CN106359907A - Stearic acid mixture, and preparation method and application thereof - Google Patents
Stearic acid mixture, and preparation method and application thereof Download PDFInfo
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- CN106359907A CN106359907A CN201610795417.0A CN201610795417A CN106359907A CN 106359907 A CN106359907 A CN 106359907A CN 201610795417 A CN201610795417 A CN 201610795417A CN 106359907 A CN106359907 A CN 106359907A
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- stearic acid
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Abstract
The invention belongs to the technical field of feed additives, and particularly relates to a stearic acid mixture, and a preparation method and application thereof. The stearic acid mixture provided by the invention comprises the following components in percentage by weight: 10-35% of stearic acid, 10-30% of magnesium stearate, 30-50% of calcium stearate and 5-10% of silicon dioxide. The stearic acid mixture provided by the invention has favorable mixing uniformity in the feed, reduces the consumption of stearic acid, and especially can enhance the meat yield of lambs after being mixed with the lamb feed.
Description
Technical field
The invention belongs to field of feed additive technology, particularly to a kind of stearic acid mixture and preparation method thereof and should
With.
Background technology
In the Feed Manufacturing course of processing, some raw materials easy moisture absorption caking or viscosity be strong, poor fluidity, pulverized in processing
In journey, often caking cannot be processed, and therefore often adds wandering agent.
Wandering agent, also known as anti-caking agent, can improve feedstuff mobility, prevents from luming, and be conducive to improving it and rush down note property and storage
The function of the stability deposited, is conducive to the accuracy of dispensing and the mix homogeneously of feedstuff.
How as anti-caking agent, large usage quantity in feedstuff, addition is 1-10% to stearic acid.But stearic acid is in feedstuff work
In industry with when have a following defect: sterling stearic acid because its density is less, loose, there is certain viscosity and lead to free-running property relatively
Difference, the mixing homogeneity therefore in feedstuff is extremely limited, has had a strong impact on using effect in feedstuff for this product.For upper
State deficiency, Chinese patent cn104186972b discloses a kind of stearic acid mixture, and component includes stearic acid, silicon dioxide, chlorine
Change calcium.The technical problem underlying that this patent solves is under identical action effect, reduces stearic consumption.
Stearic acid is not only a kind of anti-caking agent, simultaneously a kind of still energy feedstuff, due to fatty acid is directly added into can be right
Animal tumor damages for gastric microorganism, and and then affect cud in microorganism normal fermentation, be unfavorable for the health of animal.
Therefore poor except there is free-running property, we also should need to consider that stearic acid is used for how playing good nutriture value in feedstuff
Value.
Content of the invention
It is an object of the invention to provide a kind of stearic acid mixture and its preparation method and application, described stearic acid mixing
Thing has good mixing homogeneity in feedstuff, can play the effect of good anti-caking, and stearic acid dosage reduces.
Meanwhile it has unexpectedly been found that by stearic acid mixture of the present invention and feedstuff, especially after the mixing of lamb feedstuff, being conducive to improving
The quality of mutton of lamb.
The technical solution used in the present invention is as follows:
A kind of stearic acid mixture, including following components and its percetage by weight: stearic acid 10-35%, magnesium stearate 10-
30%th, calcium stearate 30-50%, silicon dioxide 5-10%.
Preferably, it is made up of following components and its percetage by weight: stearic acid 33%, magnesium stearate 21%, calcium stearate
40%th, silicon dioxide 6%.
Magnesium stearate density is 1.07, and fusing point is 88.5 DEG C, is slightly soluble in water, can resolve into stearic acid under strong acid environment
And magnesium ion.The stable in properties of magnesium stearate, not self-polymerization, there is the effect such as lubrication, anti-stick, fluidizer.
Fatty acid calcium is a kind of auxotype energy additive, and predominantly body provides energy, does not affect the normal life of body
Reason metabolism.In addition, fatty acid calcium can also produce favorable influence to the utilization of other nutrient substance.Calcium stearate is a kind of important
Fatty acid calcium, its ionization ph be 4.5-5, under animal small intestinal sour environment, be dissolved into stearic acid fat acid and calcium ion dissociate
Out, utilized by intestinal absorption.
Silicon dioxide is a kind of conventional wandering agent.
Present invention also offers a kind of preparation method of described stearic acid mixture, weigh the Hard Fat of corresponding weight portion first
Acid and silicon dioxide, the two adds the calcium stearate of corresponding weight portion, mixes again after being sufficiently mixed, be eventually adding corresponding weight
Part magnesium stearate mix homogeneously, obtains stearic acid mixture.
When described stearic acid mixture is applied in feedstuff, the not super feed relative of addition of stearic acid mixture
For 1%-2%.
Preferably, in feedstuff, stearic acid mixture addition is the 1.5% of feed relative.
Compared with prior art, stearic acid mixture not only has good mixing homogeneity in feedstuff to the present invention, subtracts
Lack stearic consumption, and and feedstuff, especially after the mixing of lamb feedstuff, be conducive to improving the meat production of lamb.
Specific embodiment
Hereinafter technical scheme is illustrated with specific embodiment, but protection scope of the present invention not limited to this:
Embodiment 1
A kind of stearic acid mixture, is made up of following component and its percetage by weight: stearic acid 35%, magnesium stearate
30%th, calcium stearate 30%, silicon dioxide 5%.
Preparation method: weigh stearic acid and the silicon dioxide of corresponding weight portion first, the two adds corresponding after being sufficiently mixed
The calcium stearate of weight portion, mixes again, is eventually adding corresponding weight portion magnesium stearate mix homogeneously, obtains stearic acid mixing
Thing.
Embodiment 2
A kind of stearic acid mixture, is made up of following component and its percetage by weight: stearic acid 20%, magnesium stearate %,
Calcium stearate 50%, silicon dioxide 9%.
Preparation method is similar to Example 1.
Embodiment 3
A kind of stearic acid mixture, is made up of following component and its percetage by weight: stearic acid 33%, magnesium stearate
21%th, calcium stearate 40%, silicon dioxide 6%.
Preparation method is similar to Example 1.
Comparative example 1
A kind of stearic acid mixture, is made up of following component and its percetage by weight: stearic acid 33%, magnesium stearate
21%th, calcium stearate 40%, calcium chloride 6%.
Preparation method is similar to Example 1.
Difference with embodiment 3 is, silicon dioxide is replaced with calcium chloride.
Comparative example 2
A kind of stearic acid mixture, is made up of following component and its percetage by weight: stearic acid 53%, calcium stearate
61%, silicon dioxide 6%.
Preparation method is similar to Example 1.
Difference with embodiment 3 is, does not add magnesium stearate, increased the consumption of calcium stearate.
The detection of each product dispersed homogeneous degree of test example 1
Test object: the stearic acid mixture that embodiment 1-3 and comparative example 1-2 prepare.
Test content: above-mentioned test object is mixed with feedstuff respectively, carries out mixing homogeneity detection, test process and knot
Fruit is as follows:
1) mixing homogeneity in feedstuff for embodiment 1 product
In feedstuff the addition of embodiment 1 product press 1.1% (press 11 kilograms of stearic acid mixtures in feedstuff per ton to add,
Press 1.93 grams of stearic acid in every 500 grams of feedstuffs) add, take 5 Feed Samples respectively in material receiving port, about 500 grams of each sample,
Survey stearic content in each sample, as shown in table 1:
Table 1 embodiment 1 stearic acid mixture dispersed homogeneous degree in feedstuff
Sample | Forage volume (g) | Stearic acid content (g) | Content ratio |
1 | 498 | 2 | 0.40% |
2 | 501 | 1.9 | 0.38% |
3 | 478 | 1.95 | 0.39% |
4 | 493 | 1.85 | 0.37% |
5 | 486 | 1.95 | 0.39% |
2) mixing homogeneity in feedstuff for embodiment 2 product:
In feedstuff the addition of embodiment 2 product press 1.5% (press 15 kilograms of stearic acid mixtures in feedstuff per ton to add,
Press 1.5 grams of stearic acid in every 500 grams of feedstuffs) add, take 5 Feed Samples respectively in material receiving port, about 500 grams of each sample,
Survey stearic content in each sample, as shown in table 2:
Table 2 embodiment 2 stearic acid mixture dispersed homogeneous degree in feedstuff
Sample | Forage volume (g) | Stearic acid content (g) | Content ratio |
1 | 488 | 1.51 | 0.31% |
2 | 499 | 1.48 | 0.30% |
3 | 500 | 1.45 | 0.29% |
4 | 496 | 1.49 | 0.30% |
5 | 498 | 1.59 | 0.32% |
3) mixing homogeneity in feedstuff for embodiment 3 product:
In feedstuff the addition of embodiment 3 product press 1.5% (press 15 kilograms of stearic acid mixtures in feedstuff per ton to add,
Press 2.48 grams of stearic acid in every 500 grams of feedstuffs) add, take 5 Feed Samples respectively in material receiving port, about 500 grams of each sample,
Survey stearic content in each sample, as shown in table 3:
Table 3 embodiment 3 stearic acid mixture dispersed homogeneous degree in feedstuff
4) mixing homogeneity in feedstuff for comparative example 1 product:
In feedstuff, the addition of comparative example 1 product (is added by 10.5 kilograms of stearic acid mixtures in feedstuff per ton by 1.05%
Plus, press 4.75 grams of stearic acid in every 500 grams of feedstuffs) add, take 5 Feed Samples, each sample about 500 respectively in material receiving port
Gram, survey stearic content in each sample, as shown in table 4:
Table 4 comparative example 1 stearic acid mixture dispersed homogeneous degree in feedstuff
Sample | Forage volume (g) | Stearic acid content (g) | Content ratio |
1 | 493 | 4.83 | 0.98% |
2 | 487 | 4.48 | 0.92% |
3 | 514 | 5.08 | 0.99% |
4 | 487 | 4.68 | 0.96% |
5 | 496 | 4.66 | 0.94% |
5) mixing homogeneity in feedstuff for comparative example 2 product:
In feedstuff the addition of comparative example 2 product press 1.5% (press 15 kilograms of stearic acid mixtures in feedstuff per ton to add,
Press 3.975 grams of stearic acid in every 500 grams of feedstuffs) add, take 5 Feed Samples, each sample about 500 respectively in material receiving port
Gram, survey stearic content in each sample, as shown in table 5:
Table 5 comparative example 2 stearic acid mixture dispersed homogeneous degree in feedstuff
Sample | Forage volume (g) | Stearic acid content (g) | Content ratio |
1 | 496 | 3.87 | 0.78% |
2 | 477 | 3.82 | 0.80% |
3 | 506 | 3.84 | 0.76% |
4 | 487 | 3.79 | 0.78% |
5 | 486 | 3.84 | 0.79% |
From table 1- table 5, in embodiment 3 stearic distribution consistency degree due to comparative example, better than embodiment 1,2, by
This may certify that stearic acid mixture of the present invention, is added in feedstuff and not only can reduce stearic consumption, and makes Hard Fat
Acid has good dispersion.
The impact to lamb meat production for each product of test example 2
Test object: the stearic acid mixture that embodiment 1-3 and comparative example 1-2 prepare.
Test content: from health, body weight homogeneous (22.24~26.01kg) 3 monthly age wean boer goat ewe lamb 36,
It is randomly divided into 4 groups by body weight, every group sets 3 repetitions, each repeats 3 sheep, using the lamb feedstuff adding above-mentioned test object
Fed.After prerun 10 days, enter and just try the phase, totally 40 days.Then lamb meat production is evaluated, result such as table 6 institute
Show.
The impact to lamb meat production for table 6 stearic acid mixture
Group | Stearic acid mixture adds | Slaughter weight (kg) | Carcass weight (kg) | Dressing percentage (%) |
1 | Embodiment 1 | 37.24±0.28* | 16.26±0.44* | 41.68±0.26* |
2 | Embodiment 2 | 38.14±0.46**## | 16.82±0.24**## | 42.16±0.84**# |
3 | Embodiment 3 | 39.56±0.42**## | 19.86±0.64**## | 43.22±0.52**## |
4 | Comparative example 1 | 36.86±0.22 | 15.76±0.46 | 40.22±0.42 |
5 | Comparative example 2 | 37.13±0.34 | 16.24±0.24 | 40.56±0.28 |
Note: * compares p < 0.05 with comparative example 1, represents significant difference;
* compares p < 0.01 with comparative example 1, represents that difference is extremely notable;
#Compare p < 0.05 with comparative example 2, represent significant difference;
##Compare p < 0.05 with comparative example 2, represent that difference is extremely notable.
As shown in Table 6, each test group slaughter weight (kg), carcass weight (kg), dressing percentage (%) are above matched group, and the
Three groups of differences are extremely notable (p < 0.01).Illustrate, feedstuff adds enforcement stearic acid mixture of the present invention and can improve lamb product
Meat performance.
Claims (5)
1. a kind of stearic acid mixture is it is characterised in that include following component and its percetage by weight: stearic acid 10-35%, hard
Fatty acid magnesium 10-30%, calcium stearate 30-50% and silicon dioxide 5-10%.
2. stearic acid mixture according to claim 1 is it is characterised in that by following component and its weight percent array
Become: stearic acid 33%, magnesium stearate 21%, calcium stearate 40% and silicon dioxide 6%.
3. stearic acid mixture according to claim 1 and 2 it is characterised in that in feedstuff the adding of stearic acid mixture
Dosage is the 1%-2% of feeding quality.
4. stearic acid mixture according to claim 3 it is characterised in that in feedstuff stearic acid mixture addition
For feeding quality 1.5%.
5. the preparation method according to the arbitrary described stearic acid mixture of claim 1-4 is it is characterised in that weigh corresponding first
The stearic acid of percetage by weight and silicon dioxide, the two adds the calcium stearate of corresponding percetage by weight after being sufficiently mixed, again
Mix, be eventually adding corresponding percetage by weight magnesium stearate mix homogeneously, obtain stearic acid mixture.
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CN103783288A (en) * | 2014-01-07 | 2014-05-14 | 宁夏大学 | Method for preventing caking of feed-grade threonine crystal |
CN104171383A (en) * | 2014-07-11 | 2014-12-03 | 杭州天农生物营养技术有限公司 | Vitamin c fat filming and coating technology |
CN104186972A (en) * | 2014-08-01 | 2014-12-10 | 颜彦 | Stearic acid mixture, and preparation method and application thereof |
CN105831424A (en) * | 2016-04-12 | 2016-08-10 | 重庆威士化工有限公司 | A feed antioxidant resisting self attenuation, a preparing method thereof and a feed antioxidation method |
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2016
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CN101467592A (en) * | 2007-12-29 | 2009-07-01 | 农村振兴厅 | Ruminant feed addictive for protecting vitamin C as well as preparation method and application thereof |
CN103535510A (en) * | 2013-09-24 | 2014-01-29 | 广州市天朝生物科技有限公司 | Feed for late-stage fattening and lactation promoting of livestock/poultry and ruminants |
CN103783288A (en) * | 2014-01-07 | 2014-05-14 | 宁夏大学 | Method for preventing caking of feed-grade threonine crystal |
CN104171383A (en) * | 2014-07-11 | 2014-12-03 | 杭州天农生物营养技术有限公司 | Vitamin c fat filming and coating technology |
CN104186972A (en) * | 2014-08-01 | 2014-12-10 | 颜彦 | Stearic acid mixture, and preparation method and application thereof |
CN105831424A (en) * | 2016-04-12 | 2016-08-10 | 重庆威士化工有限公司 | A feed antioxidant resisting self attenuation, a preparing method thereof and a feed antioxidation method |
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