CN106398551A - Mildew-resistant type wallpaper adhesive containing natural plant extract and preparation method thereof - Google Patents
Mildew-resistant type wallpaper adhesive containing natural plant extract and preparation method thereof Download PDFInfo
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- CN106398551A CN106398551A CN201610794535.XA CN201610794535A CN106398551A CN 106398551 A CN106398551 A CN 106398551A CN 201610794535 A CN201610794535 A CN 201610794535A CN 106398551 A CN106398551 A CN 106398551A
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- mildew
- mould
- proof
- wallpaper adhesive
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J1/00—Adhesives based on inorganic constituents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Synthetic Leather, Interior Materials Or Flexible Sheet Materials (AREA)
- Paper (AREA)
Abstract
The invention provides a mildew-resistant type wallpaper adhesive containing a natural plant extract. The adhesive does not contain formaldehyde, toxicity and harm, and nutrients, so that the adhesive has good mildew-resistant effects. A formula of the adhesive employs the natural plant extract product as a substitute of bactericide and mildew inhibitors whose main components are chemical compositions, mildew-resistant liquid which employs a plurality of natural plants with complex formulation and combination is added, and the mildew-resistant effects of the adhesive product are strengthened; and the product is safe and reliable, and is especially suitable for mildrew resistant finish after application to wallpaper.
Description
Technical field
The present invention relates to a kind of binding agent for wall-paper, gluing particularly to a kind of mould-proof-type wallpaper containing natural botanical extraction liquid
Agent and preparation method thereof.
Background technology
In interior decoration decoration, wall decoration also gradually adopts wallpaper and wall cloth to carry out decorations from painting emulsion paint.With
The widely using of wallpaper and wall cloth, in south and coastal area, arrives it may appear that room air with annual " plum rains " season
Humidity is excessive, temperature drift phenomenon, lead to the use of " plum rains " solar term time wallpaper occur mouldy, black, the meteorology such as rubescent
The wallpaper that factor is led to uses defect, has a strong impact on normal sale and the use of wallpaper, and the health constraining wallpaper industry is sent out
Exhibition.
At present, the wallpaper adhesive products being used in plum rain season are mainly the formaldehyde polyvinyl acetal containing formaldehyde
Water and polyvinyl acetate emulsion carry out wallpaper sticking construction, can there is the harmful substances such as free formaldehyde, VOC impact indoor environment
Quality；Meanwhile, the breeding life of mould can because the wallpaper glue of environment-friendly type is made of using organic material, be accelerated in wet condition
Long, make wallpaper, wall cloth variable color, the impact wallpaper service life that becomes mildewed and pollution indoor living environment.
In wallpaper, wall cloth construction link, in order to ensure the decorative effect of wallpaper, wall cloth, need to take a long time to carry out
Wallpaper, the parquets opposite joint of wall cloth, need the long removable time, to meet the normal construction of wallpaper, wall cloth, to be expert at present
All can there is such-and-such defect it is difficult to fully meet use demand in the wallpaper adhesive products commonly using in the industry, restriction
Wallpaper industry is advanced and is developed.
Content of the invention
The present invention provides a kind of mould-proof-type wallpaper adhesive containing natural botanical extraction liquid, and it does not contain formaldehyde, nontoxic,
Without nutriment, therefore there is preferable anti-mold effect.
The technical solution adopted for the present invention to solve the technical problems is：
A kind of mould-proof-type wallpaper adhesive containing natural botanical extraction liquid, this mould-proof-type wallpaper adhesive is included as follows with weight
The component of amount part meter：500～550 parts of deionized water, 120～200 parts of inorganic particle, 1～2 part of dispersant, 2～3 parts of coupling agent,
1～5 part of surfactant, 60～100 parts of inorganic thickening agent, 20～50 parts of polyvinyl alcohol, 30～50 parts of rosin solution, defoamer
1～2 part, 5～15 parts of water-loss reducer, 150～200 parts of mildew-retarding liquid；Mildew-retarding liquid be by following weight portion component immersion boil after system
The extract becoming：18～22 parts of willow leaf, 15～20 parts of the fruit of summer cypress, 12～18 parts of thyme, 8～13 parts of Chinese gall, Chinese cassia tree 9～15
Part, 5～8 parts of Chinese prickly ash, 9～14 parts of cacumen biotae, 5～8 parts of rhizome of cyrtomium, 5～9 parts of elm bark.Natural plant is adopted in this adhesive formulation
Thing extract adopts multiple natural plants as the substitute of the bactericide based on chemical composition, mould inhibitor, the mildew-retarding liquid of addition
Thing compounded combination, strengthens the anti-mold effect of adhesive products, safe and reliable, is particularly suited for the mould proof place after wallpaper is applied
Reason.
Preferably, inorganic particle be wollastonite in powder, talcum powder, precipitated calcium carbonate, kaolinic any one or a combination thereof,
The particle diameter of inorganic particle is 3-15 μm.Product main component is breeze system, natural material, and content of organics is few, easily mouldy
Probability low.
Preferably, dispersant is any one or combination of calgon, sodium nitrate；Coupling agent is coupled for titanate esters
Agent, any one or combination of aluminate coupling agent.Calgon gradually can absorb moisture and be in viscous jelly, with calcium, magnesium etc.
Metal ion can generate soluble complexes, is also used as dispersant, tackifier and the preservative of inorganic powder material.
Preferably, emulsifying agent be lauryl sodium sulfate, neopelex, OP-10, this Pan series or tween
Any one or combination of serial emulsifying agent.
Preferably, inorganic thickening agent is any one or combination of bentonite, aluminium-magnesium silicate, lithium magnesium silicate；Defoamer is
Tributyl phosphate, any one or combination of silicone oil；Water-loss reducer is glycerine；Inorganic thickening agent acts primarily as lubrication, also has ratio
Preferably lubricity is it is ensured that be easily coated with when using.
Preferably, the preparation method of described rosin solution is：It is placed on airtight appearance by after rosin and absolute ethyl alcohol mixing
In device, heating is dissolved, and wherein the mass fraction of rosin is 25%, and absolute ethyl alcohol is 75%.The purpose adding is thickening, improves and produces
The adhesion strength of product.
Preferably, the preparation method of described mildew-retarding liquid is：Weigh the willow leaf of formula ratio, the fruit of summer cypress, thyme, five times
Son, Chinese cassia tree, Chinese prickly ash, cacumen biotae, rhizome of cyrtomium and elm bark, add the water of 4～6 times of weight, soak 2～3 hours, boil by intense fire, it
After continue boiling by slow fire 2～3 hours, filter, take filtrate, obtain mildew-retarding liquid.
A kind of preparation method of the described mould-proof-type wallpaper adhesive containing natural botanical extraction liquid, the method is：Successively
By deionized water, inorganic particle, dispersant, coupling agent, surfactant, inorganic thickening agent, polyvinyl alcohol, disperse 30 points
It is warming up to 90～95 DEG C after more than clock, is incubated 30～50 minutes, add rosin solution, then be cooled to 50 DEG C, add defoamer, guarantor
Aqua, mildew-retarding liquid dispersion stirring 30～60 minutes, are cooled to 28～30 DEG C to after colloid modification, adopt pulse in discharging simultaneously
High light technology carries out surface disinfection to colloid, packaging, obtains product.
It is body material that the present invention mainly adopts the inorganic particle without Nutrient medium, by adding coupling agent, dispersant, breast
The materials such as agent, mildew-retarding liquid, defoamer, polyvinyl alcohol, are modified to product after the gelatinization-emulsification and cross linked reaction that heats up,
Afterwards surface disinfection is carried out to colloid by pulse strong-light technology, finally give a kind of paste of function admirable has mould proof work(
The wallpaper wall cloth adhesive of energy.It is various that the present invention is applied to stickup paper substrate, fiberglass-based, nonwoven fabric base, Bu Ji, cross bottom etc.
Wallpaper and wall cloth.
The product of the present invention has simple production process, easy to use, the advantages of directly can be coated with construction, meanwhile, product
Without formaldehyde, nontoxic；Product adopts based on inorganic particle, and the organic matter rich in Nutrient medium adds less, that is, can guarantee that product
The not mould of itself is stale-proof, and wallpaper wall cloth can also be played with effect of antimildew and antibacterial after a procedure, can meet coastal area high temperature high
The wallpaper of wet environment, wall cloth construction usage, protect the features such as wallpaper, prolongation wallpaper service life to be to promote industry healthy, optimum
Development, the good product benefited the nation and the people.
Specific embodiment
Below by specific embodiment, technical scheme is described in further detail.It should be appreciated that this
Bright enforcement is not limited to the following examples, and any pro forma flexible and/or change that the present invention is made all will fall
Enter the scope of the present invention.
In the present invention, if not refering in particular to, all of part, percentage are unit of weight, the equipment being adopted and raw material etc.
All it is commercially available or commonly used in the art.Method in following embodiments, if no special instructions, is the normal of this area
Rule method.
Rosin solution, self-control, preparation method：Rosin solution is to be placed on after rosin and absolute ethyl alcohol mixing in closed container
Heating is dissolved, and in rosin solution, the mass fraction of rosin is 25%, and absolute ethyl alcohol is 75%.
Lauryl sodium sulfate, Wujiang Dong Hao Fine Chemical Co., Ltd produces；
Aluminate coupling agent, Nanjing Pin Ning coupling agent Co., Ltd produces；
Bentonite, Anji Tian Yu bentonite Co., Ltd produces；
Kaolin, Jiangyin Guang Yuan Ultramicro-powder Co., Ltd produces；
Glycerine, Xingang Chemical Co., Ltd., Nantong produces；
Silicone oil, Qingdao De Ming Chemical Co., Ltd.；
OP-10, Shandong natural laws bioengineering Co., Ltd；
S-80, Hai'an petrochemical plant produces；
T-80, Hai'an petrochemical plant produces；
Inorganic particle is selected from wollastonite in powder, talcum powder, precipitated calcium carbonate, kaolinic any one or a combination thereof, inorganic powder
The particle diameter of body is 3-15 μm.
Embodiment 1-5
A kind of mould-proof-type wallpaper adhesive containing natural botanical extraction liquid, the component proportion of this mould-proof-type wallpaper adhesive is such as
Shown in table 1.
Table 1 (unit：kg)
Described mildew-retarding liquid be boiled by the component immersion of following weight portion after the extract made：18 parts of willow leaf, summer cypress
20 parts of son, 12 parts of thyme, 13 parts of Chinese gall, 15 parts of Chinese cassia tree, 8 parts of Chinese prickly ash, 14 parts of cacumen biotae, 8 parts of rhizome of cyrtomium, 5 parts of elm bark.Institute
The preparation method of the mildew-retarding liquid stated is：Weigh the willow leaf of formula ratio, the fruit of summer cypress, thyme, Chinese gall, Chinese cassia tree, Chinese prickly ash, arbor-vitae
Leaf, rhizome of cyrtomium and elm bark, add the water of 6 times of weight, soak 3 hours, boil by intense fire, continue boiling by slow fire 3 hours afterwards, mistake
Filter, takes filtrate, obtains mildew-retarding liquid.
The preparation method of mould-proof-type wallpaper adhesive：Successively by deionized water, inorganic particle, dispersant, coupling agent, surface
Activating agent, inorganic thickening agent, polyvinyl alcohol, dispersion is warming up to 90～95 DEG C after more than 30 minutes, is incubated 30～50 minutes,
Add rosin solution to be cooled to 50 DEG C again after stirring, add defoamer, water-loss reducer, mildew-retarding liquid to disperse stirring 30～60 minutes
To colloid modification, it is cooled to 28～30 DEG C to after colloid modification, adopt pulse strong-light technology to colloid in discharging simultaneously
Carry out surface disinfection, packaging, obtain product.
Product gray pasty colloid, the parameter such as product viscosity is shown in Table 2；Coating good leveling property can meet all kinds of wallpapers, wall
Cloth is applied in different construction environments.Product can meet temperature and be chronically at 25～35 DEG C, the south edge of relative humidity 70%
The wallpaper of Haicheng City, wall cloth construction application, wallpaper is pasted and mouldy rubescent variable color and the phenomenon that becomes mildewed all in latter 240 days about.
Table 2
From table 2, inorganic particle modification that the present invention produces have fungicidal properties wallpaper adhesive products have viscous
Degree is moderate, convenient construction, fungicidal properties index are high, is to solve " plum rains " season wallpaper Signs of Mould, extends wallpaper and uses the longevity
The wallpaper adhesive products of life, can promote wallpaper industry healthy development, wide market.
Embodiment 6-10
A kind of mould-proof-type wallpaper adhesive containing natural botanical extraction liquid, the component proportion of this mould-proof-type wallpaper adhesive is such as
Shown in table 3.The preparation method of mould-proof-type wallpaper adhesive is with embodiment 1.
Table 3 (unit：kg)
Described mildew-retarding liquid be boiled by the component immersion of following weight portion after the extract made：20 parts of willow leaf, summer cypress
16 parts of son, 12 parts of thyme, 10 parts of Chinese gall, 12 parts of Chinese cassia tree, 5 parts of Chinese prickly ash, 12 parts of cacumen biotae, 6 parts of rhizome of cyrtomium, 8 parts of elm bark.Institute
The preparation method of the mildew-retarding liquid stated is：Weigh the willow leaf of formula ratio, the fruit of summer cypress, thyme, Chinese gall, Chinese cassia tree, Chinese prickly ash, arbor-vitae
Leaf, rhizome of cyrtomium and elm bark, add the water of 4 times of weight, soak 2 hours, boil by intense fire, continue boiling by slow fire 3 hours afterwards, mistake
Filter, takes filtrate, obtains mildew-retarding liquid.Product gray pasty colloid, product viscosity is 35000～36000mPa s；Coating levelling
Property can meet well all kinds of wallpapers, wall cloth and apply in different construction environments.Product can meet temperature and be chronically at 25～35 DEG C,
The wallpaper in southern coastal cities of relative humidity 70%, wall cloth construction application, wallpaper stickup does not all occur mouldy for latter 300 days about
Rubescent variable color and the phenomenon that becomes mildewed.
Embodiment described above is one kind preferably scheme of the present invention, not the present invention is made any pro forma
Limit, also have other variants and remodeling on the premise of without departing from the technical scheme described in claim.
Claims (8)
1. a kind of mould-proof-type wallpaper adhesive containing natural botanical extraction liquid is it is characterised in that this mould-proof-type wallpaper adhesive includes
Following component in parts by weight：
500 ~ 550 parts of deionized water, 120 ~ 200 parts of inorganic particle, 1 ~ 2 part of dispersant, 2 ~ 3 parts of coupling agent, surfactant 1 ~ 5
Part, 60 ~ 100 parts of inorganic thickening agent, 20 ~ 50 parts of polyvinyl alcohol, 30 ~ 50 parts of rosin solution, 1 ~ 2 part of defoamer, water-loss reducer 5 ~ 15
Part, 150 ~ 200 parts of mildew-retarding liquid；Mildew-retarding liquid be boiled by the component immersion of following weight portion after the extract made：Willow leaf 18～
22 parts, 15～20 parts of the fruit of summer cypress, 12～18 parts of thyme, 8～13 parts of Chinese gall, 9～15 parts of Chinese cassia tree, 5～8 parts of Chinese prickly ash, arbor-vitae
9～14 parts of leaf, 5～8 parts of rhizome of cyrtomium, 5～9 parts of elm bark.
2. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：Inorganic particle is wollastonite in powder, talcum
Powder, precipitated calcium carbonate, kaolinic any one or a combination thereof, the particle diameter of inorganic particle is 3-15 μm.
3. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：Dispersant is calgon, nitric acid
Any one or combination of sodium；Coupling agent is any one or combination of titanate coupling agent, aluminate coupling agent.
4. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：Emulsifying agent be lauryl sodium sulfate,
Neopelex, any one or the combination of OP-10, this Pan series or twain series emulsifier.
5. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：Mould inhibitor is dehydroactic acid sodium, double second
Sour sodium, calcium propionate, any one or combination of Sodium Benzoate；Inorganic thickening agent be bentonite, aluminium-magnesium silicate, lithium magnesium silicate arbitrary
Plant or combine；Defoamer is any one or combination of tributyl phosphate, silicone oil；Water-loss reducer is glycerine；Bactericide is isothiazoline
Ketone compound, halogen derivatives compound, BIT, any one or combination of Hete rocyclic derivatives compound.
6. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：The preparation method of described rosin solution
For：It is placed on heating in closed container to dissolve by after rosin and absolute ethyl alcohol mixing, wherein the mass fraction of rosin is 25%, anhydrous
Ethanol is 75%.
7. mould-proof-type wallpaper adhesive according to claim 1 it is characterised in that：The preparation method of described mildew-retarding liquid
It is：Weigh willow leaf, the fruit of summer cypress, thyme, Chinese gall, Chinese cassia tree, Chinese prickly ash, cacumen biotae, rhizome of cyrtomium and the elm bark of formula ratio, add 4
The water of～6 times of weight, soaks 2～3 hours, boils by intense fire, continue boiling by slow fire afterwards 2～3 hours, filters, takes filtrate, obtain
Mildew-retarding liquid.
8. the preparation method of the mould-proof-type wallpaper adhesive containing natural botanical extraction liquid described in a kind of claim 1, its feature
It is：Successively by deionized water, inorganic particle, dispersant, coupling agent, surfactant, inorganic thickening agent, PVA mixed
Close, dispersion is warming up to 90 ~ 95 DEG C after more than 30 minutes, be incubated 30 ~ 50 minutes, add rosin solution, then be cooled to 50 DEG C, add
Defoamer, water-loss reducer, mildew-retarding liquid disperse stirring 30 ~ 60 minutes, are cooled to 28 ~ 30 DEG C to after colloid modification, in discharging simultaneously
Surface disinfection is carried out to colloid using pulse strong-light technology, packaging, obtain product.
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| CN201610794535.XA CN106398551A (en) | 2016-08-31 | 2016-08-31 | Mildew-resistant type wallpaper adhesive containing natural plant extract and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107880811A (en) * | 2017-12-07 | 2018-04-06 | 山东梦想与家智能科技有限公司 | A kind of wallpaper glue for child room finishing and preparation method thereof |
| CN111440566A (en) * | 2020-03-11 | 2020-07-24 | 安徽索亚装饰材料有限公司 | Wallpaper adhesive and preparation process thereof |
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| CN104327793A (en) * | 2014-08-06 | 2015-02-04 | 桐乡嘉力丰实业股份有限公司 | Inorganic-powder-modified mould-proof wallpaper adhesive and preparation method thereof |
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2016
- 2016-08-31 CN CN201610794535.XA patent/CN106398551A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104327793A (en) * | 2014-08-06 | 2015-02-04 | 桐乡嘉力丰实业股份有限公司 | Inorganic-powder-modified mould-proof wallpaper adhesive and preparation method thereof |
Non-Patent Citations (2)
| Title |
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| 广东省科学技术协会 编: "《2005年广东高性能、功能材料研究与产业化及发展循环经济研讨会》", 30 September 2005, 广东省科学技术协会 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107880811A (en) * | 2017-12-07 | 2018-04-06 | 山东梦想与家智能科技有限公司 | A kind of wallpaper glue for child room finishing and preparation method thereof |
| CN111440566A (en) * | 2020-03-11 | 2020-07-24 | 安徽索亚装饰材料有限公司 | Wallpaper adhesive and preparation process thereof |
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Application publication date: 20170215 |