CN106145859A - Inner wall putty powder and preparation method thereof - Google Patents

Inner wall putty powder and preparation method thereof Download PDF

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Publication number
CN106145859A
CN106145859A CN201610637506.2A CN201610637506A CN106145859A CN 106145859 A CN106145859 A CN 106145859A CN 201610637506 A CN201610637506 A CN 201610637506A CN 106145859 A CN106145859 A CN 106145859A
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CN
China
Prior art keywords
parts
nano
powder
wall putty
putty powder
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Pending
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CN201610637506.2A
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Chinese (zh)
Inventor
庞瑜
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Advertising Co Ltd Nanning East Era
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Advertising Co Ltd Nanning East Era
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Priority to CN201610637506.2A priority Critical patent/CN106145859A/en
Publication of CN106145859A publication Critical patent/CN106145859A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/14Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/0028Aspects relating to the mixing step of the mortar preparation
    • C04B40/0039Premixtures of ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2103/00Function or property of ingredients for mortars, concrete or artificial stone
    • C04B2103/60Agents for protection against chemical, physical or biological attack
    • C04B2103/67Biocides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00482Coating or impregnation materials
    • C04B2111/00491Primers

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of inner wall putty powder, described inner wall putty powder includes following weight portion material: 100 200 parts of gypsum, sierozem power 80 150 parts, nanomete talc powder 80 150 parts, nano titanium oxide 10 20 parts, nano silicon 20 50 parts, nano magnetic stone flour 15 parts, 35 parts of lanolin, borax 5 10 parts, xanthans 58 parts, agar-agar 6 10 parts, hydroxypropyl methyl cellulose 5 10 parts, sodium methyl silicate 13 parts, bacteriostatic agent 46 parts;The inner wall putty powder of the present invention is without harmful chemical agent, not containing harmful composition, will not discharging harmful substance, the present invention contains bacteriostatic agent, having antibacterial, mildew-resistant, the harmful substance in absorption air, after powder of lacquer putty for use on construction, durability length does not chaps, peels off.

Description

Inner wall putty powder and preparation method thereof
Technical field
The present invention relates to building decoration technology field, be specifically related to a kind of inner wall putty powder and preparation method thereof.
Background technology
Inner wall putty powder is a kind of construction material of large usage quantity in building decoration, must use before body of wall swabbing It is floating that inner wall putty powder carries out the bottoming such as body of wall ceiling, thus it is applied in indoor by large-area, is that people live for a long time Place, it is main component that traditional inner wall putty powder mostly is powdered whiting, adds some chemical assistants, mould inhibitor, antibacterial Agent etc., not only formula complexity, and chemical composition therein asks that when longer interior meeting discharges many harmful substances, as formaldehyde, Toluene etc., not only pollute environment, and bring harm greatly to health.
Content of the invention
It is an object of the invention to for the problems referred to above, a kind of inner wall putty powder, the inner wall putty powder of the present invention are provided Without harmful chemical agent, not containing harmful composition, will not discharging harmful substance, the present invention contains bacteriostatic agent, Having antibacterial, mildew-resistant, the harmful substance in absorption air, after powder of lacquer putty for use on construction, durability length does not chaps, peels off.
It is a still further object of the present invention to provide the preparation method of a kind of inner wall putty powder, method is simple to operation, preparation Inner wall putty powder particles out is uniform, and mobility and lubricity are good, easily brush.
The technical scheme that the present invention provides is:
A kind of inner wall putty powder, described inner wall putty powder includes following weight portion material: gypsum 100-200 part, sierozem power 80-150 part, nanomete talc powder 80-150 part, nano titanium oxide 10-20 part, nano silicon 20-50 part, nano magnetite Powder 1-5 part, lanolin 3-5 part, borax 5-10 part, xanthans 5-8 part, agar-agar 6-10 part, hydroxypropyl methyl cellulose 5-10 Part, sodium methyl silicate 1-3 part, bacteriostatic agent 4-6 part;Described bacteriostatic agent is made up of following weight portion material: plant polyphenol 1-2 part, Wormwood essential oil 2-6 part, pyrolkigneous liquid 1-2 part, montmorillonite 10-20 part.
Preferably, described plant polyphenol is made up of with vine polyphenol Tea Polyphenols, wherein the weight of Tea Polyphenols and vine polyphenol Amount ratio is 2: 1.
Preferably, described bacteriostatic agent is prepared from by following methods: montmorillonite is added after pulverizing 10 times heavy Water mixes, and adds plant polyphenol, pyrolkigneous liquid dispersion machine to disperse 0.5 hour, and rate of dispersion is 5000rmp, adds wormwood essential oil Redisperse 0.5 hour, rate of dispersion is 1000rmp, after stopping dispersion, is pulverized by high-pressure pulse nano-scale crusher after being dried Obtain described bacteriostatic agent to particle diameter 50 microns.
Preferably, described nano magnetic stone flour is by Nd2Fe14B、Sm2Co17、SmCo5Composition, described Nd2Fe14B、Sm2Co17、 SmCo5Weight ratio be 1: 2: 1.
Preferably, described nano magnetic stone flour is prepared by following methods: by Nd2Fe14B、Sm2Co17、SmCo5By weight 1 : prepare at 2: 1, adds water and mass fraction 1% neopelex of 2-5 times of weight, and rate of dispersion is that 5000rmp divides at a high speed After dissipating 1 hour, after being dried moisture, sintering temperature is 1000 DEG C and is sintered 4-6 hour, and taking-up is placed in inert gas and is cooled to Room temperature, carries out being crushed to particle diameter less than till 500 nanometers with high-pressure pulse nano-scale crusher, obtains described nano magnetic stone flour.
Preferably, described inner wall putty powder is made up of following weight portion material: 160 parts of gypsum, sierozem power 120 parts, receive Rice talcum powder 110 parts, nano titanium oxide 15 parts, nano silicon 30 parts, nano magnetic stone flour 4 parts, 4 parts of lanolin, borax 8 Part, xanthans 7 parts, agar-agar 8 parts, hydroxypropyl methyl cellulose 7 parts, sodium methyl silicate 2 parts, bacteriostatic agent 5 parts;Described bacteriostatic agent It is made up of following weight portion material: plant polyphenol 1 part, wormwood essential oil 5 parts, 2 parts of pyrolkigneous liquid, montmorillonite 18 parts.
The preparation method of the inner wall putty powder described in any of the above-described, the preparation method of described inner wall putty powder includes following Step:
1) add appropriate water to dissolve xanthans, agar-agar, add the borax pulverized to be stirred continuously formation glue Shape liquid;
2) lanolin is added ethanol in proper amount, be heated to 60 DEG C, be stirred continuously to lanolin dissolving formation lanolin ethanol Solution, lanolin ethanol solution is incubated at 55-65 DEG C;
3) gypsum is crushed to 10-20 micron and sierozem power, nanomete talc powder, nanometer through high-pressure pulse nano-scale crusher Titanium dioxide, nano silicon, nano magnetic stone flour, hydroxypropyl methyl cellulose, sodium methyl silicate, bacteriostatic agent agent add after mixing Enter the 5-10 times of water weighing, carry out high speed dispersion 1 hour;
4) add step 1) in colloidal liquid and step 2) the lanolin ethanol solution then high speed dispersion 1 of insulation little When, it is crushed to, through high-pressure pulse nano-scale crusher, the powder that particle size is 20-30 micron after being dried, obtain described interior wall greasy Sub-powder.
Beneficial effects of the present invention is as follows:
1) present invention with the addition of lanolin, plays the effect of antibacterial bacteriostatic, and as lubricant, can play the work of lubrication With making inner wall putty powder of the present invention spraying uniformly;Xanthans, agar-agar is used to replace chemical glue can substantially reduce harmful substance Release, and both cooperates so that the caking property of inner wall putty powder of the present invention significantly improves thus prevents interior wall after construction Powder of lacquer putty for use on efflorescence, come off and chap;Nano magnetic stone flour is by Nd2Fe14B、Sm2Co17、SmCo5Composition can adsorb being harmful in air Material;The bacteriostatic agent that the present invention adds does not contains harmful composition, thalline can be suppressed to grow containing plant polyphenol, and to executing Body of wall after work plays a protective role, and prevents the glue in powder of lacquer putty for use on aging and departs from body of wall, extends the durability of powder of lacquer putty for use on;Combine Close the described present invention and contain antipathogenic composition, reduce bacteria breed environmental protection, good endurance, it is adaptable to interior decoration.
2) preparation method of inner wall putty powder of the present invention, method is simple to operation, the inner wall putty powder particles preparing Uniformly, mobility and lubricity are good, easily brush.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, to make those skilled in the art's reference say Bright book word can be implemented according to this.
Embodiment 1:
Inner wall putty powder includes following weight portion material: 100 parts of gypsum, sierozem power 80 parts, nanomete talc powder 80 parts, nanometer Titanium dioxide 10 parts, nano silicon 20 parts, nano magnetic stone flour 1 part, 3 parts of lanolin, borax 5 parts, xanthans 5 parts, parmelia saxatilis 6 parts of glue, hydroxypropyl methyl cellulose 5 parts, sodium methyl silicate 1 part, bacteriostatic agent 4 parts;Described bacteriostatic agent is by following weight portion material Composition: plant polyphenol 1 part, wormwood essential oil 2 parts, 1 part of pyrolkigneous liquid, montmorillonite 10 parts.
Embodiment 2
Inner wall putty powder includes following weight portion material: 200 parts of gypsum, sierozem power 150 parts, nanomete talc powder 150 parts, receive Rice titanium dioxide 20 parts, nano silicon 50 parts, nano magnetic stone flour 5 parts, 5 parts of lanolin, borax 10 parts, xanthans 8 parts, stone 10 parts of glue of flower, hydroxypropyl methyl cellulose 10 parts, sodium methyl silicate 3 parts, bacteriostatic agent 6 parts;Described bacteriostatic agent is by following weight portion Material forms: plant polyphenol 2 parts, wormwood essential oil 6 parts, 2 parts of pyrolkigneous liquid, montmorillonite 20 part;Described plant polyphenol by Tea Polyphenols with Vine polyphenol forms, and wherein Tea Polyphenols and the weight ratio of vine polyphenol are 2: 1;Described bacteriostatic agent is prepared from by following methods: Montmorillonite adds after pulverizing the water of 10 times heavy mix, adds plant polyphenol, pyrolkigneous liquid dispersion machine to disperse 0.5 hour, Rate of dispersion is 5000rmp, adds wormwood essential oil redisperse 0.5 hour, and rate of dispersion is 1000rmp, after stopping dispersion, is dried Carry out being crushed to below particle diameter 50 microns with high-pressure pulse nano-scale crusher afterwards and obtain described bacteriostatic agent.
Embodiment 3
Inner wall putty powder includes following weight portion material: 110 parts of gypsum, sierozem power 120 parts, nanomete talc powder 100 parts, receive Rice titanium dioxide 15 parts, nano silicon 35 parts, nano magnetic stone flour 4 parts, 4 parts of lanolin, borax 8 parts, xanthans 7 parts, stone 8 parts of glue of flower, hydroxypropyl methyl cellulose 8 parts, sodium methyl silicate 2 parts, bacteriostatic agent 5 parts;Described bacteriostatic agent is by following weight portion material Material composition: plant polyphenol 2 parts, wormwood essential oil 3 parts, 1 part of pyrolkigneous liquid, montmorillonite 18 parts;Described plant polyphenol is by Tea Polyphenols and Portugal Grape polyphenol forms, and wherein Tea Polyphenols and the weight ratio of vine polyphenol are 2: 1;Described bacteriostatic agent is prepared from by following methods: will Montmorillonite adds the water of 10 times heavy to mix after pulverizing, and adds plant polyphenol, pyrolkigneous liquid dispersion machine to disperse 0.5 hour, point Scattered speed is 5000rmp, adds wormwood essential oil redisperse 0.5 hour, and rate of dispersion is 1000rmp, after stopping dispersion, after being dried Carry out being crushed to below particle diameter 50 microns with high-pressure pulse nano-scale crusher and obtain described bacteriostatic agent;Described nano magnetic stone flour by Nd2Fe14B、Sm2Co17、SmCo5Composition, described Nd2Fe14B、Sm2Co17、SmCo5Weight ratio be 1: 2: 1;Described nano magnetite Powder is prepared by following methods: by Nd2Fe14B、5m2Co17、SmCo5Prepare by weight 1: 2: 1, add 2 times of heavy water and quality Fraction 1% neopelex, rate of dispersion is 5000rmp high speed dispersion after 1 hour, after being dried moisture, sintering temperature Being 1000 DEG C to be sintered 4 hours, taking-up is placed in inert gas and is cooled to room temperature, carries out powder with high-pressure pulse nano-scale crusher It is broken to particle diameter less than till 500 nanometers, obtain described nano magnetic stone flour.
Embodiment 4
Inner wall putty powder includes following weight portion material: described inner wall putty powder is made up of following weight portion material: gypsum 160 parts, sierozem power 120 parts, nanomete talc powder 110 parts, nano titanium oxide 15 parts, nano silicon 30 parts, nano magnetite 4 parts of powder, 4 parts of lanolin, borax 8 parts, xanthans 7 parts, agar-agar 8 parts, hydroxypropyl methyl cellulose 7 parts, sodium methyl silicate 2 Part, bacteriostatic agent 5 parts;Described bacteriostatic agent is made up of following weight portion material: plant polyphenol 1 part, wormwood essential oil 5 parts, pyrolkigneous liquid 2 Part, montmorillonite 18 parts;Described bacteriostatic agent is made up of following weight portion material: plant polyphenol 1-2 part, wormwood essential oil 2-6 part, wood vinegar Liquid 1-2 part, montmorillonite 10-20 part;Described plant polyphenol is made up of with vine polyphenol Tea Polyphenols, wherein Tea Polyphenols and vine polyphenol Weight ratio be 2: 1;Described bacteriostatic agent is prepared from by following methods: montmorillonite adds after pulverizing 10 times of heavy water mix Even, add plant polyphenol, pyrolkigneous liquid dispersion machine to disperse 0.5 hour, rate of dispersion is 5000rmp, adds wormwood essential oil to divide again Dissipating 0.5 hour, rate of dispersion is 1000rmp, after stopping dispersion, carries out being crushed to grain with high-pressure pulse nano-scale crusher after being dried Obtain described bacteriostatic agent below 50 microns of footpath;Described nano magnetic stone flour is by Nd2Fe14B、Sm2Co17、SmCo5Composition, described Nd2Fe14B、Sm2Co17、SmCo5Weight ratio be 1: 2: 1;Described nano magnetic stone flour is prepared by following methods: by Nd2Fe14B、 Sm2Co17、SmCo5Prepare by weight 1: 2: 1, add water and mass fraction 1% neopelex of 5 times of weights, dispersion Speed is 5000rmp high speed dispersion after 1 hour, and after being dried moisture, sintering temperature is 1000 DEG C and is sintered 6 hours, and taking-up is put It is cooled to room temperature in inert gas, carry out being crushed to particle diameter less than till 500 nanometers with high-pressure pulse nano-scale crusher, obtain Described nano magnetic stone flour.
Embodiment 1-4 powder of lacquer putty for use on all uses embodiment 5 method to prepare
Embodiment 5
The preparation method of described inner wall putty powder, the preparation method of described inner wall putty powder comprises the following steps:
1) add appropriate water to dissolve xanthans, agar-agar, add the borax pulverized to be stirred continuously formation glue Shape liquid;
2) lanolin is added ethanol in proper amount, be heated to 60 DEG C, be stirred continuously to lanolin dissolving formation lanolin ethanol Solution, lanolin ethanol solution is incubated at 55-65 DEG C;
3) gypsum is crushed to 10-20 micron and sierozem power, nanomete talc powder, nanometer through high-pressure pulse nano-scale crusher Titanium dioxide, nano silicon, nano magnetic stone flour, hydroxypropyl methyl cellulose, sodium methyl silicate, bacteriostatic agent agent add after mixing Enter the 5-10 times of water weighing, carry out high speed dispersion 1 hour;
4) add step 1) in colloidal liquid and step 2) the lanolin ethanol solution then high speed dispersion 1 of insulation little When, it is crushed to, through high-pressure pulse nano-scale crusher, the powder that particle size is 20-30 micron after being dried, obtain described interior wall greasy Sub-powder.
Although embodiment of the present invention are disclosed as above, but it is not restricted in specification and embodiment listed Using, it can be applied to various applicable the field of the invention completely, for those skilled in the art, and can be easily Realizing other modification, therefore under the universal being limited without departing substantially from claim and equivalency range, the present invention does not limit In specific details with shown here as the embodiment with description.

Claims (7)

1. an inner wall putty powder, it is characterised in that described inner wall putty powder includes following weight portion material: gypsum 100-200 Part, sierozem power 80-150 part, nanomete talc powder 80-150 part, nano titanium oxide 10-20 part, nano silicon 20-50 part, Nano magnetic stone flour 1-5 part, lanolin 3-5 part, borax 5-10 part, xanthans 5-8 part, agar-agar 6-10 part, hydroxypropyl methyl are fine Dimension element 5-10 part, sodium methyl silicate 1-3 part, bacteriostatic agent 4-6 part;Described bacteriostatic agent is made up of following weight portion material: plant is many Phenol 1-2 part, wormwood essential oil 2-6 part, pyrolkigneous liquid 1-2 part, montmorillonite 10-20 part.
2. inner wall putty powder as claimed in claim 1, it is characterised in that described plant polyphenol is by Tea Polyphenols and vine polyphenol group Becoming, wherein Tea Polyphenols and the weight ratio of vine polyphenol are 2: 1.
3. inner wall putty powder as claimed in claim 1, it is characterised in that described bacteriostatic agent is prepared from by following methods: will Montmorillonite adds the water of 10 times heavy to mix after pulverizing, and adds plant polyphenol, pyrolkigneous liquid dispersion machine to disperse 0.5 hour, point Scattered speed is 5000rmp, adds wormwood essential oil redisperse 0.5 hour, and rate of dispersion is 1000rmp, after stopping dispersion, after being dried Carry out being crushed to below particle diameter 50 microns with high-pressure pulse nano-scale crusher and obtain described bacteriostatic agent.
4. inner wall putty powder as claimed in claim 1, it is characterised in that described nano magnetic stone flour is by Nd2Fe14B、Sm2Co17、 SmCo5Composition, described Nd2Fe14B、Sm2Co17、SmCo5Weight ratio be 1: 2: 1.
5. inner wall putty powder as claimed in claim 4, it is characterised in that described nano magnetic stone flour is prepared by following methods: will Nd2Fe14B、Sm2Co17、SmCo5Prepare by weight 1: 2: 1, add water and mass fraction 1% detergent alkylate of 2-5 times of weight Sodium sulfonate, rate of dispersion is 5000rmp high speed dispersion after 1 hour, and after being dried moisture, sintering temperature is 1000 DEG C and is sintered 4- 6 hours, taking-up was placed in inert gas and is cooled to room temperature, carries out being crushed to particle diameter with high-pressure pulse nano-scale crusher and is less than 500 Till nanometer, obtain described nano magnetic stone flour.
6. inner wall putty powder as claimed in claim 1, it is characterised in that described inner wall putty powder is by following weight portion material group Become: 160 parts of gypsum, sierozem power 120 parts, nanomete talc powder 110 parts, nano titanium oxide 15 parts, nano silicon 30 parts, receive Rice magnet powder 4 parts, 4 parts of lanolin, borax 8 parts, xanthans 7 parts, agar-agar 8 parts, hydroxypropyl methyl cellulose 7 parts, methyl silicon 2 parts of sodium of acid, bacteriostatic agent 5 parts;Described bacteriostatic agent is made up of following weight portion material: plant polyphenol 1 part, wormwood essential oil 5 parts, wood vinegar Liquid 2 parts, montmorillonite 18 parts.
7. the preparation method of the inner wall putty powder as described in arbitrary in claim 1-6, it is characterised in that described inner wall putty powder Preparation method comprise the following steps:
1) add appropriate water to dissolve xanthans, agar-agar, add the borax pulverized to be stirred continuously formation colloidal fluid Body;
2) lanolin is added ethanol in proper amount, is heated to 60 DEG C, be stirred continuously to lanolin dissolving formation lanolin ethanol solution, Lanolin ethanol solution is incubated at 55-65 DEG C;
3) gypsum is crushed to 10-20 micron and sierozem power, nanomete talc powder, nano-silica through high-pressure pulse nano-scale crusher Change titanium, nano silicon, nano magnetic stone flour, hydroxypropyl methyl cellulose, sodium methyl silicate, bacteriostatic agent agent add 5-after mixing 10 times of heavy water, carry out high speed dispersion 1 hour;
4) add step 1) in colloidal liquid and step 2) lanolin ethanol solution then high speed dispersion 1 hour of insulation, It is crushed to, through high-pressure pulse nano-scale crusher, the powder that particle size is 20-30 micron after drying, obtain described inner wall putty Powder.
CN201610637506.2A 2016-08-05 2016-08-05 Inner wall putty powder and preparation method thereof Pending CN106145859A (en)

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CN107556803A (en) * 2017-10-30 2018-01-09 陕西刮德乐新型建材有限公司 A kind of mould proof powder of lacquer putty for use on
CN109206969A (en) * 2018-10-25 2019-01-15 合肥永泰新型建材有限公司 A kind of interior wall sterilization putty new material and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107556803A (en) * 2017-10-30 2018-01-09 陕西刮德乐新型建材有限公司 A kind of mould proof powder of lacquer putty for use on
CN109206969A (en) * 2018-10-25 2019-01-15 合肥永泰新型建材有限公司 A kind of interior wall sterilization putty new material and preparation method thereof

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Application publication date: 20161123