CN106434064A - Transparent soap internally provided with fresh algae, as well as preparation method of transparent soap - Google Patents

Transparent soap internally provided with fresh algae, as well as preparation method of transparent soap Download PDF

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Publication number
CN106434064A
CN106434064A CN201610861897.6A CN201610861897A CN106434064A CN 106434064 A CN106434064 A CN 106434064A CN 201610861897 A CN201610861897 A CN 201610861897A CN 106434064 A CN106434064 A CN 106434064A
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transparent soap
phase
seaweed
new fresh
extract
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CN106434064B (en
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付晓婷
刘楠楠
许加超
高昕
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Ocean University of China
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Ocean University of China
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06Inorganic compounds
    • C11D9/08Water-soluble compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/265Organic compounds, e.g. vitamins containing oxygen containing glycerol
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/267Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/30Organic compounds, e.g. vitamins containing nitrogen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/40Proteins
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/444Dyes; Pigments

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  • Chemical & Material Sciences (AREA)
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  • Organic Chemistry (AREA)
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  • Animal Behavior & Ethology (AREA)
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  • Cosmetics (AREA)

Abstract

The invention belongs to the technical field of daily cosmetics, and in particular relates to transparent soap internally provided with fresh algae, as well as a preparation method of the transparent soap. The transparent soap comprises any one of or a combination of more of algae extracts, fresh algae and natural algae pigment. The natural algae pigment is obtained by extracting one or more of brown algae, red algae and green algae. The weight percentage of the algae extracts is 5 percent to 30 percent. The transparent soap is practical, beautiful, moisturized, nutritional, natural and non-irritant, and is truly environment-friendly transparent soap. The preparation method provided by the invention is scientific and reasonable, simple and practical in process, low in production cost and suitable for industrialized production.

Description

A kind of transparent soap of built-in new fresh seaweed and preparation method thereof
Technical field
The invention belongs to daily cosmetics technical field is and in particular to a kind of transparent soap of built-in new fresh seaweed.
Background technology
Development with entire society and growth in the living standard, people's also more and more higher of the requirement to cleaning products, special Be not the security of product it is desirable to this kind of detergent product has good cleaning effect, require to skin not damaged simultaneously again. Traditional soap, cleaning force is good, but pH value is universal higher (pH=9-11), and excitant is larger, and attractive in appearance poor with moisture retention, therefore beautiful See the practical marine alga transparent soap again having natural moisture preserving concurrently to be liked by people.
Transparent soap is the big species in soap, highlights the quality of product, pure, attractive in appearance and senior with its transparency, Increasingly obtain liking of consumer.Presently commercially available transparent soap typically adds substantial amounts of artificial essence, colouring agent, preservative Deng the activity substance content of skin care is few, and is that color is dull mostly, the problems such as rare interpolation inner matter.China's marine algae resource is rich Richness, wherein have economic worth there are about kind more than 100.Protein needed by human, fat, carbohydrate, many is contained in marine alga Plant vitamin and mineral matter, rich in nutritive value.New fresh seaweed, marine algae extract and marine alga pigment are added to energy in transparent soap Preferably nursing skin, plays cleaning nutrition, moist effect attractive in appearance.
The present invention is directed to the shortcoming of prior art, by attaching marine algae extract, improves chemicals and preservative Stimulation, the natural colouring matter that built-in new fresh seaweed adding extracts from marine alga itself makes it safe, attractive in appearance and practical, and auxiliary adds Plus sodium alginate, allantoin, jasmine extract and apple extract etc., strengthen its nourishing and moisturizing, nontoxic non-stimulated effect.
Content of the invention
In order to solve above-mentioned technical problem, the technical solution used in the present invention is as follows:It is former that the present invention is directed to product on the market The problems such as material chemicals content is many, it is poor to moisten trophism, sight is poor, provide a kind of transparent soap of built-in new fresh seaweed, no Artificial color, preservative, and the marine alga transparent soap of built-in marine alga, interpolation marine alga active component and natural colouring matter, have reality attractive in appearance With, cleaning maintenance effect.
For solving above-mentioned technical problem, the invention provides marine alga transparent soap, its bulk drug includes marine algae extract, fresh In marine alga, natural seaweed pigment any one or several combinations.
Wherein, above-mentioned natural seaweed pigment is to obtain from one of brown alga, red algae, green alga or several extraction.
Wherein, the percentage by weight of above-mentioned marine algae extract is 5%-30%.
Preferably, present invention additionally comprises the composition of following percentage by weight:Jasmine extract 0.5%-3%, apple extract Liquid 0.5%-3%.
Wherein, the preparation process of described marine algae extract is as follows:(1), after marine alga being rinsed well, dry, pulverize to obtain algae Powder;
(2) 1g algae powder is mixed with the distilled water of 10-200mL, vibrate 6-24h at 30-60 DEG C;
(3) step (2) concussion liquid is centrifuged 15min under rotating speed 4000r/min, removes bottom precipitation, obtain liquid Marine algae extract sample.
Wherein, the preparation process of described natural seaweed pigment is as follows:After fresh marine alga is cleaned up, with 1-3 times Deionized water is soaked, smashs to pieces, is vibrated 10-48h, takes out, filter out residue, obtain natural seaweed after ultrasonically treated 30-120min Pigment.
The present invention also provides a kind of preparation method of the transparent soap of built-in new fresh seaweed, comprises the following steps:
(1) successively by propane diols 6%-20%, glycerine 10%-30%, surfactant 0%-10%, stearic acid 10%- 20%th, palmitic acid 1%-10%, myristic acid 2%-10%, laurate 0.1%-10%, basic grease 0%-30% are in 70-90 DEG C heating, be allowed to be completely dissolved, obtain A phase;
(2) NaOH 1%-8%, sugared 1%-10%, alcohol 1%-8%, citric acid are sequentially added in another container 0.1%-5%, deionized water 5-20% dissolve at 70-75 DEG C, obtain B phase;
(3) by sodium alginate 0.1%-2%, allantoin 0.1%-2%, jasmine extract 0.5%-3%, apple extract 0.5%-3%, marine algae extract 5%-30% are mixed to get C phase;
(4) B is added in A phase, after saponification 20-100min at 70-85 DEG C, cools to 60 DEG C, add C phase, then Add 0.01%-3% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly Pour soap lye into in mould, wait the hardening rear demoulding to be cooled;
(5), after placing 3-7 days at aeration-drying, get product.
Wherein, described surfactant is sodium lauroyl sarcosine, cocounut oil acyl glycine potassium and cocamidopropyl propyl amide beet One or several combination in alkali, described basic grease is coconut oil, Sweet Almond Oil, olive oil, palm oil and evening primrose One or several combination in oil.
Preferably, a kind of preparation method of the transparent soap of above-mentioned built-in new fresh seaweed, further comprising the steps of:
(1) successively by propane diols 6%, glycerine 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitic acid 1%, meat Myristic acid 4%, laurate 2%, coconut oil 4%, olive oil 4% heat at 70-90 DEG C, are allowed to be completely dissolved, obtain A phase;
(2) NaOH 4%, sugar 4%, alcohol 2%, citric acid 1%, deionized water are sequentially added in another container 18.5% dissolves at 70-75 DEG C, obtains B phase;
(3) sodium alginate 0.1%, allantoin 0.3%, jasmine extract 0.5%, apple extract 0.5%, marine alga are carried Thing 10% is taken to be mixed to get C phase;
(4) B is added in A phase, after saponification 20min at 70-85 DEG C, cools to 60 DEG C, add C phase, add 0.1% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly in mould Pour soap lye into, wait the hardening rear demoulding to be cooled;
(5), after placing 3 days at aeration-drying, get product.
The invention has the advantages that:
The built-in new fresh seaweed of transparent soap that the present invention produces, adds natural seaweed pigment, can prepare containing new fresh seaweed and The various marine alga transparent soap of color, with attractive in appearance and practical feature.The present invention contains tangleweed extract, comprises many Phenol, polysaccharide, protein etc., and add marine alga natural pigment, without chemical preservative and artificial color, there is nutrition moist, warm With non-stimulated effect it is adaptable to the crowd of different sexes, age and skin quality.The present invention is practical and attractive, moisture-keeping nutrient, natural nothing Stimulate, be the marine alga transparent soap of a real environmental protection.Preparation method of the present invention is scientific and reasonable, simple for process, produces Low cost, suitable industrialized production.
Specific embodiment
The present invention is directed to the shortcoming of prior art, by attaching marine algae extract, improves chemicals and preservative Stimulation, the natural colouring matter that built-in new fresh seaweed adding extracts from marine alga itself makes it safe, attractive in appearance and practical, and auxiliary adds Plus sodium alginate, allantoin, jasmine extract and apple extract etc., strengthen its nourishing and moisturizing, nontoxic non-stimulated effect.
Below according to by embodiment, the present invention will be described in detail.
Specific embodiment:
Embodiment 1:
1. group cost implementation marine alga transparent soap composition and its percentage by weight are:
A phase:Propane diols 6%, glycerine 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitic acid 1%, nutmeg Acid 4%, laurate 2%, coconut oil 4%, olive oil 4%;
B phase:NaOH 4%, sugar 4%, alcohol 2%, citric acid 1%, deionized water 18.5%;
C phase:Sodium alginate 0.1%, allantoin 0.3%, jasmine extract 0.5%, apple extract 0.5%, marine alga carry Take thing 10%;
2. technical process:
(1) successively by propane diols 6%, glycerine 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitic acid 1%, meat Myristic acid 4%, laurate 2%, coconut oil 4%, olive oil 4% heat at 75 DEG C, are allowed to be completely dissolved, obtain A phase;
(2) sequentially add 4% in another container, sugar 4%, alcohol 2%, citric acid 1%, deionized water 18.5% be 75 Dissolve at DEG C, obtain B phase;
(3) sodium alginate 0.1%, allantoin 0.3%, jasmine extract 0.5%, apple extract 0.5%, marine alga are carried Thing 10% is taken to be mixed to get C phase;
(4) B is added in A phase, after saponification 20min at 70 DEG C, after cooling to 60 DEG C, adds C phase, add 0.1% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly in mould Pour soap lye into, wait the hardening rear demoulding to be cooled;
(5) after placing 3 days at aeration-drying, you can use.
The preparation method of the marine algae extract in above-mentioned:
(1) after sargassum fusifome being rinsed well, dry, pulverize to obtain algae powder, 1g algae powder is mixed with the water of 20mL, keep Temperature, at 30 DEG C, is extracted 24 hours under oscillating condition.
(2) step (2) concussion liquid is centrifuged 15min under rotating speed 4000r/min, removes bottom precipitation, obtain marine alga Extract.
In above-mentioned, the selecting of built-in new fresh seaweed:
Fresh sargassum fusifome sterile pure water is somewhat cleaned, and after keeping free from admixture, somewhat drying makes dry tack free, chooses breakage Blade it is ensured that overall appearance, put into stand-by in superclean bench.
In above-mentioned, the extraction of natural seaweed pigment:
After fresh sargassum fusifome is cleaned up, soaked, smash to pieces, vibrated 12h with 1 times of deionized water, with ultrasonically treated Take out after 30min, filter out residue, obtain natural brown alga pigment.
Embodiment 2:
1. group cost implementation marine alga transparent soap composition and its percentage by weight are:
A phase:Propane diols 10%, glycerine 15%, cocounut oil acyl glycine potassium 5%, sodium lauroyl sarcosine 2%, coconut oleoyl amine CAB 2%, stearic acid 4%, palmitic acid 1%, myristic acid 2%, laurate 3%, coconut oil 6%, olive oil 4%, Sweet Almond Oil 4%;
B phase:NaOH 6%, sugar 8%, alcohol 5%, citric acid 2%, deionized water 6.4%;
C phase:Sodium alginate 0.2%, allantoin 0.1%, jasmine extract 1%, apple extract 1%, marine algae extract 12%;
2. technical process:
(1) successively by propane diols 10%, glycerine 15%, cocounut oil acyl glycine potassium 5%, sodium lauroyl sarcosine 2%, cocounut oil Amido propyl betaine 2%, stearic acid 4%, palmitic acid 1%, myristic acid 2%, laurate 3%, coconut oil 6%, olive oil 4%th, Sweet Almond Oil 4% heats at 70 DEG C, is allowed to be completely dissolved, obtains A phase;
(2) NaOH 6%, sugar 8%, alcohol 5%, citric acid 2%, deionized water are sequentially added in another container 6.4% dissolves at 70 DEG C, obtains B phase;
(3) by sodium alginate 0.2%, allantoin 0.1%, jasmine extract 1%, apple extract 1%, marine algae extract 12% is mixed to get C phase;
(4) B is added in A phase, after saponification 20min at 85 DEG C, after cooling to 60 DEG C, adds C phase, add 0.3% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly in mould Pour soap lye into, wait the hardening rear demoulding to be cooled;
(5) after placing 5 days at aeration-drying, you can use.
The preparation method of the marine algae extract in above-mentioned:
(1) after tawny daylily algae being rinsed well, dry, pulverize to obtain algae powder, 1g algae powder is mixed with the water of 100mL, keep Temperature, at 60 DEG C, is extracted 24 hours under oscillating condition.
(2) it is centrifuged 15min under the conditions of 4000r/min, obtain marine algae extract.
In above-mentioned, the selecting of built-in new fresh seaweed:
New fresh laver sterile pure water is somewhat cleaned, and after keeping free from admixture, somewhat drying makes dry tack free, chooses breakage Blade, it is ensured that overall appearance, is put into stand-by in superclean bench.
In above-mentioned, the extraction of natural seaweed pigment:
After respectively fresh seaweed, tawny daylily algae being cleaned up, soaked, smash to pieces, vibrated 36h with 1 times of deionized water, with surpassing Take out after sonication 30min, filter out residue, obtain the natural seaweed pigment of natural red algae, brown alga pigment.
Embodiment 3:
1. form marine alga transparent soap composition of the present invention and its percentage by weight is:
A phase:Propane diols 10%, glycerine 10%, cocounut oil acyl glycine potassium 6%, sodium lauroyl sarcosine 2%, stearic acid 5%th, palmitic acid 5%, myristic acid 1%, laurate 3%, olive oil 4%, Sweet Almond Oil 4%;
B phase:NaOH 5%, sugar 4%, alcohol 5%, citric acid 4%, deionized water 8.2%;
C phase:Sodium alginate 0.1%, allantoin 0.2%, jasmine extract 0.5%, apple extract 2%, marine alga are extracted Thing 20%;
2. technical process:
(1) by propane diols 10%, glycerine 10%, cocounut oil acyl glycine potassium 6%, sodium lauroyl sarcosine 2%, stearic acid 5%th, palmitic acid 5%, myristic acid 1%, laurate 3%, olive oil 4%, Sweet Almond Oil 4% heat at 70 DEG C, are allowed to complete Dissolving, obtains A phase;
(2) NaOH 5%, sugar 4%, alcohol 5%, citric acid 4%, deionized water are sequentially added in another container 8.2% dissolves at 70 DEG C, obtains B phase;
(3) sodium alginate 0.1%, allantoin 0.2%, jasmine extract 0.5%, apple extract 2%, marine alga are extracted Thing 20% is mixed to get C phase;
(4) B is added in A phase, after saponification 100min at 75 DEG C, after cooling to 60 DEG C, adds C phase, add 1% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly fall in mould Enter soap lye, wait the hardening rear demoulding to be cooled;
(2) after placing 7 days at aeration-drying, you can use.
3. the preparation method of marine algae extract:
(1) after sea grape being rinsed well, dry, pulverize to obtain algae powder, 1g algae powder is mixed with the water of 50mL, keep Temperature, at 40 DEG C, is extracted 24 hours under oscillating condition.
(2) it is centrifuged 15min under the conditions of 4000r/min, obtain sample.
4. the selecting of built-in new fresh seaweed:
Fresh sea grape is somewhat cleaned with sterile pure water, and after keeping free from admixture, somewhat drying makes dry tack free, chooses breakage Blade it is ensured that overall appearance, put into stand-by in superclean bench.
5. the extraction of natural seaweed pigment:
After respectively fresh sea grape, Yi Guzao, sargassum fusifome being cleaned up, soaked, smashed to pieces with 2 times of deionized waters, Vibration 12h, with taking out after ultrasonically treated 60min, filters out residue, obtains natural green-alga, red algae, the extract of brown alga pigment.
Embodiment 4, the quality evaluation of above-described embodiment
1. using effect test:By the product of above-mentioned preparation, it is respectively issued to 15 tester's contrasts and uses.Tester It is carried out in the same manner during using sample, every kind of sample respectively uses 2 weeks.Tester according to oneself feel commented Point.Standards of grading take ten point system, and 1 point worst, and 10 points best, and fraction more high effect is more good.
2. foaming power and foam stability test:Reference《The preparation of gentle foam mildy wash and its performance study》In reality Proved recipe method, not Pei Zhi weight/mass percentage composition be 10% each product solution 3mL, be placed in 50mL tool plug graduated cylinder, plus distilled water is dilute Release to 15mL, add a cover, acutely concussion 10 times, immediate record foam volume (mL), record foam volume again after 10min.Repeat Measure 3 times, average.
3. organoleptic indicator:According to《QB/T 1913-2004 transparent soap》Soap body outward appearance and smell method of testing test.
4. transparency detection:Reference《The moulding mechanism of transparent (translucent) soap and production method》, using standard visual acuity chart (GB11533), to have twenty-twenty vision, corresponding five points of minimum " E " word of standard logarithmic visual acuity chart are seen in person's range estimation clearly to transparency Score value (L) represents, the more big then transparency of L value is better, and when L >=5.0 are translucent soap, L >=5.3 are transparent soap.
5. experimental result:
5.1 cleaning force tests:
5.2 foaming powers and foam stability test:
Index Initial volume (mL) Volume (mL) after 10min
Embodiment 1 41.01 38.01
Embodiment 2 45.00 35.01
Embodiment 3 38.49 31.65
5.3 organoleptic indicator:According to《QB/T 1913-2004 transparent soap》Soap body outward appearance and smell method of testing test.
Index Soap body outward appearance Smell
Embodiment 1 Color quality is homogeneous, transparency is good Meet regulation odor type
Embodiment 2 Color quality is homogeneous, transparency is good Meet regulation odor type
Embodiment 3 Color quality is homogeneous, transparency is good Meet regulation odor type
5.4 transparency detections:
Above-mentioned test result shows, the built-in new fresh seaweed of the transparent soap in the present invention, and color is various, existing general perfumed soap Cleaning force, have the aesthetical properties of transparent soap again, also have effect of nourishing and moisturizing concurrently, preparation method is simple, pollution is few, be a kind of The practical transparent soap of environmental protection, nutrition.
The above, be only highly preferred embodiment of the present invention, not the present invention is made with any pro forma restriction, appoints What those of ordinary skill in the art, without departing under technical solution of the present invention ambit, using in the method for the disclosure above Hold and technical solution of the present invention is made with many possible variations and modification, belong to the scope of claims protection.

Claims (9)

1. a kind of transparent soap of built-in new fresh seaweed it is characterised in that:Including marine algae extract, new fresh seaweed, natural seaweed color Any one in element or several combinations.
2. as claimed in claim 1 a kind of transparent soap of built-in new fresh seaweed it is characterised in that:Described natural seaweed pigment is Obtain from one of brown alga, red algae, green alga or several extraction.
3. as claimed in claim 1 a kind of transparent soap of built-in new fresh seaweed it is characterised in that:Described marine algae extract weight Percentage is 5%-30%.
4. as claimed in claim 1 a kind of transparent soap of built-in new fresh seaweed it is characterised in that:Also include following weight percent The composition of ratio:Jasmine extract 0.5%-3%, apple extract 0.5%-3%.
5. as claimed in claim 1 a kind of transparent soap of built-in new fresh seaweed it is characterised in that:The system of described marine algae extract Standby process is as follows:(1), after marine alga being rinsed well, dry, pulverize to obtain algae powder;
(2) 1g algae powder is mixed with the distilled water of 10-200mL, vibrate 6-24h at 30-60 DEG C;
(3) step (2) concussion liquid is centrifuged 15min under rotating speed 4000r/min, removes bottom precipitation, obtain liquid alga Extract sample.
6. as claimed in claim 1 or 2 a kind of transparent soap of built-in new fresh seaweed it is characterised in that:Described natural seaweed color The preparation process of element is as follows:After fresh marine alga is cleaned up, soaked, smash to pieces, vibrated 10- with 1-3 times of deionized water 48h, takes out after ultrasonically treated 30-120min, filters out residue, obtain natural seaweed pigment.
7. the transparent soap of a kind of built-in new fresh seaweed as described in claim 1 to 6 preparation method it is characterised in that:Including Following steps:
(1) successively by propane diols 6%-20%, glycerine 10%-30%, surfactant 0%-10%, stearic acid 10%-20%, Palmitic acid 1%-10%, myristic acid 2%-10%, laurate 0.1%-10%, basic grease 0%-30% add at 70-90 DEG C Heat, is allowed to be completely dissolved, and obtains A phase;
(2) NaOH 1%-8%, sugared 1%-10%, alcohol 1%-8%, citric acid are sequentially added in another container 0.1%-5%, deionized water 5%-20% dissolve at 70-75 DEG C, obtain B phase;
(3) by sodium alginate 0.1%-2%, allantoin 0.1%-2%, jasmine extract 0.5%-3%, apple extract 0.5%-3%, marine algae extract 5%-30% are mixed to get C phase;
(4) B is added in A phase, after saponification 20-100min at 70-85 DEG C, cools to 60 DEG C, add C phase, add 0.01%-3% natural seaweed pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly to mould Pour soap lye in tool, wait the hardening rear demoulding to be cooled;
(5), after placing 3-7 days at aeration-drying, get product.
8. as claimed in claim 6 a kind of preparation method of the transparent soap of built-in new fresh seaweed it is characterised in that:Described surface Activating agent is one or several group in sodium lauroyl sarcosine, cocounut oil acyl glycine potassium and Cocoamidopropyl betaine Close, described basic grease is one or several group in coconut oil, Sweet Almond Oil, olive oil, palm oil and evening primrose oil Close.
9. as claimed in claim 6 a kind of preparation method of the transparent soap of built-in new fresh seaweed it is characterised in that:Including following Step:
(1) successively by propane diols 6%, glycerine 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitic acid 1%, nutmeg Acid 4%, laurate 2%, coconut oil 4%, olive oil 4% heat at 70-90 DEG C, are allowed to be completely dissolved, obtain A phase;
(2) NaOH 4%, sugar 4%, alcohol 2%, citric acid 1%, deionized water 18.5% are sequentially added in another container Dissolve at 70-75 DEG C, obtain B phase;
(3) by sodium alginate 0.1%, allantoin 0.3%, jasmine extract 0.5%, apple extract 0.5%, marine algae extract 10% is mixed to get C phase;
(4) B is added in A phase, after saponification 20min at 70-85 DEG C, cools to 60 DEG C, add C phase, add 0.1% day So marine alga pigment, reverse mould after stirring, first the new fresh seaweed cleaned is put into mold bottom, slowly in mould, pour soap into Liquid, waits the hardening rear demoulding to be cooled;
(5), after placing 3 days at aeration-drying, get product.
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CN102978048A (en) * 2012-11-16 2013-03-20 广州伊凡生物科技有限公司 Weakly acidic transparent soap and preparation method thereof
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