CN106309250A - Preparation method of natural plant skin moisturizer - Google Patents
Preparation method of natural plant skin moisturizer Download PDFInfo
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- CN106309250A CN106309250A CN201610897239.2A CN201610897239A CN106309250A CN 106309250 A CN106309250 A CN 106309250A CN 201610897239 A CN201610897239 A CN 201610897239A CN 106309250 A CN106309250 A CN 106309250A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a preparation method of a natural plant skin moisturizer, belonging to the technical field of preparation of skin care products. The method comprises the following steps: pulping fresh cereus, mixing with deionized water, filtering, mixing the obtained cereus polysaccharide filtrate with anhydrous ethanol, centrifugating, washing the lower precipitate, and drying to obtain cereus polysaccharides; pulverizing fresh lotus petals to obtain granules, carrying out fixing treatment with a glutaric dialdehyde water solution, filtering, collecting the filter cake, heating the filter cake and n-hexane, filtering, collecting the filtrate, and carrying out rotary evaporation to obtain a lotus petal waxy concentrated solution; and finally, mixing the lotus petal waxy concentrated solution with the cereus polysaccharides, heating, and carrying out homogenization treatment to obtain the natural plant skin moisturizer. The raw materials are natural and safe. The prepared skin moisturizer has enduring moisturizing effect, and can keep the skin clean and dry. The moisturizer does not have any toxic or side effect, can not irritate or injure the skin after use, and has wide application prospects.
Description
Technical field
The invention discloses the preparation method of a kind of natural plants skin moisturizer, belong to skin care item preparing technical field.
Background technology
In recent years, people have had brand-new understanding for skin moisture-keeping, and people have been no longer satisfied with oils and fats in the past
Skin protection, but some salubrious replenishing water and preserving moisture products are shown special preference to.Therefore, various wetting agents and moisturizer just should
Transporting and give birth to, its market prospect is considerable.In the middle of all of cosmetic material, wetting agent occupies very important status.One
Aspect, almost all of cosmetic formulations all be unable to do without wetting agent, and it is one of basic substance of composition cosmetics；The opposing party
Face, wetting agent plays vital effect to the function of cosmetics with quality, says in a sense, determining of wetting agent
The quality of cosmetic.
Wetting agent is the hygroscopic compound that a class can absorb moisture from humid air.Wetting agent is by absorbing and keeping
Moisture reaches the effect such as moisturizing, moist, recovery elasticity of skin.Because xerodermatic true cause is that in horny layer moisture is not
Foot.Keratodermatitis acts the barrier effect controlling crust moisture loss, and for keeping the balance of moisture of skin, keratose should keep
Certain moisture is with the humidity change of antagonism external environment, say, that skin smooth to be made, softness and high resilience, it is necessary to
The water content making skin mesocuticle keeps optimum state.It is generally believed that cuticular water content should be low between 10～20%
In 10%, skin will be dried, coarse even chap.Therefore, the material that can keep keratodermatitis moisture is referred to as again by we
Wetting agent.
Traditional wetting agent can not maintain non-greasy salubrious skinfeel, and existing moisturizing while long-acting moisturizing
Agent is mainly the material of chemosynthesis, these material Diazolidinyl Ureas, and skin is caused damage, also there is health potential
Harm.
Summary of the invention
The technical problem that present invention mainly solves: can not remain the most oily while long-acting moisturizing for current wetting agent
Greasy and salubrious skinfeel, and mostly contain the material of chemosynthesis, Diazolidinyl Urea, also be there is potential hazard in health
Problem, it is provided that the preparation method of a kind of natural plants skin moisturizer, the method first new fresh Radix et Caulis Opuntiae Dillenii is made after serosity with
Deionized water hybrid filtering, mixes the cactus polyoses filtrate obtained with dehydrated alcohol, subsequently centrifugal treating lower floor being sunk
Form sediment washing, dried, obtain cactus polyoses, fresher Flos Nelumbinis petal is pulverized make granule after fix with glutaraldehyde water solution
Process, filter subsequently and collect filter cake, by itself and normal hexane heating and filtering, collect filtrate rotation and steam to obtain the concentration of Flos Nelumbinis petal waxiness
Liquid, finally by its with cactus polyoses Hybrid Heating after homogenizing process, a kind of natural plants skin moisturizer, the present invention
The natural safety of raw material, prepared skin moisturizer moistening effect is lasting, and skinfeel can be kept salubrious simultaneously, and the guarantor that the present invention prepares
Humectant is without any side effects, skin will not cause after using stimulation and damage, have broad application prospects.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping, receive subsequently
Collection Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5, mix Radix et Caulis Opuntiae Dillenii serosity with deionized water stirring, heating in water bath at 55～60 DEG C
10～15min, filter subsequently and collect filtrate, being prepared into cactus polyoses filtrate；
(2) 1:5 in mass ratio, mixes the cactus polyoses filtrate of above-mentioned preparation with absolute ethyl alcohol and stirring, ice at 0～5 DEG C
Heating in water bath 10～15min, stands 6～8h, then centrifugation 10～15min under 3500～4000r/min, under collection subsequently
Layer precipitation with absolute ethanol washing 3～5 times, at 45～50 DEG C dry 6～8h, is prepared into cactus polyoses, standby；
(3) collect fresh Flos Nelumbinis petal, with clear water washing surface lyophilization, its comminution by gas stream is collected to obtain Flos Nelumbinis petal
Grain, 1:8 in mass ratio, Flos Nelumbinis petal is mixed and fixing petal granule 40 with the glutaraldehyde water solution stirring that mass fraction is 5%
～48h；
(4) to be fixed complete after, filter and collect filter cake, in mass ratio 1:5, the stirring of filter cake and normal hexane being mixed and is placed in burning
In Bei, heating in water bath 1～2h at 55～60 DEG C, after heating in water bath completes, filter and collect filtrate, at 45～50 DEG C of backspins
Turn and be evaporated to dryness, be prepared into Flos Nelumbinis petal waxiness concentrated solution；
(5) 2:3 in mass ratio, stirs the Flos Nelumbinis petal waxiness concentrated solution of cactus polyoses standby for step (2) with above-mentioned preparation
Mix mixing, subsequently heating in water bath 25～30min at 85～90 DEG C, stand subsequently and be cooled to room temperature, be placed in homogenizing blender
Middle homogenizing 1～2min, can be prepared into a kind of natural plants skin moisturizer.
The application process of the present invention is: takes the skin moisturizer that the 0.8～1.0mL present invention prepares, is existed by its uniform application
Face, pats gently, until wetting agent fully penetrates into skin.After testing, the wetting agent that the present invention prepares has long-acting holding
Long moistening effect, moisture preserving time is up to 16～20h, can keep skin refreshing non-greasy simultaneously, and wetting agent is secondary without any poison
Effect, continuous use 1～3 months, allergy rate is only 0.05～0.1%.
The invention has the beneficial effects as follows:
(1) skin moisturizer of the present invention good penetrability to skin, it is possible to the most effective moist dry skin, has long-acting
Lasting moistening effect, and can persistently keep skin the most sticky；
(2) wetting agent that the present invention prepares has good skin-friendliness, and has no side effect, will not be to skin after using
Cause stimulation and damage, can be widely applied in medicine, cosmetics.
Detailed description of the invention
First collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping,
Collect Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5 subsequently, Radix et Caulis Opuntiae Dillenii serosity is mixed with deionized water stirring, water at 55～60 DEG C
Bath heating 10～15min, filters subsequently and collects filtrate, being prepared into cactus polyoses filtrate；1:5 the most in mass ratio, by upper
The cactus polyoses filtrate stating preparation mixes with absolute ethyl alcohol and stirring, and at 0～5 DEG C, ice-water bath heating 10～15min, the most quiet
Put 6～8h, then centrifugation 10～15min under 3500～4000r/min, collect lower sediment and with absolute ethanol washing 3
～5 times, at 45～50 DEG C, it is dried 6～8h, is prepared into cactus polyoses, standby；Regather fresh Flos Nelumbinis petal, wash with clear water
Washing surface lyophilization, its comminution by gas stream is collected to obtain Flos Nelumbinis petal granule, 1:8 in mass ratio, by Flos Nelumbinis petal and quality
Mark is glutaraldehyde water solution stirring mixing the fixing petal granule 40～48h of 5%；To be fixed complete after, filter and collect filter
Cake, in mass ratio 1:5, mix filter cake with normal hexane stirring and be placed in beaker, heating in water bath 1～2h at 55～60 DEG C,
After heating in water bath completes, filter and collect filtrate, rotary evaporated to dryness at 45～50 DEG C, it is prepared into Flos Nelumbinis petal waxiness dense
Contracting liquid；Last 2:3 in mass ratio, by the Flos Nelumbinis petal waxiness concentrated solution of above-mentioned for step standby cactus polyoses Yu above-mentioned preparation
Stirring mixing, heating in water bath 25～30min at 85～90 DEG C subsequently, stand subsequently and be cooled to room temperature, be placed in homogenizing stirring
Homogenizing 1～2min in machine, can be prepared into a kind of natural plants skin moisturizer.
Example 1
First collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping, subsequently
Collect Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5, Radix et Caulis Opuntiae Dillenii serosity is mixed with deionized water stirring, heating in water bath at 55 DEG C
10min, filters subsequently and collects filtrate, is prepared into cactus polyoses filtrate；1:5 the most in mass ratio, by the celestial being of above-mentioned preparation
People slaps polysaccharide filtrate and mixes with absolute ethyl alcohol and stirring, and at 0 DEG C, ice-water bath heating 10min, stands 6h subsequently, then at 3500r/
Centrifugation 10min under min, collects lower sediment and with absolute ethanol washing 3 times, and at 45 DEG C, dry 6h, is prepared into celestial being
Palm polysaccharide, standby；Regather fresh Flos Nelumbinis petal, with clear water washing surface lyophilization, its comminution by gas stream is collected to obtain lotus
Flower petal granule, in mass ratio 1:8, mix Flos Nelumbinis petal and fixing flower with the glutaraldehyde water solution stirring that mass fraction is 5%
Lobe granule 40h；To be fixed complete after, filter and collect filter cake, in mass ratio 1:5, the stirring of filter cake and normal hexane is mixed juxtaposition
In beaker, heating in water bath 1h at 55 DEG C, after heating in water bath completes, filter and collect filtrate, rotary evaporation at 45 DEG C
To dry, it is prepared into Flos Nelumbinis petal waxiness concentrated solution；Last 2:3 in mass ratio, by above-mentioned for step standby cactus polyoses with upper
State the Flos Nelumbinis petal waxiness concentrated solution stirring mixing of preparation, heating in water bath 25min at 85 DEG C subsequently, stand subsequently and be cooled to room
Temperature, is placed in homogenizing 1min in homogenizing blender, can be prepared into a kind of natural plants skin moisturizer.
This example operation is easy, during use, takes the skin moisturizer that the 0.8mL present invention prepares, by its uniform application at face
Portion, pats gently, until wetting agent fully penetrates into skin.After testing, the wetting agent that the present invention prepares have long-acting persistently
Moistening effect, moisture preserving time is up to 16h, simultaneously can keep skin refreshing non-greasy, and wetting agent is without any side effects, even
Continuous use 1 month, allergy rate is only 0.05%.
Example 2
First collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping, subsequently
Collect Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5, Radix et Caulis Opuntiae Dillenii serosity is mixed with deionized water stirring, heating in water bath at 58 DEG C
13min, filters subsequently and collects filtrate, is prepared into cactus polyoses filtrate；1:5 the most in mass ratio, by the celestial being of above-mentioned preparation
People slaps polysaccharide filtrate and mixes with absolute ethyl alcohol and stirring, and at 3 DEG C, ice-water bath heating 13min, stands 7h subsequently, then at 3750r/
Centrifugation 13min under min, collects lower sediment and with absolute ethanol washing 4 times, and at 48 DEG C, dry 7h, is prepared into celestial being
Palm polysaccharide, standby；Regather fresh Flos Nelumbinis petal, with clear water washing surface lyophilization, its comminution by gas stream is collected to obtain lotus
Flower petal granule, in mass ratio 1:8, mix Flos Nelumbinis petal and fixing flower with the glutaraldehyde water solution stirring that mass fraction is 5%
Lobe granule 44h；To be fixed complete after, filter and collect filter cake, in mass ratio 1:5, the stirring of filter cake and normal hexane is mixed juxtaposition
In beaker, heating in water bath 1.5h at 58 DEG C, after heating in water bath completes, filters and collects filtrate, rotating and steam at 48 DEG C
Send to do, be prepared into Flos Nelumbinis petal waxiness concentrated solution；Last 2:3 in mass ratio, by above-mentioned for step standby cactus polyoses with
The Flos Nelumbinis petal waxiness concentrated solution stirring mixing of above-mentioned preparation, heating in water bath 28min at 88 DEG C subsequently, stand subsequently and be cooled to
Room temperature, is placed in homogenizing 1.5min in homogenizing blender, can be prepared into a kind of natural plants skin moisturizer.
This example operation is easy, during use, takes the skin moisturizer that the 0.9mL present invention prepares, by its uniform application at face
Portion, pats gently, until wetting agent fully penetrates into skin.After testing, the wetting agent that the present invention prepares have long-acting persistently
Moistening effect, moisture preserving time is up to 18h, simultaneously can keep skin refreshing non-greasy, and wetting agent is without any side effects, even
Continuous use 3 months, allergy rate is only 0.08%.
Example 3
First collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping, subsequently
Collect Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5, Radix et Caulis Opuntiae Dillenii serosity is mixed with deionized water stirring, heating in water bath at 60 DEG C
15min, filters subsequently and collects filtrate, is prepared into cactus polyoses filtrate；1:5 the most in mass ratio, by the celestial being of above-mentioned preparation
People slaps polysaccharide filtrate and mixes with absolute ethyl alcohol and stirring, and at 5 DEG C, ice-water bath heating 15min, stands 8h subsequently, then at 4000r/
Centrifugation 15min under min, collects lower sediment and with absolute ethanol washing 5 times, and at 50 DEG C, dry 8h, is prepared into celestial being
Palm polysaccharide, standby；Regather fresh Flos Nelumbinis petal, with clear water washing surface lyophilization, its comminution by gas stream is collected to obtain lotus
Flower petal granule, in mass ratio 1:8, mix Flos Nelumbinis petal and fixing flower with the glutaraldehyde water solution stirring that mass fraction is 5%
Lobe granule 48h；To be fixed complete after, filter and collect filter cake, in mass ratio 1:5, the stirring of filter cake and normal hexane is mixed juxtaposition
In beaker, heating in water bath 2h at 60 DEG C, after heating in water bath completes, filter and collect filtrate, rotary evaporation at 50 DEG C
To dry, it is prepared into Flos Nelumbinis petal waxiness concentrated solution；Last 2:3 in mass ratio, by above-mentioned for step standby cactus polyoses with upper
State the Flos Nelumbinis petal waxiness concentrated solution stirring mixing of preparation, heating in water bath 30min at 90 DEG C subsequently, stand subsequently and be cooled to room
Temperature, is placed in homogenizing 2min in homogenizing blender, can be prepared into a kind of natural plants skin moisturizer.
This example operation is easy, during use, takes the skin moisturizer that the 1.0mL present invention prepares, by its uniform application at face
Portion, pats gently, until wetting agent fully penetrates into skin.After testing, the wetting agent that the present invention prepares have long-acting persistently
Moistening effect, moisture preserving time is up to 20h, simultaneously can keep skin refreshing non-greasy, and wetting agent is without any side effects, even
Continuous use 3 months, allergy rate is only 0.1%.
Claims (1)
1. the preparation method of a natural plants skin moisturizer, it is characterised in that concrete preparation process is:
(1) collect new fresh Radix et Caulis Opuntiae Dillenii and clean and remove thorn peeling, be cut into fragment and be placed in refiner broken pulping, receive subsequently
Collection Radix et Caulis Opuntiae Dillenii serosity, in mass ratio 1:5, mix Radix et Caulis Opuntiae Dillenii serosity with deionized water stirring, heating in water bath at 55～60 DEG C
10～15min, filter subsequently and collect filtrate, being prepared into cactus polyoses filtrate；
(2) 1:5 in mass ratio, mixes the cactus polyoses filtrate of above-mentioned preparation with absolute ethyl alcohol and stirring, ice at 0～5 DEG C
Heating in water bath 10～15min, stands 6～8h, then centrifugation 10～15min under 3500～4000r/min, under collection subsequently
Layer precipitation with absolute ethanol washing 3～5 times, at 45～50 DEG C dry 6～8h, is prepared into cactus polyoses, standby；
(3) collect fresh Flos Nelumbinis petal, with clear water washing surface lyophilization, its comminution by gas stream is collected to obtain Flos Nelumbinis petal
Grain, 1:8 in mass ratio, Flos Nelumbinis petal is mixed and fixing petal granule 40 with the glutaraldehyde water solution stirring that mass fraction is 5%
～48h；
(4) to be fixed complete after, filter and collect filter cake, in mass ratio 1:5, the stirring of filter cake and normal hexane being mixed and is placed in burning
In Bei, heating in water bath 1～2h at 55～60 DEG C, after heating in water bath completes, filter and collect filtrate, at 45～50 DEG C of backspins
Turn and be evaporated to dryness, be prepared into Flos Nelumbinis petal waxiness concentrated solution；
(5) 2:3 in mass ratio, stirs the Flos Nelumbinis petal waxiness concentrated solution of cactus polyoses standby for step (2) with above-mentioned preparation
Mix mixing, subsequently heating in water bath 25～30min at 85～90 DEG C, stand subsequently and be cooled to room temperature, be placed in homogenizing blender
Middle homogenizing 1～2min, can be prepared into a kind of natural plants skin moisturizer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610897239.2A CN106309250A (en) | 2016-10-14 | 2016-10-14 | Preparation method of natural plant skin moisturizer |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610897239.2A CN106309250A (en) | 2016-10-14 | 2016-10-14 | Preparation method of natural plant skin moisturizer |
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| CN106309250A true CN106309250A (en) | 2017-01-11 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109942724A (en) * | 2019-03-20 | 2019-06-28 | 广州绿蒎生物科技有限公司 | A kind of cactus polyoses and its preparation method and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109942724A (en) * | 2019-03-20 | 2019-06-28 | 广州绿蒎生物科技有限公司 | A kind of cactus polyoses and its preparation method and application |
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Application publication date: 20170111 |