CN106290118A - Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect - Google Patents
Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect Download PDFInfo
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- 230000035699 permeability Effects 0.000 title claims abstract description 75
- 239000011435 rock Substances 0.000 title claims abstract description 44
- 238000000034 method Methods 0.000 title claims abstract description 42
- 230000000694 effects Effects 0.000 title claims abstract description 15
- 230000003204 osmotic effect Effects 0.000 claims abstract description 32
- 238000007906 compression Methods 0.000 claims abstract description 20
- 230000006835 compression Effects 0.000 claims abstract description 20
- 238000011144 upstream manufacturing Methods 0.000 claims abstract description 19
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 18
- 238000005259 measurement Methods 0.000 claims abstract description 16
- 239000011148 porous material Substances 0.000 claims abstract description 16
- 229920001971 elastomer Polymers 0.000 claims abstract description 10
- 238000004458 analytical method Methods 0.000 claims abstract description 5
- 230000005540 biological transmission Effects 0.000 claims abstract description 3
- 238000012360 testing method Methods 0.000 claims description 8
- 238000005516 engineering process Methods 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- 238000005314 correlation function Methods 0.000 claims description 4
- 238000004364 calculation method Methods 0.000 claims description 3
- 238000009472 formulation Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000011160 research Methods 0.000 claims description 3
- 230000009514 concussion Effects 0.000 claims 1
- 230000010355 oscillation Effects 0.000 description 5
- 238000007789 sealing Methods 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000005325 percolation Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/082—Investigating permeability by forcing a fluid through a sample
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/082—Investigating permeability by forcing a fluid through a sample
- G01N15/0826—Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
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- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
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- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
Abstract
The invention discloses Oil in Super-low Permeability rock permeability measuring method under a kind of triaxial stress effect.It comprises the steps: to choose Oil in Super-low Permeability rock, prepares sample；With rubber sleeve, the permeable backing plate at upper and lower for sample two ends, sample are wrapped between upstream hole pressure pad block and confined pressure room base；Apply confined pressure and axial compression to particular value to sample, apply osmotic pressure to sample so that sample is saturated simultaneously；After the pressurization of sample osmotic pressure is saturated, apply amplitude, the known sine pressure wave of frequency to sample, record downstream pore pressure ripple situation and by real-time data transmission to DATA REASONING and acquisition system simultaneously；Change confined pressure, axial compression size, waveform cross-correlation method is used for the measurement of permeability, the sample in the case of different confined pressure, axial compressions is carried out permeability analysis, draw the permeability under the conditions of different confined pressure, axial compression.Overcome that prior art certainty of measurement is poor, be only provided that confined pressure, the shortcoming that cannot truly simulate deep rock mass stress under triaxial stress effect.
Description
Technical field
The present invention relates under the rock mechanics field tests in Geotechnical Engineering, more specifically triaxial stress effect
Oil in Super-low Permeability rock permeability measuring method.
Background technology
Permeability is one of important physical parameter of rock, for understanding unconventionaloil pool field and the deep of nuclear waste storage
The physical characteristic of rock mass is even more important；And along with the exploitation of shale gas in recent years, tight sand oil gas etc., need one urgently
Planting and measure the device of Oil in Super-low Permeability rock mass permeability under triaxial state of stress, experimental principle now and experimental apparatus are proposed by this
No small challenge.
The experimental apparatus of the rock permeability of great majority measurement at present all uses the principle such as steady state method or pressure pulse method, right
Oil in Super-low Permeability rock mass in the reservoir of unconventionaloil pool field, there is measuring principle backwardness, poor the lacking of certainty of measurement in this kind of method of testing
Point, therefore and the measurement of inapplicable this Oil in Super-low Permeability rock mass permeability；Measure Oil in Super-low Permeability rock permeability at present popular
Method is pressure oscillations method, and the principle of the method is by applying known osmotic pressure Reeb in rock sample upstream, surveying in downstream
Measure corresponding osmotic pressure Reeb, draw Oil in Super-low Permeability rock permeability by contrast waveform between the two.
The instrument of current domestic a small amount of employing pressure oscillations method measurement Oil in Super-low Permeability rock mass permeability then also exists certain lacking
Point；Patent " a kind of cross-correlation skill measuring Oil in Super-low Permeability rock permeability stress sensitivity of Application No. 201310518094.7
Art " in have employed pressure oscillations method and measure the permeability of Oil in Super-low Permeability rock, but this device is only provided that confined pressure, it is impossible to provide three
The trystate of axial stress, it is impossible to true simulation deep rock mass stress under triaxial stress effect.
Summary of the invention
The invention aims to provide Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect.
To achieve these goals, the technical scheme is that under triaxial stress effect, Oil in Super-low Permeability rock permeability is surveyed
Metering method, it is characterised in that: comprise the steps:
Step 1: choose Oil in Super-low Permeability rock, and it is processed into the cylinder experimental member of standard, obtain sample；
Step 2: the permeable backing plate at upper and lower for sample two ends, sample are wrapped in upstream hole pressure pad block and confined pressure with rubber sleeve
Between the base of room, and with two upper and lower two ends of clip banding rubber sleeve；
Step 3: apply confined pressure and axial compression to sample by confined pressure closed loop servo dosing pump, axial compression closed loop servo dosing pump
To particular value, apply osmotic pressure by osmotic pressure closed loop servo dosing pump to sample so that sample is saturated simultaneously；
Step 4: until sample osmotic pressure pressurization saturated after, by osmotic pressure closed loop servo dosing pump to sample apply amplitude,
The known sine pressure wave of frequency, simultaneously by the situation of hole pressure sensor record downstream, downstream pore pressure ripple and by data reality
Time be transferred to DATA REASONING and acquisition system；
Step 5: change confined pressure, axial compression size, waveform cross-correlation method is used for the measurement of permeability, to different confined pressures,
Sample in the case of axial compression carries out permeability analysis, draws the permeability under the conditions of different confined pressure, axial compression:
Computing permeability mode such as formula is 1. shown:
Wherein, η is the osmotic pressure medium coefficient of viscosity, and L is piece lengths, and β is osmotic pressure media collapse coefficient, and T is hole
In the pressure oscillations cycle, S is test specimen cross-sectional area, and V is upstream hole pressure vessel volume, and ψ, γ are to produce in formulation process
Two dimensionless numbers,
ψ and γ is tried to achieve by upstream and downstream Amplitude Ration α, the Phase delay θ measuring gained；Wherein, ψ, γ calculation is as public
Formula is 2. shown:
Wherein, α be upstream and downstream Amplitude Ration, θ be Phase delay,
According to Fischer research conclusion, upstream and downstream Amplitude Ration α, Phase delay θ can be expressed as the function of ψ, γ, for making
Functional form is simple, and the functional expression containing ψ, γ is expressed as A, X by spyD、YD、A、XD、YDIt it is a process variable.
In technique scheme, in described step 1, the described Oil in Super-low Permeability rock chosen includes shale, tight sand,
Described sample is the described cylinder experimental member being processed to diameter 5mm, long 10mm.Shale or described tight sand are wanted really
Protect internal soundness, must not have relatively macrolesion.
In technique scheme, described permeable backing plate include permeable backing plate, under permeable backing plate, described permeable backing plate
Be arranged at described sample upper end, described under permeable backing plate be arranged at described sample lower end；State in rapid 3 described, it is ensured that described examination
Sample is the most saturated, and the saturated of described sample can use hold-up or gas saturated.Ensure the sealing of test cabinet；Make confined pressure room
Strictly isolate with laboratory, prevent during applying osmotic pressure not in place on measurement result generation impact owing to sealing；Prevent
Saturated insufficient produce subsequent experimental affects.
In technique scheme, in described step 5, when data record and process, utilize signal processing technology
In cross-correlation function analyze method improve signal to noise ratio.Due to the interference of experimental apparatus itself, temperature and other signals of telecommunication, meeting
The Pore Pressure sine pressure wave measured is produced interference；For the measurement of Oil in Super-low Permeability rock permeability, this interference is to a certain degree
On have impact on the accuracy of experimental result, analyze method (as used fast Fourier (FFT) to become hence with cross-correlation function
Change) improve signal to noise ratio, thus improve experimental precision.
In technique scheme, the instrument internal pipe diameter of transport pore media is less than 1mm, and outside transport pipeline
The most a diameter of more than or equal to 2mm.
Owing to, in the experiments of measuring of Oil in Super-low Permeability rock permeability, than storage flow rate, (ratio storage flow rate is per unit volume seepage flow
System stores the ability of fluid) experimental result is affected the measurement result impact of the general rock permeability of comparison greatly, therefore want fully
Consider than the storage flow rate impact on experimental result；To this end, the instrument internal pipe diameter of transport pore media must be sufficiently small, and
Then corresponding diameter can be slightly larger for outside transport pipeline.
Present invention have the advantage that
(1) Oil in Super-low Permeability rock permeability can be measured well；
(2) it is provided that the trystate of triaxial stress, the triaxial state of stress of rock mass can have been simulated truly；
(3) test cabinet build-in test sample is tightly wrapped up by rubber sleeve, and wherein one piece of permeable backing plate is respectively placed in sample top and the bottom,
Permeable backing plate is identical with sample size, and sample and two pieces of permeable backing plates are closely seated in by rubber sleeve by two clips
Between hole pressure head and confined pressure room base；Ensure the sealing of test cabinet；Make confined pressure room strictly isolate with laboratory, prevent from executing
Owing to sealing is not in place, measurement result is produced impact during adding osmotic pressure；
(4) realize computer to the monitoring in real time of data overall process and to control, coordinate related software automatically to calculate experiment knot
Really, time saving and energy saving, it is to avoid personal error；Using signal processing technology to process data, certainty of measurement is high；
(5) simple to operate, principle is advanced and mature.
Accompanying drawing explanation
Fig. 1 is experimental provision structural representation of the present invention.
Fig. 2 is that the present invention implements to measure the relevant figure of Oil in Super-low Permeability rock permeability Pore Pressure waveform under triaxial state of stress.
2-confined pressure room base in figure, 7-upstream hole pressure pad block, the permeable backing plate of 8-, the upper permeable backing plate of 81-, permeable under 82-
Backing plate, 9-sample, 10-clip, 11-rubber sleeve, 14-confined pressure closed loop servo dosing pump, 17-axial compression closed loop servo dosing pump, 20-
Osmotic pressure closed loop servo dosing pump, 22-downstream hole pressure sensor, 23-data acquisition and processing system, I-upper pore pressure
Ripple, II-lower hole pressure wave.
Detailed description of the invention
Describe the performance of the present invention below in conjunction with the accompanying drawings in detail, but they are not intended that limitation of the invention, only
For example.Make advantages of the present invention more clear and easy to understand by explanation simultaneously.
Refering to accompanying drawing understand: Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect, it is characterised in that: include as
Lower step:
Step 1: choose Oil in Super-low Permeability rock, and it is processed into the cylinder experimental member of standard, obtain sample 9；
Step 2: the permeable backing plate 8 at sample about 9 two ends, sample 9 are wrapped in upstream hole pressure pad block 7 with rubber sleeve 11
And between confined pressure room base 2, and with two clip 10 banding rubber sleeve about 11 two ends；
Step 3: by confined pressure closed loop servo dosing pump 14, axial compression closed loop servo dosing pump 17 give sample 9 apply confined pressure with
And axial compression is to particular value, apply osmotic pressure to sample 9 by osmotic pressure closed loop servo dosing pump 20 so that sample 9 is saturated simultaneously；
Step 4: after the pressurization of sample 9 osmotic pressure is saturated, to sample 9 to apply to shake by osmotic pressure closed loop servo dosing pump 20
The known sine pressure wave of width, frequency, records the situation of downstream pore pressure ripple II also by downstream hole pressure sensor 22 simultaneously
By real-time data transmission to DATA REASONING and acquisition system 23；
Step 5: change confined pressure, axial compression size, waveform cross-correlation method is used for the measurement of permeability, to different confined pressures,
Sample 9 in the case of axial compression carries out permeability analysis, draws the permeability under the conditions of different confined pressure, axial compression；
Computing permeability mode such as formula is 1. shown:
Wherein, η is the osmotic pressure medium coefficient of viscosity, and L is piece lengths, and β is osmotic pressure media collapse coefficient, and T is hole
In the pressure oscillations cycle, S is test specimen cross-sectional area, and V is upstream hole pressure vessel volume, and ψ, γ are to produce in formulation process
Two dimensionless numbers,
ψ and γ is tried to achieve by upstream and downstream Amplitude Ration α, the Phase delay θ measuring gained；Wherein, ψ, γ calculation is as public
Formula is 2. shown:
Wherein, α be upstream and downstream Amplitude Ration, θ be Phase delay,
According to Fischer research conclusion, upstream and downstream Amplitude Ration α, Phase delay θ can be expressed as the function of ψ, γ, for making
Functional form is simple, and the functional expression containing ψ, γ is expressed as A, X by spyD、YD、A、XD、YDIt it is a process variable.
In described step 1, the described Oil in Super-low Permeability rock chosen includes shale, tight sand；Described sample 9 is processed
Become diameter 5mm, the described cylinder experimental member of long 10mm.
Described permeable backing plate 8 include permeable backing plate 81, under permeable backing plate 82, described permeable backing plate 81 is arranged at described
Sample 9 upper end, described under permeable backing plate 82 be arranged at described sample 9 lower end；State in rapid 3 described, it is ensured that described sample 9 is abundant
Saturated, the saturated of described sample 9 can use hold-up or gas saturated.
In described step 5, when data record and process, utilize the cross-correlation function analysis in signal processing technology
Method improves signal to noise ratio.
The instrument internal pipe diameter of transport pore media less than 1mm, and the outside corresponding diameter of transport pipeline more than or
Equal to 2mm.
In Fig. 2, I is upper Pore Pressure Reeb, osmotic pressure servopump apply amplitude and frequency by percolation path to rock sample
Known to rate, sinusoidal osmotic pressure Reeb, its amplitude and frequency controls by the servo control molding of servopump in triaxial pressure system 24
Block is controlled, and the measurement of its amplitude and frequency is recorded by upper osmolarity sensor 19, ultimately form the osmotic pressure of osmotic pressure-
Temporal image；Due to the impact of rock sample permeability, sine osmotic pressure Reeb, upstream is when by rock sample inside, and it shakes
Width can be decayed, and phase place also can occur hysteresis effect, namely the downstream hole pressure wave II in figure；Same, lower hole
The measurement of pressure is recorded by lower osmolarity sensor 22, ultimately forms the osmotic pressure-temporal image of lower osmotic pressure；Thus can be straight
The Amplitude Ration α and Phase delay θ that obtain upper and lower Pore Pressure amplitude seen, by the width of permeability Yu upper and lower Pore Pressure amplitude
Value ratio α and the relation of Phase delay θ, finally calculate the permeability of rock sample.
Other unaccounted part belongs to prior art.
Claims (5)
1. Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect, it is characterised in that: comprise the steps:
Step 1: choose Oil in Super-low Permeability rock, and it is processed into the cylinder experimental member of standard, obtain sample (9)；
Step 2: sample (9) the permeable backing plate (8) at two ends, sample (9) up and down are wrapped in upstream Pore Pressure with rubber sleeve (11)
Between cushion block (7) and confined pressure room base (2), and with two clips (10) banding rubber sleeve (11) up and down two ends；
Step 3: apply confined pressure to sample (9) by confined pressure closed loop servo dosing pump (14), axial compression closed loop servo dosing pump (17)
And axial compression is to particular value, apply osmotic pressure to sample (9) by osmotic pressure closed loop servo dosing pump (20) so that sample simultaneously
(9) saturated；
Step 4: after the pressurization of sample (9) osmotic pressure is saturated, applies to sample (9) by osmotic pressure closed loop servo dosing pump (20)
The known sine pressure wave of amplitude, frequency, simultaneously by downstream hole pressure sensor (22) record downstream pore pressure ripple (II)
Situation by real-time data transmission to DATA REASONING and acquisition system (23)；
Step 5: change confined pressure, axial compression size, waveform cross-correlation method is used for the measurement of permeability, to different confined pressure, axial compressions
In the case of sample (9) carry out permeability analysis, draw the permeability under the conditions of different confined pressure, axial compression；
Computing permeability mode such as formula is 1. shown:
Wherein, η is the osmotic pressure medium coefficient of viscosity, and L is piece lengths, and β is osmotic pressure media collapse coefficient, and T is pore pressure
In the concussion cycle, S is test specimen cross-sectional area, and V is upstream hole pressure vessel volume, and ψ, γ are two produced in formulation process
Dimensionless number,
ψ and γ is tried to achieve by upstream and downstream Amplitude Ration α, the Phase delay θ measuring gained；Wherein, ψ, γ calculation such as formula is 2.
Shown in:
Wherein, α be upstream and downstream Amplitude Ration, θ be Phase delay,
According to Fischer research conclusion, upstream and downstream Amplitude Ration α, Phase delay θ can be expressed as the function of ψ, γ, for making function
Form is simple, and the functional expression containing ψ, γ is expressed as A, X by spyD、YD、A、XD、YDIt it is a process variable.
Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect the most according to claim 1, it is characterised in that:
In described step 1, the described Oil in Super-low Permeability rock chosen includes shale, tight sand；Described sample (9) is for being processed to diameter
5mm, the described cylinder experimental member of long 10mm.
Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect the most according to claim 1 and 2, its feature exists
In: described permeable backing plate (8) include upper permeable backing plate (81), under permeable backing plate (82), described permeable backing plate (81) is arranged at
Described sample (9) upper end, described under permeable backing plate (82) be arranged at described sample (9) lower end；State in rapid 3 described, it is ensured that institute
Stating sample (9) the most saturated, the saturated of described sample (9) can use hold-up or gas saturated.
Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect the most according to claim 3, it is characterised in that:
In described step 5, when data record and process, utilize the cross-correlation function in signal processing technology to analyze method and improve letter
Make an uproar ratio.
Oil in Super-low Permeability rock permeability measuring method under triaxial stress effect the most according to claim 4, it is characterised in that: fortune
The instrument internal pipe diameter of defeated pore media is less than 1mm, and the outside corresponding diameter of transport pipeline is more than or equal to 2mm.
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Cited By (13)
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| CN106769472A (en) * | 2017-01-11 | 2017-05-31 | 三峡大学 | Based on the vertical mechanical load Experiment on Function device of concrete and test method under axial dispersion and the effect of lateral confined pressure |
| CN107014730A (en) * | 2017-03-15 | 2017-08-04 | 中国矿业大学 | A kind of method for simulating true groundwater erosion Nuclear Waste Repository padded coaming |
| CN107300507A (en) * | 2017-07-20 | 2017-10-27 | 山东科技大学 | Three axle Seepage Experiment boxes and application method that can be axially loaded and dual-purpose axial no-load |
| CN107894383A (en) * | 2017-11-03 | 2018-04-10 | 青岛海洋地质研究所 | Permeability measuring apparatus containing hydrate sediment and its method under condition of triaxial stress |
| CN108663300A (en) * | 2018-05-07 | 2018-10-16 | 西安石油大学 | Hyposmosis tight sand experimental provision |
| CN109211757A (en) * | 2018-11-05 | 2019-01-15 | 长安大学 | A kind of In Rock Seepage Tests device and its test method |
| CN109239310A (en) * | 2018-09-06 | 2019-01-18 | 西安石油大学 | A kind of seepage force size and its measuring device and method that stratum effective stress is influenced |
| CN109253962A (en) * | 2018-10-30 | 2019-01-22 | 山东大学 | Rock three-axis force Penetration Signature tester and test method |
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| CN109580454A (en) * | 2019-01-05 | 2019-04-05 | 中国海洋石油集团有限公司 | A method of compact reservoir Fluid Sensitivity is tested with pressure oscillation method |
| CN113029792A (en) * | 2021-03-01 | 2021-06-25 | 中国地质大学（武汉） | Shale nanopore plugging experimental device and method based on nanoparticle fluid |
| CN113758814A (en) * | 2020-06-04 | 2021-12-07 | 中国石油天然气股份有限公司 | Rock modulus measuring system and method |
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| CN106769472B (en) * | 2017-01-11 | 2019-09-24 | 三峡大学 | Based on the vertical mechanical load Experiment on Function device of concrete and test method under axial dispersion and the effect of lateral confining pressure |
| CN106769472A (en) * | 2017-01-11 | 2017-05-31 | 三峡大学 | Based on the vertical mechanical load Experiment on Function device of concrete and test method under axial dispersion and the effect of lateral confined pressure |
| CN107014730B (en) * | 2017-03-15 | 2019-01-25 | 中国矿业大学 | A method of simulating true groundwater erosion Nuclear Waste Repository padded coaming |
| CN107014730A (en) * | 2017-03-15 | 2017-08-04 | 中国矿业大学 | A kind of method for simulating true groundwater erosion Nuclear Waste Repository padded coaming |
| CN107300507A (en) * | 2017-07-20 | 2017-10-27 | 山东科技大学 | Three axle Seepage Experiment boxes and application method that can be axially loaded and dual-purpose axial no-load |
| CN107300507B (en) * | 2017-07-20 | 2020-05-05 | 山东科技大学 | Axial-loading and axial-unloading dual-purpose triaxial seepage experiment box and using method |
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