CN106389525A - Extraction method for spleen-stomach invigorating and qi replenishing decoction prescription, pinellia ternata heart-removing decoction prescription, compound salvia miltiorrhiza tablet prescription, and hemp seed pill prescription - Google Patents
Extraction method for spleen-stomach invigorating and qi replenishing decoction prescription, pinellia ternata heart-removing decoction prescription, compound salvia miltiorrhiza tablet prescription, and hemp seed pill prescription Download PDFInfo
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Abstract
The present invention relates to an extraction method for a spleen-stomach invigorating and qi replenishing decoction prescription, a pinellia ternata heart-removing decoction prescription, a compound salvia miltiorrhiza tablet prescription, and a hemp seed pill prescription. The extraction method comprises: (1) respectively carrying out steam distillation on angelica sinensis and ginger in the prescription for 1-3 h with a mixture comprising 85-90 wt% of ethanol and 10-15 wt% of water; (b) respectively extracting rheum palmatum l, apricot kernel, ginseng, milkvetch root, radix bupleuri, paeonia lactiflora pall and salvia miltiorrhiza in the prescription for 1-3 h with a mixture comprising 10-30 wt% of ethanol and 70-90 wt% of water; (c) extracting pinellia ternata in the prescription for 1-3 h with a mixture comprising 70-90 wt% of ethanol and 10-30 wt% of water; (d) respectively extracting the herbs excluded in the steps (a)-(c) for 1-3 h with water twice; and (e) merging the extracts in the steps (a)-(d).
Description
Technical field
The present invention with regard to a kind of extracting process of prescription, particularly a kind of with regard to BUZHONG YIQI TANG, banxia xiexin decoction,
FUFANG DANSHEN PIAN and the extracting process of Maziren Wan prescription
Background technology
The history of the existing thousands of years of Chinese medicine development, in Chinese medicine, contained chemical composition is sufficiently complex, has both contained multiple
Effective ingredient, also contains invalid components it is also possible to comprise toxic component.Extract its effective ingredient and add further
With separation, purification, obtain the important content that effective monomer is in Chinese medicine research field.Chinese medicine extraction is exactly
Extract wherein effective ingredient using some technology to greatest extent so that the inherent quality of Chinese medicine preparation and clinical treatment
Effect improves, and so that the effect of Chinese medicine is played to greatest extent, the extraction of Chinese medicine is the important ring of production process
Section, its process, the selection of technological process and device configuration all will be directly connected to quality and the clinic of Chinese medicine
Effect.
According to《Treatise on the spleen and stomach》, the usage of BUZHONG YIQI TANG is 1.5 grams of Radix Astragali (5 points), disease very, forced labour heat notably
1 money, 1.5 grams of liquorice (5 points), Radix Ginseng go 0.9 gram of reed (3 points), cough it, Radix Angelicae Sinensis body wine dries, or
Day dry 0.6 gram (2 points), 0.6 gram of Pericarpium Citri Reticulatae (2-3 divides), 0.6 gram of Rhizoma Cimicifugae (2-3 divides), 0.6 gram of Radix Bupleuri (2-3 divides),
White 0.9 gram (3 points), nozzle of adding medicine to, all make clothes.With 300 milliliters of water, decoct to 150 milliliters, go dregs, empty
Slightly decoction being taken hot during abdomen.
Foundation《Typhoid fever acute disease is discussed》, the use genealogy of law of general banxia xiexin decoction, with 1 liter of water, boils and takes 600 milliliters, go
Dregs, then take 300 milliliters.
Foundation《Typhoid fever acute disease is discussed》, the usage of general Maziren Wan is 100 grams of pockmarks core (2 liters), the Radix Paeoniae Alba 25
Gram (8 liang), Fructus Aurantii Immaturus process 25 grams (8 liangs), Radix Et Rhizoma Rhei is removed the peel 50 grams of (1 jin), Cortex Magnoliae Officinalis and processed, and remove the peel 30 grams of (1 jin), Fructus Prunis
Core peeling point, endures 50 grams (1 liters), right Six-element, medicine grinds as end, making pellets by mixing medical powder with honey, honey and ball such as Semen Firmianae are big.
Drink-service ten ball, taking medicine three times daily, gradually plus, with know for degree.
Content of the invention
It is an object of the invention to, a kind of BUZHONG YIQI TANG, banxia xiexin decoction, FUFANG DANSHEN PIAN and pockmarks are provided
The extracting process of core pill side, carries out, to solve prior art, its own shortcomings that Chinese medicine extraction has：In Chinese medicine
Loss of effective components, especially wherein non-water-soluble composition；Non-active ingredients can not to remove to greatest extent,
Enrichment factor is not high enough；In extracting solution in addition to effective ingredient, often impurity is more, still has a small amount of water solublity paste property to become
Point, often it is unfavorable for refining；And excessively high-temperature operation can cause a large amount of decomposition of thermal sensitivity effective ingredient.
For solving the above problems, inventors have surprisingly discovered that a kind of BUZHONG YIQI TANG, banxia xiexin decoction, compound recipe are red
Ginseng piece and the extracting process of four kinds of prescriptions of Maziren Wan, it comprises the steps of：
(a) by the Radix Angelicae Sinensis in prescription and Rhizoma Zingiberis Recenss, respectively with the mixture of 85～90wt% ethanol and 10～15wt% water
Steam distillation 1～3 hour；(b) by the Radix Et Rhizoma Rhei in prescription, Semen Armeniacae Amarum, Radix Ginseng, Radix Astragali, Radix Bupleuri, Radix Paeoniae and
Radix Salviae Miltiorrhizae, is extracted 1～3 hour with the mixture of 10～30wt% ethanol and 70～90wt% water respectively；C () is by prescription
In the Rhizoma Pinelliae, extracted 1～3 hour with the mixture of 70～90wt% ethanol and 10～30wt% water；D () will be above-mentioned
Medical material beyond step (a)～(c), respectively with water extraction 1～3 hour, is repeated twice；E () is by above-mentioned steps
A ()～(d) extract merges.
In a preferred embodiment, wherein the prescription system Radix Astragali of this BUZHONG YIQI TANG, Radix Ginseng, Radix Glycyrrhizae Preparata, white,
Rhizoma Cimicifugae, Radix Bupleuri, Rhizoma Zingiberis Recenss, Fructus Jujubae, Radix Angelicae Sinensis, Pericarpium Citri Reticulatae.
In another preferred embodiment, wherein the prescription system Rhizoma Pinelliae of this banxia xiexin decoction, Radix Scutellariae, Rhizoma Zingiberiss, Radix Ginseng,
Rhizoma Coptidis, Fructus Jujubae, Radix Glycyrrhizae Preparata.
In another preferred embodiment, the prescription of wherein this FUFANG DANSHEN PIAN is Radix Salviae Miltiorrhizae, Radix Notoginseng, Borneolum Syntheticum.
In another preferred embodiment, wherein this Maziren Wan prescription be pockmarks core, Radix Paeoniae, Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis,
Fructus Aurantii Immaturus, Semen Armeniacae Amarum.
In another preferred embodiment, wherein this step (a) system is steamed with the mixture of 90wt% ethanol and 10wt% water
Steam distillation 1 hour.
In another preferred embodiment, wherein this step (b) system is carried with the mixture of 30wt% ethanol and 70wt% water
Take 1 hour.
In another preferred embodiment, wherein this step (c) system is carried with the mixture of 70wt% ethanol and 30wt% water
Take 1 hour.
In another preferred embodiment, it filters after being contained in each (a)～(d) step further.
In another preferred embodiment, it comprises step (f) further by mixture pelleting.
Inventor finds, using above-mentioned BUZHONG YIQI TANG, banxia xiexin decoction, FUFANG DANSHEN PIAN and pockmarks core
The extract that the extracting process of pill side is obtained, has the effective ingredient of high level.
Specific embodiment
The terms " one " or " a kind of " when being used in conjunction in claim or description with "comprising",
May represent has one, but also complies with " one or more " or " at least one ".
One main purpose of the present invention be to provide a kind of BUZHONG YIQI TANG, banxia xiexin decoction, FUFANG DANSHEN PIAN and
The extracting process of four kinds of prescriptions of Maziren Wan, it comprises the steps of：(a) by the Radix Angelicae Sinensis in prescription and Rhizoma Zingiberis Recenss,
Respectively with the mixture steam distillation 1～3 hour of 85～90wt% ethanol and 10～15wt% water；B () is by prescription
Radix Et Rhizoma Rhei, Semen Armeniacae Amarum, Radix Ginseng, Radix Astragali, Radix Bupleuri, Radix Paeoniae and Radix Salviae Miltiorrhizae, respectively with 10～30wt% ethanol and 70～
The mixture of 90wt% water extracts 1～3 hour；(c) by the Rhizoma Pinelliae in prescription, with 70～90wt% ethanol and 10～
The mixture of 30wt% water extracts 1～3 hour；(d) by the medical material beyond above-mentioned steps (a)～(c), respectively with
Water extraction 1～3 hour, is repeated twice；E above-mentioned steps (a)～(d) extract is merged by ().
From the foregoing, method of the present invention system can be applicable to BUZHONG YIQI TANG, banxia xiexin decoction, compound Salviae Miltiorrhizae
Piece and Maziren Wan prescription, whether the enforcement of each step in method, depending on the medical material having in each prescription.
For example, it is an aspect of the invention to providing a kind of extracting process of BUZHONG YIQI TANG, wherein this prescription bag
Contain but be not limited to Radix Astragali, Radix Ginseng, Radix Glycyrrhizae Preparata, white, Rhizoma Cimicifugae, Radix Bupleuri, Rhizoma Zingiberis Recenss, Fructus Jujubae, Radix Angelicae Sinensis, Pericarpium Citri Reticulatae.
Additionally, when extracting BUZHONG YIQI TANG prescription, above-mentioned steps (d) more can be separately added into according to following symptom
Following prescription, and yang deficiency：Plus Cortex Cinnamomi, Radix Aconiti Lateralis Preparata, Rhizoma Zingiberiss；Indigestion and loss of appetite：Jia Shancha, Endothelium Corneum Gigeriae Galli；Dysuria：
Plus Semen Plantaginiss, Poria；Incessant chronic diarrhea：Plus Fructus Chebulae, Fructus Mume；Metrorrhagia is more than：Plus SHIXIAO SAN, Radix Sanguisorbae preparata；Warp
After phase fault：Plus Herba Leonuri, Radix Paeoniae Rubra, Radix Salviae Miltiorrhizae, Flos Carthami；Headache：Plus Rhizoma Chuanxiong, Fructus Viticises；Limbs pain：Plus
Radix Saposhnikoviae, Rhizoma Et Radix Notopterygii；Leukorrhagia is many：Plus Poria, Semen Plantaginiss；Headache person, plus withered, Herba Asari is with dispelling wind and relieving；
Cough person, plus Fructus Schisandrae Chinensis, Radix Ophiopogonis are with astringing lung-QI and relieving cough；And stagnation of QI person, plus the Radix Aucklandiae, Fructus Aurantii are with Regulate the flow of vital energy Xie Yu；Empty
People catches a cold, plus Folium Perillae is a little to increase the pungent power dissipating.
Another aspect of the present invention is with regard to a kind of extracting process of banxia xiexin decoction prescription, the prescription bag of this GEGEN TANG
Contain but be not limited to the Rhizoma Pinelliae, Radix Scutellariae, Rhizoma Zingiberiss, Radix Ginseng, Rhizoma Coptidis, Fructus Jujubae, Radix Glycyrrhizae Preparata.
Above-mentioned steps (d) more can be separately added into following prescription according to following symptom, and heart side of body painful abdominal mass is vexed：Plus Fructus Aurantii Immaturus, Fructus Citri tangerinae
Stalk；Rush down profit stomachache：Plus the Radix Aucklandiae, the Radix Paeoniae Alba；Vomiting singultuss：Plus Pericarpium Citri Reticulatae, Poria.
Another aspect of the present invention is to provide a kind of extracting process of FUFANG DANSHEN PIAN prescription, this FUFANG DANSHEN PIAN
Prescription including but not limited to Radix Salviae Miltiorrhizae, Radix Notoginseng, Borneolum Syntheticum.
Another aspect of the invention is to provide a kind of extracting process of Maziren Wan, the prescription bag of this Maziren Wan
Contain but be not limited to pockmarks core, Radix Paeoniae, Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus, Semen Armeniacae Amarum.
Above-mentioned steps (d) more can be separately added into following prescription, blood depletion constipation according to following symptom：Sovolin is returned, Fructus Persicae
Core；Hemorrhoidal hamorrhage viscerotoxic hematochezia：Plus Flos Sophorae, Cacumen Platycladi, Herba Schizonepetae；Constipation is very：Plus Natrii Sulfas；Scorching impairment of body fluid：Plus Chinese juniper
Semen Trichosanthis, Semen Platycladi；Constipation due to hemorrhoids：Plus Rhizoma Coptidis, Rhizoma Cimicifugae, Semen Persicae, Radix Angelicae Sinensis.
In above-mentioned extracting process, filter after preferably being further contained in each (a)～(d) step.
In above-mentioned extracting process, preferably can further comprise step (f) by mixture pelleting.
Above-mentioned term " extraction " is to extract wherein effective ingredient to greatest extent so that Chinese medicine using some technology
The inherent quality of preparation and clinical therapeutic efficacy improve, and so that the effect of Chinese medicine is played to greatest extent.Chinese medicine
Extraction be Chinese Traditional Medicine important unit operation, its process, the selection of technological process and equipment are joined
Put and all will be directly connected to quality and the clinical effectiveness of Chinese medicine.
In the present invention, Chinese medicine containing volatile oil, such as Radix Angelicae Sinensis, Ramulus Cinnamomi, Rhizoma Zingiberis Recenss, Rhizoma Chuanxiong, Cortex Cinnamomi, Roast Rhizoma Zingiberis Recens
Deng, wherein this volatile oil also known as quintessence oil, it is one to there are volatility, the oily liquids that can go out with vapor distillation,
There is fragrance, and this volatile oil is the polytype such as aliphatic compound, aromatic compound note class compound
The mixture of compound, inventors be surprised to learn that this volatile oil Chinese medicine preferably system is extracted to have volatile solution
Take, more preferably but the mixture that is not limited to mix with the ratio of 90wt% ethanol and 10wt% water with ethanol and water
Steam extraction.
In the present invention, containing tcm with glycosides, such as Radix Et Rhizoma Rhei, Cortex Moutan, Radix Glycyrrhizae, Semen Armeniacae Amarum, Radix Ginseng, Radix Astragali, bavin
Recklessly, SHANGZI, Semen Persicae, Radix Paeoniae, the Radix Paeoniae Alba, Radix Paeoniae Rubra, Radix Platycodoniss, Radix Clematidis etc., mostly have colourless, odorless,
Tool bitterness, minority is coloured, minority has the feature of sweet taste, and most in neutral or acid, minority is in alkalescence, big
Most of soluble in water and ethanol, easily generated sugar and aglycon by diluted acid or enzyme hydrolysiss, typically has certain optics and lives
Property, inventors be surprised to learn that the above-mentioned preferably system containing tcm with glycosides is extracted with the mixture of ethanol and water, its ratio is relatively
Good system is with the water of the ethanol mixing 70wt% of 30wt%.
In the present invention, Chinese medicine containing alkaloidss, such as Radix Aconiti Lateralis Preparata, Rhizoma Coptidis, Cortex Phellodendri, Herba Ephedrae, the Rhizoma Pinelliae etc., mostly
Number alkaloids are crystal material, colourless and have optical activity, inventors be surprised to learn that above-mentioned containing in alkaloidss
Medicine preferably system is extracted with the mixture of ethanol and water, and its ratio preferably system is with the water of the ethanol of 70wt% and 30wt%.
In the present invention, Olibanum, Myrrha, Sanguis Draxonis etc., preferably system are extracted 30 minutes with ethanol.
In the present invention, the Chinese medicine such as Os Draconis, Concha Ostreae, preferable system extracts by the way of boiling, the time preferably 2～4
Hour, most preferably 3 hours.
In the present invention, Colla cornus cervi, Colla Corii Asini, Testudiniss angle glue, Borneolum Syntheticum etc., preferably system, without extraction, direct plunge into height
In warm solution, the mixture of the extract of prescription that this pyrosol can extract for other.
In the present invention, Herba Menthae, Herba Asari etc., preferably system, with water extraction 5～15 minutes, are more preferably with water extraction 10
Minute.
Medical material in addition to above-mentioned enumerating in the present invention, preferably system, with water extraction 1 hour, merge after being repeated twice.
If Chinese medicine washes with water before extracting, these powder or particle can be made washed away, adjuvant and effective ingredient
Can be dissolved in water and be washed off so as to curative effect reduces, therefore before Chinese medicine extraction, handy water does not rinse, can only be with cold
Water soaks.The prepared slices of Chinese crude drugs after cold water soak, organizational structure can loose expansion, make effective ingredient easily fried,
Make effective ingredient easily fried.If using hot-water soak at the very start, in medical material, contained protein component will be very
Fast dissolution and freezing film, are wrapped in medical material surface, make moisture be not easy to penetrate in medical material histiocyte,
Effective ingredient also is difficult to decompose out, affects the fried of composition.
Traditional Chinese medicine extraction method includes decocting cooking method, infusion process, percolation, Gelatin improving method, circumfluence method, solvent
Extraction method, steam distillation and sublimed method etc..Solvent extraction method is most widely used method, and it is basis
The property of various effective ingredient dissolubility in Chinese herbal medicine, from molten to other compositions greatly to needing ingredient solubility
The little solvent of Xie Du, a kind of extracting method that required active component is dissolved out in medical material tissue.
Embodiment
Embodiment 1- utilizes the method for the present invention to extract BUZHONG YIQI TANG
By taking 6.0 grams of Radix Astragali, 4.0 grams of Radix Ginseng, 4.0 grams of Radix Glycyrrhizae Preparata, white 2.0 grams, Rhizoma Cimicifugae 1.0 in prescription respectively
Gram, 1.0 grams of Radix Bupleuri, 3.0 grams of Rhizoma Zingiberis Recenss, 2.0 grams of Fructus Jujubae, 2.0 grams of Radix Angelicae Sinensis, 2.0 grams of Pericarpium Citri Reticulatae, and according to this
Bright method extraction, with the extracted effective ingredient of weighing method measurement for 5.1 grams after extraction.
Comparative example 1- utilizes prior art method to extract BUZHONG YIQI TANG
By taking 6.0 grams of Radix Astragali, 4.0 grams of Radix Ginseng, 4.0 grams of Radix Glycyrrhizae Preparata, white 2.0 grams, Rhizoma Cimicifugae 1.0 in prescription respectively
Gram, 1.0 grams of Radix Bupleuri, 3.0 grams of Rhizoma Zingiberis Recenss, 2.0 grams of Fructus Jujubae, 2.0 grams of Radix Angelicae Sinensis, 2.0 grams of Pericarpium Citri Reticulatae, and according to known
Decocting method extraction, will all medical materials in water extraction 2 hours, extracted with the measurement of weighing method after extraction
Effective ingredient be 3.4 grams.
Embodiment 2- utilizes the method for the present invention to extract banxia xiexin decoction
By taking 7.5 grams of the Rhizoma Pinelliae, 4.5 grams of Radix Scutellariae, 4.5 grams of Rhizoma Zingiberiss, 4.5 grams of Radix Ginseng, Rhizoma Coptidis 1.5 in prescription respectively
Gram, 3.0 grams of Fructus Jujubae, 4.5 grams of Radix Glycyrrhizae Preparata, and according to the method for the present invention extraction, after extraction with weighing method survey
Measure extracted effective ingredient and be 4.65 grams.
Comparative example 2- utilizes prior art method to extract banxia xiexin decoction
By taking 7.5 grams of the Rhizoma Pinelliae, 4.5 grams of Radix Scutellariae, 4.5 grams of Rhizoma Zingiberiss, 4.5 grams of Radix Ginseng, Rhizoma Coptidis 1.5 in prescription respectively
Gram, 3.0 grams of Fructus Jujubae, 4.5 grams of Radix Glycyrrhizae Preparata, and according to known decocting method extraction, will all medical materials in water extraction
Take 2 hours, with the extracted effective ingredient of weighing method measurement for 3.1 grams after extraction.
Embodiment 3- utilizes the method for the present invention to extract FUFANG DANSHEN PIAN
By taking 17.5 grams of Radix Salviae Miltiorrhizae, 3.4 grams of Radix Notoginseng, 0.2 gram of Borneolum Syntheticum in prescription respectively, and according to the method for the present invention
Extraction, with the extracted effective ingredient of weighing method measurement for 7.5 grams after extraction.
Comparative example 3- utilizes prior art method to extract FUFANG DANSHEN PIAN
By taking 17.5 grams of Radix Salviae Miltiorrhizae, 3.4 grams of Radix Notoginseng, 0.2 gram of Borneolum Syntheticum in prescription respectively, and according to known decocting method
Extraction, will all medical materials in water extraction 2 hours, the effective one-tenth being extracted with the measurement of weighing method after extraction
It is divided into 5.3 grams.
Embodiment 4- utilizes the method for the present invention to extract Maziren Wan
By taking pockmarks core 468.75mg, Radix Paeoniae 156.25mg, Radix Et Rhizoma Rhei 312.50mg, Cortex Magnoliae Officinalis in prescription respectively
156.25mg, Fructus Aurantii Immaturus 156.25mg, Semen Armeniacae Amarum 156.25mg, and according to method of the present invention extraction, extraction
Afterwards with the extracted effective ingredient of weighing method measurement as 421.88mg.
Comparative example-extract Maziren Wan using prior art method
By taking pockmarks core 468.75mg, Radix Paeoniae 156.25mg, Radix Et Rhizoma Rhei 312.50mg, Cortex Magnoliae Officinalis in prescription respectively
156.25mg, Fructus Aurantii Immaturus 156.25mg, Semen Armeniacae Amarum 156.25mg, and according to known decocting method extraction, will own
Medical material in water extraction 2 hours, with the extracted effective ingredient of weighing method measurement as 281.25mg after extraction.
According to above-described embodiment and comparative example result it is seen that using the method for the present invention, compared to prior art
Water-boiling method, more effective ingredient can be extracted, and have preferably effect.
Claims (10)
1. a kind of BUZHONG YIQI TANG, the extraction side of banxia xiexin decoction, FUFANG DANSHEN PIAN and four kinds of prescriptions of Maziren Wan
Method, it comprises the steps of：
A (), by the Radix Angelicae Sinensis in prescription and Rhizoma Zingiberis Recenss, is steamed with the mixture of 85～90wt% ethanol and 10～15wt% water respectively
Steam distillation 1～3 hour；
(b) by the Radix Et Rhizoma Rhei in prescription, Semen Armeniacae Amarum, Radix Ginseng, Radix Astragali, Radix Bupleuri, Radix Paeoniae and Radix Salviae Miltiorrhizae, respectively with 10～30wt%
The mixture of ethanol and 70～90wt% water extracts 1～3 hour；
C (), by the Rhizoma Pinelliae in prescription, extracts 1～3 with the mixture of 70～90wt% ethanol and 10～30wt% water little
When；
D () by the medical material beyond above-mentioned steps (a)～(c), respectively with water extraction 1～3 hour, is repeated twice；
E above-mentioned steps (a)～(d) extract is merged by ().
2. extracting process as claimed in claim 1 it is characterised in that this BUZHONG YIQI TANG prescription be Radix Astragali, Radix Ginseng,
Radix Glycyrrhizae Preparata, white, Rhizoma Cimicifugae, Radix Bupleuri, Rhizoma Zingiberis Recenss, Fructus Jujubae, Radix Angelicae Sinensis and Pericarpium Citri Reticulatae.
3. extracting process as claimed in claim 1 it is characterised in that this banxia xiexin decoction prescription be the Rhizoma Pinelliae, Radix Scutellariae,
Rhizoma Zingiberiss, Radix Ginseng, Rhizoma Coptidis, Fructus Jujubae and Radix Glycyrrhizae Preparata.
4. extracting process as claimed in claim 1 is it is characterised in that the prescription of this FUFANG DANSHEN PIAN is Radix Salviae Miltiorrhizae, Radix Notoginseng
And Borneolum Syntheticum.
5. extracting process as claimed in claim 1 it is characterised in that this Maziren Wan prescription be pockmarks core, Radix Paeoniae,
Radix Et Rhizoma Rhei, Cortex Magnoliae Officinalis, Fructus Aurantii Immaturus and Semen Armeniacae Amarum.
6. extracting process as claimed in claim 1 is it is characterised in that this step (a) is with 90wt% ethanol and 10wt% water
Mixture steam distillation 1 hour.
7. extracting process as claimed in claim 1 is it is characterised in that this step (b) is with 30wt% ethanol and 70wt% water
Mixture extract 1 hour.
8. extracting process as claimed in claim 1 is it is characterised in that this step (c) is with 70wt% ethanol and 30wt% water
Mixture extract 1 hour.
9. extracting process as claimed in claim 1, it filters after being contained in each (a)～(d) step further.
10. extracting process as claimed in claim 1, it comprises step (f) further by mixture pelleting.
Priority Applications (1)
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| CN201510456846.0A CN106389525A (en) | 2015-07-30 | 2015-07-30 | Extraction method for spleen-stomach invigorating and qi replenishing decoction prescription, pinellia ternata heart-removing decoction prescription, compound salvia miltiorrhiza tablet prescription, and hemp seed pill prescription |
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| CN201510456846.0A CN106389525A (en) | 2015-07-30 | 2015-07-30 | Extraction method for spleen-stomach invigorating and qi replenishing decoction prescription, pinellia ternata heart-removing decoction prescription, compound salvia miltiorrhiza tablet prescription, and hemp seed pill prescription |
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| CN106389525A true CN106389525A (en) | 2017-02-15 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1569054A (en) * | 2003-07-22 | 2005-01-26 | 天津天士力制药股份有限公司 | Dripping pills of 'Xiao Chaihu' |
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- 2015-07-30 CN CN201510456846.0A patent/CN106389525A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1569054A (en) * | 2003-07-22 | 2005-01-26 | 天津天士力制药股份有限公司 | Dripping pills of 'Xiao Chaihu' |
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