CN106243783A - A kind of white pearlescent pigment preparation method based on sericite - Google Patents

A kind of white pearlescent pigment preparation method based on sericite Download PDF

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Publication number
CN106243783A
CN106243783A CN201610538861.4A CN201610538861A CN106243783A CN 106243783 A CN106243783 A CN 106243783A CN 201610538861 A CN201610538861 A CN 201610538861A CN 106243783 A CN106243783 A CN 106243783A
Authority
CN
China
Prior art keywords
sericite
mixture
pearlescent pigment
pigment preparation
method based
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610538861.4A
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Chinese (zh)
Inventor
王凯
吴金龙
朱朋利
叶晓红
高庆忠
章常玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHUZHOU GREA MINERALS Co Ltd
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CHUZHOU GREA MINERALS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHUZHOU GREA MINERALS Co Ltd filed Critical CHUZHOU GREA MINERALS Co Ltd
Priority to CN201610538861.4A priority Critical patent/CN106243783A/en
Publication of CN106243783A publication Critical patent/CN106243783A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of white pearlescent pigment preparation method based on sericite, comprise the following steps: S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；S2, thickening agent, filler, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixture B；S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, obtain mixture C；S4, by mixture C high temperature dry, heat while stirring；S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.Due to the fact that adding sericite is greatly improved the brightness of pigment, colourity and stability, easily dispersion, easily mixing and not fugitive color, operational approach of the present invention is simple, material is easy to get, low cost, can be widely applied to coating, ink, plastics and cosmetic field.

Description

A kind of white pearlescent pigment preparation method based on sericite
Technical field
The present invention relates to pearlescent pigment technical field, particularly relate to a kind of white pearlescent pigment preparation side based on sericite Method.
Background technology
Pearlescent pigment is made up of several metal thin oxide layer cladding Muscovitum.Change thin layer of metal oxide, with regard to energy Produce different pearl effects.Pearlescent pigment is compared with other pigment, and its distinctive soft pearly luster has incomparable Effect.Pearlescent pigment is widely used in the aspects such as plastics, cosmetic, coating, ink, and high-grade pearlescent pigment also supplies should in China Asking, due to people's raising to pearlescent pigment color demand, the pearlescent pigment preparing new type colorful and variable color is also current research Emphasis with market development.Then the present invention proposes a kind of white pearlescent pigment preparation method based on sericite.
Summary of the invention
The invention aims to solve shortcoming present in prior art, and propose a kind of based on sericite white Color pearlescent pigment preparation method.
A kind of white pearlescent pigment preparation method based on sericite, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, thickening agent, filler, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixture B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature dry, heat while stirring；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Preferably, in described S4, high temperature is 200-300 DEG C.
Preferably, in described S4, mixing time is 1-1.5 hour.
Preferably, in described S2, thickening agent is Polyacrylate Emulsion.
Preferably, in described S2, filler is Chinese white or wheaten starch.
Due to the fact that adding sericite is greatly improved the brightness of pigment, colourity and stability, easily disperse, easily mix Closing and not fugitive color, operational approach of the present invention is simple, material is easy to get, low cost, can be widely applied to coating, ink, plastics and Cosmetic field.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is explained orally further.
Embodiment one
A kind of based on sericite the white pearlescent pigment preparation method that the present invention proposes, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, Polyacrylate Emulsion, Chinese white, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixed Compound B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature 200 DEG C drying, heat while stirring 1.5 hours；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Embodiment two
A kind of based on sericite the white pearlescent pigment preparation method that the present invention proposes, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, Polyacrylate Emulsion, Chinese white, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixed Compound B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature 220 DEG C drying, heat while stirring 1.5 hours；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Embodiment three
A kind of based on sericite the white pearlescent pigment preparation method that the present invention proposes, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, Polyacrylate Emulsion, wheaten starch, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixed Compound B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature 250 DEG C drying, heat while stirring 1.3 hours；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Embodiment four
A kind of based on sericite the white pearlescent pigment preparation method that the present invention proposes, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, Polyacrylate Emulsion, wheaten starch, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixed Compound B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature 280 DEG C drying, heat while stirring 1.1 hours；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Embodiment five
A kind of based on sericite the white pearlescent pigment preparation method that the present invention proposes, comprises the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, Polyacrylate Emulsion, wheaten starch, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixed Compound B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature 300 DEG C drying, heat while stirring 1 hour；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
Due to the fact that adding sericite is greatly improved the brightness of pigment, colourity and stability, easily disperse, easily mix Closing and not fugitive color, operational approach of the present invention is simple, material is easy to get, low cost, can be widely applied to coating, ink, plastics and Cosmetic field
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto, and any Those familiar with the art is in the technical scope that the invention discloses, according to technical scheme and invention thereof Conceive equivalent or change in addition, all should contain within protection scope of the present invention.

Claims (5)

1. a white pearlescent pigment preparation method based on sericite, it is characterised in that comprise the following steps:
S1, sericite and Kaolin are put in grinder, be fully ground three times to obtain fine powder A；
S2, thickening agent, filler, Pulvis Talci, glycerol, natural gum are mixed, stir, obtain mixture B；
S3, fine powder A and mixture B is added to the water, adds zinc oxide and pure titinium dioxide while stirring, to be mixed uniformly, Obtain mixture C；
S4, by mixture C high temperature dry, heat while stirring；
S5, will dry after mixture C put in grinder and be fully ground, to obtain final product.
A kind of white pearlescent pigment preparation method based on sericite the most according to claim 1, it is characterised in that described In S4, high temperature is 200-300 DEG C.
A kind of white pearlescent pigment preparation method based on sericite the most according to claim 1, it is characterised in that described In S4, mixing time is 1-1.5 hour.
A kind of white pearlescent pigment preparation method based on sericite the most according to claim 1, it is characterised in that described In S2, thickening agent is Polyacrylate Emulsion.
A kind of white pearlescent pigment preparation method based on sericite the most according to claim 1, it is characterised in that described In S2, filler is Chinese white or wheaten starch.
CN201610538861.4A 2016-07-11 2016-07-11 A kind of white pearlescent pigment preparation method based on sericite Pending CN106243783A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610538861.4A CN106243783A (en) 2016-07-11 2016-07-11 A kind of white pearlescent pigment preparation method based on sericite

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610538861.4A CN106243783A (en) 2016-07-11 2016-07-11 A kind of white pearlescent pigment preparation method based on sericite

Publications (1)

Publication Number Publication Date
CN106243783A true CN106243783A (en) 2016-12-21

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107337943A (en) * 2017-07-24 2017-11-10 安徽恒昊科技有限公司 A kind of organic matter laminating method of mica powder used for cosmetic
CN107753303A (en) * 2017-11-05 2018-03-06 滁州格锐矿业有限责任公司 A kind of preparation technology of pigment used for cosmetic
CN107822906A (en) * 2017-11-05 2018-03-23 滁州格锐矿业有限责任公司 A kind of modified sericite in powder used for cosmetic and preparation method thereof

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1494415A (en) * 2001-01-08 2004-05-05 �ź㴫 Cosmetic composition with pasty to powdery texture
CN101050313A (en) * 1998-03-26 2007-10-10 默克专利股份有限公司 Pigment preparations
US20080216710A1 (en) * 2004-09-27 2008-09-11 Kentucky-Tennessee Clay Co. Method of Processing Mica
CN102695548A (en) * 2009-12-30 2012-09-26 雅芳产品公司 Cosmetic powder bead compositions
CN103937030A (en) * 2014-04-25 2014-07-23 浙江大学 Talc, sericite and silicone oil intercalation composite material and preparation method thereof
CN104017393A (en) * 2014-06-11 2014-09-03 安徽恒昊科技有限公司 Nano-zinc oxide coated sericite powder composite material and preparation method thereof
US20150376415A1 (en) * 2009-12-24 2015-12-31 Coatex S.A.S. Use of glycerol as an agent to improve the self-dispersing properties of a mineral material to be added to an aqueous composition
CN105524303A (en) * 2016-02-02 2016-04-27 安徽恒昊科技有限公司 Preparation method of sericite-containing composite with high water absorption and retention performance
CN105542519A (en) * 2016-02-02 2016-05-04 安徽恒昊科技有限公司 High-temperature wear-resistant sericite pearlescent pigment
CN105542518A (en) * 2016-02-02 2016-05-04 安徽恒昊科技有限公司 Modified high-whiteness sericite powder and preparation method thereof
CN105602294A (en) * 2016-02-02 2016-05-25 安徽恒昊科技有限公司 Method for preparing white pearlescent pigment from sericite
CN105726344A (en) * 2016-02-02 2016-07-06 安徽恒昊科技有限公司 Preparation method of cosmetic sericite having easy dispersibility

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101050313A (en) * 1998-03-26 2007-10-10 默克专利股份有限公司 Pigment preparations
CN1494415A (en) * 2001-01-08 2004-05-05 �ź㴫 Cosmetic composition with pasty to powdery texture
US20080216710A1 (en) * 2004-09-27 2008-09-11 Kentucky-Tennessee Clay Co. Method of Processing Mica
US20150376415A1 (en) * 2009-12-24 2015-12-31 Coatex S.A.S. Use of glycerol as an agent to improve the self-dispersing properties of a mineral material to be added to an aqueous composition
CN102695548A (en) * 2009-12-30 2012-09-26 雅芳产品公司 Cosmetic powder bead compositions
CN103937030A (en) * 2014-04-25 2014-07-23 浙江大学 Talc, sericite and silicone oil intercalation composite material and preparation method thereof
CN104017393A (en) * 2014-06-11 2014-09-03 安徽恒昊科技有限公司 Nano-zinc oxide coated sericite powder composite material and preparation method thereof
CN105524303A (en) * 2016-02-02 2016-04-27 安徽恒昊科技有限公司 Preparation method of sericite-containing composite with high water absorption and retention performance
CN105542519A (en) * 2016-02-02 2016-05-04 安徽恒昊科技有限公司 High-temperature wear-resistant sericite pearlescent pigment
CN105542518A (en) * 2016-02-02 2016-05-04 安徽恒昊科技有限公司 Modified high-whiteness sericite powder and preparation method thereof
CN105602294A (en) * 2016-02-02 2016-05-25 安徽恒昊科技有限公司 Method for preparing white pearlescent pigment from sericite
CN105726344A (en) * 2016-02-02 2016-07-06 安徽恒昊科技有限公司 Preparation method of cosmetic sericite having easy dispersibility

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107337943A (en) * 2017-07-24 2017-11-10 安徽恒昊科技有限公司 A kind of organic matter laminating method of mica powder used for cosmetic
CN107753303A (en) * 2017-11-05 2018-03-06 滁州格锐矿业有限责任公司 A kind of preparation technology of pigment used for cosmetic
CN107822906A (en) * 2017-11-05 2018-03-23 滁州格锐矿业有限责任公司 A kind of modified sericite in powder used for cosmetic and preparation method thereof

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Application publication date: 20161221