CN106109329A - A kind of nano sunlight screening gel and preparation method thereof - Google Patents

A kind of nano sunlight screening gel and preparation method thereof Download PDF

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Publication number
CN106109329A
CN106109329A CN201610627001.8A CN201610627001A CN106109329A CN 106109329 A CN106109329 A CN 106109329A CN 201610627001 A CN201610627001 A CN 201610627001A CN 106109329 A CN106109329 A CN 106109329A
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China
Prior art keywords
nano
gel
barium sulfate
sunlight screening
extracting solution
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Pending
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CN201610627001.8A
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Chinese (zh)
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王永福
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Individual
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Individual
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of nano sunlight screening gel, it is made up of following raw material components by weight percentage: nano barium sulfate 3 ~ 6%；Nanocrystal cellulose 0.5 ~ 5%；High-molecular gel 65 ~ 70%；Semen Granati extracting solution 5 ~ 10%；Crocus sativus 5 ~ 10%；Glyceryl monostearate 0.5 ~ 1%；Vaseline 0.5 ~ 1%；Glycerol 5 ~ 8%.The present invention utilize nano barium sulfate and nanocrystal cellulose as sun-proof effective ingredient, can effective uvioresistant and skin is free from side effects, with the addition of Semen Granati extracting solution and crocus sativus with effective antioxidation and skin whitening simultaneously.The present invention is using high-molecular gel as substrate, without greasy feeling, and contributes to Semen Granati, the absorption of Stigma Croci Cosmetic Ingredient, quickly can form nano sunlight screening film on skin simultaneously.The preparation method of the present invention is simple, rational technology, and nano sunlight screening stock dispersion is uniform, and can effectively preserve Semen Granati and croceous nutritional labeling.

Description

A kind of nano sunlight screening gel and preparation method thereof
Technical field
The present invention relates to cosmetic field, particularly to a kind of nano sunlight screening gel and preparation method thereof.
Background technology
It is sun-proof that sun care preparations is roughly divided into chemical sunscreen, physical sunscreen and Chinese medicine.Wherein chemical sunscreen cosmetics are to skin Skin injury is bigger；Physical sunscreen cosmetics are the most greasy；Chinese medicine sun care preparations cost intensive.
Summary of the invention
It is an object of the invention to: for above-mentioned the deficiencies in the prior art, it is provided that a kind of nano sunlight screening gel and preparation thereof Method.
The technical solution used in the present invention is: a kind of nano sunlight screening gel, it is by weight percentage by following raw material Component forms:
Nano barium sulfate 3 ~ 6%；
Nanocrystal cellulose 0.5 ~ 5%；
High-molecular gel 65 ~ 70%；
Semen Granati extracting solution 5 ~ 10%；
Crocus sativus 5 ~ 10%；
Glyceryl monostearate 0.5 ~ 1%；
Vaseline 0.5 ~ 1%；
Glycerol 5 ~ 8%.
As the further improvement of such scheme, the particle diameter of described nano barium sulfate is 70 ~ 80nm, and described nanocrystal is fine The particle diameter of dimension element is 30 ~ 100nm.
As the further improvement of such scheme, described nano barium sulfate is hydrophilic nano barium sulfate.
As the further improvement of such scheme, the adding proportion of described Semen Granati extracting solution and crocus sativus is 1: 1。
A kind of preparation method of nano sunlight screening gel as above, it comprises the technical steps that:
(1) by proportioning raw materials, high-molecular gel, Semen Granati extracting solution and crocus sativus are added in reactor, stir under room temperature Mix mix homogeneously, obtain gel mixture, standby；
(2) first glyceryl monostearate, vaseline and glycerol are added in reactor by proportioning raw materials, are heated with stirring to 80 DEG C, Adding nano barium sulfate and nanocrystal cellulose, mixing and stirring, control mixing speed is 800 ~ 950r/min, obtains viscous Fused mixture, standby；
(3) by step (1) and step (2) gained gel mixture and viscous mixture stirring at normal temperature mix homogeneously, stirring is controlled Speed is 500 ~ 600r/min, sterilized, cooling after finished product.
The invention has the beneficial effects as follows: the present invention utilize nano barium sulfate and nanocrystal cellulose as sun-proof effective become Point, can effective uvioresistant and skin is free from side effects, with the addition of Semen Granati extracting solution and crocus sativus to have simultaneously Effect antioxidation and skin whitening.The present invention is using high-molecular gel as substrate, without greasy feeling, and contributes to Semen Granati, Stigma Croci The absorption of Cosmetic Ingredient, quickly can form nano sunlight screening film on skin simultaneously.The preparation method of the present invention is simple, and technique is closed Reason, nano sunlight screening stock dispersion is uniform, and can effectively preserve Semen Granati and croceous nutritional labeling.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is specifically described, in order to the personnel of art are to the present invention's Understand.It is necessary that at this present invention will be further described it is emphasized that embodiment is only intended to, it is impossible to be interpreted as this The restriction of invention protection domain, art person skilled in the art, the non-intrinsically safe present invention made according to foregoing invention content The improvement of property and adjustment, should still fall within protection scope of the present invention.The most following mentioned raw material is unspecified, is Commercially available prod；The processing step mentioned the most in detail or processing step that preparation method is dawn the most known to those skilled in the art or Preparation method.
Embodiment 1
A kind of nano sunlight screening gel, it is made up of following raw material components by weight percentage:
Nano barium sulfate 6%；
Nanocrystal cellulose 5%；
High-molecular gel 65%；
Semen Granati extracting solution 7%；
Crocus sativus 7%；
Glyceryl monostearate 1%；
Vaseline 1%；
Glycerol 8%.
Wherein, the particle diameter of described nano barium sulfate is 80nm, and the particle diameter of described nanocrystal cellulose is 30nm；Described receive Nano-barium sulfate is hydrophilic nano barium sulfate.
Preparation method:
(1) by proportioning raw materials, high-molecular gel, Semen Granati extracting solution and crocus sativus are added in reactor, stir under room temperature Mix mix homogeneously, obtain gel mixture, standby；
(2) first glyceryl monostearate, vaseline and glycerol are added in reactor by proportioning raw materials, are heated with stirring to 80 DEG C, Adding nano barium sulfate and nanocrystal cellulose, mixing and stirring, control mixing speed is 800r/min, obtains thickness and mixes Compound, standby；
(3) by step (1) and step (2) gained gel mixture and viscous mixture stirring at normal temperature mix homogeneously, stirring is controlled Speed is 600r/min, sterilized, cooling after finished product.
Embodiment 2
A kind of nano sunlight screening gel, it is made up of following raw material components by weight percentage:
Nano barium sulfate 3%；
Nanocrystal cellulose 1%；
High-molecular gel 70%；
Semen Granati extracting solution 10%；
Crocus sativus 10%；
Glyceryl monostearate 0.5%；
Vaseline 0.5%；
Glycerol 5%.
Wherein, the particle diameter of described nano barium sulfate is 70nm, and the particle diameter of described nanocrystal cellulose is 100nm；Described Nano barium sulfate is hydrophilic nano barium sulfate.
Preparation method:
(1) by proportioning raw materials, high-molecular gel, Semen Granati extracting solution and crocus sativus are added in reactor, stir under room temperature Mix mix homogeneously, obtain gel mixture, standby；
(2) first glyceryl monostearate, vaseline and glycerol are added in reactor by proportioning raw materials, are heated with stirring to 80 DEG C, Adding nano barium sulfate and nanocrystal cellulose, mixing and stirring, control mixing speed is 900r/min, obtains thickness and mixes Compound, standby；
(3) by step (1) and step (2) gained gel mixture and viscous mixture stirring at normal temperature mix homogeneously, stirring is controlled Speed is 500r/min, sterilized, cooling after finished product.
Embodiment 3
A kind of nano sunlight screening gel, it is made up of following raw material components by weight percentage:
Nano barium sulfate 6%；
Nanocrystal cellulose 5%；
High-molecular gel 70%；
Semen Granati extracting solution 5%；
Crocus sativus 5%；
Glyceryl monostearate 0.5%；
Vaseline 0.5%；
Glycerol 8%.
Wherein, the particle diameter of described nano barium sulfate is 80nm, and the particle diameter of described nanocrystal cellulose is 30nm；Described receive Nano-barium sulfate is hydrophilic nano barium sulfate.
Preparation method:
(1) by proportioning raw materials, high-molecular gel, Semen Granati extracting solution and crocus sativus are added in reactor, stir under room temperature Mix mix homogeneously, obtain gel mixture, standby；
(2) first glyceryl monostearate, vaseline and glycerol are added in reactor by proportioning raw materials, are heated with stirring to 80 DEG C, Adding nano barium sulfate and nanocrystal cellulose, mixing and stirring, control mixing speed is 950r/min, obtains thickness and mixes Compound, standby；
(3) by step (1) and step (2) gained gel mixture and viscous mixture stirring at normal temperature mix homogeneously, stirring is controlled Speed is 550r/min, sterilized, cooling after finished product.
Above-described embodiment is the preferred embodiments of the present invention, all technique similar with the present invention and the equivalence change made, The protection category of the present invention all should be belonged to.

Claims (5)

1. a nano sunlight screening gel, it is characterised in that: it is made up of following raw material components by weight percentage:
Nano barium sulfate 3 ~ 6%；
Nanocrystal cellulose 0.5 ~ 5%；
High-molecular gel 65 ~ 70%；
Semen Granati extracting solution 5 ~ 10%；
Crocus sativus 5 ~ 10%；
Glyceryl monostearate 0.5 ~ 1%；
Vaseline 0.5 ~ 1%；
Glycerol 5 ~ 8%.
A kind of nano sunlight screening gel the most according to claim 1, it is characterised in that: the particle diameter of described nano barium sulfate is 70 ~ 80nm, the particle diameter of described nanocrystal cellulose is 30 ~ 100nm.
A kind of nano sunlight screening gel the most according to claim 1, it is characterised in that: described nano barium sulfate is that hydrophilic is received Nano-barium sulfate.
A kind of nano sunlight screening gel the most according to claim 1, it is characterised in that: described Semen Granati extracting solution and Stigma Croci The adding proportion of extracting solution is 1:1.
5. the preparation method of a nano sunlight screening gel as claimed in claim 1, it is characterised in that: include that following technique walks Rapid:
(1) by proportioning raw materials, high-molecular gel, Semen Granati extracting solution and crocus sativus are added in reactor, stir under room temperature Mix mix homogeneously, obtain gel mixture, standby；
(2) first glyceryl monostearate, vaseline and glycerol are added in reactor by proportioning raw materials, are heated with stirring to 80 DEG C, Adding nano barium sulfate and nanocrystal cellulose, mixing and stirring, control mixing speed is 800 ~ 950r/min, obtains viscous Fused mixture, standby；
(3) by step (1) and step (2) gained gel mixture and viscous mixture stirring at normal temperature mix homogeneously, stirring is controlled Speed is 500 ~ 600r/min, sterilized, cooling after finished product.
CN201610627001.8A 2016-08-03 2016-08-03 A kind of nano sunlight screening gel and preparation method thereof Pending CN106109329A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610627001.8A CN106109329A (en) 2016-08-03 2016-08-03 A kind of nano sunlight screening gel and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610627001.8A CN106109329A (en) 2016-08-03 2016-08-03 A kind of nano sunlight screening gel and preparation method thereof

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Publication Number Publication Date
CN106109329A true CN106109329A (en) 2016-11-16

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018100062A1 (en) * 2016-11-30 2018-06-07 Chanel Parfums Beaute Sunscreen composition comprising nanocrystalline cellulose
WO2018100065A1 (en) * 2016-11-30 2018-06-07 Chanel Parfums Beaute Cosmetic composition comprising nanocrystalline cellulose, method and use thereof
CN109316367A (en) * 2018-11-29 2019-02-12 华南理工大学 A kind of ultra light sun block lotion and preparation method thereof containing nano-cellulose
FR3070862A1 (en) * 2017-09-14 2019-03-15 Quanshen Liu SKIN WHITENING AND SOLAR PROTECTION COMPOSITION COMPRISING NANO MATERIALS AND EXTRACT FROM CHINESE MEDICINE
US11166900B2 (en) 2016-11-30 2021-11-09 Anomera Inc. Powdery cosmetic composition comprising nanocrystalline cellulose
EP3958834A4 (en) * 2019-04-22 2023-07-12 ELC Management LLC Topical delivery system containing cellulose nanofibers

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102871942A (en) * 2011-12-12 2013-01-16 东莞市约德曼防辐射材料有限公司 Method for preparing physical radiation protection and sun-screen cosmetic for oily skin and product
CN103230355A (en) * 2013-05-06 2013-08-07 中国国旅贸易有限责任公司 Sunscreen cream cosmetic composition containing nano crystal cellulose

Patent Citations (2)

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Publication number Priority date Publication date Assignee Title
CN102871942A (en) * 2011-12-12 2013-01-16 东莞市约德曼防辐射材料有限公司 Method for preparing physical radiation protection and sun-screen cosmetic for oily skin and product
CN103230355A (en) * 2013-05-06 2013-08-07 中国国旅贸易有限责任公司 Sunscreen cream cosmetic composition containing nano crystal cellulose

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018100062A1 (en) * 2016-11-30 2018-06-07 Chanel Parfums Beaute Sunscreen composition comprising nanocrystalline cellulose
WO2018100065A1 (en) * 2016-11-30 2018-06-07 Chanel Parfums Beaute Cosmetic composition comprising nanocrystalline cellulose, method and use thereof
US11166900B2 (en) 2016-11-30 2021-11-09 Anomera Inc. Powdery cosmetic composition comprising nanocrystalline cellulose
FR3070862A1 (en) * 2017-09-14 2019-03-15 Quanshen Liu SKIN WHITENING AND SOLAR PROTECTION COMPOSITION COMPRISING NANO MATERIALS AND EXTRACT FROM CHINESE MEDICINE
CN109316367A (en) * 2018-11-29 2019-02-12 华南理工大学 A kind of ultra light sun block lotion and preparation method thereof containing nano-cellulose
EP3958834A4 (en) * 2019-04-22 2023-07-12 ELC Management LLC Topical delivery system containing cellulose nanofibers

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