CN106234411A - Sleeve pipe sterilized solution and preparation method thereof - Google Patents
Sleeve pipe sterilized solution and preparation method thereof Download PDFInfo
- Publication number
- CN106234411A CN106234411A CN201610832913.9A CN201610832913A CN106234411A CN 106234411 A CN106234411 A CN 106234411A CN 201610832913 A CN201610832913 A CN 201610832913A CN 106234411 A CN106234411 A CN 106234411A
- Authority
- CN
- China
- Prior art keywords
- consumption
- weight portion
- preparation
- sleeve pipe
- sterilized solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/14—Boron; Compounds thereof
Abstract
The invention discloses the preparation method of a kind of sleeve pipe sterilized solution, wherein, described preparation method includes: silver nitrate, chitosan, ethylene glycol and sodium chloride are mixed, and forms mixed liquor M；Mixed liquor M carries out under 300 310W microwave heating, and heat time heating time is 3 10min, filter, clean after obtain nanometer silver；Carry out ultrasonic disperse after prepared nanometer silver, taurine, disodiumedetate, boric acid, glycerol and water being mixed, obtain sleeve pipe sterilized solution；Solve the problem that common sterilized solution sterilization effect is poor.
Description
Technical field
The present invention relates to sterilized solution, in particular it relates to sleeve pipe sterilized solution and preparation method thereof.
Background technology
Sleeve pipe is as a kind of conventional material, and the range in producing and living is extremely wide, makes in filter plant
Sleeve pipe need before assembling to be carried out and sterilization treatment, to improve the security performance of filter plant, and common sterilizing
Liquid sterilization effect is poor.
Therefore it provides excellent sleeve pipe sterilized solution of a kind of sterilization effect and preparation method thereof is that the present invention needs asking of solution badly
Topic.
Summary of the invention
It is an object of the invention to provide a kind of sleeve pipe sterilized solution and preparation method thereof, solve common sterilized solution sterilizing effect
The most poor problem.
To achieve these goals, the invention provides the preparation method of a kind of sleeve pipe sterilized solution, wherein, described preparation side
Method includes:
(1) silver nitrate, chitosan, ethylene glycol and sodium chloride are mixed, form mixed liquor M；
(2) mixed liquor M carrying out under 300-310W microwave heating, heat time heating time is 3-10min, filter, clean after
To nanometer silver；
(3) surpass after prepared nanometer silver, taurine, disodiumedetate, boric acid, glycerol and water being mixed
Sound disperses, and obtains sleeve pipe sterilized solution.
Present invention also offers a kind of sleeve pipe sterilized solution, wherein, described sleeve pipe sterilized solution is prepared by above-mentioned preparation method.
By technique scheme, the invention provides the preparation method of a kind of sleeve pipe sterilized solution, wherein, described preparation side
Method includes: silver nitrate, chitosan, ethylene glycol and sodium chloride are mixed, and forms mixed liquor M；Mixed liquor M is entered under 300-310W
Row microwave heating, heat time heating time is 3-10min, filter, clean after obtain nanometer silver；By prepared nanometer silver, taurine, second two
Carry out ultrasonic disperse after amine tetraacethyl disodium, boric acid, glycerol and water mixing, obtain sleeve pipe sterilized solution；Between each raw material
Synergism so that prepared sleeve pipe sterilized solution possesses excellent sterilization effect, is simultaneously used for preparing the method for this sterilized solution
Simply, raw material is easy to get.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the detailed description of the invention of the present invention is described in detail.It should be appreciated that described herein specifically
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of sleeve pipe sterilized solution, wherein, described preparation method includes: by silver nitrate,
Chitosan, ethylene glycol and sodium chloride mixing, form mixed liquor M；Mixed liquor M is carried out under 300-310W microwave heating, heating
Time is 3-10min, filter, clean after obtain nanometer silver；By prepared nanometer silver, taurine, disodiumedetate, boron
Carry out ultrasonic disperse after acid, glycerol and water mixing, obtain sleeve pipe sterilized solution.
In order to make the sleeve pipe sterilized solution sterilization ability for preparing more preferable, the present invention one preferred embodiment in, phase
For the silver nitrate of 100 weight portions, the consumption of described chitosan is 20-40 weight portion, and the consumption of described ethylene glycol is 40-60 weight
Amount part, the consumption of described sodium chloride is 1-3 weight portion；Relative to the water of 100 weight portions, the consumption of described nanometer silver is 0.5-
1.5 weight portions, the consumption of described taurine is 1-10 weight portion, and the consumption of described disodiumedetate is 2-8 weight portion,
The consumption of described boric acid is 5-15 weight portion, and the consumption of described glycerol is 2-20 weight portion.
In a kind of embodiment being more highly preferred to, relative to the silver nitrate of 100 weight portions, the consumption of described chitosan is
25-35 weight portion, the consumption of described ethylene glycol is 45-55 weight portion, and the consumption of described sodium chloride is 1.5-2.5 weight portion；Phase
For the water of 100 weight portions, the consumption of described nanometer silver is 0.8-1.2 weight portion, and the consumption of described taurine is 3-6 weight
Part, the consumption of described disodiumedetate is 4-6 weight portion, and the consumption of described boric acid is 8-12 weight portion, described the third three
The consumption of alcohol is 10-15 weight portion.
So that prepare nanometer silver can be rinsed totally, the present invention one preferred embodiment in, step
(2) acetone or alcohol is used to be carried out after filtering in.
So that nanometer silver can preferably be scattered among other raw materials, the present invention one preferred embodiment
In, in step (3), the frequency of ultrasonic disperse is 20-25KHz.
Present invention also offers a kind of sleeve pipe sterilized solution, wherein, described sleeve pipe sterilized solution is prepared by above-mentioned preparation method.
Hereinafter will be described the present invention by embodiment.In following example, silver nitrate, chitosan, second two
Alcohol, sodium chloride, taurine, disodiumedetate, boric acid and glycerol are conventional commercial product.
Embodiment 1
100g silver nitrate, 25g chitosan, 45g ethylene glycol and 1.5g sodium chloride are mixed, forms mixed liquor M；By mixed liquor
M carries out microwave heating under 300W, and heat time heating time is 3min, filter, clean after obtain nanometer silver；The nanometer that 0.8g is prepared
Ultrasonic disperse is carried out (super after silver, 3g taurine, 4g disodiumedetate, 8g boric acid, 10g glycerol and the mixing of 100g water
The scattered frequency of sound is 20KHz), obtain sleeve pipe sterilized solution A1.
Embodiment 2
100g silver nitrate, 35g chitosan, 55g ethylene glycol and 2.5 sodium chloride are mixed, forms mixed liquor M；By mixed liquor M
Carrying out microwave heating under 310W, heat time heating time is 10min, filter, clean after obtain nanometer silver；The nanometer that 1.2g is prepared
Ultrasonic disperse (ultrasonic point is carried out after silver, 6g taurine, 6g disodiumedetate, 12g boric acid, 15g glycerol and water mixing
The frequency dissipated is 25KHz), obtain sleeve pipe sterilized solution A2.
Embodiment 3
100g silver nitrate, 30g chitosan, 50g ethylene glycol and 2g sodium chloride are mixed, forms mixed liquor M；By mixed liquor M
Carrying out microwave heating under 305W, heat time heating time is 5min, filter, clean after obtain nanometer silver；By nanometer silver prepared for 1g, 4g
Ultrasonic disperse (ultrasonic point is carried out after taurine, 5g disodiumedetate, 10g boric acid, 12g glycerol and the mixing of 100g water
The frequency dissipated is 20-25KHz), obtain sleeve pipe sterilized solution A3.
Embodiment 4
It is prepared according to the method for embodiment 1, except for the difference that, relative to the silver nitrate of 100g, the use of described chitosan
Amount is 20g, and the consumption of described ethylene glycol is 40g, and the consumption of described sodium chloride is 1g；Relative to the water of 100g, described nanometer silver
Consumption be 0.5g, the consumption of described taurine is 1g, and the consumption of described disodiumedetate is 2g, the use of described boric acid
Amount is 5g, and the consumption of described glycerol is 2g, obtains sleeve pipe sterilized solution A4.
Embodiment 5
It is prepared according to the method for embodiment 1, except for the difference that, relative to the silver nitrate of 100g, the use of described chitosan
Amount is 40g, and the consumption of described ethylene glycol is 60g, and the consumption of described sodium chloride is 3g；Relative to the water of 100g, described nanometer silver
Consumption be 1.5g, the consumption of described taurine is 10g, and the consumption of described disodiumedetate is 8g, described boric acid
Consumption is 15g, and the consumption of described glycerol is 20g, obtains sleeve pipe sterilized solution A5.
Comparative example 1
It is prepared according to the method for embodiment 1, except for the difference that, relative to the silver nitrate of 100g, the use of described chitosan
Amount is 15g, and the consumption of described ethylene glycol is 35g, and the consumption of described sodium chloride is 0.8g；Relative to the water of 100g, described nanometer
The consumption of silver is 0.3g, and the consumption of described taurine is 0.8g, and the consumption of described disodiumedetate is 1g, described boric acid
Consumption be 3g, the consumption of described glycerol is 1g, obtains sleeve pipe sterilized solution D1.
Comparative example 2
It is prepared according to the method for embodiment 1, except for the difference that, relative to the silver nitrate of 100g, the use of described chitosan
Amount is 45g, and the consumption of described ethylene glycol is 65g, and the consumption of described sodium chloride is 5g；Relative to the water of 100g, described nanometer silver
Consumption be 2g, the consumption of described taurine is 12g, and the consumption of described disodiumedetate is 10g, the use of described boric acid
Amount is 18g, and the consumption of described glycerol is 22g, obtains sleeve pipe sterilized solution D2.
Test case
Sleeve pipe is placed in the distilled water after sterilizing after soaking 10min and detects the clump count in water, then by above-mentioned sleeve pipe
Take out after being respectively put in above-mentioned prepared A1-A5, D1 and D2 immersion 20min, and in the distilled water after being again placed in sterilizing
Detecting the clump count in water after soaking 10min, the result obtained is as shown in table 1.
Table 1
| Numbering | Bacterium colony (cfu/g) before soaking | Bacterium colony (cfu/g) after immersion |
| A1 | ＞ 100 | 10 |
| A2 | ＞ 100 | 15 |
| A3 | ＞ 100 | 14 |
| A4 | ＞ 100 | 22 |
| A5 | ＞ 100 | 25 |
| D1 | ＞ 100 | ＞ 100 |
| D2 | ＞ 100 | ＞ 100 |
By above table data it can be seen that the sterilized solution A1-A5 prepared within the scope of the present invention possesses excellent killing
Bacterium ability, and the sterilized solution D1 and the D2 sterilization effect that prepare within the scope of the present invention are poor, meanwhile, in currently preferred scope
The sterilization ability of the interior sterilized solution A1-A3 prepared is more excellent.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the technology concept of the present invention, technical scheme can be carried out multiple simple variant, this
A little simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technical characteristic described in above-mentioned detailed description of the invention, at not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy illustrates the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it should be considered as content disclosed in this invention equally.
Claims (6)
1. the preparation method of a sleeve pipe sterilized solution, it is characterised in that described preparation method includes:
(1) silver nitrate, chitosan, ethylene glycol and sodium chloride are mixed, form mixed liquor M；
(2) mixed liquor M carrying out under 300-310W microwave heating, heat time heating time is 3-10min, filter, clean after received
Meter Yin；
(3) ultrasonic point is carried out after prepared nanometer silver, taurine, disodiumedetate, boric acid, glycerol and water being mixed
Dissipate, obtain sleeve pipe sterilized solution.
Preparation method the most according to claim 1, wherein, relative to the silver nitrate of 100 weight portions, the use of described chitosan
Amount is 20-40 weight portion, and the consumption of described ethylene glycol is 40-60 weight portion, and the consumption of described sodium chloride is 1-3 weight portion；
Relative to the water of 100 weight portions, the consumption of described nanometer silver is 0.5-1.5 weight portion, and the consumption of described taurine is 1-
10 weight portions, the consumption of described disodiumedetate is 2-8 weight portion, and the consumption of described boric acid is 5-15 weight portion, institute
The consumption stating glycerol is 2-20 weight portion.
Preparation method the most according to claim 2, wherein, relative to the silver nitrate of 100 weight portions, the use of described chitosan
Amount is 25-35 weight portion, and the consumption of described ethylene glycol is 45-55 weight portion, and the consumption of described sodium chloride is 1.5-2.5 weight
Part；
Relative to the water of 100 weight portions, the consumption of described nanometer silver is 0.8-1.2 weight portion, and the consumption of described taurine is 3-6
Weight portion, the consumption of described disodiumedetate is 4-6 weight portion, and the consumption of described boric acid is 8-12 weight portion, described
The consumption of glycerol is 10-15 weight portion.
Preparation method the most according to claim 1, wherein, uses acetone or alcohol to be carried out in step (2) after filtering.
Preparation method the most according to claim 1, wherein, in step (3), the frequency of ultrasonic disperse is 20-25KHz.
6. a sleeve pipe sterilized solution, it is characterised in that described sleeve pipe sterilized solution is by the system described in any one in claim 1-5
Preparation Method prepares.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610832913.9A CN106234411A (en) | 2016-09-20 | 2016-09-20 | Sleeve pipe sterilized solution and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610832913.9A CN106234411A (en) | 2016-09-20 | 2016-09-20 | Sleeve pipe sterilized solution and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106234411A true CN106234411A (en) | 2016-12-21 |
Family
ID=57600310
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610832913.9A Pending CN106234411A (en) | 2016-09-20 | 2016-09-20 | Sleeve pipe sterilized solution and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106234411A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102784926A (en) * | 2012-07-16 | 2012-11-21 | 太原理工大学 | Method for preparing spherical nano-silver particles |
| CN103563983A (en) * | 2012-07-24 | 2014-02-12 | 上海纳米技术及应用国家工程研究中心有限公司 | Nano-silver peroxide composite antibacterial solution and preparation method thereof |
| CN104227017A (en) * | 2014-09-28 | 2014-12-24 | 重庆文理学院 | Preparation method of silver nanoparticle with controllable particle size |
| CN105014095A (en) * | 2015-07-31 | 2015-11-04 | 合肥微晶材料科技有限公司 | Method for preparing silver nanowire through reduction of microwave alcohol |
-
2016
- 2016-09-20 CN CN201610832913.9A patent/CN106234411A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102784926A (en) * | 2012-07-16 | 2012-11-21 | 太原理工大学 | Method for preparing spherical nano-silver particles |
| CN103563983A (en) * | 2012-07-24 | 2014-02-12 | 上海纳米技术及应用国家工程研究中心有限公司 | Nano-silver peroxide composite antibacterial solution and preparation method thereof |
| CN104227017A (en) * | 2014-09-28 | 2014-12-24 | 重庆文理学院 | Preparation method of silver nanoparticle with controllable particle size |
| CN105014095A (en) * | 2015-07-31 | 2015-11-04 | 合肥微晶材料科技有限公司 | Method for preparing silver nanowire through reduction of microwave alcohol |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103774426B (en) | Silk fabric antibacterial and mouldproof finishing agent | |
| CN104491920B (en) | A kind of preparation method of absorbable suture | |
| CN103757908B (en) | Silk fabric anti-mite finishing agent | |
| EP2853160A1 (en) | Antimicrobial composition comprising ginseng extract and green tea extract and an antimicrobial filter containing it | |
| CN102871870A (en) | Medical hand sterilizer | |
| CN106234411A (en) | Sleeve pipe sterilized solution and preparation method thereof | |
| CN107384648A (en) | A kind of germicidal soaps | |
| CN106417368A (en) | Casing sterilization solution and preparation method thereof | |
| CN106259444A (en) | Sleeve pipe sterilized solution and preparation method thereof | |
| CN107245872A (en) | A kind of process that down jackets drake feather grease is removed using compound degreasing agent | |
| CN103757892B (en) | Silk fabric mildew-proofing finishing agent | |
| CN105614730A (en) | Preparation method of vanilla marinated goose | |
| CN105494334A (en) | Environmental-friendly sterilizing agent capable of preventing and treating bacterial diseases of fruit trees and preparation method of environment-friendly sterilizing agent | |
| CN109172682A (en) | A kind of antibacterial lotion and preparation method thereof with quick fungistatic effect | |
| CN109200188A (en) | The excellent good bacteriostasis spray of energy | |
| CN106036507A (en) | Processing method of semi-finished beef products | |
| CN103668958A (en) | Impregnation-process antibacterial polyester fabric and preparation method thereof | |
| CN106235252A (en) | food seasoning | |
| CN108578321A (en) | A kind of shampoo and preparation method thereof with bacteriostasis | |
| CN105962160A (en) | Canned abalone and preparation method thereof | |
| CN104523525A (en) | Scurf-removing shampoo | |
| CN104397294A (en) | Herb tea capable of alleviating hangover and preparation method thereof | |
| CN107397693A (en) | Babywipe | |
| CN111135135B (en) | Ginger powder with mite removing and acne removing effects and preparation method and application thereof | |
| CN108277093A (en) | A kind of milk bottle cleaning agent, preparation method and application method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161221 |