CN106351037B - A kind of energy-saving dyeing method of silk floss textile - Google Patents

A kind of energy-saving dyeing method of silk floss textile Download PDF

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CN106351037B
CN106351037B CN201610745091.0A CN201610745091A CN106351037B CN 106351037 B CN106351037 B CN 106351037B CN 201610745091 A CN201610745091 A CN 201610745091A CN 106351037 B CN106351037 B CN 106351037B
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textile
accelerant
added
neopelex
energy
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CN106351037A (en
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钱安华
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Zhejiang De Yu Import & Export Co Ltd
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C7/00—Heating or cooling textile fabrics
    • D06C7/02—Setting
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621—Compounds without nitrogen
    • D06P1/622—Sulfonic acids or their salts
    • D06P1/625—Aromatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491—(Thio)urea or (cyclic) derivatives
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65125—Compounds containing ester groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/653—Nitrogen-free carboxylic acids or their salts
    • D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/667—Organo-phosphorus compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/82—Textiles which contain different kinds of fibres
    • D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
    • D06P3/8219—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and amide groups

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Coloring (AREA)

Abstract

A kind of energy-saving dyeing method of silk floss textile, using special accelerant, not only dyeing effect is uniform, and bath raio is low, and dyeing time is short, greatly reduces energy consumption and reduces the usage amount of water, is good for the environment.The accelerant includes epoxidation triglyceride, triethyl group hexyl phosphoric acid, neopelex, chelating agent, urea, lignosulfonates, dispersing agent, water and organic acid, in such a way that epoxidation triglyceride, triethyl group hexyl phosphoric acid and neopelex cooperate jointly, enhance emulsifying effectiveness, it is used in conjunction with again with additives such as chelating agent, levelling agent, dispersing agents, dye aberration is small.

Description

A kind of energy-saving dyeing method of silk floss textile
Technical field
The present invention relates to technical field of textile printing more particularly to a kind of energy-saving dyeing methods of silk floss textile.
Background technique
Cotton fiber occupies an important position in textile industry, accounts about the 65% of fiber total output.It applies at present in cotton Most important, most potential dyestuff in terms of stock-dye is reactive dye.Reactive dye and cotton fiber pass through Covalent bonding together, Fundamentally solve the problems, such as that coloured fibre wet colour fastness is poor.Simultaneously as reactive dye have chromatography complete, color is fresh Gorgeous, the advantages that technique for applying is easy, strong applicability, price is relatively cheap, it had become yield in cotton fiber dyestuff in recent years With the maximum dyestuff of the output value.It must be added to a large amount of sodium chloride or sodium sulphate in traditional reactive dyeing process, work as dye After salt is added in bath, the hydrauture of dyestuff reduces, and such dyestuff is increased by from aqueous solution to the tendency that fiber surface shifts, and balances Upper dye amount just increases.
The structure of silk and cotton fiber is different, causes the upper dye amount to color also different, and when dyeing be easy to cause color difference, especially Color difference is more serious when it is light color, and traditional ameliorative way is to extend dyeing time, a large amount of levelling agent is added, along with leaching The auxiliary processes such as method enhancing dyeing effect is rolled, but the requirement with country to dyeing energy-saving and emission-reduction is higher and higher, tradition Highly energy-consuming, water consumption method can not adapt to the requirement of Modern Textile Industry.
Summary of the invention
In order to solve the problems in background technique, the present invention provides a kind of energy-saving dyeing method of silk floss textile, can be with Greatly reduce dyeing time and water consumption.
A kind of energy-saving dyeing method of silk floss textile, comprising the following steps:
A, dye: reactive dye 2-10%, silk flosssilk wadding textile accelerant 3-5%, bath raio: 1:(10-15), pH value 7.5- 8.0, dyeing temperature control is at 80-90 DEG C, time 8-15min；
B, high-temperature shaping: temperature: 120-130 DEG C, the time: 20-30s.
The silk flosssilk wadding textile accelerant, the ingredient including following weight percent:
Chelating agent 8-12%
Urea 2-5%
Lignosulfonates 12-20%
Organic acid 15-20%
Epoxidation triglyceride 2-5%
Triethyl group hexyl phosphoric acid 0.2-0.5%
Neopelex 5-8%
Dispersing agent 10-15%
Deionized water surplus.
Preferably, the organic acid is acetic acid.
Preferably, the chelating agent is EDTA.
Preferably, the dispersing agent is Sodium Polyacrylate.
The preparation method of the silk flosssilk wadding textile accelerant, comprising the following steps:
Step 1: by epoxidation triglyceride, triethyl group hexyl phosphoric acid and the common dry method ball of neopelex Mill, and 325 meshes are crossed, obtain mixed-powder A；
Step 2: mixed-powder A is added in deionized water, is stirred evenly；
Step 3: chelating agent, urea, lignosulfonates and dispersing agent is added, stirs evenly；
Step 4: 600-800rpm stir speed under, be slowly added to organic acid, after being added completely into, be further continued for stirring 10- 15min.
Preferably, it is needed when accelerant use of the present invention and reactive dye is used cooperatively.
Preferably, the reactive dye are vinyl-sulfone reactive dyes.
The energy-saving dyeing method of silk floss textile of the present invention, using special accelerant, accelerant uses epoxidation glycerol The mode that three acid esters, triethyl group hexyl phosphoric acid and neopelex cooperate jointly, enhances emulsifying effectiveness, then with chelating The additives such as agent, levelling agent, dispersing agent are used in conjunction with, and not only dyeing effect is uniform, and bath raio is low, and dyeing time is short, significantly It reduces energy consumption and reduces the usage amount of water, be good for the environment.
Specific embodiment
Embodiment 1
A kind of silk flosssilk wadding textile accelerant, the ingredient including following weight percent:
EDTA 10%
Urea 3%
Lignosulfonates 15%
Acetic acid 17%
Epoxidation triglyceride 3%
Triethyl group hexyl phosphoric acid 0.3%
Neopelex 6%
Sodium Polyacrylate 12%
Deionized water surplus；
A kind of preparation method of silk flosssilk wadding textile accelerant, comprising the following steps:
Step 1: by epoxidation triglyceride, triethyl group hexyl phosphoric acid and the common dry method ball of neopelex Mill, and 325 meshes are crossed, obtain mixed-powder A；
Step 2: mixed-powder A is added in deionized water, is stirred evenly；
Step 3: chelating agent, urea, lignosulfonates and dispersing agent is added, stirs evenly；
Step 4: 750rpm stir speed under, be slowly added to organic acid, after being added completely into, be further continued for stirring 12min, i.e., It can；
It is needed when the described accelerant use and reactive dye be used cooperatively；
The reactive dye are vinyl-sulfone reactive dyes.
Embodiment 2
A kind of silk flosssilk wadding textile accelerant, the ingredient including following weight percent:
EDTA 12%
Urea 2%
Lignosulfonates 20%
Acetic acid 15%
Epoxidation triglyceride 5%
Triethyl group hexyl phosphoric acid 0.2%
Neopelex 8%
Sodium Polyacrylate 10%
Deionized water surplus；
A kind of preparation method of silk flosssilk wadding textile accelerant, comprising the following steps:
Step 1: by epoxidation triglyceride, triethyl group hexyl phosphoric acid and the common dry method ball of neopelex Mill, and 325 meshes are crossed, obtain mixed-powder A；
Step 2: mixed-powder A is added in deionized water, is stirred evenly；
Step 3: chelating agent, urea, lignosulfonates and dispersing agent is added, stirs evenly；
Step 4: 800rpm stir speed under, be slowly added to organic acid, after being added completely into, be further continued for stirring 10min, i.e., It can；
It is needed when the described accelerant use and reactive dye be used cooperatively；
The reactive dye are vinyl-sulfone reactive dyes.
Embodiment 3
A kind of silk flosssilk wadding textile accelerant, the ingredient including following weight percent:
EDTA 8%
Urea 5%
Lignosulfonates 12%
Acetic acid 20%
Epoxidation triglyceride 2%
Triethyl group hexyl phosphoric acid 0.5%
Neopelex 5%
Sodium Polyacrylate 15%
Deionized water surplus；
A kind of preparation method of silk flosssilk wadding textile accelerant, comprising the following steps:
Step 1: by epoxidation triglyceride, triethyl group hexyl phosphoric acid and the common dry method ball of neopelex Mill, and 325 meshes are crossed, obtain mixed-powder A；
Step 2: mixed-powder A is added in deionized water, is stirred evenly；
Step 3: chelating agent, urea, lignosulfonates and dispersing agent is added, stirs evenly；
Step 4: 600rpm stir speed under, be slowly added to organic acid, after being added completely into, be further continued for stirring 15min, i.e., It can；
It is needed when the described accelerant use and reactive dye be used cooperatively；
The reactive dye are vinyl-sulfone reactive dyes.
Embodiment 4
Using the accelerant of the embodiment of the present invention 1, silk floss textile is dyed, the specific steps are as follows:
A, it dyes: reactive dye 3%, silk flosssilk wadding textile accelerant 4%, bath raio: 1:12, pH value 7.5-8.0, dyeing temperature Control is at 88 DEG C, time 12min；
B, high-temperature shaping: temperature: 125 DEG C, the time: 25s.
Embodiment 5
Using the accelerant of the embodiment of the present invention 3, silk floss textile is dyed, the specific steps are as follows:
A, it dyes: reactive dye 10%, silk flosssilk wadding textile accelerant 3%, bath raio: 1:15, pH value 7.5-8.0, dyeing temperature Degree control is at 80 DEG C, time 8-15min；
B, high-temperature shaping: temperature: 130 DEG C, the time: 20s.
Embodiment 6
Using the accelerant of the embodiment of the present invention 2, silk floss textile is dyed, the specific steps are as follows:
A, it dyes: reactive dye 2%, silk flosssilk wadding textile accelerant 5%, bath raio: 1:10, pH value 7.5-8.0, dyeing temperature Control is at 90 DEG C, time 8min；
B, high-temperature shaping: temperature: 130 DEG C, the time: 20s.
It in embodiment 4-6, is dyed using colouring method of the invention, obtained silk floss textile dyeing effect is equal It is even, no color differnece, and also bath raio is low in dyeing course, and dyeing time is short, greatly reduces energy consumption and reduces the usage amount of water, has Conducive to environmental protection.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (2)

1. a kind of energy-saving dyeing method of silk floss textile, which comprises the following steps:
A, dye: reactive dye 2-10%, silk flosssilk wadding textile accelerant 3-5%, bath raio: 1:(10-15), pH value 7.5-8.0, dye Color temperature control is at 80-90 DEG C, time 8-15min；
B, high-temperature shaping: temperature: 120-130 DEG C, the time: 20-30s；
The silk flosssilk wadding textile accelerant, the ingredient including following weight percent:
Chelating agent 8-12%
Urea 2-5%
Lignosulfonates 12-20%
Organic acid 15-20%
Epoxidation triglyceride 2-5%
Triethyl group hexyl phosphoric acid 0.2-0.5%
Neopelex 5-8%
Dispersing agent 10-15%
Deionized water surplus；
The organic acid is acetic acid；
The chelating agent is EDTA；
The dispersing agent is Sodium Polyacrylate；
The reactive dye are vinyl-sulfone reactive dyes.
2. the energy-saving dyeing method of silk floss textile as described in claim 1, which is characterized in that the silk flosssilk wadding textile promotees The preparation method of stain, comprising the following steps:
Step 1: by epoxidation triglyceride, triethyl group hexyl phosphoric acid and the common dry ball milling of neopelex, and 325 meshes are crossed, mixed-powder A is obtained；
Step 2: mixed-powder A is added in deionized water, is stirred evenly；
Step 3: chelating agent, urea, lignosulfonates and dispersing agent is added, stirs evenly；
Step 4: 600-800rpm stir speed under, be slowly added to organic acid, after being added completely into, be further continued for stirring 10-15min, ?.
CN201610745091.0A 2016-08-29 2016-08-29 A kind of energy-saving dyeing method of silk floss textile Active CN106351037B (en)

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Publication number Priority date Publication date Assignee Title
CN110616573B (en) * 2019-06-14 2022-02-18 杭州众智纺织科技有限责任公司 Process for improving dyeing color fastness of sodium sulfate-free reactive dye for rayon

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101492887A (en) * 2008-01-22 2009-07-29 上海德桑精细化工有限公司 Phthalocyanine reactive dyeing leveling agent
CN101560736A (en) * 2009-03-19 2009-10-21 宁波新科纺织助剂有限公司 Accelerant for textile dyeing, preparation method and applications thereof
CN103726358A (en) * 2013-12-31 2014-04-16 江苏中新资源集团有限公司 Fabric dyeing accelerant
CN104562779A (en) * 2015-02-04 2015-04-29 湖州申祥丝织有限责任公司 Novel dyeing assistant for improving color fastness of textile and preparation method of novel dyeing assistant
CN104727168A (en) * 2015-03-31 2015-06-24 五邑大学 Dyeing promoter for reactive dye and using method of dyeing promoter
CN105178065A (en) * 2015-10-30 2015-12-23 朱忠良 Denim accelerating agent and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101492887A (en) * 2008-01-22 2009-07-29 上海德桑精细化工有限公司 Phthalocyanine reactive dyeing leveling agent
CN101560736A (en) * 2009-03-19 2009-10-21 宁波新科纺织助剂有限公司 Accelerant for textile dyeing, preparation method and applications thereof
CN103726358A (en) * 2013-12-31 2014-04-16 江苏中新资源集团有限公司 Fabric dyeing accelerant
CN104562779A (en) * 2015-02-04 2015-04-29 湖州申祥丝织有限责任公司 Novel dyeing assistant for improving color fastness of textile and preparation method of novel dyeing assistant
CN104727168A (en) * 2015-03-31 2015-06-24 五邑大学 Dyeing promoter for reactive dye and using method of dyeing promoter
CN105178065A (en) * 2015-10-30 2015-12-23 朱忠良 Denim accelerating agent and preparation method thereof

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