilitating to alleviate The energy bringing and crisis of resource, and the pollution that chemical reagent produces and causes during using can be reduced.
The present invention is processed with the unqualified method of biological processing of TIEGUANYIN stalky tea and Folium Camelliae sinensis, is improved by bioconversion Dark brown cellulose content, and thus prepare tea pigment dye liquor, and then use for reference native compound being combined with material in organism and surely The fixed pattern existing it is proposed that the method to the bionical dyeing and finishing of cellulose fibre for the functional mass in tea pigment and tea,
Content of the invention
Tea pigment dye liquor based on biological processing of the present invention is prepared and to cellulose fibre Biomimetic Dyeing method, wraps Include：
(1) in take 5g TIEGUANYIN tea to put sodium phosphate buffer that 100ml concentration is 0.2～2g/L, 50 in conical flask ～250rpm vibrates 0.2～2h, takes supernatant rule on plating medium coating, flat board is upside down at 20～28 DEG C and cultivates 12～48h, in described plating medium, contains following composition in 1L culture medium：Agar 1～2%, peptone 10g, yeast extracts Thing 5g, NaCl 10g, pH 5.0～7.0；
(2) respectively TIEGUANYIN stalky tea and TIEGUANYIN fannings are pulverized, TIEGUANYIN tea powder is mixed and made into 1: 2 ratio, is used for Prepared by culture medium；
(3) to the bacterium colony obtaining after the culture of step (1) middle plateform, picking different shape bacterium colony is placed in Selective agar medium, After culture 24～48h, take supernatant, detect absorbance at λ=363nm, absorbance highest bacterium is selected, described selection In culture medium, in 1L culture medium, contain following composition：Tea powder 0.01～2g/L prepared by step (2), peptone 10g, yeast carries Take thing 5g, NaCl 10g, pH 5.0～7.0；
(4) bacterium selecting step (3) is accessed in fermentation medium and cultivates to exponential phase, pipettes 5ml bacterium solution to straight Footpath is in the culture dish of 9cm, and power is that Burdick lamp pipe distance 30cm of 15W irradiates 5～20min, after the 8-24h that keeps in Dark Place, It is transferred in fermentation medium and cultivates to exponential phase, taking bacterium solution 5ml to add lithium chloride to make its concentration is 0.1～1.5%, protects Warm 0.5-10min, after centrifuge washing, bacterium is transferred in fermentation medium and cultivates to exponential phase, takes bacterium solution to train in flat board Line coating on foster base, flat board is upside down in culture 12～48h at 20～28 DEG C, and the bacterium colony choosing maximum proceeds to fermentation medium Middle culture, in described fermentation medium, contains following composition in 1L culture medium：Peptone 10g, yeast extract 5g, NaCl 10g, pH 5.0～7.0；
(5) made for step (2) tea powder is added in fermentation medium, make tea powder concentration be 0.5～5g/L, obtain tea powder training Foster base, the bacterium selected by step (4) is cultivated in the fermentation medium to logarithmic (log) phase, accesses tea powder with 5～20% inoculum concentration In culture medium, 180～250rpm, 22～28 DEG C, cultivate 24～72h, supernatant is collected by centrifugation, filter, obtain biological prepare dark brown Plain solution；
(6) citric acid 0-2g/L, vitamin C 0-6g/L, sodium sulfite are added in the pigment solution that step (5) is obtained 0-5g/L, sodium hexameta phosphate 0-3g/L, sodium chloride 0-50g/L and penetrating agent JFC 0-5g/L, 1000～18000rpm stirring 5～ 20min, obtains tea pigment dye liquor；
(7) bafta is padded the tea pigment dye liquor that step (6) obtains, two leachings two are rolled, then pick-up rate 30-80% will Fabric drying；
(8) the textile pad fixation liquid obtaining step (7), two leachings two are rolled, and pick-up rate is 40-60%, then decatize 1- 10min, arrangement 0.5-5g/L containing soap powder and sodium carbonate 0-2g/L soaped in liquid, the 20-50 DEG C of 2-10min that soaps, then Wash 1-3min at 20-50 DEG C, wash 1-3min at room temperature.
The present invention will be processed as the TIEGUANYIN stalky tea of garbage and the unqualified method of biological processing of Folium Camelliae sinensis, passes through Bioconversion improves dark brown cellulose content, and thus prepares tea pigment dye liquor, so use for reference native compound in organism with Material combine and stable existence pattern it is proposed that the tea pigment and functional mass method to the bionical dyeing and finishing of cellulose fibre, plus Cellulose base fiber fabric after work not only achieves dyeing, is provided with antibacterial and anti-ultraviolet function simultaneously.The method achieve The combination on the textile of natural function product, in the process not using binding agent and cross-linking agent and the matchmaker containing heavy metal ion The materials such as stain, decrease the use of chemical assistant and the consumption of the energy, whole process ecological, environmental protective, are that cleaning is processed Journey, and easily operated, with low cost.The natural materials function textile being produced with the method, is using natural product as arrangement Agent, not using Harmful chemicals during arrangement, is the Green Textiles meeting ecological criteria, in the present focusing on green product My god, have wide market prospect.
Specific embodiment
Prepare and to cellulose fibre Biomimetic Dyeing method for the tea pigment dye liquor based on biological processing for the present invention, adopt Following manner is embodied as.But embodiment not limited to this of the present invention.
Embodiment 1
(1) 5g TIEGUANYIN tea is taken to put in the sodium phosphate buffer for 0.3g/L for the 100ml concentration, 150rpm in conical flask Vibration 2h, takes supernatant rule on plating medium coating, flat board is upside down at 28 DEG C and cultivates 24h, plating medium one-tenth It is divided into：Agar 15g/L, peptone 10g/L, yeast extract 5g/L, NaCl 10g/L, pH 7.0.
(2) respectively TIEGUANYIN stalky tea and TIEGUANYIN fannings are pulverized, TIEGUANYIN tea powder is mixed and made into 1: 2 ratio, is used for Prepared by culture medium；
(3) to the bacterium colony obtaining after the culture of step (1) middle plateform, picking different shape bacterium colony is placed in Selective agar medium, After culture 24～48h, take supernatant, detect absorbance at λ=363nm, absorbance highest bacterium is selected, described selection In culture medium, in 1L culture medium, contain following composition：Tea powder 1g/L prepared by step (2), peptone 10g, yeast extract 5g, NaCl 10g, pH 7.0；
(4) bacterium selecting step (3) is accessed in fermentation medium and cultivates to exponential phase, pipettes 5ml bacterium solution to straight Footpath is in the culture dish of 9cm, and power is that Burdick lamp pipe distance 30cm of 15W irradiates 5min, after the 12h that keeps in Dark Place, is transferred to Cultivate in fermentation medium to exponential phase, taking bacterium solution 5ml to add lithium chloride to make its concentration is 0.2%, is incubated 5min, centrifugation After washing, bacterium is transferred in fermentation medium and cultivates to exponential phase, take bacterium solution to rule on plating medium coating, will Flat board is upside down in culture 24h at 28 DEG C, and the bacterium colony choosing maximum proceeds to culture in fermentation medium, in described fermentation medium, Following composition is contained in 1L culture medium：Peptone 10g, yeast extract 5g, NaCl 10g, pH 7.0；
(5) made for step (2) tea powder is added in fermentation medium, makes tea powder concentration be 4g/L, obtain tea powder culture medium, Bacterium selected by step (4) is cultivated in the fermentation medium to logarithmic (log) phase, accesses in tea powder culture medium with 8% inoculum concentration, 200rpm, 28 DEG C, cultivates 48h, supernatant is collected by centrifugation, filter, obtain and biological prepare tea pigment solution.
Embodiment 2
Citric acid 1g/L, vitamin C 2g/L, sodium sulfite 1.5g/L, six inclined phosphorus will be added in the tea pigment obtaining solution Sour sodium 1.5g/L, sodium chloride 10g/L and penetrating agent JFC 0.5g/L, 10000rpm stirs 5min, obtains tea pigment dye liquor；
Embodiment 3
Bafta is padded tea pigment dye liquor, two leachings two are rolled, and pick-up rate 70%, then by fabric drying.After drying Textile pad fixation liquid, two leachings two are rolled, and pick-up rate is 70%, and then decatize 3min, by arrangement 3g/L containing soap powder and sodium carbonate 2g/L soaps in liquid, 50 DEG C of 5min that soap, and then washes 2min at 40 DEG C, washes 2min at room temperature.

Claims (2)

1. a kind of tea pigment dye liquor preparation method of biological processing is it is characterised in that comprise the following steps：
(1) in take 5g TIEGUANYIN tea to be placed in sodium phosphate buffer that 100ml concentration is 0.2～2g/L, 50 in conical flask～ 250rpm vibrates 0.2～2h, takes supernatant rule on plating medium coating, and flat board is upside down in culture 12 at 20～28 DEG C ～48h；
In described plating medium, in 1L culture medium, contain following composition：Agar 1～2%, peptone 10g, yeast extract 5g, NaCl 10g, pH 5.0～7.0；
(2) respectively TIEGUANYIN stalky tea and TIEGUANYIN fannings are pulverized, TIEGUANYIN tea powder is mixed and made into 1: 2 ratio, for cultivating Prepared by base；
(3) to the bacterium colony obtaining after the culture of step (1) middle plateform, picking different shape bacterium colony is placed in Selective agar medium, culture After 24～48h, take supernatant, detect absorbance at λ=363nm, absorbance highest bacterium is selected；
In described Selective agar medium, in 1L culture medium, contain following composition：Tea powder 0.01～2g/L prepared by step (2), albumen Peptone 10g, yeast extract 5g, NaCl 10g, pH 5.0～7.0；
(4) bacterium that step (3) is selected is accessed in fermentation medium and cultivate to exponential phase, pipette 5ml bacterium solution extremely a diameter of In the culture dish of 9cm, power is that Burdick lamp pipe distance 30cm of 15W irradiates 5～20min, after the 8-24h that keeps in Dark Place, transfer Cultivate to exponential phase to fermentation medium, taking bacterium solution 5ml to add lithium chloride to make its concentration is 0.1～1.5%, insulation 0.5-10min, after centrifuge washing, bacterium is transferred in fermentation medium and cultivates to exponential phase, takes bacterium solution to cultivate in flat board Line coating on base, flat board is upside down in culture 12～48h at 20～28 DEG C, and the bacterium colony choosing maximum proceeds in fermentation medium Culture；
In described fermentation medium, in 1L culture medium, contain following composition：Peptone 10g, yeast extract 5g, NaCl 10g, PH 5.0～7.0；
(5) made for step (2) tea powder is added in fermentation medium, make tea powder concentration be 0.5～5g/L, obtain tea powder culture Base, the bacterium selected by step (4) is cultivated in the fermentation medium to logarithmic (log) phase, accesses tea powder training with 5～20% inoculum concentration In foster base, 180～250rpm, 22～28 DEG C, cultivates 24～72h, supernatant is collected by centrifugation, filter, obtain and biological prepare tea pigment Solution；
(6) citric acid 0-2g/L, vitamin C 0-6g/L, sodium sulfite 0-5g/ are added in the pigment solution that step (5) is obtained L, sodium hexameta phosphate 0-3g/L, sodium chloride 0-50g/L and penetrating agent JFC 0-5g/L, 1000～18000rpm stirring 5～ 20min, obtains tea pigment dye liquor.
2. the method to cellulose fibre Biomimetic Dyeing for the tea pigment dye liquor of the biological processing described in a kind of usage right requirement 1, It is characterized in that, comprise the following steps：
(1) bafta is padded the tea pigment dye liquor that claim 1 step (6) obtains, two leachings two are rolled, pick-up rate 30-80%, so Afterwards by fabric drying；
(2) the textile pad fixation liquid obtaining step (1), two leachings two are rolled, and pick-up rate is 40-60%, then decatize 1- 10min, arrangement 0.5-5g/L containing soap powder and sodium carbonate 0-2g/L soaped in liquid, the 20-50 DEG C of 2-10min that soaps, then Wash 1-3min at 20-50 DEG C, wash 1-3min at room temperature.
CN201610819874.9A 2016-09-12 2016-09-12 Tea Pigment dye liquor based on biological processing prepares and to cellulose fibre Biomimetic Dyeing method Active CN106436362B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107476085A (en) * 2017-09-19 2017-12-15 天津工业大学 A kind of cotton fiber Tea Pigment native staining method based on bioconversion
CN109881506A (en) * 2019-02-27 2019-06-14 天津工业大学 Indigo mud separates Alcaligenes strain and dyes to the biological reducing of vegetable indigo
CN114921112A (en) * 2022-06-09 2022-08-19 青岛大学 Preparation method and application of pure water system bacterial dye prodigiosin nano suspension dye liquor

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CN103741495A (en) * 2014-01-03 2014-04-23 天津工业大学 Bionic finishing technique for treating cotton fabric by adopting natural functional substances of extra-strong tea stems
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CN103757894A (en) * 2013-12-31 2014-04-30 天津工业大学 Method for preparing natural antibacterial and anti-ultraviolet functional finishing agent with Tieguanyin tea stalks
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107476085A (en) * 2017-09-19 2017-12-15 天津工业大学 A kind of cotton fiber Tea Pigment native staining method based on bioconversion
CN109881506A (en) * 2019-02-27 2019-06-14 天津工业大学 Indigo mud separates Alcaligenes strain and dyes to the biological reducing of vegetable indigo
CN114921112A (en) * 2022-06-09 2022-08-19 青岛大学 Preparation method and application of pure water system bacterial dye prodigiosin nano suspension dye liquor
CN114921112B (en) * 2022-06-09 2024-01-05 青岛大学 Preparation method and application of pure water system bacterial dye prodigiosin nano suspension dye solution

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