CN106147695A - Quick cured silicone glue of one 1 to 1 double-component and preparation method thereof - Google Patents
Quick cured silicone glue of one 1 to 1 double-component and preparation method thereof Download PDFInfo
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- CN106147695A CN106147695A CN201610492217.8A CN201610492217A CN106147695A CN 106147695 A CN106147695 A CN 106147695A CN 201610492217 A CN201610492217 A CN 201610492217A CN 106147695 A CN106147695 A CN 106147695A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J183/00—Adhesives based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Adhesives based on derivatives of such polymers
- C09J183/04—Polysiloxanes
- C09J183/06—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Sealing Material Composition (AREA)
Abstract
The present invention proposes the quick cured silicone glue of one 1 to 1 double-component, including fluid sealant component A and B component, component A is 1 to 1 with the mass ratio of B component, and wherein the composition of component A includes the raw material of following mass fraction: the coupling agent of the basic glue of 100 parts, the filler of 10 ~ 150 parts, the hydroxyl scavenger of 0.1 ~ 5 part, the crosslinking agent of 1 ~ 10 part and 1 ~ 10 part；The composition of B component includes the raw material of following mass fraction: the catalyst of the basic glue of 100 parts, the filler of 10 ~ 150 parts, the plasticizer of 5 ~ 20 parts and 0.1 ~ 2 part, the invention allows for the preparation method of above-mentioned organic silica gel.In multiple industries needing silica gel adhering and sealing, the present invention realizes that short time rapid link fixes purpose, greatly reduce manufacturer production operation time-consuming, improves production efficiency, when being applied especially to produce in enormous quantities, can significantly save producer's cost of labor.
Description
Technical field
The present invention relates to quick cured silicone glue of one 1 to 1 double-component and preparation method thereof.
Background technology
Adhering and sealing organic silica gel traditional at present mostly is the bi-component silicon of One Component Silicons Construction Sealant or 10 to 1
Structure sealant.
One Component Silicons Construction Sealant curing mode from outward appearance to inner essence solidifies for absorbing moisture, there is curing rate slow, and 24 is little
Shi Pingjun just solidifies 3 to 4 mm of thickness, can not meet some industry rapid link and fixes and the requirement of large area bonding.10
Although solving quick-setting problem than 1 bicomponent structure fluid sealant, but sizing equipment being required higher by 10 to 1 bi-components,
The sizing equipment that one is common on the market at present is typically difficult to the metering accurate in scale by 10 to 1, and two is existing on market
10 to 1 bi-component sizing equipment price comparisons high, simultaneously because the ratio of B component is too small, can often occur mixing uneven
Phenomenon, these factors finally have impact on universal in each manufacturing of 10 to 1 bi-components and promote, current 10 to 1 pairs of groups
Divide and seal the glass curtain wall adhering and sealing that silica gel is mainly used in building trade.
Content of the invention
The technical problem to be solved, it is simply that propose the quick cured silicone glue of one 1 to 1 double-component, can be real
The industry of existing silica gel adhering and sealing realizes the fixing purpose of short time rapid link.
The invention allows for the preparation method of above-mentioned rapid curing organic silica gel.
For solving above-mentioned technical problem, the present invention is achieved by the following technical solutions:
The quick cured silicone glue of one 1 to 1 double-component, including the quality of fluid sealant component A and B component, component A and B component
Ratio is 1 to 1, and wherein the composition of component A includes the raw material of following mass fraction: the basic glue of 100 parts, the filler of 10 ~ 150 parts,
The coupling agent of the hydroxyl scavenger of 0.1 ~ 5 part, the crosslinking agent of 1 ~ 10 part and 1 ~ 10 part；
The composition of B component includes the raw material of following mass fraction: the basic glue of 100 parts, the filler of 10 ~ 150 parts, the increasing of 5 ~ 20 parts
Mould the catalyst of agent and 0.1 ~ 2 part.
As preferably, described basis glue be described basis glue be α, alpha, omega-dihydroxy polydimethyl siloxane, methyl dimethoxy
Epoxide silica-based end-blocking dimethyl silicone polymer, trimethoxy silica-based end-blocking dimethyl silicone polymer, hydroxy silicon oil, silane-modified poly-
One or more in urethane, silane modified polyether.
As preferably, the viscosity of described basis glue is 2000～100000cps.
As preferably, described filler is nano-calcium carbonate, powdered whiting, precipitated calcium carbonate, silicon powder, precipitation hard charcoal
One or more in black, gas-phase silica, aluminium hydroxide, magnesium hydroxide, aluminum oxide, zinc oxide.
As preferably, described hydroxyl scavenger is molecular sieve, HMDS, isocyanate ester compound, fourth
One or more in lactone, caprolactone.
As preferably, described crosslinking agent is R1 nSi(OR2)4-n(R1=Me、Et、Vi、Ph；R2=Me、Et、Pr；n=0、1、
2), as in methyl silicate, tetraethyl orthosilicate, positive silicic acid propyl ester, MTMS, vinyltrimethoxy silane
One or more.
As preferably, described coupling agent is the alkane containing amido and/or epoxy radicals and/or vinyl and/or acyloxy
TMOS.
As preferably, described coupling agent is γ-aminopropyl triethoxysilane, γ-glycidyl ether oxygen propyl front three
TMOS, N-(β-aminoethyl)-γ-aminopropyl trimethoxysilane, γ-(methacryloxypropyl) propyl group trimethoxy
One or more in base silane.
As preferably, described plasticizer be dimethicone, vinyl silicone oil, containing hydrogen silicone oil, the one in white oil or
Multiple, the viscosity of plasticizer is 350 ~ 500cps.
As preferably, described catalyst is dibutyltin diacetate, dibutyl tin laurate, tin dilaurate dioctyl
One in tin, stannous octoate, Dibutyltin oxide.
The preparation method of a kind of 1 to 1 quick cured silicone glue of double-component, it is characterised in that comprise the following steps:
(1) prepare component A, add basis glue, filler in the mixer with heating and depressurized system on request, be warming up to 120
Decompression stirring 2 hours under DEG C high temperature, add hydroxyl scavenger, crosslinking agent, coupling agent, normal temperature decompression stirring half after being cooled to room temperature
Prepared component A of hour；
(2) prepare component B, add basis glue, filler in the mixer with heating and depressurized system on request, be warming up to 120
Decompression stirring 2 hours under DEG C high temperature, add plasticizer and catalyst after being cooled to room temperature, normal temperature decompression stirring prepares group half an hour
Divide B；
(3) when using, component A, B are carried out mixing according to mass ratio 1:1.
Compared with prior art, the device have the advantages that for: (1) realizes short time rapid curing, improves and produces
Efficiency；(2) sizing equipment cost is relatively low, solves the unfavorable popularization of 10 to 1 bi-components and easily mixes a uneven difficult problem, can answer
For all trades and professions needing rapid link to fix；(3) relative one pack system, can realize large area bonding.Generally speaking, the present invention
Realize that short time rapid link fixes purpose in multiple industries needing silica gel adhering and sealing, greatly reduce manufacturer production operation consumption
When, improve production efficiency, when being applied especially to produce in enormous quantities, can significantly save producer's cost of labor.
Brief description
Fig. 1 is the preparation technology flow chart of instant component A；
Fig. 2 is the preparation technology flow chart of instant component B.
Detailed description of the invention
Get information about the present invention for allowing those skilled in the art become apparent from, below in conjunction with accompanying drawing, to the present invention
It is further described.
Embodiment 1
1 to the 1 quick cured silicone glue of double-component of the present embodiment, including fluid sealant component A and B component, the wherein group of component A
Become and include the raw material of following mass fraction: the α of 100 parts of viscosity 5000cps, alpha, omega-dihydroxy polydimethyl siloxane, 120 parts receive
Rice calcium carbonate, 2 parts of molecular sieves, 2 parts of positive silicic acid propyl ester, 3 parts of MTMSs, 1 part of γ-aminopropyl-triethoxy silicon
Alkane, 1 part of γ-glycidyl ether oxygen propyl trimethoxy silicane, its preparation process is: by the α of 100 parts of viscosity 5000cps, ω-
Dialkyl polydimethylsiloxane and 120 parts of nano-calcium carbonates add in the mixer with heating and depressurized system, are warming up to 120
Decompression stirring 2 hours under DEG C high temperature, add 2 parts of molecular sieves, 2 parts of positive silicic acid propyl ester, 3 parts of methyl trimethoxy epoxides after being cooled to room temperature
Silane, 1 part of γ-aminopropyl triethoxysilane, 1 part of γ-glycidyl ether oxygen propyl trimethoxy silicane, normal temperature decompression is stirred
Mix and prepare component A half an hour；
The composition of B component includes the raw material of following mass fraction: the α of 80 parts of viscosity 20000cps, alpha, omega-dihydroxy polydimethyl silicon
Oxygen alkane, the methyl dimethoxy epoxide silica-based end-blocking dimethyl silicone polymer of 20 parts of viscosity 5000cps, 120 parts of nano-calcium carbonates, 15 parts
The dimethicone of viscosity 350cps and 0.1 part of stannous octoate, its preparation process is: by the α of 80 parts of viscosity 20000cps, ω-
Dialkyl polydimethylsiloxane, the methyl dimethoxy epoxide silica-based end-blocking dimethyl silicone polymer and 120 of 20 parts of viscosity 5000cps
Part nano-calcium carbonate adds in the mixer with heating and depressurized system, is warming up under 120 DEG C of high temperature decompression and stirs 2 hours, cold
But the dimethicone of 15 parts of viscosity 350cps and 0.1 part of stannous octoate normal temperature decompression stirring is added to prepare half an hour to room temperature
Component B；
Prepared component A and B component 1:1 in mass ratio are mixed, i.e. can be used for the adhering and sealing of every profession and trade.
Embodiment 2
1 to the 1 quick cured silicone glue of double-component of the present embodiment, including fluid sealant component A and B component, the wherein group of component A
Become and include the raw material of following mass fraction: the α of 70 parts of viscosity 50000cps, alpha, omega-dihydroxy polydimethyl siloxane, 30 parts
The trimethoxy of 2000cps silica-based end-blocking dimethyl silicone polymer, 12 parts of Nano carbon whites, 5 parts of HMDSs, 8 parts
Tetraethyl orthosilicate alkane, 5 parts of γ-(methacryloxypropyl) propyl trimethoxy silicanes, its preparation process is as follows: by 70 parts of viscosity
The α of 50000cps, alpha, omega-dihydroxy polydimethyl siloxane, the trimethoxy silica-based end-blocking polydimethylsiloxanes of 30 parts of 2000cps
Alkane and 12 parts of Nano carbon whites add in the mixer with heating and depressurized system, are warming up under 120 DEG C of high temperature decompression stirring 2 little
When, add 5 parts of HMDSs, 8 parts of tetraethyl orthosilicate alkane, 5 parts of γ-(methacryloxypropyl) propyl group after being cooled to room temperature
Trimethoxy silane, normal temperature decompression stirring prepares component A half an hour；
The composition of B component includes the raw material of following mass fraction: the α of 100 parts of viscosity 20000cps, alpha, omega-dihydroxy polydimethyl
Siloxanes, 10 parts of Nano carbon whites, the dimethicone of 10 parts of viscosity 350cps and 1 part of dibutyltin diacetate, it prepares step
Suddenly it is: by the α of 100 parts of viscosity 20000cps, alpha, omega-dihydroxy polydimethyl siloxane and 10 parts of Nano carbon whites add band heating
It with in the mixer of depressurized system, is warming up under 120 DEG C of high temperature decompression stirring 2 hours, after being cooled to room temperature, add 10 parts of viscosity
The dimethicone of 350cps and 1 part of dibutyltin diacetate normal temperature decompression stirring prepare component B half an hour；
Mixing prepared component A and B component 1:1 in mass ratio, i.e. can be used for every profession and trade has the adhering and sealing of transparent requirement.
Embodiment 3
1 to the 1 quick cured silicone glue of double-component of the present embodiment, including fluid sealant component A and B component, the wherein group of component A
Become to include the raw material of following mass fraction: the α of 100 parts of viscosity 2000cps, alpha, omega-dihydroxy polydimethyl siloxane, 100 parts of hydrogen
Aluminum oxide, 50 parts of zinc oxide, 3 parts of molecular sieves, 6 parts of phenyltrimethoxysila,e, 2.5 parts of γ-aminopropyl triethoxysilanes,
Its preparation process is as follows: by the α of 100 parts of viscosity 2000cps, alpha, omega-dihydroxy polydimethyl siloxane, 100 parts of aluminium hydroxides and
50 parts of zinc oxide add in the mixer with heating and depressurized system, are warming up under 120 DEG C of high temperature decompression stirring 2 hours, cooling
Adding 3 parts of molecular sieves, 6 parts of phenyltrimethoxysila,e, 2.5 parts of γ-aminopropyl triethoxysilanes to room temperature, normal temperature subtracts
Pressure stirring prepares component A half an hour；
The composition of B component includes the raw material of following mass fraction: the α of 50 parts of viscosity 50000cps, alpha, omega-dihydroxy polydimethyl silicon
Oxygen alkane, the α of 50 parts of viscosity 500cps, alpha, omega-dihydroxy polydimethyl siloxane, 120 parts of aluminium hydroxide, 30 parts of zinc oxide, 20 parts
The dimethicone of viscosity 500cps and 0.8 part of dibutyl tin laurate, its preparation process is as follows: by 50 parts of viscosity
The α of 50000cps, alpha, omega-dihydroxy polydimethyl siloxane, the α of 50 parts of viscosity 500cps, alpha, omega-dihydroxy polydimethyl silica
Alkane, 120 parts of aluminium hydroxides and 30 parts of zinc oxide add in the mixer with heating and depressurized system, are warming up under 120 DEG C of high temperature
Decompression stirring 2 hours, is cooled to after room temperature add the dimethicone of 20 parts of viscosity 500cps and 0.8 part of di lauric dibutyl
The decompression stirring of tin normal temperature prepares component B half an hour；
Mixing prepared component A and B component 1:1 in mass ratio, i.e. can be used for every profession and trade has the adhering and sealing of flame-retardancy requirements.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (10)
1. the quick cured silicone glue of a double-component, it is characterised in that include fluid sealant component A and B component, component A with
The mass ratio of B component is 1 to 1, and wherein the composition of component A includes the raw material of following mass fraction: the basic glue of 100 parts, 10 ~
The coupling agent of the filler of 150 parts, the hydroxyl scavenger of 0.1 ~ 5 part, the crosslinking agent of 1 ~ 10 part and 1 ~ 10 part；The composition of B component
Including the raw material of following mass fraction: the basic glue of 100 parts, the filler of 10 ~ 150 parts, the plasticizer of 5 ~ 20 parts and 0.1 ~ 2 part
Catalyst.
2. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described basis glue is α,
Alpha, omega-dihydroxy polydimethyl siloxane, methyl dimethoxy epoxide silica-based end-blocking dimethyl silicone polymer, the silica-based end-blocking of trimethoxy are poly-
One or more in dimethyl siloxane, hydroxy silicon oil, silicane-modified polyurethane, silane modified polyether.
3. 1 to the 1 quick cured silicone glue of double-component according to claim 2, it is characterised in that: described basis glue viscous
Degree is 2000～100000cps.
4. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described filler is nanometer
Calcium carbonate, powdered whiting, precipitated calcium carbonate, silicon powder, precipitated silica, gas-phase silica, aluminium hydroxide, magnesium hydroxide,
One or more in aluminum oxide, zinc oxide.
5. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described hydroxyl scavenger
For one or more in molecular sieve, HMDS, isocyanate ester compound, butyrolactone, caprolactone.
6. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described crosslinking agent is
R1 nSi(OR2)4-n(R1=Me、Et、Vi、Ph；R2=Me、Et、Pr；N=0, the 1st, 2).
7. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described coupling agent for containing
There is the alkoxy silane of amido and/or epoxy radicals and/or vinyl and/or acyloxy.
8. 1 to the 1 quick cured silicone glue of double-component according to claim 7, it is characterised in that: described coupling agent is
γ-aminopropyl triethoxysilane, γ-glycidyl ether oxygen propyl trimethoxy silicane, N-(β-aminoethyl)-γ-
One or more in aminopropyl trimethoxysilane, γ-(methacryloxypropyl) propyl trimethoxy silicane.
9. 1 to the 1 quick cured silicone glue of double-component according to claim 1, it is characterised in that: described plasticizer is two
One or more in methyl-silicone oil, vinyl silicone oil, containing hydrogen silicone oil, white oil, described catalyst be dibutyltin diacetate, two
One in dibutyl tin laurate, tin dilaurate dioctyl tin, stannous octoate, Dibutyltin oxide.
10. a preparation method for 1 to the 1 quick cured silicone glue of double-component according to any one of claim 1 ~ 9, its
It is characterised by comprising the following steps:
(1) prepare component A, add basis glue, filler in the mixer with heating and depressurized system on request, be warming up to 120
Decompression stirring 2 hours under DEG C high temperature, add hydroxyl scavenger, crosslinking agent, coupling agent, normal temperature decompression stirring half after being cooled to room temperature
Prepared component A of hour；
(2) prepare component B, add basis glue, filler in the mixer with heating and depressurized system on request, be warming up to 120
Decompression stirring 2 hours under DEG C high temperature, add plasticizer and catalyst after being cooled to room temperature, normal temperature decompression stirring prepares group half an hour
Divide B；
(3) when using, component A, B are carried out mixing according to mass ratio 1:1.
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| CN201610492217.8A CN106147695A (en) | 2016-06-29 | 2016-06-29 | Quick cured silicone glue of one 1 to 1 double-component and preparation method thereof |
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| CN201610492217.8A CN106147695A (en) | 2016-06-29 | 2016-06-29 | Quick cured silicone glue of one 1 to 1 double-component and preparation method thereof |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106868891A (en) * | 2017-04-20 | 2017-06-20 | 东莞市科多有机硅材料有限公司 | Silk-screen printing spends silica gel and preparation method thereof with nature xerography |
| CN107502265A (en) * | 2017-09-20 | 2017-12-22 | 东莞市科惠工业材料有限公司 | A kind of very fast glue |
| CN107699183A (en) * | 2017-09-29 | 2018-02-16 | 东莞市科惠工业材料有限公司 | A kind of ground heating floor installs glue |
| CN108467706A (en) * | 2018-03-28 | 2018-08-31 | 卡本复合材料（天津）有限公司 | A kind of one pack system assembled architecture outer wall splicing seams MS fluid sealants and preparation method thereof |
| CN109096983A (en) * | 2018-07-09 | 2018-12-28 | 广州城建职业学院 | A kind of preparation method of two-component condensed type building structure sealant |
| CN109666435A (en) * | 2018-12-06 | 2019-04-23 | 成都硅宝科技股份有限公司 | A kind of mould proof silane modified polyether glue of bi-component and preparation method thereof |
| WO2019095468A1 (en) * | 2017-11-16 | 2019-05-23 | 刘展标 | Glass/ceramic container and method for manufacturing same |
| CN110373151A (en) * | 2019-08-23 | 2019-10-25 | 深圳市红叶杰科技有限公司 | A kind of room temperature fast-curing wire and cable packaging silicon rubber and preparation method thereof |
| CN110387210A (en) * | 2019-07-31 | 2019-10-29 | 中广核达胜加速器技术有限公司 | A kind of preparation method based on the cured adhesive of EB and the mica tape with it |
| CN110591635A (en) * | 2019-07-05 | 2019-12-20 | 惠州瑞德新材料科技股份有限公司 | Sealant and preparation method thereof |
| CN110591638A (en) * | 2019-11-04 | 2019-12-20 | 镇江博慎新材料有限公司 | Low-proportion bi-component dealcoholized organosilicon sealant and preparation method and application thereof |
| CN110684358A (en) * | 2019-10-14 | 2020-01-14 | 东莞市跨越电子有限公司 | Filling foaming encapsulation silica gel for new energy power battery, preparation method and application |
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Cited By (24)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106868891B (en) * | 2017-04-20 | 2018-05-04 | 东莞市科多有机硅材料有限公司 | Silk-screen printing nature xerography flower silica gel and preparation method thereof |
| CN106868891A (en) * | 2017-04-20 | 2017-06-20 | 东莞市科多有机硅材料有限公司 | Silk-screen printing spends silica gel and preparation method thereof with nature xerography |
| CN107502265A (en) * | 2017-09-20 | 2017-12-22 | 东莞市科惠工业材料有限公司 | A kind of very fast glue |
| CN107699183A (en) * | 2017-09-29 | 2018-02-16 | 东莞市科惠工业材料有限公司 | A kind of ground heating floor installs glue |
| WO2019095468A1 (en) * | 2017-11-16 | 2019-05-23 | 刘展标 | Glass/ceramic container and method for manufacturing same |
| CN108467706A (en) * | 2018-03-28 | 2018-08-31 | 卡本复合材料（天津）有限公司 | A kind of one pack system assembled architecture outer wall splicing seams MS fluid sealants and preparation method thereof |
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