CN106116559B - A kind of electric field-assisted ceramic low-temp quick-combustion device - Google Patents
A kind of electric field-assisted ceramic low-temp quick-combustion device Download PDFInfo
- Publication number
- CN106116559B CN106116559B CN201610776999.8A CN201610776999A CN106116559B CN 106116559 B CN106116559 B CN 106116559B CN 201610776999 A CN201610776999 A CN 201610776999A CN 106116559 B CN106116559 B CN 106116559B
- Authority
- CN
- China
- Prior art keywords
- power supply
- electric field
- heating plate
- acquisition device
- data acquisition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/26—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
- C04B35/2608—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead
- C04B35/2633—Compositions containing one or more ferrites of the group comprising manganese, zinc, nickel, copper or cobalt and one or more ferrites of the group comprising rare earth metals, alkali metals, alkaline earth metals or lead containing barium, strontium or calcium
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/26—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
- C04B35/2641—Compositions containing one or more ferrites of the group comprising rare earth metals and one or more ferrites of the group comprising alkali metals, alkaline earth metals or lead
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/26—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
- C04B35/2666—Other ferrites containing nickel, copper or cobalt
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B21/00—Open or uncovered sintering apparatus; Other heat-treatment apparatus of like construction
- F27B21/02—Sintering grates or tables
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/02—Ohmic resistance heating
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
- C04B2235/3227—Lanthanum oxide or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3262—Manganese oxides, manganates, rhenium oxides or oxide-forming salts thereof, e.g. MnO
- C04B2235/3268—Manganates, manganites, rhenates or rhenites, e.g. lithium manganite, barium manganate, rhenium oxide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3275—Cobalt oxides, cobaltates or cobaltites or oxide forming salts thereof, e.g. bismuth cobaltate, zinc cobaltite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
- F27D2019/0003—Monitoring the temperature or a characteristic of the charge and using it as a controlling value
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
- F27D2019/0093—Maintaining a temperature gradient
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27M—INDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
- F27M2001/00—Composition, conformation or state of the charge
- F27M2001/03—Charges containing minerals
- F27M2001/035—China
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27M—INDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
- F27M2003/00—Type of treatment of the charge
- F27M2003/04—Sintering
Abstract
The invention discloses a kind of electric field-assisted ceramic low-temp quick-combustion devices, including heating plate, DC power supply, infrared camera and data acquisition device；The heating plate is separately connected the positive and negative anodes of DC power supply for placement and heating sample, sample both ends；Heating plate corresponding position is provided with infrared camera, and infrared camera connects data acquisition device；The present invention provides thermal energy by heating plate for ceramics, under the auxiliary of DC electric field, realizes the low temperature Fast Sintering of ceramic material；The variation and linear contraction that each stage specimen temperature of in-situ observation flash burning may be implemented by infrared camera and data acquisition device, significantly reduce the requirement of energy consumption and equipment.
Description
Technical field
The present invention relates to a kind of ceramic low-temp quick-combustion devices, and in particular to a kind of electric field-assisted ceramic low-temp quick-combustion device.
Background technique
Ceramics have the performances such as superior mechanics, electricity, optics, acoustics, magnetics, attract tremendous attention in industrial application,
Use scope also increasingly expands；Sintering is an indispensable process of ceramic densifying, this process needs to consume a large amount of
Energy, while a series of environmental problems can be caused；In response to energy saving and protection environment call, researcher is continually developed
New sintering technology；Such as microwave sintering, HIP sintering, discharge plasma sintering etc.；These sintering methods are not only saved
The energy, also improves the performance of material, is made that contribution for the extensive use of material；One is proposed by Rishi Raj within 2010
The new ceramic post sintering method-flash burning of kind；For this sintering method under electric field-assisted, cause is can be realized in ceramic material in a few seconds
The furnace temperature of densification, sintering is significantly lower than other sintering methods；Existing flash burning device has the following problems: first is that heating equipment phase
To more expensive, it is not easy to popularize；Second is that sintering is carried out in closed furnace body, it is not easy to observation in real time in situ；Third is that existing
Some flash burning devices are relatively complicated, are not easy to operate；Fourth is that the rate of heat addition is relatively slow, it is raw to be not easy to quick chemical industry
It produces；Fifth is that flash burning device before can only measure the temperature change of a point during flash burning, be not capable of measuring sample part or
Bulk temperature distribution.
Summary of the invention
It is simple, convenient, fast that the present invention provides a kind of structures, and the electric field-assisted ceramic low-temp of observation convenient to carry out is burnt fastly
Device.
The technical solution adopted by the present invention is that: a kind of electric field-assisted ceramic low-temp quick-combustion device, including heating plate, direct current
Source, infrared camera and data acquisition device；The heating plate is separately connected direct current for placement and heating sample, sample both ends
The positive and negative anodes in source；Heating plate corresponding position is provided with infrared camera, and infrared camera connects data acquisition device.
Further, the heating plate is arranged on warm table.
Further, the heater plate surface is provided with one layer of 99 alumina wafer.
Further, the sample both ends pass through the positive and negative anodes of high temperature alloy silk connection DC power supply respectively.
Further, the high temperature alloy silk be nichrome wire, memory alloy wire, lectrothermal alloy wire, platinumiridio silk,
One of tungsten rhenium alloy wire, Aludirome silk.
Further, voltmeter is connected between the DC power supply and data acquisition device.
Further, ammeter is connected between the DC power supply and data acquisition device.
Further, voltmeter is connected with by data line between the DC power supply and data acquisition device；Directly
Ammeter is connected with by data line between galvanic electricity source and data acquisition device.
Further, the infrared camera data acquiring frequency is adjustable between 10-200 Hz.
The beneficial effects of the present invention are:
(1) present invention provides thermal energy by setting heating plate for ceramic post sintering, and ceramics are realized under the auxiliary of DC electric field
Low temperature Fast Sintering；
(2) present invention setting infrared camera can be with the variation of each stage specimen temperature of in-situ observation flash burning and linear receipts
Contracting；
(3) the configuration of the present invention is simple, easy to use, quick, effectively reduces the requirement of energy consumption and equipment, can be used for ceramics
Continuous production.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention.
In figure: 1- warm table, 2- infrared camera, 3- DC power supply, 4- data acquisition device, 5- sample, 6- heating plate, 7-
High temperature alloy silk, 8- ammeter, 9- voltmeter, 10- data line.
Specific embodiment
The present invention will be further explained below with reference to the attached drawings and specific examples.
As shown in Figure 1, a kind of electric field-assisted ceramic low-temp quick-combustion device, including heating plate 6, DC power supply 3, infrared camera
2 and data acquisition device 4；For the heating plate 6 for placement and heating sample 5,5 both ends of sample are separately connected DC power supply 3
Positive and negative anodes；6 corresponding position of heating plate is provided with infrared camera 2, and infrared camera 2 connects data acquisition device 4.
In use, providing required temperature by heating plate 6 for the sintering of sample 5, and direct current is formed by external dc power supply 3
Field excitation rapid mass transfer realizes the low temperature quick densifying of ceramic material, and can be observed and be burnt by 2 real-time in-situ of infrared camera
Tie each 5 temperature of stage sample and linear contraction；The voltage of DC power supply 3 is continuously adjustable in 0-1000V, and accuracy is ±
0.5%；The electric current of DC power supply 3 is continuously adjusted between 0-30V, and accuracy is ± 0.5%, when can satisfy lot of materials flash burning
Requirement to voltage and current；Heating plate 6 can provide sufficiently high temperature for ceramic post sintering, reduce and want to high-temperature service
It asks；6 temperature of heating plate is in room temperature to 500oBetween C be continuously adjusted, heating rate is fast, can be completed within ten minutes from room temperature to
500oThe heating of C；The measurement of temperature measurement and ceramic body size can be achieved at the same time in infrared camera 2；Temperature measurement range from
40oC-2500oC, the accuracy of temperature measurement is ± 1oC；Dimensional measurement ranges 0-500mm, the accuracy of dimensional measurement ±
1mm；Data acquisition device 4 can temperature to sample 5 and size carry out real-time display, provide convenience for sintering process；By
The display of the snapshots and data acquisition device 4 of infrared camera 2, can observe the linear contraction of sample 5 in real time.
Further, the heating plate 6 is arranged on warm table 1；It is heated up by warm table 1 to heating plate 6.
Further, 6 surface of heating plate is provided with one layer of 99 alumina wafer.
Further, 5 both ends of sample pass through the positive and negative anodes that high temperature alloy silk 7 connects DC power supply 3 respectively.
Further, the high temperature alloy silk 7 is nichrome wire, memory alloy wire, lectrothermal alloy wire, platinumiridio
One of silk, tungsten rhenium alloy wire, Aludirome silk.
Further, voltmeter 9 is connected between the DC power supply 3 and data acquisition device 4；Connecting voltmeter 9 can
To realize the real-time display to voltage, convenience is provided for sintering process control.
Further, ammeter 8 is connected between the DC power supply 3 and data acquisition device 4；Connecting ammeter 8 can
To realize the real-time display to electric current, convenience is provided for sintering process control.
Further, voltmeter is connected with by data line 10 between the DC power supply 3 and data acquisition device 4
9；Ammeter 8 is connected with by data line 10 between DC power supply 3 and data acquisition device 4.
Further, 2 data acquiring frequency of infrared camera is adjustable between 10-200 Hz.
Embodiment 1
La is sintered using apparatus of the present invention0.6Sr0.4Co0.2Fe0.8O3Specific step is as follows for ceramics:
1) both ends of band sample 5 are connected to the positive and negative anodes of DC power supply 3 by high temperature alloy silk 7, then by sample 5
It lies on 99 alumina wafers on 6 surface of heating plate；
2) warm table 1 is set in 300oC is started to warm up, and after reaching set temperature, is kept the temperature 30min, is made the temperature of sample 5
Degree and 1 surface temperature of warm table reach balance；
3) when warm table 1 is kept the temperature, 30V is set by voltage, electric current is set as 7.2A；
4) infrared camera 2, voltmeter 9, ammeter 8 and data acquisition device 4, real-time temperature collection, linear shrinkage, electricity are connected
Pressure and current data；
5) it after keeping the temperature 30min, connects DC power supply 3 and keeps the temperature 60s in this case, then after flash burning occurs in sample 5
DC power supply 3, warm table 1 are closed, sintering terminates.
Embodiment 2
La is sintered using apparatus of the present invention0.6Sr0.4Co0.2Fe0.8O3Specific step is as follows for ceramics:
1) both ends of band sample 5 are connected to the positive and negative anodes of DC power supply 3 by high temperature alloy silk 7, then by sample 5
It lies on 99 alumina wafers on 6 surface of heating plate；
2) warm table 1 is set in 200oC is started to warm up, and after reaching set temperature, is kept the temperature 30min, is made the temperature of sample 5
Degree and 1 surface temperature of warm table reach balance；
3) when warm table 1 is kept the temperature, 60V is set by voltage, electric current is set as 7.2A；
4) infrared camera 2, voltmeter 9, ammeter 8 and data acquisition device 4, real-time temperature collection, linear shrinkage, electricity are connected
Pressure and current data；
5) it after keeping the temperature 30min, connects DC power supply 3 and keeps the temperature 60s in this case, then after flash burning occurs in sample 5
DC power supply 3, warm table 1 are closed, sintering terminates.
Embodiment 3
Co is sintered using apparatus of the present invention2MnO4Specific step is as follows for ceramics:
1) both ends of band sample 5 are connected to the positive and negative anodes of DC power supply 3 by high temperature alloy silk 7, then by sample 5
It lies on 99 alumina wafers on 6 surface of heating plate；
2) warm table 1 is set in 300oC is started to warm up, and after reaching set temperature, is kept the temperature 30min, is made the temperature of sample 5
Degree and 1 surface temperature of warm table reach balance；
3) when warm table 1 is kept the temperature, 50V is set by voltage, electric current is set as 10A；
4) infrared camera 2, voltmeter 9, ammeter 8 and data acquisition device 4, real-time temperature collection, linear shrinkage, electricity are connected
Pressure and current data；
5) it after keeping the temperature 30min, connects DC power supply 3 and keeps the temperature 60s in this case, then after flash burning occurs in sample 5
DC power supply 3, warm table 1 are closed, sintering terminates.
Embodiment 4
La is sintered using apparatus of the present invention0.6Sr0.4Co0.2Fe0.8O3Specific step is as follows for ceramics:
1) both ends of band sample 5 are connected to the positive and negative anodes of DC power supply 3 by high temperature alloy silk 7, then by sample 5
It lies on 99 alumina wafers on 6 surface of heating plate；
2) warm table 1 is set in 200oC is started to warm up, and after reaching set temperature, is kept the temperature 30min, is made the temperature of sample 5
Degree and 1 surface temperature of warm table reach balance；
3) when warm table 1 is kept the temperature, 100V is set by voltage, electric current is set as 10A；
4) infrared camera 2, voltmeter 9, ammeter 8 and data acquisition device 4, real-time temperature collection, linear shrinkage, electricity are connected
Pressure and current data；
5) it after keeping the temperature 30min, connects DC power supply 3 and keeps the temperature 60s in this case, then after flash burning occurs in sample 5
DC power supply 3, warm table 1 are closed, sintering terminates.
The present invention provides thermal energy by heating plate 6 for ceramics, under the auxiliary of DC electric field, realizes the low temperature of ceramic material
Fast Sintering；Each 5 temperature of stage sample of in-situ observation flash burning may be implemented by infrared camera 2 and data acquisition device 4
Variation and linear contraction, significantly reduce the requirement of energy consumption and equipment, can be used for the continuous production of ceramics.
Claims (7)
1. a kind of electric field-assisted ceramic low-temp quick-combustion device, it is characterised in that: including heating plate (6), DC power supply (3), infrared
Camera (2) and data acquisition device (4)；For placement and heating sample (5), sample (5) both ends connect the heating plate (6) respectively
Connect the positive and negative anodes of DC power supply (3)；Heating plate (6) corresponding position is provided with infrared camera (2), and infrared camera (2) connects data
Acquisition device (4)；The heating plate (6) is arranged on warm table (1)；Heating plate (6) surface is provided with one layer of 99 oxidation
Aluminium flake.
2. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 1, it is characterised in that: the sample (5)
Both ends pass through the positive and negative anodes of high temperature alloy silk (7) connection DC power supply (3) respectively.
3. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 2, it is characterised in that: the high temperature alloy
Silk (7) is one of nichrome wire, memory alloy wire, platinumiridio silk, tungsten rhenium alloy wire, Aludirome silk.
4. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 1, it is characterised in that: the DC power supply
(3) it is connected between data acquisition device (4) voltmeter (9).
5. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 1, it is characterised in that: the DC power supply
(3) it is connected between data acquisition device (4) ammeter (8).
6. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 4 or 5, it is characterised in that: the direct current
Voltmeter (9) are connected with by data line (10) between power supply (3) and data acquisition device (4)；DC power supply (3) sum number
Ammeter (8) are connected with according to data line (10) are passed through between acquisition device (4).
7. a kind of electric field-assisted ceramic low-temp quick-combustion device according to claim 1, it is characterised in that: the infrared camera
(2) data acquiring frequency is adjustable between 10-200Hz.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610776999.8A CN106116559B (en) | 2016-08-30 | 2016-08-30 | A kind of electric field-assisted ceramic low-temp quick-combustion device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610776999.8A CN106116559B (en) | 2016-08-30 | 2016-08-30 | A kind of electric field-assisted ceramic low-temp quick-combustion device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106116559A CN106116559A (en) | 2016-11-16 |
| CN106116559B true CN106116559B (en) | 2018-12-25 |
Family
ID=57272567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610776999.8A Active CN106116559B (en) | 2016-08-30 | 2016-08-30 | A kind of electric field-assisted ceramic low-temp quick-combustion device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106116559B (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630974A (en) * | 2016-11-25 | 2017-05-10 | 中国工程物理研究院材料研究所 | Flash sintering method of low-temperature flash sintering ceramic and obtained ceramic and device thereof |
| CN108645204A (en) * | 2018-07-17 | 2018-10-12 | 浙江晨华科技有限公司 | A kind of sintering furnace with flash burning technology |
| CN110357633B (en) * | 2019-07-11 | 2021-05-18 | 上海交通大学 | Method for rapidly preparing titanium-aluminum-carbon ceramic at room temperature |
| CN110606751B (en) * | 2019-09-18 | 2021-09-17 | 上海交通大学 | Method for graphene-assisted room-temperature flash firing of ceramic material |
| CN112683062B (en) * | 2020-12-08 | 2022-09-02 | 国网江西省电力有限公司电力科学研究院 | Ultrafast sintering method and device for ceramic material |
| CN116460295B (en) * | 2023-04-27 | 2024-04-12 | 江苏科融新材料有限公司 | Preparation method of tungsten-lanthanum alloy wire |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102765946A (en) * | 2012-07-05 | 2012-11-07 | 中国科学院宁波材料技术与工程研究所 | Current assisted method for quickly preparing powder |
| CN105784596A (en) * | 2016-03-08 | 2016-07-20 | 浙江大学 | Multifunctional sample room capable of being used for thermal infrared camera |
| CN206089473U (en) * | 2016-08-30 | 2017-04-12 | 西南交通大学 | Supplementary ceramic low temperature of electric field burns device soon |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013098054A1 (en) * | 2011-12-28 | 2013-07-04 | Arcam Ab | Method and apparatus for detecting defects in freeform fabrication |
-
2016
- 2016-08-30 CN CN201610776999.8A patent/CN106116559B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102765946A (en) * | 2012-07-05 | 2012-11-07 | 中国科学院宁波材料技术与工程研究所 | Current assisted method for quickly preparing powder |
| CN105784596A (en) * | 2016-03-08 | 2016-07-20 | 浙江大学 | Multifunctional sample room capable of being used for thermal infrared camera |
| CN206089473U (en) * | 2016-08-30 | 2017-04-12 | 西南交通大学 | Supplementary ceramic low temperature of electric field burns device soon |
Non-Patent Citations (2)
| Title |
|---|
| Electric Field Assisted Sintering of Cubic Zirconia at 390°C;John A. Downs等;《Journal of the American Ceramic Society》;20130322;第96卷(第5期);第1342页左栏第1段至1343页左栏第1段 * |
| 陶瓷坯体烧成过程中红外热图像库管理***;曾令可等;《红外技术》;19940731;摘要，第21页第4段至第23页第4段，图1-3 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106116559A (en) | 2016-11-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106116559B (en) | A kind of electric field-assisted ceramic low-temp quick-combustion device | |
| CN206089473U (en) | Supplementary ceramic low temperature of electric field burns device soon | |
| Zapata-Solvas et al. | Preliminary investigation of flash sintering of SiC | |
| Anselmi-Tamburini et al. | Fundamental investigations on the spark plasma sintering/synthesis process: II. Modeling of current and temperature distributions | |
| Ren et al. | Densification kinetics of flash sintered 3mol% Y2O3 stabilized zirconia | |
| M’Peko et al. | Field-assisted sintering of undoped BaTiO3: Microstructure evolution and dielectric permittivity | |
| Francis et al. | Flash‐sinterforging of nanograin zirconia: field assisted sintering and superplasticity | |
| Yoshida et al. | Densification behaviour and microstructural development in undoped yttria prepared by flash-sintering | |
| Kermani et al. | Ultrafast high-temperature sintering (UHS) of fine grained α-Al2O3 | |
| Vanmeensel et al. | Modelling of the temperature distribution during field assisted sintering | |
| CN110577399B (en) | Multi-field coupling flash sintering system based on induction heating | |
| CN106630974A (en) | Flash sintering method of low-temperature flash sintering ceramic and obtained ceramic and device thereof | |
| CN108947542A (en) | The direct flash burning molding method for preparing of ceramic powder stock | |
| CN112390629B (en) | Device and method for rapidly sintering ceramic | |
| De Florio et al. | Sintering of zirconia–yttria ceramics studied by impedance spectroscopy | |
| Minier et al. | A comparative study of nickel and alumina sintering using spark plasma sintering (SPS) | |
| Liu et al. | Densification of pure magnesium by spark plasma sintering-discussion of sintering mechanism | |
| JP2010056064A (en) | High-frequency induction heating device of ceramic material, and nonpressurized sintering method using the same | |
| CN108534553A (en) | The device and method of block body ceramic material is quickly prepared using high-frequency induction heating | |
| CN110425877A (en) | Ceramic post sintering device and ceramic post sintering method | |
| CN111912227A (en) | Rapid sintering equipment and sintering method for dynamically loading coupled alternating current | |
| Liang et al. | Pressure‐assisted flash sintering of ZnO ceramics | |
| CN105906347A (en) | Method for preparing nanocrystal aluminum nitride ceramics | |
| CN210427243U (en) | Ultrahigh-temperature mechanical testing device for efficient non-magnetic ceramic | |
| CN109373761B (en) | Multi-field coupling material processing system |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |