CN106225927B - A kind of detection method of colored fibre form and aspect - Google Patents

A kind of detection method of colored fibre form and aspect Download PDF

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Publication number
CN106225927B
CN106225927B CN201610526230.0A CN201610526230A CN106225927B CN 106225927 B CN106225927 B CN 106225927B CN 201610526230 A CN201610526230 A CN 201610526230A CN 106225927 B CN106225927 B CN 106225927B
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China
Prior art keywords
sample
silk
cup
detection method
aberration
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CN201610526230.0A
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Chinese (zh)
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CN106225927A (en
Inventor
潘洪庆
陈霞
郑立康
冯赛花
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JIANGSU DESAI CHEMICAL FIBER CO Ltd
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JIANGSU DESAI CHEMICAL FIBER CO Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/46Measurement of colour; Colour measuring devices, e.g. colorimeters

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Spectrometry And Color Measurement (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The present invention relates to a kind of detection method of colored fibre form and aspect, it is divided into the measure of no silk noil form and aspect:(1) sample of neat even thickness in the middle of no 15 grams of silk noil sample, clip is weighed;(2) will carefully it be shredded without silk noil with scissors, of length no more than 3mm;(3) sample is laid in aberration cup;(4) it will be placed on regulation soft interface, be gently compacted with counterweight in aberration cup;(5) first group of data is tested;(6) sample is handled again and stirred, repeat 3~4 steps, tested 3 times, calculate its average value;(7) according to GB/T8170 by the L a b values revisions of the convention to 2 significant digits.The principle of the present invention is that automatic colour difference meter is that tristimulus method determines color.Sample is placed under standard sources, respectively by three photoelectric tubes that red, green, blue colour filter is housed, and produced photoelectric current and luminous energy is directly proportional, and its value is shown with numeral on colour difference meter.

Description

A kind of detection method of colored fibre form and aspect
【Technical field】
It is a kind of detection method of colored fibre form and aspect specifically the present invention relates to fiber form and aspect field of measuring technique.
【Background technology】
Color measuring term.One of attribute of color, so as to distinguishing a variety of colors such as red, yellow, green, blue with title.Color Phase, i.e., the appearance appellation of all kinds of colors, such as bright red, Prussian blue, lemon yellow.Form and aspect are the primary features of color, are that difference is various The most accurate standard of different color.In fact the color beyond any black-white-gray has the attribute of form and aspect, and form and aspect are namely It is made up of primary colors, secondary color and secondary color.The feature of form and aspect is decided by spectral composition and the reflection of colored objects surface of light source Each wavelength radiation ratio to the sensation produced by human eye.When measuring color, hue angle H and dominant wavelength λ d (nm) table can be used Show.It is according to the dominant wavelength of the XZY series expressions of the color colour sensation corresponding with complementary dominant wavelength in the polymer.It is general high poly- Thing is compared with standard color systcm solution in the molten state in itself, and the color standard consistent with its is known as the number of phases of showing signs of anger, due to high polymer Species is a lot, and standard color systcm is also a lot.Working standard colour system is prepared by national Specification method.From optical significance Say, form and aspect difference is produced by the length of optical wavelength.Even same class color, can also be divided into several form and aspect, such as yellow face Color can be divided into middle Huang, the colour of loess, lemon yellow etc., and grey color can then be divided into red grey, bluish grey, purple ash etc..Have in spectrum it is red, orange, Yellow, green, blue, purple six kinds basic coloured light, the eyes of people can tell the color of about 180 kinds of different form and aspect.
Colored fibre is that appropriate pigment or dyestuff is mixed during production of chemical fibre, is directly prepared into colored fibre Method, is coloured before also known as spinning.Chemical fibre coloring is different from normal dyeing mechanism.The former is that to be evenly dispersed in colouring agent poly- In zoarium, through the agent of spinning technique after stain i.e. by set in the fibre, coloring process belongs to physical change;The latter is to be spun into fiber Dye again afterwards, it is desirable to which dyestuff or pigment have certain adhesion and affinity with condensate, and dyeing course principally falls into chemical change Change.
【The content of the invention】
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of detection method of colored fibre form and aspect.
The purpose of the present invention is achieved through the following technical solutions:
A kind of detection method of colored fibre form and aspect, it is concretely comprised the following steps:
Wherein it is divided into the measure of no silk noil form and aspect:
(1) sample of neat even thickness in the middle of no 15 grams of silk noil sample, clip is weighed.
(2) will carefully it be shredded without silk noil with scissors, of length no more than 3mm.
(3) sample is laid in aberration cup.
(4) it will be placed on regulation soft interface, be gently compacted with counterweight in aberration cup.
(5) first group of data is tested.
(6) sample is handled again and stirred, repeat 3~4 steps, tested 3 times, calculate its average value.
(7) according to GB/T8170 by the Lab values revision of the convention to 2 significant digits.
(8) points for attention:
A) this sample is careful not to suck trickle sample filaments because being the silk shredded, during analysis, with wearing appliances for labor protection.
B) it is completed and cleans out sample cup for liquid, colour difference meter and desktop.
Also it is exactly finished silk color molybdenum determination:
(1) finished silk has been taken, it has once been combed on carding machine fluffy.
(2) the sample 6g combed is weighed, carefully along being put into specimen cup well, compacting is patted, reads Lab values.
(3) sample is taken out from specimen cup again and repeats (2) operation 3 times, averaged.
(4) according to the GB/T8170 data revision of the convention to 2 significant digits.
Measuring instrument:Automatic colour difference meter:D65 light sources, 10 DEG C of visual angles, Hunterlab colour systems.
Specimen cup:Quartz glass.
Compared with prior art, the positive effect of the present invention is:
The principle of the present invention is that automatic colour difference meter is that tristimulus method determines color.Sample is placed under standard sources, is led to respectively Three photoelectric tubes that red, green, blue colour filter is housed are crossed, produced photoelectric current and luminous energy is directly proportional, and its value is with numeral in aberration Shown on meter.
Purpose:Control the appearance color of silk.
Our company, without section particle production, is not cut into slices using fused mass directly spinning and is controlled adjustment to the form and aspect of product, because Oil-free wire chemical property is substantially similar with polyester fondant, it is contemplated that carry out form and aspect prison to polyester product using the form and aspect result without silk noil Control, in order to which production of polyester carries out real-time policer operation to product form and aspect.Coloured finished fiber with the naked eye can not accurately judge it Aberration, therefore in view of being tested it using colour difference meter, it is to avoid naked eyes judge the significant errors produced.
【Embodiment】
A kind of embodiment of the detection method of colored fibre form and aspect of the invention presented below.
Embodiment 1
A kind of detection method of colored fibre form and aspect, it is concretely comprised the following steps:
Wherein it is divided into the measure of no silk noil form and aspect:
(1) sample of neat even thickness in the middle of no 15 grams of silk noil sample, clip is weighed.
(2) will carefully it be shredded without silk noil with scissors, of length no more than 3mm.
(3) sample is laid in aberration cup.
(4) it will be placed on regulation soft interface, be gently compacted with counterweight in aberration cup.
(5) first group of data is tested.
(6) sample is handled again and stirred, repeat 3~4 steps, tested 3 times, calculate its average value.
(7) according to GB/T8170 by the Lab values revision of the convention to 2 significant digits.
(8) points for attention:
A) this sample is careful not to suck trickle sample filaments because being the silk shredded, during analysis, with wearing appliances for labor protection.
B) it is completed and cleans out sample cup for liquid, colour difference meter and desktop.
Measuring instrument:Automatic colour difference meter:D65 light sources, 10 DEG C of visual angles, Hunterlab colour systems.
Specimen cup:Quartz glass.
Embodiment 2
Finished silk color molybdenum determination:
(1) finished silk has been taken, it has once been combed on carding machine fluffy.
(2) the sample 6g combed is weighed, carefully along being put into specimen cup well, compacting is patted, reads Lab values.
(3) sample is taken out from specimen cup again and repeats (2) operation 3 times, averaged.
(4) according to the GB/T8170 data revision of the convention to 2 significant digits.
Measuring instrument:Automatic colour difference meter:D65 light sources, 10 DEG C of visual angles, Hunterlab colour systems.
Specimen cup:Quartz glass.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art Member, without departing from the inventive concept of the premise, can also make some improvements and modifications, these improvements and modifications also should be regarded as In protection scope of the present invention.

Claims (3)

1. a kind of detection method of colored fibre form and aspect, it is characterised in that it is concretely comprised the following steps:
Wherein it is divided into the measure of no silk noil form and aspect:
(1) sample of neat even thickness in the middle of no 15 grams of silk noil sample, clip is weighed;
(2) will carefully it be shredded without silk noil with scissors, of length no more than 3mm;
(3) sample is laid in aberration cup;
(4) it will be placed on regulation soft interface, be gently compacted with counterweight in aberration cup;
(5) first group of data is tested;
(6) sample is handled again and stirred, repeat 3~4 steps, tested 3 times, calculate its average value;
(7) according to GB/T8170 by the L a b values revisions of the convention to 2 significant digits.
2. a kind of detection method of colored fibre form and aspect as claimed in claim 1, it is characterised in that
This sample is careful not to suck trickle sample filaments because being the silk shredded, during analysis.
3. a kind of detection method of colored fibre form and aspect as claimed in claim 1, it is characterised in that the survey of finished silk form and aspect It is fixed:
(1) finished silk has been taken, it has once been combed on carding machine fluffy;
(2) the sample 6g combed is weighed, carefully along being put into specimen cup well, compacting is patted, reads L a b values;
(3) sample is taken out from specimen cup again and repeats (2) operation 3 times, averaged;
(4) according to the GB/T8170 data revision of the convention to 2 significant digits.
CN201610526230.0A 2016-07-05 2016-07-05 A kind of detection method of colored fibre form and aspect Active CN106225927B (en)

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Application Number Priority Date Filing Date Title
CN201610526230.0A CN106225927B (en) 2016-07-05 2016-07-05 A kind of detection method of colored fibre form and aspect

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CN106225927B true CN106225927B (en) 2017-09-29

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103541039A (en) * 2012-08-08 2014-01-29 江苏德赛化纤有限公司 Multifunctional modified polyester staple fiber and preparation method of same
CN204173239U (en) * 2014-10-16 2015-02-25 巨石集团有限公司 For identifying the device that silvalin is rolled into a ball
CN104838255A (en) * 2012-11-15 2015-08-12 弗兰霍菲尔运输应用研究公司 Measuring a fibre direction of a carbon fibre material and producing an object in a carbon-fibre composite construction

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002296115A (en) * 2001-04-02 2002-10-09 Unitec:Kk Method of measuring tone of light emitting body, measuring device for the same, and measuring device for brightness of light emitting body

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103541039A (en) * 2012-08-08 2014-01-29 江苏德赛化纤有限公司 Multifunctional modified polyester staple fiber and preparation method of same
CN104838255A (en) * 2012-11-15 2015-08-12 弗兰霍菲尔运输应用研究公司 Measuring a fibre direction of a carbon fibre material and producing an object in a carbon-fibre composite construction
CN204173239U (en) * 2014-10-16 2015-02-25 巨石集团有限公司 For identifying the device that silvalin is rolled into a ball

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