CN106306114A - Coixseed bran oil microcapsule and preparation method thereof - Google Patents
Coixseed bran oil microcapsule and preparation method thereof Download PDFInfo
- Publication number
- CN106306114A CN106306114A CN201610694652.9A CN201610694652A CN106306114A CN 106306114 A CN106306114 A CN 106306114A CN 201610694652 A CN201610694652 A CN 201610694652A CN 106306114 A CN106306114 A CN 106306114A
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- CN
- China
- Prior art keywords
- microcapsule
- semen coicis
- rice oil
- wall material
- emulsion
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000003094 microcapsule Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 244000077995 Coix lacryma jobi Species 0.000 title abstract 4
- 239000000463 material Substances 0.000 claims abstract description 34
- 239000000839 emulsion Substances 0.000 claims abstract description 23
- 235000010489 acacia gum Nutrition 0.000 claims abstract description 16
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims abstract description 16
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 12
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 12
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 8
- 210000000582 semen Anatomy 0.000 claims description 43
- 241000209094 Oryza Species 0.000 claims description 34
- 235000007164 Oryza sativa Nutrition 0.000 claims description 34
- 235000009566 rice Nutrition 0.000 claims description 34
- 238000003756 stirring Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 230000001804 emulsifying effect Effects 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 5
- -1 by mass percentage Substances 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 abstract description 4
- 238000001694 spray drying Methods 0.000 abstract description 3
- 239000011162 core material Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 36
- 239000000047 product Substances 0.000 description 7
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 5
- 239000003995 emulsifying agent Substances 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241000700159 Rattus Species 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 150000003951 lactams Chemical class 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000003760 magnetic stirring Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000004531 microgranule Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 125000002811 oleoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 235000002378 plant sterols Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000010734 process oil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/06—Preservation of finished products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention discloses a coixseed bran oil microcapsule and a preparation method thereof. The microcapsule is formed by embedding coixseed bran oil with wall materials accounting for, by weight 70%-75% of the coixseed bran oil microcapsule; the wall materials are prepared from, by weight, 40%-45% of Arabic gum and 50%-55% of maltodextrin. The preparation method includes the steps of preparation of wall material solutions, preparation of wall-material primary emulsions, preparation of microcapsule emulsions, spray drying and the like. Under the condition that the emulsions and organic solvents are not added, emulsibility of the Arabic gum is fully utilized, and adding order of the wall materials and core materials is changed; the microcapsule is prepared with the spray drying method, so that the obtained microcapsule is high in stability and embedding rate.
Description
Technical field
The present invention relates to a kind of Semen Coicis rice oil microcapsule and preparation method thereof, belong to the microcapsule system in foods processing technique
Standby field.
Background technology
Semen Coicis bran is the exterior materials that Semen Coicis removes when being processed into polished rice, i.e. the seed coat of Semen Coicis accounts for the total matter of whole Semen Coicis
The 6%-10% of amount, oil content is 20%～25%, more high than the oil content of Semen Coicis, but is taken as honest and clean all the time
The animal feed of valency and be not fully utilized, not only cause the significant wastage of Semen Coicis bran resource, also have impact on agricultural and sideline product
The deep processing and utilization of product.The most less to the research of Semen Coicis bran, existing research shows: rich in multiple unsaturation in Semen Coicis rice oil
Fatty acid and bioactive ingredients, the several functions active component such as including plant sterol, alkanol, oleoyl, lactams and flavone, tool
There are the effects such as anticancer, antitumor, antiinflammatory, antioxidation and blood sugar lowering.
Microcapsule technology is a kind of embedding techniques, scattered solid, liquid or gas entrapment will form the technology of microgranule；
It is intended to protect sensitive materials, improves materiel machining characteristic and control its release during storage and use.By Semen Coicis
After rice oil is prepared as microcapsule powder, under the protection of outer layer dense film, decrease external environment (such as O2, pH, moisture, temperature
Deng) destruction to Semen Coicis rice oil, particularly Oxidative demage, substantially increase the storage-stable of Semen Coicis rice oil.Additionally, Semen Coicis bran
Become solid-state by liquid after oil microcapsule, it is simple to process, transport and preserve, and product good water solubility, weighing are conveniently, widen
The range of application of Semen Coicis rice oil.
In existing technology, to the research of grease microcapsule the most all uses interpolation organic solvent or the method for emulsifying agent
Process oil phase to be allowed to merge with aqueous phase, but the active substance in the fragile bad oil of organic solvent and flavor component, and current research table
Bright, the use of emulsifying agent can change the intestinal microbial population of rat thus cause the generation of Obesity of Rats disease.There is presently no for
The related art of the comparative maturity of Semen Coicis rice oil microcapsule.
Summary of the invention
It is an object of the invention to: under conditions of without emulsifying agent, it is provided that a kind of Semen Coicis rice oil microcapsule and preparation thereof
Method, solves Semen Coicis rice oil oxidative rancidity problem in production, storing and intermediate links, improves the stability of product, widen
Its range of application.
The present invention is achieved through the following technical solutions this purpose:
First, the present invention proposes a kind of Semen Coicis rice oil microcapsule, its micro-glue made with wall material embedding Semen Coicis rice oil
Capsule, wherein, wall material amount accounts for the 70%～75% of this Semen Coicis rice oil microcapsule quality；Wall material is by arabic gum and maltodextrin system
Becoming, in wall material raw material, by mass percentage, arabic gum accounts for 40%～45%, and maltodextrin accounts for 50%～55%.
The preparation method of this Semen Coicis rice oil microcapsule comprises the steps:
(1) prepared by wall material solution: added by arabic gum in the hot water of 60～70 DEG C, and stirring and dissolving prepares wall material
Solution；
(2) prepared by wall material just emulsion: being added in the wall material solution that step (1) obtains by Semen Coicis rice oil, temperature is maintained at
40～60 DEG C, stirring and emulsifying 10～15 minutes, then add maltodextrin as wall material in the ratio of arabic gum and maltodextrin
Filler, stirring and emulsifying 15～20 minutes, prepare wall-forming material just emulsion；It is initially charged after Semen Coicis rice oil forms first emulsion and adds again
Enter maltodextrin, it is therefore an objective to make full use of the emulsibility of arabic gum, strengthen the stability of microcapsule, avoid additionally adding simultaneously
Emulsifying agent.
(3) preparation of microcapsule emulsion: the wall material that step (2) is prepared just emulsion high speed disperser with
The VELOCITY SHEAR 8 of 20000r/min～10 minutes, stop to emulsion and be cooled to room temperature, then with high speed disperser with 10000r/
The VELOCITY SHEAR of min 10 minutes, then under the pressure of 30～40Mpa, homogenizing prepares microcapsule emulsion for twice；
(4) it is spray-dried: the microcapsule emulsion that step (3) prepares is spray-dried；The air intake of spray dryer
Mouthful temperature controls at 180 DEG C, and air outlet temperature is 80～90 DEG C, and sample introduction flow is 4ml/min, stir under the conditions of normal pressure and temperature into
Sample, prepares Semen Coicis rice oil microcapsule.
Wherein, in step (1), the consumption of water is arabic gum in this microcapsule, maltodextrin and three kinds of raw materials of Semen Coicis rice oil
1.8～2.3 times of gross weight.
Beneficial effects of the present invention: (1) present invention prepares Semen Coicis rice oil microcapsule with Semen Coicis rice oil for raw material, " change give up into
Precious ", resource sufficient, solve intensive processing and the storing of Semen Coicis rice oil, the problem of oxidation of becoming sour of Semen Coicis product, widen simultaneously
The range of application of Semen Coicis rice oil.(2) present invention is under conditions of without emulsifying agent and organic solvent, makes full use of arabic gum
Emulsibility, change wall material and the order of addition of core, use spray drying method to prepare microcapsule, its microcapsule prepared is stable
Property is strong, embedding rate is high.
Detailed description of the invention
For deepening to understand the present invention, below in conjunction with embodiment, the present invention is described in further detail, this embodiment
It is only used for explaining the present invention, is not intended that limiting the scope of the present invention.The amendment made on the basis of the present invention or change
Enter, if it will be apparent to those skilled in the art that, then belong to the scope of protection of present invention.In herein below such as relating to
Quantity or ratio, if no special instructions, all represent mass unit or mass ratio.
Embodiment 1:
(1) weigh 11.67g arabic gum to be placed in the beaker of 200ml, add 65ml distilled water, at the water-bath bar of 60 DEG C
Stir to being completely dissolved under part, make wall material solution.
(2) weigh 8.75g Semen Coicis rice oil, be slowly added into while stirring in arabic gum wall material solution, then use
The water-bath magnetic stirring apparatus of 600rpm under 40～60 degrees celsius, stirring and emulsifying 10～15 minutes, add 14.58g wheat
Bud dextrin, as wall material filler, stirring and emulsifying 15～20 minutes, prepares wall-forming material just emulsion.
(3) by first emulsion high speed disperser with the speed homogenizing 8 of 20000r/min～10 minutes, stay for some time
Emulsion is cooled to room temperature, then with high speed disperser with the speed homogenizing 10 minutes of 10000r/min, then 30～
Under the pressure of 40Mpa, homogenizing prepares microcapsule emulsion for twice.
(4) by above-mentioned microcapsule emulsion intake air temperature 180 degrees Celsius, air outlet temperature is 80～90 degrees Celsius,
Sample introduction flow is to be spray-dried under conditions of 4ml/min, prepares Semen Coicis rice oil microcapsule.The embedding of Semen Coicis rice oil microcapsule
Rate is 87.46%.
The mensuration of surface oil content: weigh micro encapsulation Semen Coicis bran quintessence oil 2.0000g, be laid on buchner funnel, uses
Filter after 20mL petroleum ether (boiling range 30--60 DEG C) washing 1min, then wash filter paper, buchner funnel at twice with 20mL petroleum ether.
Merging filtrate, in the conical flask after 50ml constant weight, is waved in the water-bath of 65 degrees Celsius after being evaporated petroleum ether, conical flask is placed in
In the baking oven of 103 degrees Celsius, dry to constant weight.
Surface oil content=surface oil weight/sample weight × 100%
The mensuration of total oil content: accurately weigh microencapsulated products about 1g (M), with the distillation moisture of 10ml 60 degrees Celsius
Being dissolved in for several times in 100ml tool plug graduated cylinder, adding 1.25ml concentration is the ammonia of 25%, and fully mixing is placed on 60 DEG C water
Bath is heated 5 minutes, then shakes 2 minutes, be subsequently adding 10ml ethanol, cool down in cold water after fully shaking up, add 25ml second
Ether, shakes 0.5 minute, adds 25ml petroleum ether (boiling range is 30～60 DEG C), then shakes 0.5 minute, stands and within 30 minutes, is allowed to point
Layer, reads the volume (V) of supernatant liquid, with pipet sucking-off certain volume (V1) supernatant in the fine taper bottle after constant weight
(M1), in the water-bath of 65 degrees Celsius, volatilize solvent, conical flask is placed in the baking oven of 103 degrees Celsius, dry to constant weight (M2)。
Product embedding rate=(1-surface oil content/total oil content) × 100%
Certainly, being more than the concrete exemplary applications of the present invention, the present invention also has other embodiment, and all employings are equal to
Replace or the technical scheme of equivalent transformation formation, within all falling within protection domain of the presently claimed invention.
Claims (3)
1. a Semen Coicis rice oil microcapsule, the microcapsule made with wall material embedding Semen Coicis rice oil, it is characterised in that: described wall material
Quality accounts for the 70%～75% of this Semen Coicis rice oil microcapsule quality；Described wall material is made up of arabic gum and maltodextrin, at wall
In material raw material, by mass percentage, arabic gum accounts for 40%～45%, and maltodextrin accounts for 50%～55%.
2. the preparation method of a Semen Coicis rice oil microcapsule as claimed in claim 1, it is characterised in that the method includes as follows
Step:
(1) prepared by wall material solution: added by arabic gum in the hot water of 60～70 DEG C, and stirring and dissolving prepares wall material solution；
(2) prepared by wall material just emulsion: added by Semen Coicis rice oil in the wall material solution that step (1) obtains, temperature be maintained at 40～
60 DEG C, stirring and emulsifying 10～15 minutes, then add maltodextrin as the filling of wall material in the ratio of arabic gum and maltodextrin
Agent, stirring and emulsifying 15～20 minutes, prepare wall-forming material just emulsion；
(3) preparation of microcapsule emulsion: the wall material that step (2) is prepared just emulsion high speed disperser with
The VELOCITY SHEAR 8 of 20000r/min～10 minutes, stop to emulsion and be cooled to room temperature, then with high speed disperser with 10000r/
The VELOCITY SHEAR of min 10 minutes, then under the pressure of 30～40Mpa, homogenizing prepares microcapsule emulsion for twice；
(4) it is spray-dried: the microcapsule emulsion that step (3) prepares is spray-dried；The air inlet temperature of spray dryer
Degree controls at 180 DEG C, and air outlet temperature is 80～90 DEG C, and sample introduction flow is 4ml/min, stirs sample introduction under the conditions of normal pressure and temperature,
Prepare Semen Coicis rice oil microcapsule.
The preparation method of Semen Coicis rice oil microcapsule the most according to claim 2, it is characterised in that: the use of water in step (1)
Amount is arabic gum, maltodextrin and 1.8～2.3 times of three kinds of raw material gross weights of Semen Coicis rice oil in this microcapsule.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610694652.9A CN106306114A (en) | 2016-08-22 | 2016-08-22 | Coixseed bran oil microcapsule and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610694652.9A CN106306114A (en) | 2016-08-22 | 2016-08-22 | Coixseed bran oil microcapsule and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106306114A true CN106306114A (en) | 2017-01-11 |
Family
ID=57744546
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610694652.9A Pending CN106306114A (en) | 2016-08-22 | 2016-08-22 | Coixseed bran oil microcapsule and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106306114A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108236108A (en) * | 2017-12-18 | 2018-07-03 | 中山大学 | A kind of preparation method of ganoderma lucidum spore oil microcapsule powder |
| CN111012831A (en) * | 2018-10-10 | 2020-04-17 | 泰州医药城国科化物生物医药科技有限公司 | Wild jujube kernel oil microcapsule powder and preparation method and application thereof |
| CN112121128A (en) * | 2020-08-27 | 2020-12-25 | 福建中医药大学 | Coix seed coat oil microcapsule and preparation process thereof |
| CN113647474A (en) * | 2021-08-30 | 2021-11-16 | 黑龙江八一农垦大学 | Preparation method of broom corn millet shell oil microcapsule |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104757531A (en) * | 2014-11-05 | 2015-07-08 | 四川省植物工程研究院 | Chinese prickly ash seed oil micro capsule and preparation method thereof |
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2016
- 2016-08-22 CN CN201610694652.9A patent/CN106306114A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104757531A (en) * | 2014-11-05 | 2015-07-08 | 四川省植物工程研究院 | Chinese prickly ash seed oil micro capsule and preparation method thereof |
Non-Patent Citations (2)
| Title |
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| 任迪峰: "《现代食品加工技术》", 31 August 2015, 中国农业科学技术出版社 * |
| 林莉等: "响应面法优化水酶法提取薏米糠油工艺研究", 《中国油脂》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108236108A (en) * | 2017-12-18 | 2018-07-03 | 中山大学 | A kind of preparation method of ganoderma lucidum spore oil microcapsule powder |
| CN111012831A (en) * | 2018-10-10 | 2020-04-17 | 泰州医药城国科化物生物医药科技有限公司 | Wild jujube kernel oil microcapsule powder and preparation method and application thereof |
| CN112121128A (en) * | 2020-08-27 | 2020-12-25 | 福建中医药大学 | Coix seed coat oil microcapsule and preparation process thereof |
| CN113647474A (en) * | 2021-08-30 | 2021-11-16 | 黑龙江八一农垦大学 | Preparation method of broom corn millet shell oil microcapsule |
| CN113647474B (en) * | 2021-08-30 | 2023-10-03 | 黑龙江八一农垦大学 | Preparation method of broom corn millet shell oil microcapsule |
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Application publication date: 20170111 |