CN106418688A - Preparation method of aroma releasing gel fiber filter rod - Google Patents
Preparation method of aroma releasing gel fiber filter rod Download PDFInfo
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- CN106418688A CN106418688A CN201610823103.7A CN201610823103A CN106418688A CN 106418688 A CN106418688 A CN 106418688A CN 201610823103 A CN201610823103 A CN 201610823103A CN 106418688 A CN106418688 A CN 106418688A
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- Prior art keywords
- fragrant
- preparation
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- liquid
- gel
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0225—Applying additives to filter materials with solid additives, e.g. incorporation of a granular product
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/40—Fibres of carbon
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to a preparation method of an aroma releasing gel fiber filter rod. The preparation method comprises the steps of blend fiber powder preparation, balsam preparation, aroma releasing gel preparation, soaking, mixing, shaping and the like. Compared with the prior art, the aroma releasing gel blend fiber filter rod is stable in aroma releasing effect and lasting in aroma keeping. In the suction process, due to the fact that the dosage of gel is low, the gel is easy to dissolve, aroma releasing of fiber particles is convenient, the effect is stable, and meanwhile, aroma releasing is uniform in the whole suction process.
Description
【Technical field】
The invention belongs to tobacco technology manufacture field.More particularly it relates to a kind of release fragrant gelatinous fibre filter stick
Preparation method.
【Background technology】
With reaching its maturity of perfuming cigarette technique, filter stick perfuming process becomes the primary study side of tobacco productive corporation
To.Meanwhile, countries tobacco general bureau adheres to Medicated cigarette low tar trend always, and for tobacco leaf production enterprise, flavouring mends fragrant technology
Particularly critical.However, cigarette shreds section perfuming process can be produced high temperature by Medicated cigarette in burning restricted, this high temperature meeting again
The characteristic chicken flavor that flavouring mends fragrant technology imparting is led to change.Therefore, low temperature releases fragrant technology, and that is, filter stick perfuming technology is current
Overcome the important technical of high temperature aromatizing technology defect.
Filter stick perfuming technology is broadly divided into capsule, fragrant line, granule etc. at present.Cigarette capsule is released fragrant technology and is tended at present
Ripe, but its intensity index awaits improving, and capsule intensity is low, and rupture leakage is fragrant, leads to capsule filter stick yield rate low；Capsule intensity
Height leads to release fragrant difficulty；And it is relatively costly.Granule releases perfume and fragrant line is released perfume and be there is a problem of that guarantor's perfume lasting is poor simultaneously.Glue simultaneously
Capsule carries the fragrant essence that can only select decanoyl/octanoyl glycerides and carries out dripping.It is the another short of this technology that capsule wall material meets water dissolution
Plate.
CN 105595417 discloses the preparation method that fragrant filter stick released by a kind of wire gel.This method is firstly the need of use
Substantial amounts of gel, under the suction temperatures of about 60 DEG C of cigarette filter rod section, gel can not dissolve out completely, the flavoring substances of interpolation
Releasing perfume (or spice) will be insufficient, leads to perfume quantity not enough, and will increase more complicated equipment to realize spray on tow for the gel
Penetrate technique.
For prior art defect, the present inventor on the basis summarizing prior art, by lot of experiments with
Analysis, completes the present invention finally.
【Content of the invention】
[technical problem to be solved]
It is an object of the invention to provide a kind of preparation method releasing fragrant gelatinous fibre filter stick.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of preparation method releasing fragrant gelatinous fibre filter stick.
The step of this preparation method is as follows：
A, the preparation of blend fibre powder
Blend fibre line is processed through crush-cutting, pulverizing, screening and decontamination, obtains blend fibre powder；
B, fragrant liquid preparation
Using pure water or decanoyl/octanoyl glycerides solvent and Pericarpium Citri Reticulatae flavor confect obtain a kind of concentration be by weight 12～
18% fragrant liquid；
C, release the preparation of fragrant gel
Allow carrageenan, Polyethylene Glycol, sodium alginate, agar and water according to weight ratio 0.2～1.5：5～8：0.1～0.2：
0.1～0.2：0.1～0.2 mixed preparing obtains a kind of coagulant liquid, is then added on, toward in described coagulant liquid, the perfume (or spice) that step B obtains
Liquid, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is immersed in the fragrant liquid that step B obtains, separates and obtain releasing perfume (or spice)
Blend fibre powder；
E, mixture
Under conditions of 40～60 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant solidifying
Glue is according to weight ratio 1.5～2.0：0.3～0.8 stirring mixing, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, through opium pipe molding, hardens, obtains described releasing
Fragrant gel blend fibre filter stick.
According to another kind of preferred implementation of the present invention, in step, the size of described blend fibre line powder is 0.2
～1.2mm.
According to another kind of preferred implementation of the present invention, in stepb, described Pericarpium Citri Reticulatae spice Fructus actinidiae chinensiss spice,
Folium Bambusae spice or osmanthus spice replace.
According to another kind of preferred implementation of the present invention, in step C, carrageenan, Polyethylene Glycol, sodium alginate, fine jade
The stirring under conditions of 40～60 DEG C of temperature of fat and water mixes 0.3～1.0 hour.
According to another kind of preferred implementation of the present invention, in step C, described coagulant liquid with described perfume liquid weight ratio
It is 0.8～1.2：0.4～0.6.
According to another kind of preferred implementation of the present invention, in step D, described blend fibre powder soaks in fragrant liquid
0.5～1.0 hour.
According to another kind of preferred implementation of the present invention, in step E, described releases fragrant blend fibre powder and releases fragrant coagulating
Glue stirring mixing 0.5～1.0 hour.
According to another kind of preferred implementation of the present invention, in step F, on the developed surface of whole diacetate fiber, institute
State release fragrant gel blend fibre powder amount be every millimeter of filter stick be 1.4～1.6mg.
The present invention is described in more detail below.
The present invention relates to a kind of preparation method releasing fragrant gelatinous fibre filter stick.
The step of this preparation method is as follows：
A, the preparation of blend fibre powder
Blend fibre line is processed through crush-cutting, pulverizing, screening and decontamination, obtains blend fibre powder；
Described blend fibre is that a kind of safety, intensity is high, toughness is strong, the most suitable load perfume base material of multiple-void structure.
If using other base materials, the starch plantses granule of the drying that for example bonds, soak carry perfume during can lead to granule loose,
Because strength problem can not meet preparation method of the present invention after fragmentation, and drying.
The blend fibre line that the present invention uses is finished product blend fibre line, and such as Caulis et Folium Lini is mixed with cotton blend line, silkworm silk and cotton
Spin, carbon fiber and cotton blend line.They are all the products sold in the market, for example, had by Wuxi City natural textile industry
The cotton ramie blended spinning line that limit company is sold with trade name cotton ramie blended spinning line, by Dongguan City Yue Xiong Fabritex S.r.l with trade name silkworm
The silk cotton union twist yarn that silk flosssilk wadding union twist yarn is sold.
In the present invention, using conventional knife, described blend fibre line is cut into the line segment of a length of 1.0～1.5cm, this
Kind line segment reuses common pulverizer and is pulverized, and with conventional screen screening, collects the line that fiber size is 0.2～1.2mm
Section, obtains blend fibre powder.Meanwhile, the color of blend fibre line can be selected according to actual requirement.
In the present invention, if described blend fibre powder be smaller in size than 0.2mm, because the internal diacetate fiber of filter stick is deposited
In gap, fiber powder is undersized to have the potential safety hazard sucking human lung；If the size of described blend fibre powder is more than
, then there is fiber crossovers, overlapping situation in 1.2mm in nipping process, lead to skewness impact aspiration procedure releases perfume (or spice)
Amount.Therefore, the size of described blend fibre powder is rational for 0.2～1.2mm.
B, fragrant liquid preparation
Using pure water or decanoyl/octanoyl glycerides solvent and Pericarpium Citri Reticulatae flavor confect obtain a kind of concentration be by weight 12～
18% fragrant liquid；
According to the present invention, according to actual needs, can be replaced with Fructus actinidiae chinensiss spice, Folium Bambusae spice or osmanthus spice described
Pericarpium Citri Reticulatae spice.
Pericarpium Citri Reticulatae spice, Fructus actinidiae chinensiss spice, Folium Bambusae spice or osmanthus spice that the present invention uses are all to sell in the market
Product, the Pericarpium Citri Reticulatae spice for example sold with trade name Pericarpium Citri Reticulatae spice by Shanghai oasis source spice company limited.
In the present invention, the concentration as fruital liquid is less than 12%, then impact Pericarpium Citri Reticulatae is fragrant not enough, and suction is inconspicuous；As fruital
The concentration of liquid is higher than 18%, then can be excessive because of Pericarpium Citri Reticulatae perfume quantity, the harmony of the overall flue gas of impact.Therefore, fragrant liquid concentration is
12～18% is suitable.
C, release the preparation of fragrant gel
Allow carrageenan, Polyethylene Glycol, sodium alginate, agar and water according to weight ratio 0.2～1.5：5～8：0.1～0.2：
0.1～0.2：0.1～0.2 mixed preparing obtains a kind of coagulant liquid, is then added on, toward in described coagulant liquid, the perfume (or spice) that step B obtains
Liquid, is uniformly mixed, and obtains described releasing fragrant gel；
In the present invention, Main Function in preparing coagulant liquid for the carrageenan is as a kind of thickening agent, adjusts coagulant liquid
Mobility, it has certain bond effect simultaneously.
Main Function in preparing coagulant liquid for the Polyethylene Glycol is as a kind of mushy stage transformational substance, and Polyethylene Glycol is permissible
It is solid-state when less than 40 DEG C, dissolves for liquid during higher than 40 DEG C, liquid releases perfume (or spice), solid-state lock is fragrant.
Main Function in preparing coagulant liquid for the sodium alginate is dispersant, and the blend fibre powder of mixing is uniformly dispersed
In coagulant liquid.
Main Function in preparing coagulant liquid for the agar is to adjust gel solid state intensity and setting rate.
In the present invention, when other amounts of components are in described scope, if the consumption of carrageenan is less than 0.2, coagulate
Glue mobility is very good, during vinegar fine entrance at a high speed opium pipe mouth, can affect the dispersed of fiber grain powder；If the use of carrageenan
Amount is more than 1.5, then coagulant liquid viscosity during bonding is excessive, and impact roller is in vinegar fibre face Painting effect；Therefore, the use of carrageenan
It is suitable for measuring as 0.2～1.5.
When other amounts of components are in described scope, if the consumption of Polyethylene Glycol is less than 5, liquid condition is converted to
The effect of solid-state is poor, is unfavorable for that coagulant liquid solid-state lock is fragrant；If the consumption of Polyethylene Glycol is more than 8, Medicated cigarette temperature filter tip temperature
40～60 DEG C can not be fully by solid state transformed for liquid；Therefore, the consumption of Polyethylene Glycol is 5～8 to be appropriate.
When other amounts of components are in described scope, if the consumption of sodium alginate is less than 0.1, blend fibre granule
Powder can produce precipitation it is impossible to dispersed in coagulant liquid, and impact roller non-uniform phenomenon in coating process；If Sargassum
The consumption of sour sodium is more than 0.2, then because coagulant liquid is excessively sticky, be unfavorable for the scattered uniformity of blend fibre powder；Therefore, Sargassum
The consumption of sour sodium is 0.1～0.2 to be feasible.
When other amounts of components are in described scope, if the consumption of agar is less than 0.1, coagulant liquid is changed by liquid
Slow, the coagulant liquid solid-state effect insufficient strength for process during solid-state, impact lock is fragrant；If the consumption of agar is more than 0.2, filter stick
In solid gel dissolve in temperature 60 C that effect is bad to produce floccule it may appear that dissolving insufficient, fragrant effect is released in impact
Really；Therefore, the consumption of agar is rational for 0.1～0.2.
Preferably, the weight ratio of carrageenan, Polyethylene Glycol, sodium alginate and agar is 0.4～1.2：5.8～7.2：0.12
～0.18：0.12～0.18.
It is highly preferred that the weight ratio of carrageenan, Polyethylene Glycol, sodium alginate and agar is 0.6～0.8：6.2～6.8：
0.14～0.16：0.14～0.16.
Preferably, the stirring under conditions of 40～60 DEG C of temperature of carrageenan, Polyethylene Glycol, sodium alginate, agar and water is mixed
Close 0.3～1.0 hour.
In the present invention, described coagulant liquid and the weight ratio of described perfume liquid are 0.8～1.2：0.4～0.6.If coagulant liquid
Exceed this scope with the weight ratio of fragrant liquid, the performance releasing fragrant gel will be produced with harmful effect, such as coagulant liquid and fragrant liquid weight
Amount ratio is 0.7:0.3, the fragrant liquid measure containing in gel is not enough, and fragrant amount released by gel after dissolving insufficient, if coagulant liquid and fragrant liquid
Weight is than for 1.2:0.7, then fragrant liquid excessive addition in coagulant liquid, gel is released perfume and is measured excessive, the association of the overall flue gas of impact after dissolving
Tonality.
D, immersion
At room temperature, the blend fibre powder that step A obtains is immersed in the fragrant liquid that step B obtains, separates and obtain releasing perfume (or spice)
Blend fibre powder；
The main purpose soaked in this step is to allow fragrant liquid to penetrate in blend fibre powder, so that blend fibre powder is had
The fragrance of spice contained by fragrant liquid.
Described blend fibre powder soak time in fragrant liquid is 0.5～1.0 hour.Time too short or oversize obviously all
It is unfavorable.
E, mixture
Under conditions of 40～60 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant solidifying
Glue is according to weight ratio 1.5～2.0：0.3～0.8 stirring mixing, obtains one kind and releases fragrant gel blend fibre powder；
According to the present invention, releasing fragrant blend fibre powder and release fragrant gel stirring the main purpose mixing is in the vinegar fibre table launching
Face can uniformly disperse and bond, and when preventing vinegar fibre from rapidly entering opium pipe mouth, blend fibre powder is assembled or dropped, and impact dispersion is all
Even property.
In this step, described release fragrant blend fibre powder and release fragrant gel and stir under conditions of 40～60 DEG C of temperature
Mixing 0.5～1.0 hour.
Temperature during stirring mixing is critically important.If temperature is less than 40 DEG C, carrageenan, agar dissolving are insufficient,
With the presence of floccule, mix uneven；If temperature is higher than 60 DEG C, because of filter stick, under cigarette smoking state, temperature is less than 60
DEG C, impact coagulant liquid and blend fibre powder release perfume (or spice)；Therefore, temperature during stirring mixing is 40～60 DEG C is appropriate.
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, through opium pipe molding, hardens, obtains described releasing
Fragrant gel blend fibre filter stick.
The filter-stick forming device that the present invention uses is the equipment being usually used in technical field of tobacco processing, such as by Shen Feiyan
The ZL22A type filter-stick forming device that machine factory is sold with trade name fibrous filter candle forming machine.
According to the present invention, on the developed surface of whole diacetate fiber, the described amount releasing fragrant gel blend fibre powder is every milli
Rice filter stick is 1.4～1.6mg.
If it exceeds the scope of this amount is all worthless, because the addition releasing fragrant gel blend fibre powder is less than
1.4mg/mm filter stick, filter stick perfuming amount is not enough, releases fragrant effect poor, if addition is more than 1.6mg/mm, because perfuming is excessive, shadow
Ring the harmony of flue gas.
The present invention prepare a kind of at 40～60 DEG C of temperature heat of solution be liquid, and discharge the fragrant gel of releasing of fragrance and mix
Spin fibrous filter candle.Because being wrapped in inside gel, in solid, shaped, fragrance preserves persistently filter stick internal fiber granule at room temperature.
When cigarette shreds burning, additional suction, about 40～60 DEG C of main flume temperature can be through filter stick inlet port chamber, now in filter stick
Gelatinous fibre can be released fragrant fiber grain and separated with the gel layer wrapping up its outer layer by solid state transformed for liquid, releases fragrant fiber release
Go out fragrance, reach flavouring, mend fragrant effect.The present invention releases fragrant gel blend fibre filter stick and can hold perfume (or spice) for a long time, also solves simultaneously
Stable and uniform releases this technical problem of perfume.
[beneficial effect]
The invention has the beneficial effects as follows：Compared with prior art, the present invention releases fragrant gel blend fibre filter stick and releases fragrant effect
Stable, hold fragrant long.In aspiration procedure, because amount of gel is low, gel is easy to dissolve, and facilitates fiber grain to release perfume (or spice), effect is steady
Fixed, whole aspiration procedure releases perfume uniformly simultaneously.
【Brief description】
【Specific embodiment】
Will be better understood that the present invention by following embodiments.
Embodiment 1：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.0cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 0.2mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Obtain the fragrant liquid that a kind of concentration is by weight 15% using decanoyl/octanoyl glycerides solvent and Pericarpium Citri Reticulatae flavor confect；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 0.4 according to weight：6.2：0.1：0.1：0.1 mixing
Preparation obtains a kind of coagulant liquid, then according to coagulant liquid compares 0.8 with the weight of fragrant liquid：0.5, it is added on step toward in described coagulant liquid
The fragrant liquid that rapid B obtains, is uniformly mixed, obtain described in release fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.5 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of 40 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.5 according to weight：0.4 stirring mixing 0.6 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.4mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 2：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.2cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 0.4mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Obtain the fragrant liquid that a kind of concentration is by weight 12% using decanoyl/octanoyl glycerides solvent and Fructus actinidiae chinensiss flavor confect；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 1.2 according to weight：6.8：0.2：0.1：0.2 mixing
Preparation obtains a kind of coagulant liquid, then according to coagulant liquid compares 1.2 with the weight of fragrant liquid：0.4, it is added on step toward in described coagulant liquid
The fragrant liquid that rapid B obtains, is uniformly mixed, obtain described in release fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 1.0 hours in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of temperature 60 C, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.8 according to weight：0.6 stirring mixing 0.8 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.6mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 3：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.5cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 0.8mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Obtain the fragrant liquid that a kind of concentration is by weight 18% using decanoyl/octanoyl glycerides solvent and Folium Bambusae flavor confect；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 0.2 according to weight：5：0.1：0.2：0.1 mixing is joined
A kind of coagulant liquid is obtained, then according to coagulant liquid compares 1.0 with the weight of fragrant liquid：0.6, it is added on step toward in described coagulant liquid
The fragrant liquid that B obtains, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.6 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of temperature 50 C, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 2.0 according to weight：0.3 stirring mixing 0.5 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.5mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 4：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.4cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 1.2mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Prepared with osmanthus spice using decanoyl/octanoyl glycerides solvent and obtain the fragrant liquid that a kind of concentration is by weight 14%；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 1.5 according to weight：8：0.2：0.2：0.1 mixing is joined
A kind of coagulant liquid is obtained, then according to coagulant liquid compares 0.8 with the weight of fragrant liquid：0.5, it is added on step toward in described coagulant liquid
The fragrant liquid that B obtains, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.8 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of temperature 45 C, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.6 according to weight：0.8 stirring mixing 1.0 hours, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.4mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 5：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.1cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 1.0mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Obtain the fragrant liquid that a kind of concentration is by weight 14% using pure water and Pericarpium Citri Reticulatae flavor confect；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 0.6 according to weight：5.8：0.1：0.2：0.1 mixing
Preparation obtains a kind of coagulant liquid, then according to coagulant liquid compares 1.2 with the weight of fragrant liquid：0.4, it is added on step toward in described coagulant liquid
The fragrant liquid that rapid B obtains, is uniformly mixed, obtain described in release fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.9 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of 55 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.8 according to weight：0.4 stirring mixing 0.9 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.6mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 6：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.3cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 0.6mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Prepared with osmanthus spice using decanoyl/octanoyl glycerides solvent and obtain the fragrant liquid that a kind of concentration is by weight 15%；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 0.8 according to weight：7.2：0.2：0.2 mixed preparing
Obtain a kind of coagulant liquid, then according to coagulant liquid compares 1.0 with the weight of fragrant liquid：0.6, it is added on step B toward in described coagulant liquid
The fragrant liquid obtaining, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.8 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of temperature 50 C, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.6 according to weight：0.6 stirring mixing 0.8 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.5mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 7：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.5cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 0.2mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Using pure water or decanoyl/octanoyl glycerides solvent and Pericarpium Citri Reticulatae spice, Fructus actinidiae chinensiss spice, Folium Bambusae spice or osmanthus spice
Prepare and obtain the fragrant liquid that a kind of concentration is by weight 12%；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 1.5 according to weight：5.8：0.2：0.1 mixed preparing
Obtain a kind of coagulant liquid, then according to coagulant liquid compares 1.2 with the weight of fragrant liquid：0.6, it is added on step B toward in described coagulant liquid
The fragrant liquid obtaining, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 0.8 hour in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of 55 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.6 according to weight：0.4 stirring mixing 0.8 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.5mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Embodiment 8：The preparation present invention releases fragrant gelatinous fibre filter stick
The implementation steps of this embodiment are as follows：
A, the preparation of blend fibre powder
By blend fibre line through the line segment for 1.0cm for the crush-cutting, pulverizing, screening, collect the line that fiber size is 1.2mm
Section, removes impurity, obtains blend fibre powder；
B, fragrant liquid preparation
Using pure water or decanoyl/octanoyl glycerides solvent and Pericarpium Citri Reticulatae spice, Fructus actinidiae chinensiss spice, Folium Bambusae spice or osmanthus spice
Prepare and obtain the fragrant liquid that a kind of concentration is by weight 18%；
C, release the preparation of fragrant gel
Carrageenan, Polyethylene Glycol, sodium alginate, agar and water is allowed to compare 1.2 according to weight：5：0.2：0.1 mixed preparing obtains
To a kind of coagulant liquid, then according to coagulant liquid compares 1.0 with the weight of fragrant liquid：0.5, it is added on step B toward in described coagulant liquid and obtain
The fragrant liquid arriving, is uniformly mixed, and obtains described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is soaked 1.0 hours in the fragrant liquid that step B obtains, separate
To releasing fragrant blend fibre powder；
E, mixture
Under conditions of temperature 50 C, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
Compare 1.7 according to weight：0.5 stirring mixing 0.8 hour, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blending by what step E obtained
Fiber powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, and reaching every millimeter of filter stick is 1.4mg, through opium pipe
Molding, hardening, obtain described releasing fragrant gel blend fibre filter stick.
Test example 1：Cigarette sample comparative evaluation
The preparation of prior art perfuming filter stick control sample is as follows：
According to filter lengths 1.5mg/mm standard, Guangzhou Xiang Long company is joined with trade name Pericarpium Citri Reticulatae essence decanoyl/octanoyl glycerides
Make the fragrant liquid that concentration is by weight 15%, be obtained using blend fibre line immersion way plus release fragrant line.It is then added to red
Comparison cigarette sample is obtained in the filter stick in the Tashan Mountain 1956.
The present invention releases the preparation of fragrant gel blend fibre filter stick：
According to filter lengths 1.5mg/mm standard, fragrant gel blend fibre filter stick is released in preparation in embodiment 1 and carries out four points
Cut, take wherein one section to replace control sample Hongta 1956 cigarette filter rod, the 25mg/ of so every Medicated cigarette props up.
These samples balance 24h in climatic chamber under conditions of 20 DEG C of temperature and relative humidity 60%, then often
Minor tick 48h is just according to GB 5606.4 2005《Medicated cigarette sense organ technical requirements》Standard method smoked panel test, determine suction effect
Really.Smoking result is listed in Table 1 below.
Table 1：The smoking result of test specimen
Table 1 smoking result shows, compared with prior art, the present invention releases fragrant gel blend fibre filter stick fragrance release all
Even, scent duration is long, and cigarette smoking process can be kept in aspiration procedure to release fragrant concordance, and the technology meeting manufacturing enterprise will
The pleasure of the senses of summation consumer.
Claims (8)
1. a kind of preparation method releasing fragrant gelatinous fibre filter stick is it is characterised in that the step of this preparation method is as follows：
A, the preparation of blend fibre powder
Blend fibre line is processed through crush-cutting, pulverizing, screening and decontamination, obtains blend fibre powder；
B, fragrant liquid preparation
Obtain a kind of concentration using pure water or decanoyl/octanoyl glycerides solvent with Pericarpium Citri Reticulatae flavor confect for by weight 12～18%
Fragrant liquid；
C, release the preparation of fragrant gel
Allow carrageenan, Polyethylene Glycol, sodium alginate, agar and water according to weight ratio 0.2～1.5：5～8：0.1～0.2：0.1～
0.2：0.1～0.2 mixed preparing obtains a kind of coagulant liquid, is then added on, toward in described coagulant liquid, the fragrant liquid that step B obtains, stirs
Mix mix homogeneously, obtain described releasing fragrant gel；
D, immersion
At room temperature, the blend fibre powder that step A obtains is immersed in the fragrant liquid that step B obtains, separates and obtain releasing fragrant blending
Fiber powder；
E, mixture
Under conditions of 40～60 DEG C of temperature, by releasing of obtaining of step D fragrant blend fibre powder and step C obtain release fragrant gel by
According to weight ratio 1.5～2.0：0.3～0.8 stirring mixing, obtains one kind and releases fragrant gel blend fibre powder；
F, molding
On filter-stick forming device, in opium pipe front end, diacetate fiber is uniformly sprawled, release fragrant gel blend fibre by what step E obtained
Powder passes through water-bath roller uniform application on whole diacetate fiber developed surface, through opium pipe molding, hardens, and obtains described perfume of releasing and coagulates
Glue blend fibre filter stick.
2. preparation method according to claim 1 it is characterised in that in step, the size of described blend fibre line powder
It is 0.2～1.2mm.
3. preparation method according to claim 1 is it is characterised in that in stepb, described Pericarpium Citri Reticulatae spice Fructus actinidiae chinensiss
Spice, Folium Bambusae spice or osmanthus spice replace.
4. preparation method according to claim 1 is it is characterised in that in step C, carrageenan, Polyethylene Glycol, alginic acid
The stirring under conditions of 40～60 DEG C of temperature of sodium, agar and water mixes 0.3～1.0 hour.
5. preparation method according to claim 1 is it is characterised in that in step C, described coagulant liquid and described perfume liquid
Weight ratio is 0.8～1.2：0.4～0.6.
6. it is characterised in that in step D, described blend fibre powder is in fragrant liquid for preparation method according to claim 1
Middle immersion 0.5～1.0 hour.
7. according to claim 1 it is characterised in that in step E, described releases fragrant blend fibre powder and releases fragrant gel
Stirring mixing 0.5～1.0 hour.
8. gelatinous fibre filter stick according to claim 1 is it is characterised in that in step F, in the exhibition of whole diacetate fiber
Open on face, described release fragrant gel blend fibre powder amount be every millimeter of filter stick be 1.4～1.6mg.
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| RU2771572C1 (en) * | 2018-07-31 | 2022-05-05 | Никовенчерс Трейдинг Лимитед | Aerosol production |
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| CN106418688B (en) | 2019-04-09 |
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Inventor after: Yu Yumei Inventor after: Guo Chongfeng Inventor after: Yang Tao Inventor after: Shen Yanwen Inventor after: Fan Xinlei Inventor before: Guo Chongfeng Inventor before: Yang Tao Inventor before: Shen Yanwen Inventor before: Fan Xinlei |
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Address after: 650220 floor 5, building 2, Yunnan returnees Pioneer Park, No. 80, chunman Avenue, Luoyang sub district office, Kunming area, China (Yunnan) pilot Free Trade Zone, Kunming, Yunnan Patentee after: Yunnan Bazi Biotechnology Co.,Ltd. Address before: No. 501, unit 7, building 2, shuiyikangqiao, high tech Zone, Kunming, Yunnan 650106 Patentee before: YUNNAN BAGU BIOTECHNOLOGY Co.,Ltd. |
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Denomination of invention: A preparation method of fragrance releasing gel fiber filter rod Effective date of registration: 20230710 Granted publication date: 20190409 Pledgee: Bank of China Limited Kunming Panlong Sub branch Pledgor: Yunnan Bazi Biotechnology Co.,Ltd. Registration number: Y2023530000045 |