CN106147084A - A kind of antibacterial medical packaging material and preparation method thereof - Google Patents
A kind of antibacterial medical packaging material and preparation method thereof Download PDFInfo
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- CN106147084A CN106147084A CN201610711658.2A CN201610711658A CN106147084A CN 106147084 A CN106147084 A CN 106147084A CN 201610711658 A CN201610711658 A CN 201610711658A CN 106147084 A CN106147084 A CN 106147084A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
- C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L27/04—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C08L27/06—Homopolymers or copolymers of vinyl chloride
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/02—Applications for biomedical use
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/16—Applications used for films
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
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Abstract
nullThe invention discloses a kind of antibacterial medical packaging material and preparation method thereof，Described antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 20 45 parts，Permethrin 12 25 parts，Polyethylene terephthalate 8 18 parts，Nano titanium oxide 3 10 parts，Nanometer silver 28 parts，Polyimide 12 25 parts，Polyglycolic acid 10 22 parts，Zinc oxide 38 parts，Acrylamide 5 12 parts，Ammonium dihydrogen phosphate 3 10 parts，6 14 parts of polyester fiber，Arcton 11 1 2.5 parts，Polyether sulfone 2.5 7 parts，Diphenyl dichlorosilane 4 11 parts，Calcium carbonate 27 parts，Titanate coupling agent 26 parts，Cumyl peroxide 5 12 parts，Alkyl benzene calcium sulfonate 39 parts，Dimethylaminopropylamine 28 parts，Ethylene-vinyl acetate copolymer 3 13 parts.Compared with prior art, the antibacterial medical packaging material in the present invention has the advantages such as intensity is high, preparation method is simple, has good antibacterial effect simultaneously concurrently, can effectively suppress microbial activities, is particularly suited for field of medicaments.
Description
Technical field
The present invention relates to a kind of packaging material, particularly relate to a kind of antibacterial medical packaging material and preparation method thereof.
Background technology
Packaging material are widely used in the every field of Chinese society, such as, medical package field and food packaging applications
Deng, in order to improve the sanitary condition of medical industry or food service industry, before packaging, producer needs to enter medicine or packaging material for food
Row sterilization treatment.But, drug packing material surface breed bacteria but cannot effectively solve, thus makes the sanitary condition of medicine
Become impact.
Summary of the invention
It is an object of the invention to provide a kind of antibacterial medical packaging material, it has, and intensity is high, tensile resistence is strong and resists
The advantages such as bacterium is effective.
For achieving the above object, the present invention provides following technical scheme:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 20-45 part, Permethrin
12-25 part, polyethylene terephthalate 8-18 part, nano titanium oxide 3-10 part, nanometer silver 2-8 part, polyimide 12-25
Part, polyglycolic acid 10-22 part, zinc oxide 3-8 part, acrylamide 5-12 part, ammonium dihydrogen phosphate 3-10 part, polyester fiber 6-14
Part, Arcton 11 1-2.5 part, polyether sulfone 2.5-7 part, diphenyl dichlorosilane 4-11 part, calcium carbonate 2-7 part, titanate esters is even
Connection agent 2-6 part, cumyl peroxide 5-12 part, alkyl benzene calcium sulfonate 3-9 part, dimethylaminopropylamine 2-8 part, ethyl vinyl acetate
Ethylene copolymer 3-13 part.
Preferably, described antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 34 parts, chlorine
Chrysanthemum ester 16 parts, polyethylene terephthalate 12 parts, nano titanium oxide 8 parts, nanometer silver 5 parts, polyimide 23 parts, poly-hydroxyl
Acetic acid 16 parts, zinc oxide 4 parts, acrylamide 8 parts, ammonium dihydrogen phosphate 5 parts, 11 parts of polyester fiber, Arcton 11 1.4 parts, poly-
Ether sulfone 4.5 parts, diphenyl dichlorosilane 8 parts, calcium carbonate 6 parts, titanate coupling agent 3.6 parts, cumyl peroxide 9 parts, alkane
Base benzenesulfonic acid calcium 7 parts, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 10 parts.
Preferably, described antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 36 parts, chlorine
Chrysanthemum ester 21 parts, polyethylene terephthalate 15 parts, nano titanium oxide 6 parts, nanometer silver 5.6 parts, polyimide 18 parts, poly-hydroxyl
Guanidine-acetic acid 17 parts, zinc oxide 5 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 8 parts, 13 parts of polyester fiber, Arcton 11 2 parts, poly-
Ether sulfone 4 parts, diphenyl dichlorosilane 8 parts, calcium carbonate 5 parts, titanate coupling agent 5 parts, cumyl peroxide 11 parts, alkylbenzene
Sulfoacid calcium 7 parts, dimethylaminopropylamine 4 parts, ethylene-vinyl acetate copolymer 7 parts.
Preferably, described antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 40 parts, chlorine
Chrysanthemum ester 20 parts, polyethylene terephthalate 12 parts, nano titanium oxide 6 parts, nanometer silver 5 parts, polyimide 22 parts, poly-hydroxyl
Acetic acid 15 parts, zinc oxide 6 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 10 parts, 9 parts of polyester fiber, Arcton 11 2.3 parts, poly-
Ether sulfone 5.4 parts, diphenyl dichlorosilane 10 parts, calcium carbonate 6.8 parts, titanate coupling agent 3.6 parts, cumyl peroxide 11
Part, alkyl benzene calcium sulfonate 8 parts, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 11 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Compared with prior art, the invention has the beneficial effects as follows:
Antibacterial medical packaging material in the present invention has the advantages such as intensity is high, preparation method is simple, has concurrently good simultaneously
Antibacterial effect, can effectively suppress microbial activities, be particularly suited for field of medicaments.
Detailed description of the invention
Describe technical scheme in detail below in conjunction with embodiment, but protection domain is not limited thereto.
Embodiment one:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 30 parts, Permethrin 24 parts,
Polyethylene terephthalate 13 parts, nano titanium oxide 9 parts, nanometer silver 7 parts, polyimide 23 parts, polyglycolic acid 12 parts,
Zinc oxide 5 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 7 parts, 11 parts of polyester fiber, Arcton 11 1.7 parts, polyether sulfone 5.6
Part, diphenyl dichlorosilane 9 parts, calcium carbonate 5.6 parts, titanate coupling agent 4.5 parts, cumyl peroxide 8 parts, benzene sulfonamide
Acid calcium 8 parts, dimethylaminopropylamine 4.3 parts, ethylene-vinyl acetate copolymer 7 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Embodiment two:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 33 parts, Permethrin 22 parts,
Polyethylene terephthalate 14 parts, nano titanium oxide 7 parts, nanometer silver 7 parts, polyimide 20 parts, polyglycolic acid 15 parts,
Zinc oxide 4.6 parts, acrylamide 9 parts, ammonium dihydrogen phosphate 10 parts, 8 parts of polyester fiber, Arcton 11 2 parts, polyether sulfone 5.6 parts,
Diphenyl dichlorosilane 9 parts, calcium carbonate 6 parts, titanate coupling agent 6 parts, cumyl peroxide 12 parts, alkyl benzene calcium sulfonate 3
Part, dimethylaminopropylamine 3 parts, ethylene-vinyl acetate copolymer 8 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Embodiment three:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 42 parts, Permethrin 17 parts,
Polyethylene terephthalate 13 parts, nano titanium oxide 7 parts, nanometer silver 6 parts, polyimide 23 parts, polyglycolic acid 13 parts,
Zinc oxide 4.6 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 8 parts, 12 parts of polyester fiber, Arcton 11 1.6 parts, polyether sulfone 5.8
Part, diphenyl dichlorosilane 10 parts, calcium carbonate 5 parts, titanate coupling agent 3.2 parts, cumyl peroxide 9 parts, benzene sulfonamide
Acid calcium 9 parts, dimethylaminopropylamine 4 parts, ethylene-vinyl acetate copolymer 11 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Embodiment four:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 34 parts, Permethrin 16 parts,
Polyethylene terephthalate 12 parts, nano titanium oxide 8 parts, nanometer silver 5 parts, polyimide 23 parts, polyglycolic acid 16 parts,
Zinc oxide 4 parts, acrylamide 8 parts, ammonium dihydrogen phosphate 5 parts, 11 parts of polyester fiber, Arcton 11 1.4 parts, polyether sulfone 4.5 parts,
Diphenyl dichlorosilane 8 parts, calcium carbonate 6 parts, titanate coupling agent 3.6 parts, cumyl peroxide 9 parts, alkyl benzene calcium sulfonate 7
Part, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 10 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Embodiment five:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 36 parts, Permethrin 21 parts,
Polyethylene terephthalate 15 parts, nano titanium oxide 6 parts, nanometer silver 5.6 parts, polyimide 18 parts, polyglycolic acid 17
Part, zinc oxide 5 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 8 parts, 13 parts of polyester fiber, Arcton 11 2 parts, polyether sulfone 4 parts,
Diphenyl dichlorosilane 8 parts, calcium carbonate 5 parts, titanate coupling agent 5 parts, cumyl peroxide 11 parts, alkyl benzene calcium sulfonate 7
Part, dimethylaminopropylamine 4 parts, ethylene-vinyl acetate copolymer 7 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Embodiment six:
A kind of antibacterial medical packaging material is made up of the raw material of following parts by weight: polrvinyl chloride 40 parts, Permethrin 20 parts,
Polyethylene terephthalate 12 parts, nano titanium oxide 6 parts, nanometer silver 5 parts, polyimide 22 parts, polyglycolic acid 15 parts,
Zinc oxide 6 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 10 parts, 9 parts of polyester fiber, Arcton 11 2.3 parts, polyether sulfone 5.4
Part, diphenyl dichlorosilane 10 parts, calcium carbonate 6.8 parts, titanate coupling agent 3.6 parts, cumyl peroxide 11 parts, alkylbenzene
Sulfoacid calcium 8 parts, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 11 parts.
The preparation method of described antibacterial medical packaging material, comprises the following steps:
(1) each raw material components is weighed in proportion；
(2) open reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1)
Each raw material components, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room
Temperature, prepares this antibacterial medical packaging finished material.
Finally illustrating, above example is only in order to illustrate technical scheme and unrestricted, although with reference to relatively
The present invention has been described in detail by good embodiment, it will be understood by those within the art that, can be to the skill of the present invention
Art scheme is modified or equivalent, and without deviating from objective and the scope of the technical program, it all should be contained in the present invention
Right in the middle of.
Claims (5)
1. an antibacterial medical packaging material, it is characterised in that be made up of the raw material of following parts by weight: polrvinyl chloride 20-45
Part, Permethrin 12-25 part, polyethylene terephthalate 8-18 part, nano titanium oxide 3-10 part, nanometer silver 2-8 part, polyacids
Imines 12-25 part, polyglycolic acid 10-22 part, zinc oxide 3-8 part, acrylamide 5-12 part, ammonium dihydrogen phosphate 3-10 part is poly-
Ester fiber 6-14 part, Arcton 11 1-2.5 part, polyether sulfone 2.5-7 part, diphenyl dichlorosilane 4-11 part, calcium carbonate 2-7
Part, titanate coupling agent 2-6 part, cumyl peroxide 5-12 part, alkyl benzene calcium sulfonate 3-9 part, dimethylaminopropylamine 2-8
Part, ethylene-vinyl acetate copolymer 3-13 part.
Antibacterial medical packaging material the most according to claim 1, it is characterised in that by the raw material system of following parts by weight
Become: polrvinyl chloride 34 parts, Permethrin 16 parts, polyethylene terephthalate 12 parts, nano titanium oxide 8 parts, nanometer silver 5 parts,
Polyimide 23 parts, polyglycolic acid 16 parts, zinc oxide 4 parts, acrylamide 8 parts, ammonium dihydrogen phosphate 5 parts, 11 parts of polyester fiber,
Arcton 11 1.4 parts, polyether sulfone 4.5 parts, diphenyl dichlorosilane 8 parts, calcium carbonate 6 parts, titanate coupling agent 3.6 parts, mistake
Oxidation diisopropylbenzene (DIPB) 9 parts, alkyl benzene calcium sulfonate 7 parts, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 10 parts.
Antibacterial medical packaging material the most according to claim 1, it is characterised in that by the raw material system of following parts by weight
Become: polrvinyl chloride 36 parts, Permethrin 21 parts, polyethylene terephthalate 15 parts, nano titanium oxide 6 parts, nanometer silver 5.6
Part, polyimide 18 parts, polyglycolic acid 17 parts, zinc oxide 5 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 8 parts, polyester fiber
13 parts, Arcton 11 2 parts, polyether sulfone 4 parts, diphenyl dichlorosilane 8 parts, calcium carbonate 5 parts, titanate coupling agent 5 parts, peroxide
Change diisopropylbenzene (DIPB) 11 parts, alkyl benzene calcium sulfonate 7 parts, dimethylaminopropylamine 4 parts, ethylene-vinyl acetate copolymer 7 parts.
Antibacterial medical packaging material the most according to claim 1, it is characterised in that by the raw material system of following parts by weight
Become: polrvinyl chloride 40 parts, Permethrin 20 parts, polyethylene terephthalate 12 parts, nano titanium oxide 6 parts, nanometer silver 5 parts,
Polyimide 22 parts, polyglycolic acid 15 parts, zinc oxide 6 parts, acrylamide 10 parts, ammonium dihydrogen phosphate 10 parts, polyester fiber 9
Part, Arcton 11 2.3 parts, polyether sulfone 5.4 parts, diphenyl dichlorosilane 10 parts, calcium carbonate 6.8 parts, titanate coupling agent 3.6
Part, cumyl peroxide 11 parts, alkyl benzene calcium sulfonate 8 parts, dimethylaminopropylamine 6 parts, ethylene-vinyl acetate copolymer 11
Part.
5. according to the preparation method of the antibacterial medical packaging material according to any one of claim 1-4, it is characterised in that include
Following steps:
(1) each raw material components is weighed in proportion；
(2) opening reactor, temperature of reactor is adjusted to 185-200 DEG C, after temperature stabilization, add in step (1) is each former
Material component, after high-temperature stirring is uniform, obtains packaging material mixture；
(3) with double screw extruder, the packaging material mixture in step (2) is carried out high temperature extrusion pelletize；
(4), after twin-screw extruder pelletize, the raw material single-screw extrusion machine after extrusion is carried out blowfilm shaping, is cooled to room temperature,
Prepare this antibacterial medical packaging finished material.
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| CN201610711658.2A CN106147084A (en) | 2016-08-24 | 2016-08-24 | A kind of antibacterial medical packaging material and preparation method thereof |
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Cited By (3)
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| CN108129806A (en) * | 2017-12-22 | 2018-06-08 | 桐城市桃花制刷有限公司 | A kind of antibacterial vegetables plastic package material and preparation method thereof |
| CN112225973A (en) * | 2020-10-13 | 2021-01-15 | 河南工业大学 | Insect-proof packaging material and preparation method thereof |
| CN113499389A (en) * | 2021-07-08 | 2021-10-15 | 同曦集团有限公司 | Antibacterial anti-mite spray and preparation method and application thereof |
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| CN108129806A (en) * | 2017-12-22 | 2018-06-08 | 桐城市桃花制刷有限公司 | A kind of antibacterial vegetables plastic package material and preparation method thereof |
| CN112225973A (en) * | 2020-10-13 | 2021-01-15 | 河南工业大学 | Insect-proof packaging material and preparation method thereof |
| CN113499389A (en) * | 2021-07-08 | 2021-10-15 | 同曦集团有限公司 | Antibacterial anti-mite spray and preparation method and application thereof |
| CN113499389B (en) * | 2021-07-08 | 2022-07-29 | 同曦集团有限公司 | Antibacterial anti-mite spray and preparation method and application thereof |
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