CN106334338A - Single-stage elution device for animal and plant raw materials and method and application thereof - Google Patents

Single-stage elution device for animal and plant raw materials and method and application thereof Download PDF

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Publication number
CN106334338A
CN106334338A CN201611017445.6A CN201611017445A CN106334338A CN 106334338 A CN106334338 A CN 106334338A CN 201611017445 A CN201611017445 A CN 201611017445A CN 106334338 A CN106334338 A CN 106334338A
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washing
animal
separating liquid
leaching
plant material
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不公告发明人
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0223—Moving bed of solid material
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/108—Production of fats or fatty oils from raw materials by extracting after-treatment, e.g. of miscellae
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention provides a single-stage elution device for animal and plant raw materials and a method and application thereof and belongs to the technical field of animal and plant extraction. The single-stage elution device is characterized in that a discharging port of a leaching device (1) is in pipe connection with a feeding port of a washing and dehydration device, and a liquid outlet of the washing and dehydration device is connected with a separated liquid output pipe (15) and a separated liquid return pipe (14) respectively; a material outlet of the washing and dehydration device is connected with a first conveyor (5) and a second a conveyor (6) respectively; the output end of the separated liquid return pipe (14) and the output end of the first conveyor (5) are connected with the leaching device (1); the washing and dehydration device comprises a rinsing machine (10) and a centrifugal dehydrator (11). The single-stage elution device for animal and plant raw materials can thoroughly achieve rapid and effective solid-liquid separation, smashes the raw materials into fin powder for membrane separation and extraction, has higher yield and leaching efficiency, can obviously improve the concentration of the permeate, decreases solvent consumption and reduces the production costs.

Description

A kind of single-stage washing device for animal-plant material and its method and purposes
Technical field
A kind of single-stage washing device for animal-plant material and its method and purposes, belong to animals and plants extractive technique neck Domain.
Background technology
Animal-plant material leaches and refers to using suitable solvent or method, from animal-plant material (whole or certain part) Middle extraction processes acquisition effective ingredient (effective ingredient can be dissolved in solvent).In existing industrial mass production, animal-plant material How the extracting mode of middle effective ingredient, obtain sheet-shaped material using by dry for animal-plant material, tabletting, sheet-shaped material sprayed molten Agent, the extracting solution of results.Or, animal-plant material is ground into centimetre grade particles and adds solvent (as ethanol solution) hot reflux to carry Take, when solid-liquid separation is carried out to extracting solution many using centimetre or grade defecator carry out coarse filtration, then carry out separating essence System (as extraction, distillation).
Applicant finds under study for action, existing leaching device there is problems in that first, existing film leaching device, The concentration of gained permeate is low, needs to complete to extract using substantial amounts of solvent, not only increased the cost of solvent in extraction process, Also add later separation, energy consumption that is refined, concentrating permeate.Secondly, it is found by the applicant that the yield of existing leaching device is relatively Low, it is difficult to abolish the cell wall of animal-plant material by the way of tabletting or Centimeter Level coarse pulverization, even if extending spray or soaking Time, effective ingredient is also difficult to leach in solvent, causes to extract insufficient.
Content of the invention
The technical problem to be solved in the present invention is: overcome the deficiencies in the prior art, provide a kind of for animal-plant material Single-stage washing device, raw material pulverizing to fine-powdered can be floated eluent, tool by the single-stage washing device that this is used for animal-plant material There are higher yield and leaching efficiency, and the concentration of gained permeate can be significantly improved, reduce the consumption of solvent, reduce life Produce cost.
The technical solution adopted for the present invention to solve the technical problems is: this is used for the single-stage eluting dress of animal-plant material Put it is characterised in that: include leaching device, washing/dehydrating device and pulverizer, pulverizer passes through feed line and leaches dress Put and be connected, leaching device discharging opening is connected with washing/dehydrating device charging aperture pipeline by mashing pump, washing/dehydrating device Liquid outlet is connected to separating liquid outlet tube and separating liquid return duct；The material outlet of washing/dehydrating device is connected to One conveyer and second conveyor；The outfan of separating liquid return duct and the first conveyer is all connected with leaching device；Washing Dehydration device includes potcher and centrifugal dehydrator.
Washing/dehydrating device, by the way of potcher is combined with dewaterer, carries out de- liquid work after completing to rinse work Sequence, is thoroughly taken off liquid by centrifugal dewaterer and is processed, can thoroughly be deviate from the liquid in material, further to material Guarantee solid-liquid separation effect, meanwhile, can be that follow-up baking operation provides and ensures again, be easy to flash baking.
Described potcher and centrifugal dehydrator are split-type structural, and potcher and centrifugal dehydrator are along material conveying direction Pipeline connects successively.
Described washing/dehydrating device is the eluting all-in-one that potcher and centrifugal dehydrator are wholely set.
Described washing/dehydrating device also includes dehydrator, and potcher, centrifugal dehydrator and dehydrator are integrated setting Eluting drying integral machine.
Described washing/dehydrating device also includes dehydrator, and potcher, centrifugal dehydrator and dehydrator are defeated along material successively Direction pipeline is sent to connect, the solid material outlet side of centrifugal dehydrator is connected with dehydrator.
Solvent recycler is connected with described dehydrator, the liquid outlet of solvent recycler passes through pipeline and centrifugal dehydrator Liquid outlet be connected.
Described pulverizer is Dry-crusher or wet type powder machine, when pulverizer is Dry-crusher, on leaching device It is connected with solvent delivery pipe, solvent delivery pipe is provided with thermoregulator and valve；When pulverizer is wet type powder machine, pulverizer Upper connection solvent delivery pipe.
Pulverizer can be dry grinding machine or wet crushing mill, and when being that wet crushing mill is pulverized, pulverizer is passed through leaching device institute With solvent as pulverizing liquid.Solvent access tube is provided with thermoregulator and valve, is capable of the intake of adjusting solvent, mends Fill solvent, and can solvent temperature in adjusting solvent access tube and leaching device, so that the solvent in leaching device is maintained at Optimum extraction temperature, improves extraction efficiency.
Filter membrane used by described washing/dehydrating device is microfiltration level filter membrane or nanofiltration level filter membrane.
The grinding particle size of described pulverizer is micron order or nanoscale, and the grinding particle size of pulverizer is more than washing dehydration and fills The separation aperture put, the grinding particle size of pulverizer is 990 ~ 1 microns.
It is equipped with control valve on described separating liquid outlet tube, separating liquid return duct, the first conveyer and second conveyor, It is respectively equipped with reflux pump on separating liquid return duct and second conveyor；On described separating liquid outlet tube and the first conveyer respectively It is provided with feeding engine.
Setting reflux pump, can will transmit through liquid and concentrated solution passes back into leaching device in time and is circulated leaching.Separating liquid Outlet tube is provided with the first feeding engine, the permeate of high concentration can be delivered to follow-up refining step in time.First conveyer It is provided with the second feeding engine, can be easy to exclude concentrated solution in time.Due to containing feed particles in concentrated solution, easily in pipeline Middle deposition, the design of the second reflux pump and the second feeding engine can also be easy to the quick conveying of concentrated solution, prevents pipeline because of raw material Granule blocks.
In addition, the explanation for present invention applicant also includes following content:
Animal-plant material can sufficiently be pulverized by pulverizer, raw material is put in leaching device in the form of powdery, powder Broken rear raw material fine powder reaches micron order or nanoscale (990 microns ~ 0.5 nanometer), and the grinding particle size of preferred pulverizer is 990 ~ 1 Micron, under this grinding particle size, Grin-ding energ7 is little, and filter efficiency is high；The grinding particle size of further preferred pulverizer is 700 ~ 2 Micron, the cell wall that can fully abolish most plants under this grinding particle size makes the effective ingredient in animal and plant cellss abundant Leach, improve yield, the grinding particle size of further preferred pulverizer is 600 ~ 35 microns, under this grinding particle size leaching efficiency is relatively Good and crush efficiency and filter efficiency are higher.Therefore, compared to existing technology in raw material tabletting sprayed extract or by raw material It is crushed to a centimetre grade particles extraction, the design that leaching device of the present invention is connected with pulverizer by feed line is so that have The yield of effect composition and leaching efficiency are significantly improved.
And applicant designs, and is filtered using washing device, solves the problems, such as filtration difficulty, the pulverizing of pulverizer Particle diameter is more than the pore size filter of washing device.Washing device can be single film filter, or the membrane filtrations for multiple parallel connections Device.The material of washing device is ceramic filtration membrane or organic polymer filter membrane (filter membrane and solvent need immiscible).
For the filtering accuracy of washing device, filter membrane used by applicant's design washing device is microfiltration level filter membrane or nanofiltration level Filter membrane.Preferably, the separation aperture of washing device is 0.005 ~ 50 micron, this pore diameter range interior energy effective filter stock granule, And ensure, compared with filtration efficiency, to realize large-scale continuous production.It is further preferred that the separation aperture of washing device is 0.5 ~ 30 Micron, this scope separate aperture interior energy enough efficiently separate fatty oil, volatile oil, glycoside, terpenoid, flavonoid, in phenolic compound At least one, and there is higher separation efficiency.
A kind of operational approach of the single-stage washing device for animal-plant material is it is characterised in that comprise the steps:
A) raw material pulverizing is powder by pulverizer, to improve effective ingredient yield and leaching efficiency in leaching device；To pulverize Dusty raw materials afterwards and solvent are pressed proportioning and are added leaching device, and mixing in leaching device is leached；The thing that leaching device is discharged Material, enters washing/dehydrating device by mashing pump and filters；
B) in washing/dehydrating device filter process, close separating liquid outlet tube, open separating liquid return duct and the first conveyer, point The separating liquid separating out and solid material are recycled in leaching device repeatedly, circulation extraction, until the separation in separating liquid return duct When liquid concentration is increased to stationary value, closes separating liquid return duct, open separating liquid outlet tube, so that separating liquid is discharged；
C) when in separating liquid outlet tube, separating liquid concentration starts continuous decrease, now the raw material in leaching device has passed through solvent Fully extract, stop, to supplementing solvent in leaching device, closing the first conveyer, discharge solid material, separating liquid is passed through to separate Liquid outlet tube is discharged.
Extract oils and fatss, the extraction of Chinese medicine extract, spice extraction volatile oil or edible animals and plants raw material in oil plant and extract leaching Propose the application of oily aspect.
Compared with prior art, the beneficial effect that a kind of single-stage washing device for animal-plant material of the present invention has Fruit is:
1st, washing/dehydrating device, by the way of potcher is combined with dewaterer, carries out de- liquid work after completing to rinse work Sequence, is thoroughly taken off liquid by centrifugal dewaterer and is processed, can thoroughly be deviate from the liquid in material, further to material Guarantee solid-liquid separation effect, meanwhile, can be that follow-up baking operation provides and ensures again, be easy to flash baking.
2nd, the single-stage washing device that this is used for animal-plant material has higher yield and leaching efficiency, and can be obvious The concentration improving gained permeate, the consumption reducing solvent, reduces production cost.First, applicant devises leaching device and leads to Cross feed line to be connected with pulverizer, raw material pulverizing is fine-powdered by pulverizer, can abolish the cell of animal-plant material Wall and cell membrane, make effective ingredient fully leach in solvent so that the yield of effective ingredient and leaching efficiency are significantly improved. Secondly, applicant devises leaching device and is connected with membrane filter, compares existing defecator, using membrane filter Micron-sized granule can be filtered, the animal-plant material after the less pulverizing of granule therefore can be added in leaching device (broken Except animal-plant material cell wall), so that the raw material after pulverizing and solvent is fully contacted in leaching device, be sufficiently complete solid-liquid extraction Take, improve the yield of effective ingredient in animal-plant material；Due to filtering accuracy height (less than or equal to micron order) of membrane filter, Solid-liquid separation, the impurity effectively removing in permeate can effectively be carried out.Finally, applicant devises permeate return duct and concentration The liquid outlet of liquid return duct is all connected with leaching device, permeate outlet tube, permeate return duct, concentrated solution outlet tube and It is equipped with control valve on concentrated solution return duct；Separating obtained permeate and concentrated solution are back in leaching device repeatedly, Leaching device fully being extracted, until permeate reaches discharging from permeate outlet tube during higher concentration, not only being improved Yield, and decrease the consumption of solvent, reduce cost.The permeate of high concentration is higher, also reduces subsequently refined, dense Energy consumption during contracting permeate, in a disguised form reduces cost.
3rd, the single-stage washing device that this is used for animal-plant material further increases leaching efficiency.Applicant devises solvent Storage tank.Solvent tank is provided with thermoregulator, can adjust the temperature of solvent, improves leaching efficiency.
4th, this is used for the single-stage washing device compact conformation of animal-plant material, can continuously circulate extraction.Dense by closing Contracting liquid outlet tube, open concentrated solution return duct so that concentrated solution is back to leaching device repeatedly is extracted, using the present invention's The single-stage washing device of animal-plant material, just can continuously be circulated extraction.
5th, this is used for the single-stage washing device low cost of animal-plant material and applied widely.This is used for animal-plant material Single-stage washing device be not only able to extract plant material additionally it is possible to be used for extracting animal material, can be used in multiple fields, example If (extracting almond oil in as extracting bean oil in from Semen sojae atricolor, Semen Armeniacae Amarum, extract in Serpentiss fatty tissue for extracting oils and fatss in oil plant Adeps Serpentiss), the extraction of Chinese medicine extract (extract volatile oil as Ramulus Cinnamomi, ethyl acetate extracts Semen Cassiae extract, methanol as solvent Extract Radix Ginseng in glycoside), spice extract volatile oil (as Flos Rosae Rugosae, castoreum extract volatile oil) or edible animals and plants raw material extract Extraction oil (as extracted carrot oil in Radix Dauci Sativae, extracting algal oil in Sargassum).
Brief description
Fig. 1 is a kind of structural representation of single-stage washing device for animal-plant material of embodiment 1.
Fig. 2 is a kind of structural representation of single-stage washing device for animal-plant material of embodiment 2.
Fig. 3 is a kind of structural representation of single-stage washing device for animal-plant material of embodiment 3.
Fig. 4 is a kind of structural representation of single-stage washing device for animal-plant material of embodiment 4.
Wherein: 1, leaching device 101, feed line 102, solvent delivery pipe 103, thermoregulator 2, wash De- all-in-one 3, pulverizer 301, feeder 4, mashing pump 5, the first conveyer 6, second conveyor 7, backflow Control valve 8, reflux pump 9, separating liquid output control valve 10, potcher 1001, rinsing outlet tube 11, centrifuge dehydration Machine 1101, de- liquid discharge control valve 1102, de- liquid discharge pipe 1103, de- liquid material outlet tube 12, dehydrator 1201st, dry liquid dump valve 1202, separating liquid recovery tube 13, eluting drying integral machine 14, separating liquid return duct 15, Separating liquid outlet tube 16, solvent recycler 17, rinse solvent supplement pipeline.
Specific embodiment
Fig. 1 is highly preferred embodiment of the present invention, and with reference to Fig. 1 ~ 4, the present invention is described further.
Embodiment 1
With reference to Fig. 1, a kind of single-stage washing device for animal-plant material, including leaching device 1, washing/dehydrating device and pulverizing Machine 3, pulverizer 3 is Dry-crusher or wet type powder machine, when pulverizer is Dry-crusher, leaching device 1 is connected with molten Agent delivery pipe 102, solvent delivery pipe 102 is provided with thermoregulator 103 and valve；When pulverizer 3 is wet type powder machine, pulverize Solvent delivery pipe 102 is connected on machine 3.As shown in figure 1, pulverizer 3 is wet type powder machine, pulverizer 3 is connected with solvent delivery Pipe 102 and feed line 101, leaching device 1 is connected with pulverizer 3 by feed line 101, leaching device 1 discharging Mouth is connected with washing/dehydrating device charging aperture pipeline by mashing pump 4, and the liquid outlet of washing/dehydrating device is connected to and separates Liquid outlet tube 15 and separating liquid return duct 14, separating liquid outlet tube 15 is provided with separating liquid output control valve 9.
Washing/dehydrating device is the eluting all-in-one 2 that potcher 10 and centrifugal dehydrator 11 are wholely set.Potcher 10 is Inside is provided with the washing machine carrying out repeated multiple times flushing of motor stirrer, and the side of potcher 10 is provided with rinse solvent and supplements Pipeline 17, rinse solvent supplements pipeline 17 and is provided with corresponding control valve.The concentrated solution outlet of washing/dehydrating device connects respectively There are the first conveyer 5 and second conveyor 6；The outfan of separating liquid return duct 14 and second conveyor 6 all with leaching device 1 It is connected；Control can be equipped with separating liquid outlet tube 15, separating liquid return duct 14, the first conveyer 5 and second conveyor 6 Valve 8.Wherein, agitator can be provided with leaching device 1, leaching device 1 periphery is provided with heater it is also possible to not set heating dress Put.Backwashing water access tube can be provided with washing/dehydrating device.The material of filter membrane used by washing/dehydrating device be inorganic filter membrane or Organic polymer filter membrane, specifically, inorganic filter membrane is ceramic filtration membrane, and organic polymer filter membrane is with leaching device 1 solvent for use not Mutually phased soln.
On separating liquid return duct 14 and reflux pump can be respectively equipped with second conveyor 6.On separating liquid outlet tube 15 and the Feeding engine can be respectively equipped with one conveyer 5.The separation aperture of washing/dehydrating device is 0.005 ~ 50 micron, and washing dehydration fills It is set to NF membrane or micro-filtration membrane, specifically, the separation aperture of washing/dehydrating device is 0.5 ~ 30 micron.The pulverizing grain of pulverizer 3 Spend for 700 ~ 2 microns, the grinding particle size of pulverizer 3 is more than the separation aperture of washing/dehydrating device.Specifically, the powder of pulverizer 3 Particle degree is 600 ~ 35 microns.Pipeline between mashing pump 4 and washing/dehydrating device is provided with pressure gauge.Washing/dehydrating device can Think single film filter, or compose in parallel for multiple film filters.
Embodiment 2
With reference to Fig. 2, except including the structure of embodiment 1, pulverizer 3 is dry type powder machine to the present embodiment, and leaching device 1 connects There is solvent delivery pipe 102, solvent delivery pipe 102 is provided with thermoregulator 103 and valve.Specifically, thermoregulator 103 is Pipe heat exchanger and temperature sensor, thermoregulator 103 can adjust solvent to optimum temperature, improves leaching efficiency.Raw material Cribellum and feeder were also provided with delivery pipe 101, the raw material in order to pulverize to pulverizer 3 carries out sieving, feeding.Powder Broken machine 3 can also replace with grinder, and animal-plant material can be ground into micron particles, effectively by pulverizer 3 and grinder Abolish cell wall, improve yield.
Potcher 10 and centrifugal dehydrator 11 are split-type structural, and potcher 10 and centrifugal dehydrator 11 are along material conveying side Connect to pipeline successively.The feeding end that outlet tube 1001 connects centrifugal dehydrator 11 is passed through to rinse in potcher 10 bottom, and centrifugation is de- Water dispenser 11 side is provided with de- liquid discharge pipe 1102, and de- liquid discharge pipe 1102 is provided with de- liquid and discharges control valve 1101, centrifuge dehydration Machine 11 connects separating liquid outlet tube 15 by de- liquid discharge pipe 1102.
The operational approach that this is used for the single-stage washing device of animal-plant material is as follows:
A) raw material pulverizing is powder by pulverizer 3, to improve effective ingredient yield and leaching efficiency in leaching device 1；By powder Dusty raw materials after broken and solvent are pressed proportioning and are added leaching device 1, and mixing in leaching device 1 is leached；Leaching device 1 is discharged Material, by mashing pump 4 enter washing/dehydrating device in filter；
B) in washing/dehydrating device filter process, close separating liquid outlet tube 15, open separating liquid return duct 14 and the first conveying Machine 5, the separating liquid isolated and solid material are recycled in leaching device 1 repeatedly, circulation extraction, until separating liquid return duct 14 In separating liquid concentration when being increased to stationary value, close separating liquid return duct 14, open separating liquid outlet tube 15, so that separating liquid is arranged Go out；
C) when in separating liquid outlet tube 15, separating liquid concentration starts continuous decrease, now the raw material in leaching device 1 passes through Solvent fully extracts, and stops, to supplementing solvent in leaching device 1, closing the first conveyer 5, discharges solid material, separating liquid (contains Effective ingredient and solvent) discharged by separating liquid outlet tube 15.Using above to separating liquid return duct 14, the first conveyer 5 and The control of control valve on second conveyor 6, realizes the circulation extraction of single-stage system.
Embodiment 3
With reference to Fig. 3, the present embodiment also includes dehydrator 12, potcher except including the structure of embodiment 1, washing/dehydrating device 10th, centrifugal dehydrator 11 and dehydrator 12 are integrated the eluting drying integral machine 13 of setting, on the liquid outlet of washing/dehydrating device It is connected with solvent recycler 16.Pulverizer is Dry-crusher, and leaching device 1 is connected with solvent delivery pipe 102, solvent delivery Pipe 102 is provided with thermoregulator 103 and valve；Pulverizer 3 can be also wet type powder machine, and pulverizer 3 connects solvent delivery Pipe 102.Material sequentially passes through rinsing, the de- operation such as liquid, drying in washing/dehydrating device, ultimately forms dry material and divides Separate out the solvent liquid coming to reclaim, be properly completed solid-liquid separation, other operation principles are same as Example 2 with work process.
Embodiment 4
With reference to Fig. 4, the present embodiment also includes dehydrator 12, potcher except including the structure of embodiment 1, washing/dehydrating device 10th, centrifugal dehydrator 11 and dehydrator 12 connect along material conveying direction pipeline successively, the solid material outlet side of centrifugal dehydrator 11 It is connected with dehydrator 12.Solvent recycler 16 is connected with dehydrator 12, the liquid outlet of solvent recycler 16 pass through pipeline with The liquid outlet of centrifugal dehydrator 11 is connected.Other operation principles are same as Example 3 with work process.
The above, be only presently preferred embodiments of the present invention, is not the restriction that the present invention is made with other forms, appoints What those skilled in the art possibly also with the disclosure above technology contents changed or be modified as equivalent variations etc. Effect embodiment.But every without departing from technical solution of the present invention content, according to the present invention technical spirit to above example institute Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.

Claims (10)

1. a kind of single-stage washing device for animal-plant material it is characterised in that: include leaching device (1), washing dehydration dress Put and pulverizer (3), pulverizer (3) is connected with leaching device (1) by feed line (101), leaching device (1) discharging Mouthful it is connected with washing/dehydrating device charging aperture pipeline by mashing pump (4), the liquid outlet of washing/dehydrating device is connected to point Chaotropic outlet tube (15) and separating liquid return duct (14)；The material outlet of washing/dehydrating device is connected to the first conveyer And second conveyor (6) (5)；Separating liquid return duct (14) is all connected with leaching device (1) with the outfan of the first conveyer (5) Connect；Washing/dehydrating device includes potcher (10) and centrifugal dehydrator (11).
2. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described drift Washing machine (10) and centrifugal dehydrator (11) are split-type structural, and potcher (10) and centrifugal dehydrator (11) are along material conveying direction Pipeline connects successively.
3. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described washes Wash the eluting all-in-one (2) that dehydration device is that potcher (10) and centrifugal dehydrator (11) are wholely set.
4. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described washes Wash dehydration device and also include dehydrator (12), potcher (10), centrifugal dehydrator (11) and dehydrator (12) are integrated setting Eluting drying integral machine (13).
5. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described washes Wash dehydration device and also include dehydrator (12), potcher (10), centrifugal dehydrator (11) and dehydrator (12) are defeated along material successively Direction pipeline is sent to connect, the solid material outlet side of centrifugal dehydrator (11) is connected with dehydrator (12).
6. a kind of single-stage washing device for animal-plant material according to claim 5 it is characterised in that: described baking Solvent recycler (16) is connected with dry machine (12), the liquid outlet of solvent recycler (16) passes through pipeline and centrifugal dehydrator (11) Liquid outlet be connected.
7. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described washes Washing filter membrane used by dehydration device is microfiltration level filter membrane or nanofiltration level filter membrane.
8. a kind of single-stage washing device for animal-plant material according to claim 1 it is characterised in that: described point It is equipped with control valve on chaotropic outlet tube (15), separating liquid return duct (14), the first conveyer (5) and second conveyor (6), It is respectively equipped with reflux pump on separating liquid return duct (14) and second conveyor (6)；Described separating liquid outlet tube (15) and first Conveyer is respectively equipped with feeding engine on (5).
9. a kind of operational approach of the single-stage washing device for animal-plant material described in claim 1 is it is characterised in that wrap Include following steps:
A) raw material pulverizing is powder by pulverizer (3), to improve effective ingredient yield and leaching efficiency in leaching device (1)； Dusty raw materials after pulverizing and solvent are added leaching device (1), mixing in leaching device (1) is leached；Leaching device (1) The material discharged, enters washing/dehydrating device by mashing pump (4) and filters；
B) in washing/dehydrating device filter process, close separating liquid outlet tube (15), open separating liquid return duct (14) and first Conveyer (5), the separating liquid isolated and solid material are recycled in leaching device (1) repeatedly, circulation extraction, until separating liquid When separating liquid concentration in return duct (14) is increased to stationary value, closes separating liquid return duct (14), open separating liquid outlet tube (15) separating liquid, is made to discharge；
C) when in separating liquid outlet tube (15), separating liquid concentration starts continuous decrease, now the raw material in leaching device (1) has been Fully extracted by solvent, stop, to supplementing solvent in leaching device (1), closing the first conveyer, discharge solid material, separate Liquid passes through separating liquid outlet tube (15) and discharges.
10. a kind of single-stage washing device for animal-plant material described in claim 1 purposes it is characterised in that: in oil Material extraction oils and fatss, the extraction of Chinese medicine extract, spice extraction volatile oil or edible animals and plants raw material extract answering of the oily aspect of extraction With.
CN201611017445.6A 2016-11-19 2016-11-19 Single-stage elution device for animal and plant raw materials and method and application thereof Pending CN106334338A (en)

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CN201611017445.6A CN106334338A (en) 2016-11-19 2016-11-19 Single-stage elution device for animal and plant raw materials and method and application thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110215734A (en) * 2019-06-17 2019-09-10 安徽紫山农业科技有限公司 A kind of extract equipment and its extracting method of biological medicine

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011056826A2 (en) * 2009-11-04 2011-05-12 E. I. Du Pont De Nemours And Company Methods and compositions for extracting flavor and fragrance compounds and solubilizing essential oils
CN102919427A (en) * 2012-11-15 2013-02-13 戴群 Black tea extract for effectively retaining original tea aroma and taste and preparation method and application of same
EP2655583B1 (en) * 2010-12-23 2015-03-11 Charabot Process for obtaining a scented extract of fresh flowers and/or leaves using natural solvents
CN204502456U (en) * 2014-12-31 2015-07-29 中国计量学院 Plant extract device
CN206334387U (en) * 2016-11-19 2017-07-18 王芹 A kind of single-stage washing device for animal-plant material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011056826A2 (en) * 2009-11-04 2011-05-12 E. I. Du Pont De Nemours And Company Methods and compositions for extracting flavor and fragrance compounds and solubilizing essential oils
EP2655583B1 (en) * 2010-12-23 2015-03-11 Charabot Process for obtaining a scented extract of fresh flowers and/or leaves using natural solvents
CN102919427A (en) * 2012-11-15 2013-02-13 戴群 Black tea extract for effectively retaining original tea aroma and taste and preparation method and application of same
CN204502456U (en) * 2014-12-31 2015-07-29 中国计量学院 Plant extract device
CN206334387U (en) * 2016-11-19 2017-07-18 王芹 A kind of single-stage washing device for animal-plant material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110215734A (en) * 2019-06-17 2019-09-10 安徽紫山农业科技有限公司 A kind of extract equipment and its extracting method of biological medicine
CN110215734B (en) * 2019-06-17 2021-11-23 安徽紫山农业科技有限公司 Extraction equipment and extraction method of biological medicine

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