CN106231862A - The technique preparing electronic equipment conductive graphite sheet based on white carbon black - Google Patents

The technique preparing electronic equipment conductive graphite sheet based on white carbon black Download PDF

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Publication number
CN106231862A
CN106231862A CN201610603043.8A CN201610603043A CN106231862A CN 106231862 A CN106231862 A CN 106231862A CN 201610603043 A CN201610603043 A CN 201610603043A CN 106231862 A CN106231862 A CN 106231862A
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China
Prior art keywords
carbon black
white carbon
graphite sheet
conductive graphite
electronic equipment
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CN201610603043.8A
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Chinese (zh)
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CN106231862B (en
Inventor
汪劲松
王鸣
蔡森
毛明权
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Lvliang Black Cat New Material Co.,Ltd.
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Wuhu Mitec Co Ltd
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    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05KPRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K7/00Constructional details common to different types of electric apparatus
    • H05K7/20Modifications to facilitate cooling, ventilating, or heating
    • H05K7/2039Modifications to facilitate cooling, ventilating, or heating characterised by the heat transfer by conduction from the heat generating element to a dissipating body

Abstract

The invention discloses the technique preparing electronic equipment conductive graphite sheet based on white carbon black, including 1) raw material;2) precomminution;3) pre-screening;4) except ferrum;5) separating twice;6) regrading;7) mixing;8) die mould and heating;9) high temperature graphitization;10) gum;11) cutting;This processing technique step is scientific and reasonable, the processing technique of prior art is improved, the process that raw material is become more meticulous, make its granularity more uniformity, improve the qualification rate of finished product, and then improve electric conductivity and the heat conductivity of conductive graphite sheet, and its chemical stability can also be improved by this technique, reduce its thermal expansivity, and easily machine-shaping.

Description

The technique preparing electronic equipment conductive graphite sheet based on white carbon black
Technical field
The present invention relates to the conductive graphite sheet of a kind of electronics field, particularly relate to one and prepare electronics based on white carbon black The equipment technique of conductive graphite sheet.
Background technology
Conductive graphite sheet is a kind of brand-new heat conduction and heat radiation material, along two square uniform heat conduction, shielding thermal source and assembly Simultaneously improving the performance of consumption electronic product, color is usually black, and material is that native graphite is through exquisiteness processing, heat conductivity In the horizontal direction be up to 1500W/M-K, use IC, CPU, MOS, LED, fin, LCD-TV, notebook computer, communication apparatus, Wireless exchange board, DVD, handheld device etc..
Conductive graphite sheet is because of nonmetallic materials, but has heat conductivity the highest as metal and electric conductivity, Its heat-conductivity conducting is the most relatively better than aluminium foil or Copper Foil, but the conduction that conductive graphite sheet is produced in existing production technology Property and heat conductivity more reach optimal, essentially consist in raw material processing stage, place to conductive graphite tablet raw material in prior art Reason becomes more meticulous not, causes in its raw material containing more impurity component so that the quality of the conductive graphite sheet that final production goes out is not Enough height, qualification rate reduces, and can affect it preferably to shop property and heat conductivity.
Summary of the invention
For the problem of above-mentioned existence, it is desirable to provide prepare the work of electronic equipment conductive graphite sheet based on white carbon black Skill, this processing technique step is scientific and reasonable, improves the processing technique of prior art, the place becoming more meticulous raw material Reason so that it is granularity more uniformity, improves the qualification rate of finished product, and then improves the electric conductivity of conductive graphite sheet and lead Hot, and its chemical stability can also be improved by this technique, reduce its thermal expansivity, and easily machine-shaping.
To achieve these goals, the technical solution adopted in the present invention is as follows:
The technique preparing electronic equipment conductive graphite sheet based on white carbon black, comprises the following steps:
1) raw material: choose the white carbon black raw material as conductive graphite sheet;
2) precomminution: above-mentioned white carbon black is crushed in advance through disintegrating apparatus the medium size of 60-80mm;
3) pre-screening: the white carbon black that above-mentioned warp crushes is sieved by vibrosieve, removes larger particles impurity in anthracite;
4) except ferrum: size-reduced white carbon black is carried out in being placed in trash separator except ferrum operates;
5) separating twice: the cooled white carbon black completed is ground into, through disintegrating apparatus, the little granule that grain diameter is 0.3-0.5mm;
6) regrading: carry out three level screen through the little granule of white carbon black of separating twice respectively through screening plant, filter out size Consistent granule is out;
7) mixing: little for white carbon black granule and binding agent are carried out kneading, forms compound;
8) die mould and heating: in a mold by compressing for above-mentioned compound, being pressed into square sheet shape, its thickness is at 0.01- Between 0.02mm, form conductive graphite sheet base substrate, arrange in mould and add hot channel, by adding hot channel, compressing is led Hot graphite flake base substrate tentatively heats, heating and temperature control between 200-300 DEG C, heat time heating time 30min;
9) high temperature graphitization: carry out pyrographite in the conductive graphite sheet base substrate of above-mentioned heating is fed directly to high temperature graphitization stove Change operation;
10) gum: the conductive graphite sheet after high temperature graphitization is cooled to when 50-60 DEG C heat-resisting two-sided its bottom surface coating one layer Glue, and one layer of release paper is adhered in conductive graphite sheet bottom surface;
11) cutting: the conductive graphite sheet base substrate after graphitization forms the conductive graphite sheet of finished product, and cooling down, Jin Ertong Cross cutting equipment and cut into the size of needs.
As preferably, the trash separator in described step (3) includes trash extraction box, charging aperture, discharging opening and crutcher, At the charging aperture of described trash extraction box, vertically arranged at least one piece is removed iron plate, and is additionally provided with net at the charging aperture of described trash extraction box Sieve uniform distributor.
As preferably, arranging rotary open type lid at described charging aperture, described rotary open type lid one end is certainly By holding, the other end is hingedly connected on the casing of described trash extraction box by jointed shaft.
As preferably, described step (7) three level screen, is respectively through 400 mesh, 200 mesh and 100 mesh by little for white carbon black granule Mesh screen carries out three level screen.
As preferably, in described step (8), the little granule of white carbon black and binding agent carry out kneading with the ratio of 5:1, wherein bond Agent is coal tar pitch.
The invention has the beneficial effects as follows: compared with prior art, the present invention thes improvement is that,
One, sets up except ferrum operates, and because containing the impurity such as irony in the raw material of pulverizing, therefore needs by trash separator its inside Impurity is purged, and so can improve the purity of raw material, so improve the quality of processing, electric conductivity and heat conductivity as well as Improve, also remove during the irony impurity in raw material is prevented from following process oxidized;
Its two, increase the screening stage, the final uniformity improving raw material is had a very big impact by setting up of screening stage, this Bright mentality of designing is to be sieved by three grades of screen clothes, thus can be further ensured that the uniformity of raw material degree, improves yield rate;
Its three, the present invention also set up die mould and heating before high temperature graphitization, heated immediately after die mould completes, be into A transition before row high temperature graphitization, so can improve the efficiency of high temperature graphitization, enters high temperature after reducing again die mould Gap in graphitizing furnace.
Its four, use the gum processing method under keeping warm mode, improve the activity of glue molecule, gum can not only be improved Effect, and gum efficiency can also be improved, and then improve the adhesiving effect of conductive graphite sheet and circuit board etc..
Detailed description of the invention
In order to make those of ordinary skill in the art be better understood on technical scheme, below in conjunction with embodiment Technical scheme is further described.
The technique preparing electronic equipment conductive graphite sheet based on white carbon black, comprises the following steps:
1) raw material: choose the white carbon black raw material as conductive graphite sheet;
2) precomminution: above-mentioned white carbon black is crushed in advance the medium size of 60-80mm through disintegrating apparatus, because of carbon raw material granularity Excessive, in calcination process, not only do not ensure the uniform quality after calcining, and affected by calciner, to charging and Discharge causes difficulty, it is ensured that the follow-up degree of depth that is capable of is calcined;
3) pre-screening: the white carbon black that above-mentioned warp crushes is sieved by vibrosieve, removes larger particles impurity in anthracite;
4) except ferrum: size-reduced white carbon black is carried out in being placed in trash separator except ferrum operates;
Trash separator includes trash extraction box, charging aperture, discharging opening and crutcher, vertically sets at the charging aperture of described trash extraction box Put at least one piece and remove iron plate, and at the charging aperture of described trash extraction box, be additionally provided with mesh screen uniform distributor, at described charging aperture Arranging rotary open type lid, described rotary open type lid one end is free end, and the other end is hingedly connected to by jointed shaft On the casing of described trash extraction box, the mesh of mesh screen uniform distributor is 60 or 80 mesh, so by by former for the graininess of precomminution Material enters mesh screen uniform distributor and is spread out uniform blanking, and the granule of blanking will spread out, it is simple to is inhaled by impurity and is removing On iron plate;
Except iron plate is vertically set up in parallel multiple in trash extraction box, each two is removed and is set to blanking channel between iron plate, precomminution Granule is from throat-fed, by being inhaled by irony impurity except on iron plate except iron plate during blanking, is rotation because of lid again Turn open-type lid, therefore when reaching certain thickness except ferrum, open lid, periodically clear up except iron plate, in order to avoid impact Dust removal rate and effect, it is simple, convenient that lid is arranged to rotary open type lid, it is possible to quickly realizes installing except the cleaning of iron plate Operation.
5) separating twice: the cooled white carbon black completed is ground into, through disintegrating apparatus, little that grain diameter is 0.3-0.5mm Grain;
6) regrading: carry out three level screen through the little granule of white carbon black of separating twice respectively through screening plant, filter out size Out, three level screen, is that through 400 mesh, 200 mesh and 100 mesh mesh screens, little for white carbon black granule is carried out three grades respectively to consistent granule Screening;The final uniformity improving raw material is had a very big impact by setting up of screening stage, and mentality of designing of the present invention is to pass through Three grades of screen clothes sieve, and thus can be further ensured that the uniformity of raw material degree, improve yield rate;
7) mixing: little for white carbon black granule and binding agent are carried out kneading, forms compound, and the little granule of white carbon black and binding agent are with 5:1's Ratio carries out kneading, and wherein binding agent is coal tar pitch;
8) die mould and heating: in a mold by compressing for above-mentioned compound, being pressed into square sheet shape, its thickness is at 0.01- Between 0.02mm, form conductive graphite sheet base substrate, arrange in mould and add hot channel, by adding hot channel, compressing is led Hot graphite flake base substrate tentatively heats, heating and temperature control between 200-300 DEG C, heat time heating time 30min;The present invention is at height Also set up die mould and heating before temperature graphitization, heat immediately after die mould completes, be by before high temperature graphitization Individual transition, so can improve the efficiency of high temperature graphitization, enters the gap in high temperature graphitization stove after reducing again die mould;
9) high temperature graphitization: carry out pyrographite in the conductive graphite sheet base substrate of above-mentioned heating is fed directly to high temperature graphitization stove Changing operation, the graphitization temperature scope in pyrographite stove is 1100-1200 DEG C, graphitization time 15-20min;
10) gum: in order to preferably adhere to IC and circuit board, need to carry out gum processing, through pyrographite on conductive graphite sheet Coat one layer of heat-resisting double faced adhesive tape in its bottom surface when conductive graphite sheet after change is cooled to 50-60 DEG C, and in conductive graphite sheet bottom surface Adhere to one layer of release paper;The present invention is to carry out gum technique when conductive graphite sheet temperature is down to certain limit, and it is than room temperature Advantage is that the bioactive molecule enabling to heat-resisting double faced adhesive tape increases, and preferably realizes double faced adhesive tape and release paper and conductive graphite sheet Bonding, improve gum effect and efficiency;
11) cutting: the conductive graphite sheet base substrate after graphitization forms the conductive graphite sheet of finished product, and cooling down, Jin Ertong Cross cutting equipment and cut into the size of needs.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and Equivalent defines.

Claims (5)

1. the technique preparing electronic equipment conductive graphite sheet based on white carbon black, it is characterised in that comprise the following steps:
1) raw material: choose the white carbon black raw material as conductive graphite sheet;
2) precomminution: above-mentioned white carbon black is crushed in advance through disintegrating apparatus the medium size of 60-80mm;
3) pre-screening: the white carbon black that above-mentioned warp crushes is sieved by vibrosieve, removes larger particles impurity in anthracite;
4) except ferrum: size-reduced white carbon black is carried out in being placed in trash separator except ferrum operates;
5) separating twice: the cooled white carbon black completed is ground into, through disintegrating apparatus, the little granule that grain diameter is 0.3-0.5mm;
6) regrading: carry out three level screen through the little granule of white carbon black of separating twice respectively through screening plant, filter out size Consistent granule is out;
7) mixing: little for white carbon black granule and binding agent are carried out kneading, forms compound;
8) die mould and heating: in a mold by compressing for above-mentioned compound, being pressed into square sheet shape, its thickness is at 0.01- Between 0.02mm, form conductive graphite sheet base substrate, arrange in mould and add hot channel, by adding hot channel, compressing is led Hot graphite flake base substrate tentatively heats, heating and temperature control between 200-300 DEG C, heat time heating time 30min;
9) high temperature graphitization: carry out pyrographite in the conductive graphite sheet base substrate of above-mentioned heating is fed directly to high temperature graphitization stove Change operation;
10) gum: the conductive graphite sheet after high temperature graphitization is cooled to when 50-60 DEG C heat-resisting two-sided its bottom surface coating one layer Glue, and one layer of release paper is adhered in conductive graphite sheet bottom surface;
11) cutting: the conductive graphite sheet base substrate after graphitization forms the conductive graphite sheet of finished product, and cooling down, Jin Ertong Cross cutting equipment and cut into the size of needs.
The technique preparing electronic equipment conductive graphite sheet based on white carbon black the most according to claim 1, it is characterised in that: institute The trash separator stated in step (3) includes trash extraction box, charging aperture, discharging opening and crutcher, in the charging of described trash extraction box At Kou, vertically arranged at least one piece is removed iron plate, and is additionally provided with mesh screen uniform distributor at the charging aperture of described trash extraction box.
The technique preparing electronic equipment conductive graphite sheet based on white carbon black the most according to claim 2, it is characterised in that: Arranging rotary open type lid at described charging aperture, described rotary open type lid one end is free end, and the other end is by hinged Axle is hingedly connected on the casing of described trash extraction box.
The technique preparing electronic equipment conductive graphite sheet based on white carbon black the most according to claim 1, it is characterised in that: institute State step (7) three level screen, be that little for white carbon black granule is carried out three level screen through 400 mesh, 200 mesh and 100 mesh mesh screens respectively.
The technique preparing electronic equipment conductive graphite sheet based on white carbon black the most according to claim 1, it is characterised in that: institute Stating the little granule of white carbon black and binding agent in step (8) and carry out kneading with the ratio of 5:1, wherein binding agent is coal tar pitch.
CN201610603043.8A 2016-07-28 2016-07-28 The technique that electronic equipment conductive graphite piece is prepared based on carbon black Active CN106231862B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113444499A (en) * 2021-06-25 2021-09-28 深圳市三科斯电子材料有限公司 Double-sided adhesive high-thermal-conductivity synthetic graphite flake and preparation method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101214945A (en) * 2007-12-26 2008-07-09 东华大学 Method for preparing high-strength thermal insulation asphalt carbon foam material
CN103805144A (en) * 2014-03-04 2014-05-21 中国科学院宁波材料技术与工程研究所 Graphene heat conducting film and preparation method thereof
TW201422524A (en) * 2012-12-10 2014-06-16 國立清華大學 Low-temperature manufacturing method and system for spheroidal graphite
CN104528693A (en) * 2009-05-26 2015-04-22 创业发展联盟技术有限公司 Carbon material and method for producing the same
US20150191357A1 (en) * 2012-07-23 2015-07-09 Graduate School At Shenzhen, Tsinghua University High-density and high-hardness graphene-based porous carbon material, method for making the same, and applications using the same
US20150360952A1 (en) * 2014-06-12 2015-12-17 Board Of Regents, The University Of Texas System Method for manufacturing of three-dimensional freestanding porous thin-graphite with hierarchical porosity
CN105419095A (en) * 2015-12-21 2016-03-23 赵社涛 Method for producing carbon black composite powder material

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101214945A (en) * 2007-12-26 2008-07-09 东华大学 Method for preparing high-strength thermal insulation asphalt carbon foam material
CN104528693A (en) * 2009-05-26 2015-04-22 创业发展联盟技术有限公司 Carbon material and method for producing the same
US20150191357A1 (en) * 2012-07-23 2015-07-09 Graduate School At Shenzhen, Tsinghua University High-density and high-hardness graphene-based porous carbon material, method for making the same, and applications using the same
TW201422524A (en) * 2012-12-10 2014-06-16 國立清華大學 Low-temperature manufacturing method and system for spheroidal graphite
CN103805144A (en) * 2014-03-04 2014-05-21 中国科学院宁波材料技术与工程研究所 Graphene heat conducting film and preparation method thereof
US20150360952A1 (en) * 2014-06-12 2015-12-17 Board Of Regents, The University Of Texas System Method for manufacturing of three-dimensional freestanding porous thin-graphite with hierarchical porosity
CN105419095A (en) * 2015-12-21 2016-03-23 赵社涛 Method for producing carbon black composite powder material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113444499A (en) * 2021-06-25 2021-09-28 深圳市三科斯电子材料有限公司 Double-sided adhesive high-thermal-conductivity synthetic graphite flake and preparation method thereof
CN113444499B (en) * 2021-06-25 2022-03-11 深圳市三科斯电子材料有限公司 Double-sided adhesive high-thermal-conductivity synthetic graphite flake and preparation method thereof

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Effective date of registration: 20191218

Address after: No. 36, Baima Industrial Park, Gaogang District, Taizhou City, Jiangsu Province

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Address before: 241006 Anhui Province, Wuhu City Economic Development Zone East Ouyang Hu Lu No. 28

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Effective date of registration: 20200514

Address after: 033000 Dongxu Shangzhuang village, Xiaoyi City, Luliang City, Shanxi Province

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Address after: 032300 Dong Xu Shang Zhuang Cun, Xiaoyi City, Luliang City, Shanxi Province

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