CN106324028A - Testing device and testing method for determining thermal insulation effect of thermal barrier coating - Google Patents

Testing device and testing method for determining thermal insulation effect of thermal barrier coating Download PDF

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Publication number
CN106324028A
CN106324028A CN201610936618.8A CN201610936618A CN106324028A CN 106324028 A CN106324028 A CN 106324028A CN 201610936618 A CN201610936618 A CN 201610936618A CN 106324028 A CN106324028 A CN 106324028A
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Prior art keywords
barrier coating
sample
thermal barrier
temperature
type thermocouple
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CN201610936618.8A
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夏光明
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Metallurgical Material Research Institute Of Hunan Province
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Metallurgical Material Research Institute Of Hunan Province
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Publication of CN106324028A publication Critical patent/CN106324028A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

The invention discloses a testing device and method for determining a thermal insulation effect of a thermal barrier coating. The testing device comprises a heating plate; an asbestos panel is fixedly mounted at the top of the heating plate; an asbestos hole groove is formed in the asbestos panel; a to-be-tested disk-shaped test sample of the thermal barrier coating is fixedly mounted in the asbestos hole groove; an S-shaped thermocouple is mounted on the thermal barrier coating of the test sample; a K-shaped thermocouple is mounted on the front surface of the test sample; the S-shaped thermocouple and the K-shaped thermocouple are connected with a temperature acquisition unit; the temperature acquisition unit is fixedly connected with a receiving port of a computer. The testing device for determining the thermal insulation effect of the thermal barrier coating has the advantages of wide application range, simplicity and convenience for operation, high efficiency and the like; and the problems that a flame flow process has no reference sample, the heating time is short, time of reaching stable surface and back surface temperature of the sample is short and the thermal insulation temperature of the thermal barrier coating cannot be tested relatively well.

Description

A kind of test device and method measuring thermal barrier coating effect of heat insulation
Technical field
The present invention relates to the blade material technical field of electromotor, a kind of survey measuring thermal barrier coating effect of heat insulation Electricity testing device and method.
Background technology
Along with modern industry and scientific and technological developing rapidly, the parts such as aero-engine and gas turbine are faced with the height of harshness Temperature operating mode Service Environment.Power station combustion gas turbine or the blade material Ni-based height of many employings of Large Civil Aircraft electromotor at present Temperature alloy, although alloy has preferable mechanical behavior under high temperature, but its high-temperature corrosion resistance performance is the most not ideal enough, and price is high Expensive, the cost changing blade is the most of a relatively high.To this end, would generally use at component surface spraying thermal barrier coating to isolate high temperature The combustion gas directly effect to parts, protects the matrix material that is heated, delays conduction of heat, and then make parts the longest Phase, safe and stable military service.
The thermal insulation of coating is to evaluate an important performance indexes of thermal barrier coating performance, and the size of effect of heat insulation is directly closed Being tied to the size of parts coating system operating temperature, the most also produced heat should in Thermal Cycling for remote-effects coating The size of power.The method measuring thermal barrier coating heat-proof quality at present has: flame flame stream method, specifically sprays at substrate material surface Coating, oxyacetylene torch heating sample surfaces, respectively with thermocouple measurement sample surfaces and the temperature value at the back side, before institute's test sample product The temperature difference on rear two sides is adiabatic temperature.The shortcoming of the method is not have reference sample, and heat time heating time is short, sample surfaces and the back of the body It is short that surface temperature reaches stable required time, it is impossible to preferably test thermal barrier coating adiabatic temperature, so proposing one to measure thermal boundary The test device of coating effect of heat insulation solves posed problems above.
Summary of the invention
(1) solve the technical problem that
For the deficiencies in the prior art, the invention provides a kind of test device measuring thermal barrier coating effect of heat insulation and side Method, possess have wide range of applications, easy and simple to handle and efficiency advantages of higher, solving flame flame stream method does not has reference sample, and adds The heat time is short, and it is short that sample surfaces and back temperature reach stable required time, it is impossible to preferably test thermal barrier coating adiabatic temperature Problem.
(2) technical scheme
For realizing the purpose above-mentioned having wide range of applications, easy and simple to handle and efficiency is high, first aspect present invention provides one Measuring the test device of thermal barrier coating effect of heat insulation, including heating plate, the top of described heating plate is installed with asbestos panel, Described asbestos panel be internally provided with asbestos hole slot, be installed with disc-shaped sample to be measured in described asbestos hole slot, described The back of sample to be tested is provided with S type thermocouple, is provided with K-type thermocouple, described S type thermocouple before described sample to be tested Being connected with Temperature sampler with K-type thermocouple, the receiving port by wire with computer of described Temperature sampler is fixed Connect.
Preferably, described sample to be tested 4, S type thermocouple lead are positioned at the inside of asbestos panel.
Preferably, described asbestos hole slot is isodistantly spaced the inner cavity top being distributed in asbestos panel, and the quantity of asbestos hole slot Can be designed according to the quantity of reference sample, position is in the centre of asbestos panel as far as possible.
Preferably, the contact of described K-type thermocouple is connected with the front center point of substrate.
Preferably, the connected mode of described S type thermocouple and K-type thermocouple and substrate is fusion welds.
Preferably, the contact of S type thermocouple is connected with the back side central point of substrate.
Second aspect present invention provides a kind of method of testing measuring thermal barrier coating effect of heat insulation, comprises the steps:
S1, by sample to be tested material back side fusion welds S type thermocouple, and be fixed in the asbestos panel of improvement;
S2, by the back side of sample to be tested towards heating plate, before K-type thermocouple is set, directly and atmosphere, by K-type The contact of thermocouple is close to the front center of sample to be tested;
S3, to heating plate electrified regulation, temperature signal is sent to Temperature sampler by S type thermocouple;
S4, reaching design temperature when the temperature of heating plate, and after a period of stabilisation, stop heating, sample air cooling, by temperature The temperature data of degree harvester is depicted as temperature curve, then the effect of heat insulation Δ T of thermal barrier coating is exactly the back side of thermal barrier coating Temperature with without temperature difference before thermal barrier coating.
(3) beneficial effect
Compared with prior art, the invention provides a kind of test device measuring thermal barrier coating effect of heat insulation, possess with Lower beneficial effect:
1, the test device of this mensuration thermal barrier coating effect of heat insulation, by arranging asbestos hole slot, asbestos hole slot ensure that Institute's test sample thermally equivalent, to guarantee comparability and the verity of Multi-example measured result.
2, the test device of this mensuration thermal barrier coating effect of heat insulation, prepares thermal barrier coating by same substrate material surface, To have thermal barrier coating sample (1#, 2#, 3#) or with without the difference fusion welds S type thermocouple of thermal barrier coating sample and K-type thermoelectricity Even, then it is respectively mounted in the asbestos hole slot of the asbestos panel being fixed on improvement, is allowed to define comparative sample, can be more accurately Obtaining the adiabatic temperature of same substrate material surface difference thermal barrier coating, and effect of heat insulation simple, intuitive, determination efficiency is high.
3, the test device of this mensuration thermal barrier coating effect of heat insulation, before sample to be tested and back side fusion welds S type respectively Thermocouple and K-type thermocouple, directly contact with the center of sample, can accurately measure before sample and the temperature at the back side, To ensure to measure the accuracy of thermal barrier coating adiabatic temperature.
Accompanying drawing explanation
Fig. 1 is present configuration schematic diagram.
In figure: 1 heating plate, 2 asbestos panels, 3 asbestos hole slots, 4 samples to be tested, 5S type thermocouple, 6K type thermocouple, 7 temperature Degree harvester, 8 computers.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Describe, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments wholely.Based on Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under not making creative work premise Embodiment, broadly falls into the scope of protection of the invention.
Referring to Fig. 1, a kind of test device measuring thermal barrier coating effect of heat insulation, including heating plate 1, the top of heating plate 1 Portion is installed with asbestos panel 2, asbestos panel 2 be internally provided with asbestos hole slot 3, asbestos hole slot 3, asbestos hole slot 3 can Ensure test 4 thermally equivalent to be measured, to guarantee comparability and the verity of sample to be tested 4 Multi-example measured result, asbestos hole slot 3 It is isodistantly spaced the inner cavity top being distributed in asbestos panel 2, and the quantity of asbestos hole slot 3 can set according to the quantity of reference sample Meter, position is in the centre of asbestos panel as far as possible.The back side of sample to be tested 4 and above distinguish fusion welds S type thermoelectricity Even 5 and K-type thermocouple 6, directly contact with sample to be tested 4 center, can accurately measure before sample to be tested 4 and the back side Temperature, to ensure the accuracy of measured thermal barrier coating adiabatic temperature, will have thermal barrier coating sample (1#, 2#, 3#) or hot with nothing The back side of barrier coating sample and above fusion welds S type thermocouple 5 and K-type thermocouple 6 respectively, be then respectively mounted to be fixed on and change In the asbestos hole slot 3 of the asbestos panel 2 entered, it is allowed to define comparative sample, same substrate material surface can be obtained more accurately The adiabatic temperature of different thermal barrier coatings, and effect of heat insulation simple, intuitive, determination efficiency is high, and the back of sample to be tested 4 is provided with S Type thermocouple 5, the contact of S type thermocouple 5 is connected with the back side central point of sample to be tested 4, S type thermocouple 5 and K-type thermocouple 6 It is fusion welds with the connected mode of sample to be tested 4, before sample to be tested 4, is provided with K-type thermocouple 6, K-type thermocouple 6 Contact be connected with the front center point of sample to be tested 4, sample to be tested 4, S type thermocouple 5 lead-in wire be respectively positioned on the interior of asbestos panel 2 Portion, the junction of S type thermocouple 5 and K-type thermocouple 6 is installed with Temperature sampler 7, Temperature sampler 7 with computer 8 Receiving port fixing connect, computer 8 is analyzed record to effect of heat insulation.
The electric elements occurred in this article all electrically connect with extraneous 220V civil power.
In use, sample to be tested 4 material back side fusion welds S type thermocouple 5, then it is fixed on the asbestos of improvement In panel 2, the back side of sample to be tested 4, towards heating plate 1, is provided with K-type thermocouple 6 before sample to be tested 4, direct and air Contacting, the contact of K-type thermocouple 6 is close to the front center of sample to be tested 4, and to heating plate 1 electrified regulation, S type thermocouple 5 will Temperature signal is sent to Temperature sampler 7, when the temperature of heating plate 1 reaches design temperature, and after a period of stabilisation, stops adding Heat, sample air cooling, the temperature data of Temperature sampler 7 is depicted as temperature curve, then the effect of heat insulation Δ T of thermal barrier coating is exactly There is the back temperature of thermal barrier coating and without temperature difference before thermal barrier coating.
In sum, the test device and method of this mensuration thermal barrier coating effect of heat insulation, put asbestos hole slot 3 by setting, Asbestos hole slot 3 ensure that institute's sample to be tested 4 thermally equivalent, to guarantee the comparability of Multi-example measured result on sample to be tested 4 With verity, same substrate material surface is prepared thermal barrier coating, will be had thermal barrier coating (1#, 2#, 3#) or try with without thermal barrier coating The back side of sample and above fusion welds S type thermocouple 5 and K-type thermocouple 6 respectively, be then respectively mounted the asbestos being fixed on improvement In the asbestos hole slot 3 of panel 2, it is allowed to define comparative sample, same substrate material surface difference thermal boundary can be obtained more accurately The adiabatic temperature of coating, and effect of heat insulation simple, intuitive, determination efficiency is high, the back side of sample to be tested 4 and above melting welding respectively Welding S type thermocouple 5 and K-type thermocouple 6, directly contact with sample to be tested 4 center, can accurately measure sample to be tested 4 The back side and temperature above, to ensure to measure the accuracy of thermal barrier coating adiabatic temperature, solving flame flame stream method does not has reference Sample, and heat time heating time is short, it is short that sample surfaces and back temperature reach stable required time, it is impossible to preferably tests thermal barrier coating The problem of adiabatic temperature.
It should be noted that in this article, the relational terms of such as first and second or the like is used merely to a reality Body or operation separate with another entity or operating space, and deposit between not necessarily requiring or imply these entities or operating Relation or order in any this reality.And, term " includes ", " comprising " or its any other variant are intended to Comprising of nonexcludability, so that include that the process of a series of key element, method, article or equipment not only include that those are wanted Element, but also include other key elements being not expressly set out, or also include for this process, method, article or equipment Intrinsic key element.In the case of there is no more restriction, statement " including ... " key element limited, it is not excluded that Including process, method, article or the equipment of described key element there is also other identical element.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, permissible Understand and these embodiments can be carried out multiple change without departing from the principles and spirit of the present invention, revise, replace And modification, the scope of the present invention be defined by the appended.

Claims (7)

1. measure a test device for thermal barrier coating effect of heat insulation, including heating plate (1), it is characterised in that: described heating plate (1) top is installed with asbestos panel (2), described asbestos panel (2) be internally provided with asbestos hole slot (3), described stone Being installed with disc-shaped sample (4) to be measured in cotton hole slot (3), the back of described sample to be tested (4) is provided with S type thermocouple (5), be provided with before described sample to be tested (4) K-type thermocouple (6), described S type thermocouple (5) and K-type thermocouple (6) with Temperature sampler (7) connects, and described Temperature sampler (7) is fixing with the receiving port of computer (8) to be connected.
A kind of test device measuring thermal barrier coating effect of heat insulation the most according to claim 1, it is characterised in that: described Sample to be tested 4, S type thermocouple (5) lead-in wire is positioned at the inside of asbestos panel (2).
A kind of test device measuring thermal barrier coating effect of heat insulation the most according to claim 1, it is characterised in that: described stone Cotton hole slot (3) is isodistantly spaced the inner cavity top being distributed in asbestos panel (2), and the quantity of asbestos hole slot (3) can be according to reference The quantity of product is designed, and position is in the centre of asbestos panel (2) as far as possible.
A kind of test device measuring thermal barrier coating effect of heat insulation the most according to claim 1, it is characterised in that: described K The contact of type thermocouple (7) is connected with the front center point of sample to be tested (4).
A kind of test device measuring thermal barrier coating effect of heat insulation the most according to claim 1, it is characterised in that: described S The connected mode of type thermocouple (5) and K-type thermocouple (6) and sample to be tested (4) is fusion welds.
A kind of test device measuring thermal barrier coating effect of heat insulation the most according to claim 1, it is characterised in that: described S The contact of type thermocouple (5) is connected with the back side central point of sample to be tested (4).
7. measure a method of testing for thermal barrier coating effect of heat insulation, based on above-mentioned mensuration thermal boundary as described in claim 1 to 6 The test device of coating effect of heat insulation, it is characterised in that comprise the steps:
S1, by sample to be tested material back side fusion welds S type thermocouple, and be fixed in the asbestos panel of improvement;
S2, by the back side of sample to be tested towards heating plate, before K-type thermocouple is set, directly and atmosphere, by K-type thermoelectricity Even contact is close to the front center of sample to be tested;
S3, to heating plate electrified regulation, temperature signal is sent to Temperature sampler by S type thermocouple;
S4, reach design temperature when the temperature of heating plate, and after a period of stabilisation, stop heating, sample air cooling, temperature is adopted The temperature data of storage is depicted as temperature curve, then the effect of heat insulation Δ T of thermal barrier coating is exactly the back temperature of thermal barrier coating With without temperature difference before thermal barrier coating.
CN201610936618.8A 2016-10-22 2016-10-22 Testing device and testing method for determining thermal insulation effect of thermal barrier coating Withdrawn CN106324028A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107941848A (en) * 2017-10-20 2018-04-20 北京绿时顺风科技有限公司 The apparatus and method for directly measuring block materials thermal barrier coating adiabatic temperature
CN108020577A (en) * 2017-11-20 2018-05-11 航天材料及工艺研究所 A kind of thermally protective materials prevent heat-insulated test system, test method and heat treatment method
CN108088869A (en) * 2017-11-30 2018-05-29 中国航空工业集团公司沈阳飞机设计研究所 A kind of thermal protection system Heat-Insulation Test device
CN110501085A (en) * 2018-12-11 2019-11-26 中国航空工业集团公司北京长城计量测试技术研究所 A kind of thermal barrier coating heat-proof quality measurement method based on film thermometric
CN113588709A (en) * 2021-07-26 2021-11-02 北京航空航天大学 Turbine blade thermal barrier coating thermal insulation effect evaluation and prediction method
CN113804724A (en) * 2021-09-29 2021-12-17 中北大学 Method for testing heat insulation performance of thermal protection ceramic coating

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110080522A (en) * 2010-01-06 2011-07-13 성균관대학교산학협력단 Measuring device of insulation for thermal barrier coating using furnace
CN103592329A (en) * 2013-10-24 2014-02-19 西安交通大学 Method for testing heat insulation temperature of thermal barrier coating
CN104792819A (en) * 2015-04-16 2015-07-22 东方电气集团东方汽轮机有限公司 Heat barrier coating heat insulation effect testing device for fuel machine
CN204679436U (en) * 2015-04-28 2015-09-30 上海新力动力设备研究所 Solid propellant rocket external thermal protection coating carries on the back warm test macro
CN206177858U (en) * 2016-10-22 2017-05-17 湖南省冶金材料研究院 Testing arrangement of thermal -insulated effect of survey thermal barrier coating

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110080522A (en) * 2010-01-06 2011-07-13 성균관대학교산학협력단 Measuring device of insulation for thermal barrier coating using furnace
CN103592329A (en) * 2013-10-24 2014-02-19 西安交通大学 Method for testing heat insulation temperature of thermal barrier coating
CN104792819A (en) * 2015-04-16 2015-07-22 东方电气集团东方汽轮机有限公司 Heat barrier coating heat insulation effect testing device for fuel machine
CN204679436U (en) * 2015-04-28 2015-09-30 上海新力动力设备研究所 Solid propellant rocket external thermal protection coating carries on the back warm test macro
CN206177858U (en) * 2016-10-22 2017-05-17 湖南省冶金材料研究院 Testing arrangement of thermal -insulated effect of survey thermal barrier coating

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107941848A (en) * 2017-10-20 2018-04-20 北京绿时顺风科技有限公司 The apparatus and method for directly measuring block materials thermal barrier coating adiabatic temperature
CN108020577A (en) * 2017-11-20 2018-05-11 航天材料及工艺研究所 A kind of thermally protective materials prevent heat-insulated test system, test method and heat treatment method
CN108088869A (en) * 2017-11-30 2018-05-29 中国航空工业集团公司沈阳飞机设计研究所 A kind of thermal protection system Heat-Insulation Test device
CN110501085A (en) * 2018-12-11 2019-11-26 中国航空工业集团公司北京长城计量测试技术研究所 A kind of thermal barrier coating heat-proof quality measurement method based on film thermometric
CN113588709A (en) * 2021-07-26 2021-11-02 北京航空航天大学 Turbine blade thermal barrier coating thermal insulation effect evaluation and prediction method
CN113588709B (en) * 2021-07-26 2022-07-19 北京航空航天大学 Turbine blade thermal barrier coating heat insulation effect evaluation and prediction method
CN113804724A (en) * 2021-09-29 2021-12-17 中北大学 Method for testing heat insulation performance of thermal protection ceramic coating
CN113804724B (en) * 2021-09-29 2024-03-29 中北大学 Method for testing heat insulation performance of thermal protection ceramic coating

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Inventor after: Qin Song

Inventor after: Xia Guangming

Inventor after: Min Xiaobing

Inventor after: Yan Shuqun

Inventor after: Zhou Jianqiao

Inventor before: Xia Guangming

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Address after: 410000 No. 9 Jiayuan Road, Huanli Street, Changsha Economic Development Zone, Changsha City, Hunan Province

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