CN106309235B - A kind of shampoo and preparation method thereof - Google Patents
A kind of shampoo and preparation method thereof Download PDFInfo
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- CN106309235B CN106309235B CN201610843003.0A CN201610843003A CN106309235B CN 106309235 B CN106309235 B CN 106309235B CN 201610843003 A CN201610843003 A CN 201610843003A CN 106309235 B CN106309235 B CN 106309235B
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- tea
- shampoo
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- deionized water
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- 239000002453 shampoo Substances 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 38
- 239000008367 deionised water Substances 0.000 claims abstract description 37
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 29
- IYFATESGLOUGBX-YVNJGZBMSA-N Sorbitan monopalmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O IYFATESGLOUGBX-YVNJGZBMSA-N 0.000 claims abstract description 23
- 235000019486 Sunflower oil Nutrition 0.000 claims abstract description 22
- 239000002600 sunflower oil Substances 0.000 claims abstract description 22
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 claims abstract description 19
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000796 flavoring agent Substances 0.000 claims abstract description 19
- 235000013355 food flavoring agent Nutrition 0.000 claims abstract description 19
- 229940100608 glycol distearate Drugs 0.000 claims abstract description 19
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000011780 sodium chloride Substances 0.000 claims abstract description 19
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 19
- 244000303965 Cyamopsis psoralioides Species 0.000 claims abstract description 18
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 18
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 18
- 235000019270 ammonium chloride Nutrition 0.000 claims abstract description 18
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 18
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 18
- 125000002091 cationic group Chemical group 0.000 claims abstract description 18
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 18
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims abstract description 14
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims abstract description 14
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 244000269722 Thea sinensis Species 0.000 claims abstract 10
- 239000000839 emulsion Substances 0.000 claims description 20
- 229910001562 pearlite Inorganic materials 0.000 claims description 16
- 239000002002 slurry Substances 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 13
- 238000010257 thawing Methods 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 235000009508 confectionery Nutrition 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- QLNJFJADRCOGBJ-UHFFFAOYSA-N propionamide Chemical compound CCC(N)=O QLNJFJADRCOGBJ-UHFFFAOYSA-N 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 2
- 244000147568 Laurus nobilis Species 0.000 claims 1
- 235000017858 Laurus nobilis Nutrition 0.000 claims 1
- 235000005212 Terminalia tomentosa Nutrition 0.000 claims 1
- 238000009210 therapy by ultrasound Methods 0.000 claims 1
- 210000004209 hair Anatomy 0.000 abstract description 7
- 201000004384 Alopecia Diseases 0.000 abstract description 3
- 208000001840 Dandruff Diseases 0.000 abstract description 3
- 102000011782 Keratins Human genes 0.000 abstract description 3
- 108010076876 Keratins Proteins 0.000 abstract description 3
- 231100000360 alopecia Toxicity 0.000 abstract description 3
- 241001122767 Theaceae Species 0.000 description 51
- 238000001914 filtration Methods 0.000 description 7
- 238000001816 cooling Methods 0.000 description 5
- BDOYKFSQFYNPKF-UHFFFAOYSA-N 2-[2-[bis(carboxymethyl)amino]ethyl-(carboxymethyl)amino]acetic acid;sodium Chemical compound [Na].[Na].OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O BDOYKFSQFYNPKF-UHFFFAOYSA-N 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 244000060011 Cocos nucifera Species 0.000 description 3
- 235000013162 Cocos nucifera Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- -1 oleoyl amine Chemical class 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 241000699670 Mus sp. Species 0.000 description 2
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 description 2
- 229960003237 betaine Drugs 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 2
- 210000003780 hair follicle Anatomy 0.000 description 2
- 239000011241 protective layer Substances 0.000 description 2
- 210000003491 skin Anatomy 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- 229920002907 Guar gum Polymers 0.000 description 1
- IPMYMEWFZKHGAX-UHFFFAOYSA-N Isotheaflavin Natural products OC1CC2=C(O)C=C(O)C=C2OC1C(C1=C2)=CC(O)=C(O)C1=C(O)C(=O)C=C2C1C(O)CC2=C(O)C=C(O)C=C2O1 IPMYMEWFZKHGAX-UHFFFAOYSA-N 0.000 description 1
- UXRMWRBWCAGDQB-UHFFFAOYSA-N Theaflavin Natural products C1=CC(C2C(CC3=C(O)C=C(O)C=C3O2)O)=C(O)C(=O)C2=C1C(C1OC3=CC(O)=CC(O)=C3CC1O)=CC(O)=C2O UXRMWRBWCAGDQB-UHFFFAOYSA-N 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- LLJZKKVYXXDWTB-UHFFFAOYSA-N acetic acid;sodium Chemical compound [Na].[Na].CC(O)=O LLJZKKVYXXDWTB-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- AJXBTRZGLDTSST-UHFFFAOYSA-N amino 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)ON AJXBTRZGLDTSST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical class C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000665 guar gum Substances 0.000 description 1
- 235000010417 guar gum Nutrition 0.000 description 1
- 229960002154 guar gum Drugs 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- HLERILKGMXJNBU-UHFFFAOYSA-N norvaline betaine Chemical compound CCCC(C([O-])=O)[N+](C)(C)C HLERILKGMXJNBU-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- FATBGEAMYMYZAF-KTKRTIGZSA-N oleamide Chemical compound CCCCCCCC\C=C/CCCCCCCC(N)=O FATBGEAMYMYZAF-KTKRTIGZSA-N 0.000 description 1
- FATBGEAMYMYZAF-UHFFFAOYSA-N oleicacidamide-heptaglycolether Natural products CCCCCCCCC=CCCCCCCCC(N)=O FATBGEAMYMYZAF-UHFFFAOYSA-N 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000527 sonication Methods 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- IPMYMEWFZKHGAX-ZKSIBHASSA-N theaflavin Chemical compound C1=C2C([C@H]3OC4=CC(O)=CC(O)=C4C[C@H]3O)=CC(O)=C(O)C2=C(O)C(=O)C=C1[C@@H]1[C@H](O)CC2=C(O)C=C(O)C=C2O1 IPMYMEWFZKHGAX-ZKSIBHASSA-N 0.000 description 1
- 229940026509 theaflavin Drugs 0.000 description 1
- 235000014620 theaflavin Nutrition 0.000 description 1
- MEYZYGMYMLNUHJ-UHFFFAOYSA-N tunicamycin Natural products CC(C)CCCCCCCCCC=CC(=O)NC1C(O)C(O)C(CC(O)C2OC(C(O)C2O)N3C=CC(=O)NC3=O)OC1OC4OC(CO)C(O)C(O)C4NC(=O)C MEYZYGMYMLNUHJ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Botany (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of shampoos and preparation method thereof, it is composed of the following components by mass percentage: sunflower oil 0.50~1.0%, span 40 0.05~0.10%, Fu tea extract 2~6%, glycol distearate 1.0~3.0%, octadecyl alcolol 0.5~2.0%, Cocoamidopropyl betaine 1.0~5.0%, guar hydroxypropyltrimonium ammonium chloride 0.3~0.7%, cationic hydroxyethyl cellulose 0.3~0.7%, lauryl alcohol ammonium sulfate 10~20%, sodium chloride 2~6%, disodium ethylene diamine tetraacetate 0.10~0.20%, isothiazolinone 0.10~0.20%, flavouring agent 0.0010~0.0030%, surplus is deionized water, the sum of said components mass percent is 100 %.Shampoo of the present invention has and cleans anti-dandruff, reparation keratin, prevents the function of disconnected hair alopecia.
Description
Technical field
The invention belongs to medical, daily cosmetics technical fields, and in particular to a kind of shampoo, the invention further relates to this to wash
The preparation method of shampoo.
Background technique
Common shampoo is generally alkaline (PH > 7), is because alkaline shampoo has good clean effect, still
But hair quality is had damage, make hair scale piece open, it is easy to enable hair coarse, do, disperse, repairing performance it is poor.Become crude to be not easy
It arranges.And human skin epidermis pH value is 5.5, this tunic belongs to neutral protective layer, for keeping the acid-base balance of skin,
And weakly alkaline shampoo (pH > 7) can carry out slight damage to this layer of protective layer.And acid shampoo is (pH < 7), can make head
It is smooth to send out docile, is easy to arrange.But due to acid ingredients such as acid shampoo addition citric acids, oil-control, salubrious sense are not
Such as alkaline shampoo.Fu tea is a kind of unique solid fermentation tea, rich in the beneficial coronoid process dissipate capsule bacterium of human body, theaflavin, tea
Polyphenol, adding Fu tea extraction in shampoo can reach adjusting hair follicle metabolism, prevent the effect of disconnected hair.
Summary of the invention
The object of the present invention is to provide a kind of shampoo, which not only has the function of that cleaning is anti-dandruff, can also repair
Multiple keratin prevents disconnected hair alopecia.
Another object of the present invention is to provide a kind of preparation method of shampoo.
The technical scheme adopted by the invention is that a kind of shampoo, composed of the following components by mass percentage: sunflower seeds
Oil 0.50~1.0%, span 40 0.05~0.10%, Fu tea extract 2~6%, glycol distearate 1.0~
3.0%, octadecyl alcolol 0.5~2.0%, Cocoamidopropyl betaine 1.0~5.0%, guar hydroxypropyltrimonium ammonium chloride
0.3~0.7%, cationic hydroxyethyl cellulose 0.3~0.7%, lauryl alcohol ammonium sulfate 10~20%, sodium chloride 2~6%,
Disodium ethylene diamine tetraacetate 0.10~0.20%, isothiazolinone 0.10~0.20%, flavouring agent 0.0010~0.0030%, it is remaining
Amount is deionized water, and the sum of said components mass percent is 100%.
Another technical solution of the present invention is a kind of preparation method of shampoo, specifically according to the following steps
Implement:
Step 1, it weighs respectively by mass percentage: sunflower oil 0.50~1.0%, span 40 0.05~0.10%, Fu
Tea extract 2~6%, glycol distearate 1.0~3.0%, octadecyl alcolol 0.5~2.0%, Cocoamidopropyl betaine
1.0~5.0%, guar hydroxypropyltrimonium ammonium chloride 0.3~0.7%, cationic hydroxyethyl cellulose 0.3~0.7%, the moon
Cinnamic alcohol ether ammonium sulfate 10~20%, sodium chloride 2~6%, disodium ethylene diamine tetraacetate 0.10~0.20%, isothiazolinone 0.10
~0.20%, flavouring agent 0.0010~0.0030%, surplus are deionized water, and the sum of said components mass percent is 100%；
Step 2, that sunflower oil, span 40 and Fu tea extract are mixed and made into emulsion is spare；
Step 3, coconut oleoyl amine third is added after glycol distearate, octadecyl alcolol being heated to 70~90 DEG C of complete thawings
Base glycine betaine is added to be stirred continuously in portions of de-ionized water at 40~80 DEG C is made pearlite slurry；
Step 4, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, be stirred continuously at 20~35 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirring
The obtained pearlite slurry of step 3, the emulsion that step 2 obtains and isothiazolinone, flavouring agent are added after uniformly, obtains shampoo.
The features of the present invention also characterized in that
Fu tea extract is after mixing Fu tea original tea with deionized water in step 1, decoct 30 at 100~120 DEG C~
50min is cooled to 20~35 DEG C, and filtering, sterilizing obtain.
Fu tea original tea and the mass ratio of deionized water are 1:20~240.
Sterilizing is sterilizing 10min~15min under the conditions of 120~150 DEG C.
Step 2 specifically: Fu tea extract is added after mixing sunflower oil and span 40 at 30~50 DEG C with 8000
~12000r/min stirring homogenizes 2~5min and obtains emulsion.
Step 2 specifically: sunflower oil and span 40 mixing after be added Fu tea extract, then 30~50 DEG C, 400~
It is ultrasonically treated 2~5min under 600w, emulsion is made.
The invention has the advantages that shampoo of the present invention, is effectively combined acquisition with Fu tea extract by each component
Weakly acidic shampoo；Dispersion degree is high after effective component in Fu tea is emulsified agent package, and the effective component of tealeaves is uniformly dispersed,
Performance is stablized, and foam is more, lasting fragrance clearly elegant with rear hair, cleans anti-dandruff and can also repair keratin, prevents from breaking
Alopecia is sent out, hair follicle stimulating promotes the growth of hair.The production method of shampoo of the invention is simple, easy to accomplish.
Shampoo of the present invention, stability is good, and washing effect is good, and pH value is 5.5~6.5, and gas release is good, and viscosity exists
Between 2000~10000cp.
Detailed description of the invention
Fig. 1 is the gas release comparison histogram of shampoo of the present invention and two kinds of commercial shampoos.
Specific embodiment
The following describes the present invention in detail with reference to the accompanying drawings and specific embodiments.
Shampoo of the present invention, it is composed of the following components by mass percentage: sunflower oil 0.50~1.0%, span 40
0.05~0.10%, Fu tea extract 2~6%, glycol distearate 1.0~3.0%, octadecyl alcolol 0.5~2.0%, coconut palm
Oleamide propyl betaine 1.0~5.0%, guar hydroxypropyltrimonium ammonium chloride 0.3~0.7%, cationic hydroxyethyl are fine
Dimension element 0.3~0.7%, lauryl alcohol ammonium sulfate 10~20%, sodium chloride 2~6%, disodium ethylene diamine tetraacetate 0.10~
0.20%, isothiazolinone 0.10~0.20%, flavouring agent 0.0010~0.0030%, surplus are deionized water, said components
The sum of mass percent is 100%.
The preparation method of above-mentioned shampoo, is specifically implemented according to the following steps:
It step 1, is in mass ratio to be decocted after 1:20~240 mix at 100~120 DEG C with deionized water by Fu tea original tea
30~50min is cooled to 20~35 DEG C, and filtering, the 10min~15min that sterilizes under the conditions of 120~150 DEG C obtain the extraction of Fu tea
Liquid；
Step 2, it weighs respectively by mass percentage: sunflower oil 0.50~1.0%, span 40 0.05~0.10%, Fu
Tea extract 2~6%, glycol distearate 1.0~3.0%, octadecyl alcolol 0.5~2.0%, Cocoamidopropyl betaine
1.0~5.0%, guar hydroxypropyltrimonium ammonium chloride 0.3~0.7%, cationic hydroxyethyl cellulose 0.3~0.7%, the moon
Cinnamic alcohol ether ammonium sulfate 10~20%, sodium chloride 2~6%, disodium ethylene diamine tetraacetate 0.10~0.20%, isothiazolinone 0.10
~0.20%, flavouring agent 0.0010~0.0030%, surplus are deionized water, and the sum of said components mass percent is 100%；
Step 3, will sunflower oil and span 40 mix after Fu tea extract is added at 30~50 DEG C with 8000~
12000r/min stirring homogenizes 2~5min and obtains emulsion；
Or Fu tea extract is added after sunflower oil and span 40 mixing, then surpass at 30~50 DEG C, 400~600w
Emulsion is made in 2~5min of sonication；
Step 4, coconut oleoyl amine third is added after glycol distearate, octadecyl alcolol being heated to 70~90 DEG C of complete thawings
Base glycine betaine is added to be stirred continuously in portions of de-ionized water at 40~80 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, be stirred continuously at 20~35 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirring
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added after uniformly, obtains shampoo.
Taking 4 groups every group 20 weight is the healthy mice of 18~20g, takes back skin of abdomen 2cm × 3cm (long × wide), makes
With shampoo of the present invention and two kinds of commercially available shampoos, (control A is cold with the control not emulsified C25 times washing with control B) and only
After weigh, eluting rate is compared, the results are shown in Table 1.By shampoo of the present invention and two kinds of commercially available shampoo (control A
Only the cold eluting rate with the control C not emulsified compares with control B) and inventive formulation, as shown in table 1, of the present invention group of D
Eluting rate significantly lower than two kinds of commercial shampoos product A and product B and only it is cold with do not emulsify control C eluting rate.
1 healthy mice of table uses shampoo of the present invention and two kinds of commercially available shampoos
(control A and control B) and the only cold eluting rate comparing result with the control C not emulsified
As seen from the above table, the eluting rate of of the present invention group of D is significantly lower than two kinds of commercial shampoos product A and product B and only
The cold eluting rate with the control C not emulsified.
Shampoo of the present invention and two kinds of commercially available shampoos (control A and control B) and inventive formulation are only cold with not newborn
The gas release comparison histogram of the control group of change is as shown in Figure 1.Gas release indicates a kind of cleaning capacity of shampoo.Will more than
Four kinds of samples respectively take 2ml that 10ml water isothermal vibration 10min under 37 DEG C, 260kw output power is added, and record gas release.From Fig. 1
In it is found that the gas release of general commercial shampoos is maintained at 25ml hereinafter, if only according to inventive formulation using general cold
Shampoo with method preparation also can only achieve the foaming capacity of commercial shampoos, but using prepared by preparation method of the invention
Shampoo gas release can be more than the foaming capacity of commercial shampoos.
Embodiment 1
It step 1, is in mass ratio after 1:40 is mixed, in 100 DEG C of decoction 30min, cooling with deionized water by Fu tea original tea
To 35 DEG C, filtering, the 10min that sterilizes under the conditions of 120 DEG C obtain Fu tea extract；
Step 2, it weighs respectively by mass percentage: sunflower oil 0.50%, span 40 0.05%, Fu tea extract
2%, glycol distearate 1.0%, octadecyl alcolol 0.5%, Cocoamidopropyl betaine 1.0%, guar gum hydroxypropyl three
Ammonio methacrylate 0.3%, cationic hydroxyethyl cellulose 0.3%, lauryl alcohol ammonium sulfate 10%, sodium chloride 2%, ethylenediamine tetraacetic
Acetic acid disodium 0.1%, isothiazolinone 0.1%, flavouring agent 0.0010%, deionized water 82.149%, said components quality hundred
Dividing the sum of ratio is 100%；
Step 3, Fu tea extract is added after sunflower oil and span 40 being mixed to stir evenly at 50 DEG C with 8000r/min
Change 5min and obtains emulsion；
Step 4, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 70 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 40 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, is stirred continuously at 20 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
Embodiment 2
It step 1, is in mass ratio after 1:240 is mixed, in 120 DEG C of decoction 50min, cooling with deionized water by Fu tea original tea
To 35 DEG C, filtering, the 15min that sterilizes under the conditions of 150 DEG C obtain Fu tea extract；
Step 2, weigh respectively by mass percentage: sunflower oil 1.0%, span 40 0.1%, Fu tea extract 6%,
Glycol distearate 3.0%, octadecyl alcolol 2.0%, Cocoamidopropyl betaine 5.0%, guar hydroxypropyltrimonium
Ammonium chloride 0.7%, cationic hydroxyethyl cellulose 0.7%, lauryl alcohol ammonium sulfate 20%, sodium chloride 6%, ethylenediamine tetra-acetic acid
Disodium 0.2%, isothiazolinone 0.2%, flavouring agent 0.0030%, deionized water 55.097%, said components mass percent
The sum of be 100%；
Step 3, Fu tea extract is added after sunflower oil and span 40 being mixed to stir at 30 DEG C with 12000r/min
It homogenizes 2min and obtains emulsion；
Step 4, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 90 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 80 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, is stirred continuously at 35 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
Embodiment 3
It step 1, is in mass ratio after 1:20 is mixed, in 110 DEG C of decoction 40min, cooling with deionized water by Fu tea original tea
To 20 DEG C, filtering, the 13min that sterilizes under the conditions of 130 DEG C obtain Fu tea extract；
Step 2, weigh respectively by mass percentage: sunflower oil 0.2%, span 40 0.03%, Fu tea extract 4%,
Glycol distearate 2.0%, octadecyl alcolol 1.0%, Cocoamidopropyl betaine 2.0%, guar hydroxypropyltrimonium
Ammonium chloride 0.6%, cationic hydroxyethyl cellulose 0.4%, lauryl alcohol ammonium sulfate 15%, sodium chloride 4%, ethylenediamine tetra-acetic acid
Disodium 0.15%, isothiazolinone 0.18%, flavouring agent 0.002%, deionized water 70.438%, said components mass percent
The sum of be 100%；
Step 3, Fu tea extract is added after sunflower oil and span 40 being mixed, then at 40 DEG C, 400w at ultrasound
Emulsion is made in reason 3min；
Step 4, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 80 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 50 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, is stirred continuously at 25 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
Embodiment 4
It step 1, is in mass ratio after 1:100 is mixed, in 100 DEG C of decoction 50min, cooling with deionized water by Fu tea original tea
To 30 DEG C, filtering, the 14min that sterilizes under the conditions of 140 DEG C obtain Fu tea extract；
Step 2, weigh respectively by mass percentage: sunflower oil 0.3%, span 40 0.04%, Fu tea extract 5%,
Glycol distearate 1.5%, octadecyl alcolol 1.5%, Cocoamidopropyl betaine 3.0%, guar hydroxypropyltrimonium
Ammonium chloride 0.4%, cationic hydroxyethyl cellulose 0.6%, lauryl alcohol ammonium sulfate 18%, sodium chloride 5%, ethylenediamine tetra-acetic acid
Disodium 0.18%, isothiazolinone 0.12%, flavouring agent 0.001%, deionized water 64.359%, said components mass percent
The sum of be 100%；
Step 3, Fu tea extract is added after sunflower oil and span 40 being mixed, then at 30 DEG C, 600w at ultrasound
Emulsion is made in reason 5min；
Step 4, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 75 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 70 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, is stirred continuously at 30 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
Embodiment 5
It step 1, is in mass ratio after 1:180 is mixed, in 110 DEG C of decoction 30min, cooling with deionized water by Fu tea original tea
To 20 DEG C, filtering, the 12min that sterilizes under the conditions of 120 DEG C obtain Fu tea extract；
Step 2, weigh respectively by mass percentage: sunflower oil 0.4%, span 40 0.02%, Fu tea extract 3%,
Glycol distearate 2.5%, octadecyl alcolol 0.5%, Cocoamidopropyl betaine 4.0%, guar hydroxypropyltrimonium
Ammonium chloride 0.5%, cationic hydroxyethyl cellulose 0.5%, lauryl alcohol ammonium sulfate 12%, sodium chloride 3%, ethylenediamine tetra-acetic acid
Disodium 0.12%, isothiazolinone 0.15%, flavouring agent 0.0030%, deionized water 73.307%, said components quality percentage
Than the sum of be 100%；
Step 3, Fu tea extract is added after sunflower oil and span 40 being mixed, then at 50 DEG C, 500w at ultrasound
Emulsion is made in reason 2min；
Step 4, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 85 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 60 DEG C is made pearlite slurry；
Step 5, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added
Enter in remaining deionized water, is stirred continuously at 25 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 4, the emulsion that step 3 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
Claims (4)
1. a kind of preparation method of shampoo, which is characterized in that be specifically implemented according to the following steps:
Step 1, weigh respectively by mass percentage: sunflower oil 0.50~1.0%, span 40 0.05~0.10%, Fu tea mention
Take liquid 2~6%, glycol distearate 1.0~3.0%, octadecyl alcolol 0.5~2.0%, Cocoamidopropyl betaine 1.0
~5.0%, guar hydroxypropyltrimonium ammonium chloride 0.3~0.7%, cationic hydroxyethyl cellulose 0.3~0.7%, laurel
Ether sulfate ammonium 10~20%, sodium chloride 2~6%, disodium ethylene diamine tetraacetate 0.10~0.20%, isothiazolinone 0.10~
0.20%, flavouring agent 0.0010~0.0030%, surplus are deionized water, and the sum of said components mass percent is 100%；
Step 2, Fu tea extract is added after sunflower oil and span 40 being mixed at 30~50 DEG C with 8000~12000r/
Min stirring homogenize 2~5min obtain emulsion or will sunflower oil and span 40 mix after Fu tea extract is added, then 30~
50 DEG C, emulsion is made in 2~5min of ultrasonic treatment under 400~600w；
Step 3, cocamidopropyl propyl amide sweet tea is added after glycol distearate, octadecyl alcolol being heated to 70~90 DEG C of complete thawings
Dish alkali is added to be stirred continuously in portions of de-ionized water at 40~80 DEG C is made pearlite slurry；
Step 4, guar hydroxypropyltrimonium ammonium chloride, cationic hydroxyethyl cellulose, lauryl alcohol ammonium sulfate are added surplus
In remaining deionized water, it is stirred continuously at 20~35 DEG C uniformly, adds sodium chloride, disodium ethylene diamine tetraacetate stirs evenly
The obtained pearlite slurry of step 3, the emulsion that step 2 obtains and isothiazolinone, flavouring agent are added afterwards, obtains shampoo.
2. the preparation method of shampoo according to claim 1, which is characterized in that Fu tea extract is by Fu in step 1
After tea original tea is mixed with deionized water, in 100~120 DEG C of 30~50min of decoction, 20~35 DEG C is cooled to, filters, sterilize
It arrives.
3. the preparation method of shampoo according to claim 2, which is characterized in that the Fu tea original tea and deionized water
Mass ratio is 1:20~240.
4. the preparation method of shampoo according to claim 2 or 3, which is characterized in that sterilizing is in 120~150 DEG C of items
Sterilize 10min~15min under part.
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| CN110680782A (en) * | 2019-10-29 | 2020-01-14 | 陕西仙喜辣木茯茶有限公司 | Shampoo capable of nourishing hair roots |
| CN113694115A (en) * | 2019-11-28 | 2021-11-26 | 沣潮医药科技（上海）有限公司 | Application of Fuzhuan tea extract in preparation of skin conditioning product |
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| CN103126935A (en) * | 2013-03-21 | 2013-06-05 | 上海滇虹药业有限公司 | Two-in-one shampoo and preparation method thereof |
| CN105232385A (en) * | 2015-10-28 | 2016-01-13 | 龙胜各族自治县农产品购销农民专业合作社 | Tea bran shampoo and preparation method thereof |
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| CN103126935A (en) * | 2013-03-21 | 2013-06-05 | 上海滇虹药业有限公司 | Two-in-one shampoo and preparation method thereof |
| CN105232385A (en) * | 2015-10-28 | 2016-01-13 | 龙胜各族自治县农产品购销农民专业合作社 | Tea bran shampoo and preparation method thereof |
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