CN106245216A - A kind of production method of Herba Pileae Scriptae fiber raschel blanket - Google Patents

A kind of production method of Herba Pileae Scriptae fiber raschel blanket Download PDF

Info

Publication number
CN106245216A
CN106245216A CN201610683941.9A CN201610683941A CN106245216A CN 106245216 A CN106245216 A CN 106245216A CN 201610683941 A CN201610683941 A CN 201610683941A CN 106245216 A CN106245216 A CN 106245216A
Authority
CN
China
Prior art keywords
herba pileae
pileae scriptae
raschel blanket
fiber raschel
scriptae fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610683941.9A
Other languages
Chinese (zh)
Other versions
CN106245216B (en
Inventor
郑其明
刘荣道
吴明贤
厉巽巽
陈玉霜
毛森贤
毛青山
陈金霞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Truelove Blanket Industry Technology Co Ltd
Original Assignee
Zhejiang Truelove Blanket Industry Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang Truelove Blanket Industry Technology Co Ltd filed Critical Zhejiang Truelove Blanket Industry Technology Co Ltd
Priority to CN201610683941.9A priority Critical patent/CN106245216B/en
Publication of CN106245216A publication Critical patent/CN106245216A/en
Application granted granted Critical
Publication of CN106245216B publication Critical patent/CN106245216B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04B—KNITTING
    • D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
    • D04B21/02—Pile fabrics or articles having similar surface features
    • D04B21/04—Pile fabrics or articles having similar surface features characterised by thread material
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B21/00—Successive treatments of textile materials by liquids, gases or vapours
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B9/00—Solvent-treatment of textile materials
    • D06B9/04—Successively applying two or more different solvent-based treating materials
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C27/00—Compound processes or apparatus, for finishing or dressing textile fabrics, not otherwise provided for
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
    • D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
    • D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic System
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/82—Textiles which contain different kinds of fibres
    • D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
    • D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
    • D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/82—Textiles which contain different kinds of fibres
    • D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
    • D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
    • D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
    • D06P3/8233—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye using dispersed dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02—After-treatment
    • D06P5/04—After-treatment with organic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02—After-treatment
    • D06P5/04—After-treatment with organic compounds
    • D06P5/08—After-treatment with organic compounds macromolecular
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02—After-treatment
    • D06P5/10—After-treatment with compounds containing metal
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

Abstract

The present invention relates to woollen blanket preparation field, disclose the production method of a kind of Herba Pileae Scriptae fiber raschel blanket, including: 1), weaving: to plush yarn and wire gauze successively warping, weave, cut open floss, prepare Herba Pileae Scriptae fiber raschel blanket semi-finished product；2), prefinishing: by fabric sizing, bristle, hot light, clot；3), dyeing and finishing: by textile dyeing, then to its reduction cleaning, be then passed through acetum and neutralize, wash out cylinder, drying, steaming and color fixing, flexible smooth process, the most again dry；4), Final finishing: fabric drying sizing, front hot light, front bristle, front are scalded cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching；5), product inspection, packaging warehouse-in.The Herba Pileae Scriptae fiber raschel blanket fine hair of the present invention is submissive, stand upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, good permeability, and has the feature of antibiotic health care, environmental protection.

Description

A kind of production method of Herba Pileae Scriptae fiber raschel blanket
Technical field
The present invention relates to woollen blanket preparation field, particularly relate to the production method of a kind of Herba Pileae Scriptae fiber raschel blanket.
Background technology
Along with the raising of people's material and culture level, the requirement of textile is also being improved, is not requiring nothing more than warming, beautiful by people See, and more focus on comfortableness and functional.Functional textile becomes one of following developing trend of textile industry, will be with Fine count fiber textile, non-woven fabrics, composite, ep-type material etc. collectively form the big tendency of following textile.Section now The exploitation developing into functional textile of skill provides guarantee, the most also for textile enterprise's development and product restructuring, rises To bigger facilitation the added value that improves textile.Study and produce the ecological and healthy function that is beneficial to man Property textile product, have become as the world today development trend.
In general, the functionalization of textile is mainly realized by two approach: one is the functional treatment by fabric Realizing, this is also the main path of current functional textile exploitation；Two is the functionalization of textile fabric.Along with science and technology Development and the gradually enhancing of people's environmental protection consciousness, the limitation of fabric functional Final finishing processing method is increasingly subject to people Concern, do not only exist the durability of function, the comfortableness of use and safety by the method functional product of obtaining of processing Defect in terms of property, and inevitable to environment in arranging the course of processing.Merit is processed by functional fiber Energy property textile then can overcome many drawbacks of fabric functional Final finishing, is the development trend obtaining functional textile.
Hosiery industry, under the leading of new and high technology, is actively adjusted the product mix, and payes attention to new raw material and the exploitation of new product, Particularly fibre in differentiation and the exploitation of functional fiber kind, greatly promote the development of hosiery industry.At Rachael blanket Field, along with exploitation and utilization and the progress of technology of novel material, the most constantly widens its product scope.Except conventional Outside Rachael blanket, develop high in technological content Rachael blanket and become an important developing direction.The each big authority in the world spins The research of loom structure shows, the development trend in textile product field is to pursue comfortableization and multifunction.
Present consumer does not require nothing more than Rachael blanket and has warmth retention property, has that matte is plentiful, soft comfortable, plain height Expensive, slim and graceful feel style and fabric good permeability, moisture absorption and desorption property are good, and have antibiotic health care, green ring to woollen blanket The multifunctionalities such as guarantor have had demand.But on market, Rachael blanket, typically based on acrylon and terylene woollen blanket, also has at home Least a portion of cotton and Pilus Caprae seu Ovis Rachael blanket, quality scale is relatively low or expensive, it is impossible to meets the market demand, therefore develops Disclosure satisfy that the Rachael blanket of consumer demand becomes a kind of trend.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides the production method of a kind of Herba Pileae Scriptae fiber raschel blanket. The Herba Pileae Scriptae fiber raschel blanket of the present invention has that fine hair is submissive, stands upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, thoroughly The advantage that gas is good, additionally has the feature such as antibiotic health care, environmental protection.
The concrete technical scheme of the present invention is: the production method of a kind of Herba Pileae Scriptae fiber raschel blanket, fine with Herba Pileae Scriptae Dimension long filament, as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product.
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot.
3), dyeing and finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, Then with reduction cleaning liquid, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing are carried out reduction cleaning, after reduction cleaning first Neutralize by peracetic acid solution, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing, use flexible smooth agent fine to Herba Pileae Scriptae Dimension Rachael blanket semi-finished product carry out flexible smooth process, the most again dry.
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing carry out drying and shaping successively, front is scalded Light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front boiling hot are cut, the back side Scald cut, cutting sew up, obtain Herba Pileae Scriptae fiber raschel blanket finished product.
5), product inspection, packaging warehouse-in.
The inventive method is according to the feature of Herba Pileae Scriptae fiber filament, in conjunction with the performance of HDR5DPLM30 raschel machine, Design the upper machine tissue meeting its characteristic.Prefinishing technique is formulated according to Herba Pileae Scriptae fiber filament performance；White to cut open after floss Grey cloth first carries out pre-setting and hot light and processes, and makes the carpet surface fine hair crimpness before dyeing reduce, pieces dissipate pine be conducive to dyeing, soft Supple-settlement and Final finishing processing.
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: pass through after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Melt spinning machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for Herba Pileae Scriptae fiber filament The 8-12% of gross mass.
The present invention selects Herba Pileae Scriptae fiber to be natural material as Rachael blanket plush yarn, Herba Pileae Scriptae, has antibacterial disappearing Scorching, effect of reducing swelling and alleviating pain, harmless, good to the affinity of skin.The present invention using use Herba Pileae Scriptae fiber as raw material, This fiber is a kind of novel plants antimicrobial fiber.By organizational structure reasonable in design for this raw material, ingenious combination chaining, latitude substrate Cloth raw material, by the research and development to key technologies such as warp knit weaving, prefinishing, printing and dyeing and Final finishing productions, thus improves The quality of product and added value, make woollen blanket on the basis of holding is soft, fine and smooth, smooth, more have antibiotic health care, breathe freely and feel nice and cool Feature.Product in use, along with the continuous CONTACT WITH FRICTION of human body skin Yu fiber, by the effective component in Herba Pileae Scriptae not Disconnected release from fiber, and absorbed by human body, the successful development of this project meets the needs of Green Textiles, i.e. ensure that The characteristic of the comfortable softness of Rachael blanket, more outstanding natural, green, healthy concept.
As preferably, tricot machine described in step 1) is HDR5DPLM30 type raschel machine, and braiding speed is 420r/ Min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses through flat Braiding, form of entrying is for completely to wear；Wherein, the specification of described Herba Pileae Scriptae fiber filament is 150D/72F, the specification of polyester drawn yarns For 150D/36F.
As preferably, step 2) sizing time, Herba Pileae Scriptae fiber raschel blanket semi-finished product are at room temperature immersed treatment fluid In, treatment fluid to 50 DEG C, is then incubated 45min, after being cooled to room temperature with the speed of 3 DEG C/min with the ramp of 2 DEG C/min Herba Pileae Scriptae fiber raschel blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
As preferably, before carrying out dyeing and finishing, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are carried out pre-place Reason: Herba Pileae Scriptae fiber raschel blanket semi-finished product submergence is carried out impregnation process, wherein Herba Pileae Scriptae fiber raschel in ethanol Woollen blanket semi-finished product are 1:(2-4 with the mass ratio of ethanol), dip time is 20-40min.
Owing to fiber surface has one layer of oil film, therefore when dyeing, due to the obstruct of oil film, dyestuff not easily penetrate into into Fibrous inside, causes Color poor.And before dyeing, fabric is carried out in ethanol impregnation process, it is possible to dissolve part oil Film so that it is lower thickness, it is simple to dyestuff penetration enters fibrous inside, increases color fastness.However it is necessary that control dip time and second Alcohol consumption, it is to avoid oil film excessive dissolution and cause fibre-fibre friction, finally affect glossiness and the smoothness of fiber surface.
As preferably, when step 3) dyes, high-temperature and high pressure dyeing process is selected to dye: to prepare dying easily at normal temperatures Liquid, the pH of described dye liquor controls at 5.6-6.8；Then Herba Pileae Scriptae fiber raschel blanket semi-finished product are immersed in dye liquor, grass Corallium Japonicum Kishinouye fiber raschel blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first will dye Liquid is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then with the speed of 1 DEG C/min, dye liquor is warming up to 125-135 DEG C, finally solid Color 60min；Dye wherein uses during dark product Palanilp nonionic dye；Mibct is used during dye light-coloured prods Keton polyester dispersion dyestuff.
In the present invention, according to Herba Pileae Scriptae fiber morphosis, aggregated structure, physical and mechanical properties, to chemical drugs The performances such as the sensitivity of agent, fibrillation formulate suitable dyeing and finishing technology.Herba Pileae Scriptae fiber is a kind of polyester-based fibers, and molten point is relatively Low, non-refractory, especially sensitive to alkali, it is easy to hydrolysis damage；In acid bath, fiber also can occur significantly to hydrolyze damage Wound, in order to ensure affinity, dye-uptake, dyeing speed and the level-dyeing property of Herba Pileae Scriptae fiber La Er woollen blanket, has selected low temperature, nothing Alkali, the Colour Difference condition of low acid；In dye during dark color, select PalanilP nonionic dye；During dye light-coloured prods, select Mibct keton polyester dispersion dyestuff, is dyeed by SYC-300 high-temperature pressure dyeing, it is possible to reduce environmental pollution.
As preferably, reduction cleaning liquid described in step 3) includes the synthesis detergent of 1.5-2.5g/L, 1.0-1.5g/L Tea saponin, the sodium alginate of 10-15g/L Sargassum powder and 1.0-2.0g/L and water, bath raio 1:25, temperature 50-55 DEG C, clean Time 25-35min；During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, 5- The tea polyphenols of 10g/L and the nano titanium oxide of 0.3-0.5g/L；After reduction cleaning, the concentration of acetum used is 0.5wt%； When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes lecithin, puts down Lubrication prescription, tween 80 and water, the weight of wherein said lecithin is the 2.5-3% of water weight, and the weight of smooth agent is the 1.5-of water weight 2%, the weight of tween is the 0.5-1% of water weight.
In the present invention, owing to Herba Pileae Scriptae fiber is the most alkaline-resisting, low-temperature neutral bath time at softness, is used to process, in reduction cleaning During soft treatment, after cleanout fluid cleans, softness is smooth, gloss is beautiful to make Herba Pileae Scriptae fiber raschel blanket have, also Adding Sargassum powder in former cleanout fluid is to make it form a tunic to protect woollen blanket at carpeted surface, having anti-oxidation merit Energy；Tea saponin is a kind of nonionic surfactant, therefore, it is possible to use as abluent, tea saponin is clear with common simultaneously Lotion is compared, and has preferable stability, it is possible to give full play to the surface activity of himself in the water environment of various hardness.This Outer tea saponin also has certain color fixative blast, increases the effect of color fastness, when after Woollen blanket printing fixation fiber, it is possible to promote Its outward appearance vividness.Na is added when dye is dark3CO3And sodium hydrosulfite, more effectively remove the loose colour of fiber surface；Add tea polyphenols With nano titanium oxide, then it is to improve the anti-oxidation function of woollen blanket and anti-microbial property.
Lecithin is oily matter, has good lubricant effect, it is possible to absorbed by fiber, thus promotes the toughness of fiber And feel so that the fine hair of woollen blanket has good anti-pressure ability.In addition lecithin is harmless to health, for green material.Tell Temperature has good emulsification, also is able to increase the dissolubility of lecithin simultaneously.
As preferably, described lecithin is through modification: mixed with the lactic acid solution that concentration is 50-60wt% by lecithin Closing the stirring of uniform post-heating, wherein said lecithin is 100:(4-6 with the mass ratio of lactic acid solution), heating-up temperature is 70-80 DEG C, heat time heating time 40-60min；Being gradually added into quality to reactant liquor during heated and stirred is described lecithin 20-25% Concentration is the hydrogen peroxide solution of 30wt%；To reactant liquor dropping sodium hydroxide solution to neutral, the most very after heated and stirred terminates Empty dried prepared hydroxylating modified lecithin.
The mobility of common lecithin is poor, and viscosity is higher, is unfavorable for being absorbed by fiber and in fiber surface film forming, The mobility of modified lecithin is therefore greatly increased, and is easier to be absorbed and in fiber surface film forming by fiber.
As preferably, in step 4) Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110-120 DEG C, speed 17-20m/min of shaping；Bristle uses the double roller brushing machine of MB211E type, speed 3- 4m/min, enters machine along hair, and bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130 DEG C, speed 7-10m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, enters Herba Pileae Scriptae fiber raschel blanket front Row scalds to be cut, temperature 120-130 DEG C, speed 8-10m/min；Fluffing uses ME331E raising machine, to Herba Pileae Scriptae fiber raschel hair Blanket reverse side fluffs, speed 8-10m/min.
As preferably, the preparation method of described Herba Pileae Scriptae functional agglomerate is as follows: takes bamboo powder and adds to its 8-12 times of quality The sodium hydroxide solution that concentration is 8-12wt% in, after being uniformly dispersed, heating under reduced pressure to 110-130 DEG C, insulation discongest 6-8h； It is filtrated to get bamboo powder after discongesting, then bamboo powder is added to the ethanol solution that concentration is 70-80wt% of its 8-12 times of quality, add Heat is incubated 3-5h after 80-90 DEG C, again filters, adds water insoluble matter and pull an oar, and making beating to slurry beating degree is 14- 16 ° of SR, then carry out defibrination, and defibrination is 18-22 ° of SR to slurry beating degree, wash and obtain after distillation of reducing pressure after making beating Cellulose；Cellulose is added to the ionic liquid of its 18-22 times of quality, obtains cellulose solution；By cellulose solution- Freeze 1-2 days in a low temperature of 18 DEG C to-22 DEG C, then take out frost thing, thaw with flowing water, prepare cellulose aquagel, then use Dehydrated alcohol carries out solvent displacement, after being then passed through vacuum drying and grinding, prepares cellulose aerogels granule；By cellulose gas Gel particle impregnated in and carries out saturated absorption in Herba Pileae Scriptae extracting solution, takes out after absorption；The fibre of Herba Pileae Scriptae extracting solution will be adsorbed with Dimension element aerogel particle, acrylic acid, Polyethylene Glycol, Ammonium persulfate. and water 1-3:1:1:0.02:15-25 in mass ratio mixing, stir Mix uniform post-heating to 50-60 DEG C, insulated and stirred reaction 4-6h, it is cooled to room temperature after reaction, obtains viscous liquid, through overdrying Dry and grind after, prepare Herba Pileae Scriptae functional agglomerate.
Common Herba Pileae Scriptae fiber be by spinning after fiber impregnation process in Herba Pileae Scriptae extracting solution, thus prepare grass coral Coral fiber, but the Herba Pileae Scriptae fiber prepared in this way can gradually drop after repeatedly washing.The Herba Pileae Scriptae of the present invention Fiber is that Herba Pileae Scriptae functional agglomerate and polyester slice are together carried out melt spinning.Wherein, the preparation of Herba Pileae Scriptae functional agglomerate Cheng Zhong, first prepares cellulose, and cellulolytic activity prepared by the inventive method is high, easily cross-links.Cellulose is made cellulose gas After gel particle, Herba Pileae Scriptae extracting solution is carried out dipping absorption, anti-with acrylic acid, Polyethylene Glycol, Ammonium persulfate. and water the most again Herba Pileae Scriptae functional agglomerate should be prepared.This Herba Pileae Scriptae functional agglomerate, as carrier, has good adsorptivity to Herba Pileae Scriptae extracting solution And slow-release function.Additionally, due to the cellulose aerogels containing bigger serface in this Herba Pileae Scriptae functional agglomerate, also there is suction Moisture releasing performance, the advantage of good permeability.
As preferably, the preparation method of described Herba Pileae Scriptae extracting solution is: takes clean Herba Pileae Scriptae leaf and pulls an oar it, Prepare Herba Pileae Scriptae serosity, described Herba Pileae Scriptae serosity is joined in the ethanol solution that concentration is 70-80wt% and carries out Microwave-assisted Extraction Take, filter after extraction and prepare Herba Pileae Scriptae extracting solution, wherein Herba Pileae Scriptae serosity and the mass ratio 1:(12-16 of ethanol solution), microwave Extract power 650-750W, extraction time 3-5min, Extracting temperature 65-75 DEG C.
It is compared with the prior art, the invention has the beneficial effects as follows: the Herba Pileae Scriptae fiber raschel blanket of the present invention has floss Hair color pool is good, submissive, stand upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, the advantage of good permeability and antibiotic health care, green The feature that colour circle is protected.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
The production method of a kind of Herba Pileae Scriptae fiber raschel blanket, using Herba Pileae Scriptae fiber filament as plush yarn raw material, with terylene Drafting silk, as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, braiding speed be 420r/min, L1 with L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, entrys Form is for completely to wear；Wherein, the specification of described Herba Pileae Scriptae fiber filament is 150D/72F, and the specification of polyester drawn yarns is 150D/ 36F。
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot.Fixed During type, at room temperature being immersed in treatment fluid by Herba Pileae Scriptae fiber raschel blanket semi-finished product, treatment fluid is with the speed liter of 2 DEG C/min Temperature, to 50 DEG C, is then incubated 45min, is become by Herba Pileae Scriptae fiber raschel blanket half after being cooled to room temperature with the speed of 3 DEG C/min Product take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, Then with reduction cleaning liquid, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing are carried out reduction cleaning, after reduction cleaning first Neutralize by peracetic acid solution, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing, use flexible smooth agent fine to Herba Pileae Scriptae Dimension Rachael blanket semi-finished product carry out flexible smooth process, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dye liquor at normal temperatures, the pH control of described dye liquor System is about 6.2；Then Herba Pileae Scriptae fiber raschel blanket semi-finished product are immersed in dye liquor, Herba Pileae Scriptae fiber raschel blanket Semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with the speed of 1.5 DEG C/min It is warming up to 90 DEG C, then dye liquor is warming up to 130 DEG C with the speed of 1 DEG C/min, last fixation 60min；Wherein dark product in dye Palanilp nonionic dye is used during product；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid include 2g/L synthesis detergent, the tea saponin of 1.25g/L, 12.5g/L Sargassum powder with The sodium alginate of 1.5g/L and water, bath raio 1:25, temperature 52 DEG C, scavenging period 30min；During the dark product of dye, described reduction is clear Washing liquid also includes the sodium carbonate of 1.5g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 7.5g/L and the nano titanium oxide of 0.4g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes ovum Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the 2.75% of water weight, and the weight of smooth agent is water weight 1.75%, the weight of tween is the 0.75% of water weight.
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing carry out drying and shaping successively, front is scalded Light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front boiling hot are cut, the back side Scald cut, cutting sew up, obtain Herba Pileae Scriptae fiber raschel blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse Mao Jinji, patent door width 158-162cm, temperature 115 DEG C, speed 18m/min of shaping；Bristle uses the double roller bristle of MB211E type Machine, speed 3.5m/min, enter machine along hair, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature Spend 125 DEG C, speed 8m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, to Herba Pileae Scriptae fiber raschel blanket front Carry out scalding and cut, temperature 125 DEG C, speed 9m/min；Fluffing uses ME331E raising machine, to Herba Pileae Scriptae fiber raschel blanket reverse side Fluff, speed 9m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: pass through after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Melt spinning machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for Herba Pileae Scriptae fiber filament The 10% of gross mass.
Embodiment 2
The production method of a kind of Herba Pileae Scriptae fiber raschel blanket, using Herba Pileae Scriptae fiber filament as plush yarn raw material, with terylene Drafting silk, as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, braiding speed be 420r/min, L1 with L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, entrys Form is for completely to wear；Wherein, the specification of described Herba Pileae Scriptae fiber filament is 150D/72F, and the specification of polyester drawn yarns is 150D/ 36F。
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot.Fixed During type, at room temperature being immersed in treatment fluid by Herba Pileae Scriptae fiber raschel blanket semi-finished product, treatment fluid is with the speed liter of 2 DEG C/min Temperature, to 50 DEG C, is then incubated 45min, is become by Herba Pileae Scriptae fiber raschel blanket half after being cooled to room temperature with the speed of 3 DEG C/min Product take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are carried out pre-place Reason: Herba Pileae Scriptae fiber raschel blanket semi-finished product submergence is carried out impregnation process, wherein Herba Pileae Scriptae fiber raschel in ethanol Woollen blanket semi-finished product are 1:3 with the mass ratio of ethanol, and dip time is 30min.
Pretreated Herba Pileae Scriptae fiber raschel blanket semi-finished product are positioned in dyeing liquor and dye, then with also Former cleanout fluid carries out reduction cleaning to the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing, successively through vinegar after reduction cleaning Acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, uses flexible smooth agent to Herba Pileae Scriptae fiber raschel after steaming and color fixing Woollen blanket semi-finished product carry out flexible smooth process, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dye liquor at normal temperatures, the pH control of described dye liquor System is 6.8；Then being immersed in dye liquor by Herba Pileae Scriptae fiber raschel blanket semi-finished product, Herba Pileae Scriptae fiber raschel blanket half becomes Product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first heated up with the speed of 1.5 DEG C/min by dye liquor To 90 DEG C, then dye liquor is warming up to 130 DEG C with the speed of 1 DEG C/min, last fixation 60min；Wherein in dye during dark product Use Palanilp nonionic dye；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid include 2g/L synthesis detergent, the tea saponin of 1.25g/L, 12.5g/L Sargassum powder with The sodium alginate of 1.5g/L and water, bath raio 1:25, temperature 52 DEG C, scavenging period 30min；During the dark product of dye, described reduction is clear Washing liquid also includes the sodium carbonate of 1.5g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 7.5g/L and the nano titanium oxide of 0.4g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes ovum Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the 2.8% of water weight, and the weight of smooth agent is water weight 1.8%, the weight of tween is the 0.7% of water weight.
Wherein said lecithin is through modification: after being mixed homogeneously with the lactic acid solution that concentration is 55wt% by lecithin Heated and stirred, wherein said lecithin is 100:5 with the mass ratio of lactic acid solution, and heating-up temperature is 75 DEG C, heat time heating time 50min；Being gradually added into, to reactant liquor, the concentration that quality is described lecithin 22.5% during heated and stirred is the double of 30wt% Oxygen aqueous solution；To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxyl Base modified lecithin.
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing carry out drying and shaping successively, front is scalded Light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front boiling hot are cut, the back side Scald cut, cutting sew up, obtain Herba Pileae Scriptae fiber raschel blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse Mao Jinji, patent door width 158-162cm, temperature 115 DEG C, speed 19m/min of shaping；Bristle uses the double roller bristle of MB211E type Machine, speed 3.5m/min, enter machine along hair, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature Spend 125 DEG C, speed 8m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, to Herba Pileae Scriptae fiber raschel blanket front Carry out scalding and cut, temperature 125 DEG C, speed 9m/min；Fluffing uses ME331E raising machine, to Herba Pileae Scriptae fiber raschel blanket reverse side Fluff, speed 9m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: pass through after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Melt spinning machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for Herba Pileae Scriptae fiber filament The 8% of gross mass.
In the present embodiment, the preparation method of described Herba Pileae Scriptae functional agglomerate is as follows: takes bamboo powder and adds to its 8 times of quality The sodium hydroxide solution that concentration is 8wt% in, after being uniformly dispersed, heating under reduced pressure to 110 DEG C, insulation discongest 8h；Filter after discongesting Obtain bamboo powder, then bamboo powder added to the ethanol solution that concentration is 70wt% of its 8 times of quality, after being heated to 80 DEG C, be incubated 5h, Again filtering, add water insoluble matter and pull an oar, making beating is 14 ° of SR to slurry beating degree, then carries out defibrination, and defibrination is extremely Slurry beating degree is 18 ° of SR, washes and obtain cellulose after distillation of reducing pressure after making beating；Cellulose is added to its 18 times of matter In the ionic liquid of amount, obtain cellulose solution；Cellulose solution is freezed 2 days in a low temperature of-18 DEG C, then takes out frost Thing, thaws with flowing water, prepares cellulose aquagel, then carries out solvent displacement with dehydrated alcohol, is then passed through vacuum drying and grinds After mill, prepare cellulose aerogels granule；Cellulose aerogels granule be impregnated in Herba Pileae Scriptae extracting solution and carries out saturated absorption, Take out after absorption；By be adsorbed with the cellulose aerogels granule of Herba Pileae Scriptae extracting solution, acrylic acid, Polyethylene Glycol, Ammonium persulfate. and Water 2:1:1:0.02:20 in mass ratio mixes, and the post-heating that stirs is to 55 DEG C, and insulated and stirred reacts 5h, is cooled to after reaction Room temperature, obtains viscous liquid, after being dried and grinding, prepares Herba Pileae Scriptae functional agglomerate.
Wherein, the preparation method of described Herba Pileae Scriptae extracting solution is: takes clean Herba Pileae Scriptae leaf and pulls an oar it, prepares Herba Pileae Scriptae serosity, joins described Herba Pileae Scriptae serosity in the ethanol solution that concentration is 75wt% and carries out microwave radiation exaraction, extracts Rear filtration prepares Herba Pileae Scriptae extracting solution, wherein Herba Pileae Scriptae serosity and mass ratio 1:14, the microwave extraction power 700W of ethanol solution, Extraction time 4min, Extracting temperature 70 DEG C.
Embodiment 3
The production method of a kind of Herba Pileae Scriptae fiber raschel blanket, using Herba Pileae Scriptae fiber filament as plush yarn raw material, with terylene Drafting silk, as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, braiding speed be 420r/min, L1 with L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, entrys Form is for completely to wear；Wherein, the specification of described Herba Pileae Scriptae fiber filament is 150D/72F, and the specification of polyester drawn yarns is 150D/ 36F。
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot.Fixed During type, at room temperature being immersed in treatment fluid by Herba Pileae Scriptae fiber raschel blanket semi-finished product, treatment fluid is with the speed liter of 2 DEG C/min Temperature, to 50 DEG C, is then incubated 45min, is become by Herba Pileae Scriptae fiber raschel blanket half after being cooled to room temperature with the speed of 3 DEG C/min Product take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are carried out pre-place Reason: Herba Pileae Scriptae fiber raschel blanket semi-finished product submergence is carried out impregnation process, wherein Herba Pileae Scriptae fiber raschel in ethanol Woollen blanket semi-finished product are 1:2 with the mass ratio of ethanol, and dip time is 40min.
Pretreated Herba Pileae Scriptae fiber raschel blanket semi-finished product are positioned in dyeing liquor and dye, then with also Former cleanout fluid carries out reduction cleaning to the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing, successively through vinegar after reduction cleaning Acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, uses flexible smooth agent to Herba Pileae Scriptae fiber raschel after steaming and color fixing Woollen blanket semi-finished product carry out flexible smooth process, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dye liquor at normal temperatures, the pH control of described dye liquor System is about 5.6；Then Herba Pileae Scriptae fiber raschel blanket semi-finished product are immersed in dye liquor, Herba Pileae Scriptae fiber raschel blanket Semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with the speed of 1.5 DEG C/min It is warming up to 90 DEG C, then dye liquor is warming up to 125 DEG C with the speed of 1 DEG C/min, last fixation 60min；Wherein dark product in dye Palanilp nonionic dye is used during product；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid include 1.5g/L synthesis detergent, the tea saponin of 1.0g/L, 10g/L Sargassum powder with The sodium alginate of 1.0g/L and water, bath raio 1:25, temperature 50 C, scavenging period 35min；During the dark product of dye, described reduction is clear Washing liquid also includes the sodium carbonate of 1g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5g/L and the nano titanium oxide of 0.3g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes ovum Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the 2.5% of water weight, and the weight of smooth agent is water weight 1.5%, the weight of tween is the 0.5% of water weight.
Wherein said lecithin is through modification: after being mixed homogeneously with the lactic acid solution that concentration is 50wt% by lecithin Heated and stirred, wherein said lecithin is 100:4 with the mass ratio of lactic acid solution, and heating-up temperature is 70 DEG C, heat time heating time 60min；It is gradually added into, to reactant liquor, the dioxygen that concentration is 30wt% that quality is described lecithin 20% during heated and stirred Aqueous solution；To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxyl Change modified lecithin.
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing carry out drying and shaping successively, front is scalded Light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front boiling hot are cut, the back side Scald cut, cutting sew up, obtain Herba Pileae Scriptae fiber raschel blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse Mao Jinji, patent door width 158-162cm, temperature 110 DEG C, speed 17m/min of shaping；Bristle uses the double roller bristle of MB211E type Machine, speed 3m/min, enter machine along hair, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120 DEG C, speed 7m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, enters Herba Pileae Scriptae fiber raschel blanket front Row scalds to be cut, temperature 120 DEG C, speed 8m/min；Fluffing uses ME331E raising machine, enters Herba Pileae Scriptae fiber raschel blanket reverse side Row fluffing, speed 8m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: pass through after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Melt spinning machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for Herba Pileae Scriptae fiber filament The 12% of gross mass.
In the present embodiment, the preparation method of described Herba Pileae Scriptae functional agglomerate is as follows: takes bamboo powder and adds to its 12 times of matter In the sodium hydroxide solution that concentration is 12wt% of amount, after being uniformly dispersed, heating under reduced pressure to 130 DEG C, 6h is discongested in insulation；After discongesting It is filtrated to get bamboo powder, then bamboo powder is added to the ethanol solution that concentration is 80wt% of its 12 times of quality, protect after being heated to 90 DEG C Temperature 3h, again filters, adds water insoluble matter and pull an oar, and making beating is 16 ° of SR to slurry beating degree, then carries out defibrination, Defibrination to slurry beating degree is 22 ° of SR, washes and obtain cellulose after distillation of reducing pressure after making beating；Cellulose is added to it In the ionic liquid of 22 times of quality, obtain cellulose solution；Cellulose solution is freezed 1 day in a low temperature of-22 DEG C, then takes Go out to freeze thing, thaw with flowing water, prepare cellulose aquagel, then carry out solvent displacement with dehydrated alcohol, be then passed through vacuum and do Dry and grind after, prepare cellulose aerogels granule；Cellulose aerogels granule be impregnated in Herba Pileae Scriptae extracting solution and satisfy And absorption, take out after absorption；The cellulose aerogels granule of Herba Pileae Scriptae extracting solution, acrylic acid, Polyethylene Glycol, over cure will be adsorbed with Acid ammonium and water 3:1:1:0.02:25 in mass ratio mixing, the post-heating that stirs is to 60 DEG C, and insulated and stirred reaction 4h, after reaction It is cooled to room temperature, obtains viscous liquid, after being dried and grinding, prepare Herba Pileae Scriptae functional agglomerate.
Wherein, the preparation method of described Herba Pileae Scriptae extracting solution is: takes clean Herba Pileae Scriptae leaf and pulls an oar it, prepares Herba Pileae Scriptae serosity, joins described Herba Pileae Scriptae serosity in the ethanol solution that concentration is 80wt% and carries out microwave radiation exaraction, extracts Rear filtration prepares Herba Pileae Scriptae extracting solution, wherein Herba Pileae Scriptae serosity and mass ratio 1:16, the microwave extraction power 750W of ethanol solution, Extraction time 3min, Extracting temperature 75 DEG C.
Embodiment 4
The production method of a kind of Herba Pileae Scriptae fiber raschel blanket, using Herba Pileae Scriptae fiber filament as plush yarn raw material, with terylene Drafting silk, as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, braiding speed be 420r/min, L1 with L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, entrys Form is for completely to wear；Wherein, the specification of described Herba Pileae Scriptae fiber filament is 150D/72F, and the specification of polyester drawn yarns is 150D/ 36F。
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot.Fixed During type, at room temperature being immersed in treatment fluid by Herba Pileae Scriptae fiber raschel blanket semi-finished product, treatment fluid is with the speed liter of 2 DEG C/min Temperature, to 50 DEG C, is then incubated 45min, is become by Herba Pileae Scriptae fiber raschel blanket half after being cooled to room temperature with the speed of 3 DEG C/min Product take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are carried out pre-place Reason: Herba Pileae Scriptae fiber raschel blanket semi-finished product submergence is carried out impregnation process, wherein Herba Pileae Scriptae fiber raschel in ethanol Woollen blanket semi-finished product are 1:4 with the mass ratio of ethanol, and dip time is 20min.
Pretreated Herba Pileae Scriptae fiber raschel blanket semi-finished product are positioned in dyeing liquor and dye, then with also Former cleanout fluid carries out reduction cleaning to the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing, successively through vinegar after reduction cleaning Acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, uses flexible smooth agent to Herba Pileae Scriptae fiber raschel after steaming and color fixing Woollen blanket semi-finished product carry out flexible smooth process, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dye liquor at normal temperatures, the pH control of described dye liquor System is about 6；Then Herba Pileae Scriptae fiber raschel blanket semi-finished product are immersed in dye liquor, Herba Pileae Scriptae fiber raschel blanket half Finished product is 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with the speed liter of 1.5 DEG C/min Dye liquor, to 90 DEG C, is then warming up to 135 DEG C with the speed of 1 DEG C/min, last fixation 60min by temperature；Wherein dark product in dye Time use Palanilp nonionic dye；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid include 2.5g/L synthesis detergent, the tea saponin of 1.5g/L, 15g/L Sargassum powder with The sodium alginate of 2.0g/L and water, bath raio 1:25, temperature 55 DEG C, scavenging period 25-35min；During the dark product of dye, described reduction Cleanout fluid also includes the sodium carbonate of 2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 10g/L and the nano titanium oxide of 0.5g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes ovum Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the 3% of water weight, and the weight of smooth agent is water weight 2%, the weight of tween is the 1% of water weight.
Wherein said lecithin is through modification: after being mixed homogeneously with the lactic acid solution that concentration is 60wt% by lecithin Heated and stirred, wherein said lecithin is 100:6 with the mass ratio of lactic acid solution, and heating-up temperature is 80 DEG C, heat time heating time 60min；It is gradually added into, to reactant liquor, the dioxygen that concentration is 30wt% that quality is described lecithin 25% during heated and stirred Aqueous solution；To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxyl Change modified lecithin.
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing carry out drying and shaping successively, front is scalded Light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front boiling hot are cut, the back side Scald cut, cutting sew up, obtain Herba Pileae Scriptae fiber raschel blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse Mao Jinji, patent door width 158-162cm, temperature 120 DEG C, speed 20m/min of shaping；Bristle uses the double roller bristle of MB211E type Machine, speed 4m/min, enter machine along hair, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 130 DEG C, speed 10m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, enters Herba Pileae Scriptae fiber raschel blanket front Row scalds to be cut, temperature 130 DEG C, speed 10m/min；Fluffing uses ME331E raising machine, to Herba Pileae Scriptae fiber raschel blanket reverse side Fluff, speed 10m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: pass through after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Melt spinning machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for Herba Pileae Scriptae fiber filament The 9% of gross mass.
In the present embodiment, the preparation method of described Herba Pileae Scriptae functional agglomerate is as follows: takes bamboo powder and adds to its 10 times of matter In the sodium hydroxide solution that concentration is 10wt% of amount, after being uniformly dispersed, heating under reduced pressure to 120 DEG C, 7h is discongested in insulation；After discongesting It is filtrated to get bamboo powder, then bamboo powder is added to the ethanol solution that concentration is 75wt% of its 10 times of quality, protect after being heated to 85 DEG C Temperature 4h, again filters, adds water insoluble matter and pull an oar, and making beating is 15 ° of SR to slurry beating degree, then carries out defibrination, Defibrination to slurry beating degree is 20 ° of SR, washes and obtain cellulose after distillation of reducing pressure after making beating；Cellulose is added to it In the ionic liquid of 20 times of quality, obtain cellulose solution；Cellulose solution is freezed in a low temperature of-20 DEG C 1.5 days, then Take out frost thing, thaw with flowing water, prepare cellulose aquagel, then carry out solvent displacement with dehydrated alcohol, be then passed through vacuum After being dried and grinding, prepare cellulose aerogels granule；Cellulose aerogels granule be impregnated in Herba Pileae Scriptae extracting solution and carry out Saturated absorption, takes out after absorption；The cellulose aerogels granule of Herba Pileae Scriptae extracting solution, acrylic acid, Polyethylene Glycol, mistake will be adsorbed with Ammonium sulfate and water 1:1:1:0.02:15 in mass ratio mixes, and the post-heating that stirs is to 50 DEG C, and insulated and stirred reacts 6h, reaction After be cooled to room temperature, obtain viscous liquid, through being dried and grind after, prepare Herba Pileae Scriptae functional agglomerate.
Wherein, the preparation method of described Herba Pileae Scriptae extracting solution is: takes clean Herba Pileae Scriptae leaf and pulls an oar it, prepares Herba Pileae Scriptae serosity, joins described Herba Pileae Scriptae serosity in the ethanol solution that concentration is 70wt% and carries out microwave radiation exaraction, extracts Rear filtration prepares Herba Pileae Scriptae extracting solution, wherein Herba Pileae Scriptae serosity and mass ratio 1:12, the microwave extraction power 650W of ethanol solution, Extraction time 5min, Extracting temperature 65 DEG C.
Raw materials used, equipment in the present invention, unless otherwise noted, is the conventional raw material of this area, equipment；In the present invention Method therefor, unless otherwise noted, is the conventional method of this area.
The above, be only presently preferred embodiments of the present invention, not impose any restrictions the present invention, every according to the present invention Any simple modification, change and the equivalent transformation that above example is made by technical spirit, all still falls within the technology of the present invention side The protection domain of case.

Claims (10)

1. the production method of a Herba Pileae Scriptae fiber raschel blanket, it is characterised in that using Herba Pileae Scriptae fiber filament as plush yarn Raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare Herba Pileae Scriptae fiber and draw house That woollen blanket semi-finished product；
2), prefinishing: carry out described Herba Pileae Scriptae fiber raschel blanket semi-finished product shaping, bristle, hot light, clot；
3), dyeing and finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then With reduction cleaning liquid, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing are carried out reduction cleaning, warp after elder generation after reduction cleaning Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, uses flexible smooth agent to draw Herba Pileae Scriptae fiber after steaming and color fixing She Er woollen blanket semi-finished product carry out flexible smooth process, the most again dry；
4), Final finishing: the Herba Pileae Scriptae fiber raschel blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot Cut, cutting is sewed up, and obtains Herba Pileae Scriptae fiber raschel blanket finished product；
5), product inspection, packaging warehouse-in；
The preparation method of described Herba Pileae Scriptae fiber filament is as follows: by melted after polyester slice, Herba Pileae Scriptae functional agglomerate being blended Spinning-drawing machine carries out spinning, prepares Herba Pileae Scriptae fiber filament；Wherein said Herba Pileae Scriptae functional agglomerate accounts for the total matter of Herba Pileae Scriptae fiber filament The 8-12% of amount.
2. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that described in step 1) Tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling lining Latitude, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear；Wherein, described The specification of Herba Pileae Scriptae fiber filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
3. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that step 2) sizing Time, Herba Pileae Scriptae fiber raschel blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid is with the ramp of 2 DEG C/min To 50 DEG C, then it is incubated 45min, is cooled to Herba Pileae Scriptae fiber raschel blanket semi-finished product after room temperature with the speed of 3 DEG C/min Take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
4. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that carrying out dyeing and finishing Before, the Herba Pileae Scriptae fiber raschel blanket semi-finished product after prefinishing are carried out pretreatment: by Herba Pileae Scriptae fiber raschel blanket half Finished product submergence carries out impregnation process in ethanol, and wherein Herba Pileae Scriptae fiber raschel blanket semi-finished product are 1 with the mass ratio of ethanol: (2-4), dip time is 20-40min.
5. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that in step 3) During dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls at 5.6- 6.8；Then Herba Pileae Scriptae fiber raschel blanket semi-finished product are immersed in dye liquor, Herba Pileae Scriptae fiber raschel blanket semi-finished product with The mass ratio of dye liquor is 1:10；Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 with the speed of 1.5 DEG C/min DEG C, then dye liquor is warming up to 125-135 DEG C with the speed of 1 DEG C/min, last fixation 60min；Wherein in dye during dark product Use Palanilp nonionic dye；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
6. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that described in step 3) Reduction cleaning liquid include the synthesis detergent of 1.5-2.5g/L, the tea saponin of 1.0-1.5g/L, 10-15g/L Sargassum powder with 1.0- The sodium alginate of 2.0g/L and water, bath raio 1:25, temperature 50-55 DEG C, scavenging period 25-35min；During the dark product of dye, described Reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5-10g/L and the nanometer of 0.3-0.5g/L Titanium dioxide；After reduction cleaning, the concentration of acetum used is 0.5wt%；When flexible smooth processes, with flexible smooth agent pair Fabric carries out arranging the 2-3 second；Described flexible smooth agent includes lecithin, smooth agent, tween 80 and water, wherein said lecithin Weight be water weight 2.5-3%, the weight of smooth agent be water weight 1.5-2%, the weight of tween be water weight 0.5-1%.
7. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 6, it is characterised in that described lecithin warp Cross modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 50-60wt% by lecithin stirs, wherein said ovum phosphorus The mass ratio of fat and lactic acid solution is 100:(4-6), heating-up temperature is 70-80 DEG C, heat time heating time 40-60min；In heated and stirred During be gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 20-25%；In heating It is the most neutral that stirring terminates backward reactant liquor dropping sodium hydroxide solution, finally prepares hydroxylating modified lecithin after vacuum drying.
8. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 1, it is characterised in that step 4) Final finishing In, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110-120 DEG C, sizing speed Degree 17-20m/min；Bristle uses the double roller brushing machine of MB211E type, speed 3-4m/min, enters machine along hair, and bristle spaces 2.5mm； Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130 DEG C, speed 7-10m/min；Scald and cut employing MB322E type high-speed and high-efficiency scalds shearing machine, carries out Herba Pileae Scriptae fiber raschel blanket front scalding and cuts, temperature 120-130 DEG C, speed 8-10m/min；Fluffing uses ME331E raising machine, fluffs Herba Pileae Scriptae fiber raschel blanket reverse side, speed 8-10m/ min。
9. the production method of the Herba Pileae Scriptae fiber raschel blanket as described in claim 1-8 is arbitrary, it is characterised in that described grass The preparation method of Corallium Japonicum Kishinouye functional agglomerate is as follows: takes bamboo powder and adds the hydroxide that concentration is 8-12wt% to its 8-12 times of quality In sodium solution, after being uniformly dispersed, heating under reduced pressure is to 110-130 DEG C, and 6-8h is discongested in insulation；Bamboo powder it is filtrated to get after discongesting, then will Bamboo powder adds to the ethanol solution that concentration is 70-80wt% of its 8-12 times of quality, is incubated 3-5h after being heated to 80-90 DEG C, then Secondary filtering, add water insoluble matter and pull an oar, making beating is 14-16 ° of SR to slurry beating degree, then carries out defibrination, defibrination It is 18-22 ° of SR to slurry beating degree, washes after making beating and obtain cellulose after distillation of reducing pressure；Cellulose is added to it In the ionic liquid of 18-22 times of quality, obtain cellulose solution；Cellulose solution is freezed in a low temperature of-18 DEG C to-22 DEG C 1-2 days, then take out frost thing, thaw with flowing water, prepare cellulose aquagel, then carry out solvent displacement with dehydrated alcohol, so After through vacuum drying and grind after, prepare cellulose aerogels granule；Cellulose aerogels granule be impregnated in Herba Pileae Scriptae carry Take and liquid carries out saturated absorption, take out after absorption；By be adsorbed with the cellulose aerogels granule of Herba Pileae Scriptae extracting solution, acrylic acid, Polyethylene Glycol, Ammonium persulfate. and water 1-3:1:1:0.02:15-25 in mass ratio mix, the post-heating that stirs to 50-60 DEG C, Insulated and stirred reaction 4-6h, is cooled to room temperature, obtains viscous liquid after reaction, after being dried and grinding, prepare Herba Pileae Scriptae Functional agglomerate.
10. the production method of Herba Pileae Scriptae fiber raschel blanket as claimed in claim 9, it is characterised in that described Herba Pileae Scriptae The preparation method of extracting solution is: takes clean Herba Pileae Scriptae leaf and pulls an oar it, prepares Herba Pileae Scriptae serosity, by described Herba Pileae Scriptae Serosity joins in the ethanol solution that concentration is 70-80wt% and carries out microwave radiation exaraction, filters and prepare Herba Pileae Scriptae extraction after extraction Liquid, wherein Herba Pileae Scriptae serosity and the mass ratio 1:(12-16 of ethanol solution), microwave extraction power 650-750W, extraction time 3- 5min, Extracting temperature 65-75 DEG C.
CN201610683941.9A 2016-08-18 2016-08-18 A kind of production method of Chloranthus glaber fiber raschel blanket Active CN106245216B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610683941.9A CN106245216B (en) 2016-08-18 2016-08-18 A kind of production method of Chloranthus glaber fiber raschel blanket

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610683941.9A CN106245216B (en) 2016-08-18 2016-08-18 A kind of production method of Chloranthus glaber fiber raschel blanket

Publications (2)

Publication Number Publication Date
CN106245216A true CN106245216A (en) 2016-12-21
CN106245216B CN106245216B (en) 2019-01-04

Family

ID=57592304

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610683941.9A Active CN106245216B (en) 2016-08-18 2016-08-18 A kind of production method of Chloranthus glaber fiber raschel blanket

Country Status (1)

Country Link
CN (1) CN106245216B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106978645A (en) * 2017-05-08 2017-07-25 上海新纺织产业用品有限公司 A kind of manufacture method of rough surface polyester fiber
CN109137184A (en) * 2018-09-03 2019-01-04 江苏箭鹿毛纺股份有限公司 A kind of preparation method of Chloranthus glaber antibacterial fancy suiting
CN111996656A (en) * 2020-08-26 2020-11-27 江苏优室家纺织品有限公司 Pineapple flannelette fabric and production process thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101731577A (en) * 2010-02-10 2010-06-16 浙江大学 Ultrasonically auxiliary extracting method of polyphenol substance in waxberry pomace
CN104047099A (en) * 2014-06-25 2014-09-17 江苏东源纺织科技实业有限公司 Manufacturing technology of health-care type blended knitted fabric
CN104047185A (en) * 2014-06-25 2014-09-17 江苏东源纺织科技实业有限公司 Production process of healthcare type blended high-elasticity knitted fabric
CN104327017A (en) * 2014-11-25 2015-02-04 武汉大学 Method for extracting and purifying fucoxanthin
CN105326279A (en) * 2015-10-30 2016-02-17 浙江真爱毯业科技有限公司 Production method of mint-fiber Raschel blanket

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101731577A (en) * 2010-02-10 2010-06-16 浙江大学 Ultrasonically auxiliary extracting method of polyphenol substance in waxberry pomace
CN104047099A (en) * 2014-06-25 2014-09-17 江苏东源纺织科技实业有限公司 Manufacturing technology of health-care type blended knitted fabric
CN104047185A (en) * 2014-06-25 2014-09-17 江苏东源纺织科技实业有限公司 Production process of healthcare type blended high-elasticity knitted fabric
CN104327017A (en) * 2014-11-25 2015-02-04 武汉大学 Method for extracting and purifying fucoxanthin
CN105326279A (en) * 2015-10-30 2016-02-17 浙江真爱毯业科技有限公司 Production method of mint-fiber Raschel blanket

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106978645A (en) * 2017-05-08 2017-07-25 上海新纺织产业用品有限公司 A kind of manufacture method of rough surface polyester fiber
CN109137184A (en) * 2018-09-03 2019-01-04 江苏箭鹿毛纺股份有限公司 A kind of preparation method of Chloranthus glaber antibacterial fancy suiting
CN111996656A (en) * 2020-08-26 2020-11-27 江苏优室家纺织品有限公司 Pineapple flannelette fabric and production process thereof

Also Published As

Publication number Publication date
CN106245216B (en) 2019-01-04

Similar Documents

Publication Publication Date Title
CN105326279B (en) A kind of production method of mint fibers Rachael blanket
CN105332158B (en) A kind of production method of antistatic Rachael blanket
CN105310377B (en) A kind of production method of spontaneous heating fiber raschel blanket
CN105326280B (en) Production process of Viloft fiber Raschel blanket
CN102312342B (en) Multifunctional thermal underwear fabric and processing method thereof
CN101525803B (en) Nursing type blended fabric and production method thereof
CN105310378B (en) Production process of fiber velvet Raschel blanket
CN102733183B (en) Fiber fabric with heating function, and preparation method thereof
CN103361866B (en) A kind of fiber crops knitting fabric of Sai Er coffee carbon fiber and preparation method thereof
CN105326282B (en) Production technology of corn fiber Raschel blanket
CN102162167A (en) Production process of heating functional knitted fabric
CN106012148A (en) Preparation method of cotton-hemp insulation chameleon fiber blended yarn
CN106245216B (en) A kind of production method of Chloranthus glaber fiber raschel blanket
CN104273709A (en) Method for improving heat-insulating performance of wool knitted garment
CN108914315A (en) A kind of spring sweat absorption antibacterial underwear fabric
CN106192182A (en) A kind of infrared spontaneous heating cold-proof underwear
CN106245215B (en) A kind of production method of alginate fibre Rachael blanket
CN106319935B (en) A kind of production method for covering Naris fiber raschel blanket
CN104109940B (en) A kind of fiber crops Sai Er fiber raschel blanket and production technology thereof
CN103603155A (en) Method for processing pure-cotton cool-feeling knitted fabric
CN106167951B (en) A kind of production technology of rabbit suede Rachael blanket
CN106222871B (en) A kind of production technology of Lyocell fire resistance fibres Rachael blanket
CN105326281B (en) Production method of aloe fiber Raschel blanket
CN102747526A (en) Coffee carbon jade fiber knitting fabric
CN106377125B (en) A kind of intelligent environmental balances the production method of Rachael blanket

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant