CN106332901A - Insecticidal granules of emamectin and cyfluthrin and preparation method thereof - Google Patents
Insecticidal granules of emamectin and cyfluthrin and preparation method thereof Download PDFInfo
- Publication number
- CN106332901A CN106332901A CN201610630760.XA CN201610630760A CN106332901A CN 106332901 A CN106332901 A CN 106332901A CN 201610630760 A CN201610630760 A CN 201610630760A CN 106332901 A CN106332901 A CN 106332901A
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- China
- Prior art keywords
- affirm
- cyfloxylate
- merck
- granular insecticide
- mixing
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses insecticidal granules of emamectin and cyfluthrin, wherein the insecticidal granules are composed of the following components by the weight percentage: 0.1%-5% of emamectin, 0.1%-10% of cyfluthrin, 0.1%-2% of a stabilizer, 0.1%-5% of a synergist, 1%-5% of a wetting dispersant, 0.1%-2% of a binder, 0.1%-2% of a film coating agent, and a filler added to make the total amount of 100%. The invention also discloses a preparation method of the insecticidal granules. The insecticidal granules not only can kill underground insects effectively but also can improve soil; the prepared granules have the advantages of low manufacturing cost, high control efficiency, and long lasting effect, and can effectively prevent and treat the underground insects in a crop growing period.
Description
Technical field
The present invention relates to a kind of granular insecticide containing Affirm (Merck Co.) and cyfloxylate and preparation method thereof,
Belong to field of pesticide preparation.
Background technology
The life such as cutworm, grub, flea beetle, weevil, nematode insect in the earth formation, area in all parts of the country is all distributed, main
The crops such as peanut to be caused harm, sweet potato, pulse family, Solanaceae, Cruciferae, major part lives in the above soil layer of soil 15cm, gnaws work
Thing root, basal part of stem, root tuber etc. cause the underproduction, and propagate soft rot.Disease, worm, grass preventing and treating He Shui, fertile management are production estimation
During one of important step, the particularly harm of nematode become one of main diseases and insect pests of crops in recent years, and science is closed
Reason administrative skill is the effective means that agricultural is increased production, increased income.
The a large amount of use of agricultural chemicals leads to soil productivity to be degenerated, and one kind that the present invention provides contains Affirm (Merck Co.) and fluorine
The desinsection sustained-release granular formulation of cypermethrin, has sustained release, the features such as preventive effect is high, the lasting period is long, can effectively reduce plant growth
The usage amount of phase agricultural chemicals, and can prevent and treat subterranean pest-insect while improved soil so that agriculture life can preferably be served by agricultural chemicals
Produce.
Content of the invention
Technical problem to be solved: the present invention provides one kind for prior art deficiency and contains Affirm (Merck Co.)
With the granular insecticide of cyfloxylate, in agricultural production, applied once both can prevent and treat cutworm, grub, flea beetle, weevil, line
The subterranean pest-insects such as worm, and its preventive effect and lasting period are improved by its slow releasing function, accomplish only need to apply once in crop growth period
The subterranean pest-insect in whole growth period can be prevented and treated, overcoming under the conditions of prior art user will twice or insecticide is used for multiple times
Way.
Present invention also offers the preparation method containing Affirm (Merck Co.) and the granular insecticide of cyfloxylate.
The present invention is achieved through the following technical solutions:
A kind of granular insecticide containing Affirm (Merck Co.) and cyfloxylate, by following components in percentage by weight
Composition: Affirm (Merck Co.) 0.1%-5%, cyfloxylate 0.1%-10%, stabilizer 0.1%-2%, synergist
0.1%-5%, wetting dispersing agent 1%-5%, binding agent 0.1%-2%, coating agent 0.1%-2%, filler is mended to 100%.
Described stabilizer is epoxidized soybean oil, epoxychloropropane, the mixing of one or more of bht, bha.
Described synergist is APES, phenethyl phenol polyethenoxy ether, butanedioic acid sulfonate, dodecane
The mixing of one or more of base benzene sulfonic acid sodium salt, polycarboxylate, AEO.
Described wetting dispersing agent is naphthalene sulfonate, lauryl sodium sulfate, pull open powder, sodium lignin sulfonate, sulfomethylated lignin
The mixing of one or more of sour calcium.
Described binding agent is polyethylene glycol, dextrin, sodium carboxymethylcellulose, PVP, guar gum, xanthan
The mixing of one or more of glue.
Described coating agent is one of polyvinyl alcohol, methacrylate, Lauryl Alcohol fat, water-base resin, fatty alcohol
Or several mixing.
Described filler is one or more of kaolin, bentonite, diatomite, attapulgite, white carbon, sepiolite
Mixing.
Filled a prescription according to above, the desinsection sustained-release granular formulation containing Affirm (Merck Co.) and cyfloxylate of the present invention can
Using following methods preparation:
(1) carry out after air-flow crushing after, Affirm (Merck Co.) and cyfloxylate, wetting dispersing agent, filler being mixed
Make Affirm (Merck Co.) and cyfloxylate female powder；
(2), granulate using by Affirm (Merck Co.) and cyfloxylate female powder, and successively wrapped using coating agent
Cover, pesticide slow-release granule after being dried, is obtained.
Affirm (Merck Co.) and the desinsection sustained-release granular formulation of cyfloxylate that the present invention provides, using can in farmland
While preventing and treating subterranean pest-insect, improved soil, so that the use of agricultural chemicals is more friendly to environment, is conducive to modern agriculture
Sustainable development.
Specific embodiment
The technology contents of the present invention, in order to be better understood from the essence of the present invention, are described with example below, but the present invention
Content be not limited thereto.
Embodiment one: 5% Affirm (Merck Co.) cyfloxylate sustained-release granular formulation.
Preparation method:
(1) accurately weigh 1% Affirm (Merck Co.), 4% cyfloxylate active compound, 3% pull open powder, 3% naphthalene sulfonate,
After 5% white carbon is mixed with surplus sepiolite, carry out ultra micro air-flow crushing, gained Affirm (Merck Co.) cyfloxylate female powder
Particle diameter is necessarily less than 325 mesh.
(2) Affirm (Merck Co.) cyfloxylate female powder is carried out for adhesive using the PVP aqueous solution
Granulation, carries out repeating coating using water-base resin in granulation process, obtains 5% Affirm (Merck Co.) cyfluthrin after drying
Chrysanthemum ester sustained-release granular formulation.
Embodiment two: 3.5% Affirm (Merck Co.) cyfloxylate sustained-release granular formulation.
Preparation method:
(1) 0.5% Affirm (Merck Co.) active compound, 3% cyfloxylate active compound, 3% lignin sulfonic acid, are accurately weighed
After calcium, 5% diatomite are mixed with surplus bentonite, carry out ultra micro air-flow crushing, gained Affirm (Merck Co.) cyfloxylate
Female powder particle diameter is necessarily less than 325 mesh.
(2) Affirm (Merck Co.) cyfloxylate female powder is granulated for adhesive using Aqueous Solutions of Polyethylene Glycol,
Carry out repeating coating using polyvinyl alcohol in granulation process, after drying, obtain 3.5% Affirm (Merck Co.) cyfluthrin chrysanthemum
Ester sustained-release granular formulation.
Embodiment three: 2% Affirm (Merck Co.) cyfloxylate sustained-release granular formulation.
Preparation method:
(1), accurately weigh 1% Affirm (Merck Co.), 1% cyfloxylate active compound, 2% lauryl sodium sulfate, 3%
After calcium lignosulfonate is mixed with balance kaolin, carry out ultra micro air-flow crushing, gained Affirm (Merck Co.) cyfloxylate
Female powder particle diameter is necessarily less than 325 mesh.
(2) Affirm (Merck Co.) cyfloxylate female powder is carried out for adhesive using sodium carboxymethyl cellulose solution
Granulation, carries out repeating coating using methyl acrylate in granulation process, obtains 2% Affirm (Merck Co.) fluorine chlorine after drying
Cyano chrysanthemate sustained-release granular formulation.
Example IV: field control effectiveness test.
Field control effectiveness test shows, the 2% Affirm (Merck Co.) cyfloxylate granule of the present invention uses 500
Gram/acre preventing and treating watermelon nematode, after medicine, 15 days preventive effects reach 95.6%, better than comparison medicament 5% Affirm (Merck Co.) microemulsion and
The 85.8% and 83.9% of 1% Affirm (Merck Co.) granule, the harm that after medicine, 90 days remain to effective control watermelon nematode, prevent
Effect reaches 92.8%, better than comparison medicament 5% Affirm (Merck Co.) microemulsion and 1% Affirm (Merck Co.) granule
81.9% and 80.8%.
Claims (8)
1. the granular insecticide of a kind of Affirm (Merck Co.) and cyfloxylate is it is characterised in that by following percentage by weight
Group be grouped into: Affirm (Merck Co.) 0.1%-5%, cyfloxylate 0.1%-10%, stabilizer 0.1%-2%, synergy
Agent 0.1%-5%, wetting dispersing agent 1%-5%, binding agent 0.1%-2%, coating agent 0.1%-2%, filler is mended to 100%.
2. the granular insecticide of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature exists
In: described stabilizer is the mixing of epoxidized soybean oil, epoxychloropropane, one or more of bht, bha.
3. the granular insecticide of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature exists
In: described synergist is APES, phenethyl phenol polyethenoxy ether, butanedioic acid sulfonate, detergent alkylate
The mixing of one or more of sodium sulfonate, polycarboxylate, AEO.
4. the granular insecticide of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature exists
In: described wetting dispersing agent is naphthalene sulfonate, lauryl sodium sulfate, pull open powder, sodium lignin sulfonate, calcium lignosulfonate one
Plant or several mixing.
5. the granular insecticide method of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature
It is: described binding agent is polyethylene glycol, dextrin, sodium carboxymethylcellulose, PVP, guar gum, xanthans
One or more of mixing.
6. the granular insecticide of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature exists
In: described coating agent is one or more of polyvinyl alcohol, methacrylate, Lauryl Alcohol fat, water-base resin, fatty alcohol
Mixing.
7. the granular insecticide of a kind of Affirm (Merck Co.) according to claim 1 and cyfloxylate, its feature exists
In: described filler is the mixed of one or more of kaolin, bentonite, attapulgite, diatomite, white carbon, sepiolite
Close.
8. the preparation method of the granular insecticide of the Affirm (Merck Co.) described in a kind of claim 1 and cyfloxylate:
(1) carry out making first ammonia after air-flow crushing after, Affirm (Merck Co.) and cyfloxylate, wetting dispersing agent, filler being mixed
Base AVM and cyfloxylate female powder；(2), granulate using by Affirm (Merck Co.) and cyfloxylate female powder, and by
Layer is coated using coating agent, and pesticide slow-release granule is obtained after being dried.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610630760.XA CN106332901A (en) | 2016-08-03 | 2016-08-03 | Insecticidal granules of emamectin and cyfluthrin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610630760.XA CN106332901A (en) | 2016-08-03 | 2016-08-03 | Insecticidal granules of emamectin and cyfluthrin and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106332901A true CN106332901A (en) | 2017-01-18 |
Family
ID=57824992
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610630760.XA Pending CN106332901A (en) | 2016-08-03 | 2016-08-03 | Insecticidal granules of emamectin and cyfluthrin and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106332901A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108990642A (en) * | 2018-10-16 | 2018-12-14 | 南京林衡农业科技有限公司 | A kind of pine nematodiasis wood stump processing unit and control method |
| CN112956480A (en) * | 2021-02-04 | 2021-06-15 | 四川眉山凯尔化工有限公司 | Pesticide raw material formula |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030050194A1 (en) * | 2001-09-07 | 2003-03-13 | Hopkinson Michael J. | Surfactant systems for agriculturally active compounds |
| CN101066055A (en) * | 2007-04-29 | 2007-11-07 | 湖南万家丰科技有限公司 | Pesticide composition containing emamectin benzoate |
| CN101233856A (en) * | 2007-12-07 | 2008-08-06 | 福建农林大学 | Emamectin-benzoate and cyhalothrin microemulsion |
| CN101518256A (en) * | 2008-02-27 | 2009-09-02 | 潘贞德 | A set of soluble liquid insecticides with cyfluthrin and highly efficient cyfluthrin as raw materials |
| CN101720777A (en) * | 2009-12-06 | 2010-06-09 | 山西科锋农业科技有限公司 | Emamectin benzoate and efficient cyfluthrin pesticide mixture preparation |
| CN103004858A (en) * | 2012-11-28 | 2013-04-03 | 李建中 | Insecticidal composition containing methylamino abamectin and pyrethroid compound |
-
2016
- 2016-08-03 CN CN201610630760.XA patent/CN106332901A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030050194A1 (en) * | 2001-09-07 | 2003-03-13 | Hopkinson Michael J. | Surfactant systems for agriculturally active compounds |
| CN101066055A (en) * | 2007-04-29 | 2007-11-07 | 湖南万家丰科技有限公司 | Pesticide composition containing emamectin benzoate |
| CN101233856A (en) * | 2007-12-07 | 2008-08-06 | 福建农林大学 | Emamectin-benzoate and cyhalothrin microemulsion |
| CN101518256A (en) * | 2008-02-27 | 2009-09-02 | 潘贞德 | A set of soluble liquid insecticides with cyfluthrin and highly efficient cyfluthrin as raw materials |
| CN101720777A (en) * | 2009-12-06 | 2010-06-09 | 山西科锋农业科技有限公司 | Emamectin benzoate and efficient cyfluthrin pesticide mixture preparation |
| CN103004858A (en) * | 2012-11-28 | 2013-04-03 | 李建中 | Insecticidal composition containing methylamino abamectin and pyrethroid compound |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108990642A (en) * | 2018-10-16 | 2018-12-14 | 南京林衡农业科技有限公司 | A kind of pine nematodiasis wood stump processing unit and control method |
| CN112956480A (en) * | 2021-02-04 | 2021-06-15 | 四川眉山凯尔化工有限公司 | Pesticide raw material formula |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20170118 |