CN106075537B - A kind of creeping chill gel rubber material and the preparation method and application thereof - Google Patents
A kind of creeping chill gel rubber material and the preparation method and application thereof Download PDFInfo
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/40—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
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- A—HUMAN NECESSITIES
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- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/18—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing inorganic materials
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/20—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing organic materials
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/22—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
- A61L15/24—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/22—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/44—Medicaments
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
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- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/41—Anti-inflammatory agents, e.g. NSAIDs
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Abstract
The invention discloses a kind of creeping chill gel rubber material and the preparation method and application thereof, the creeping chill gel rubber material is prepared by vegetation water, filler, creeping chill nucleating agent, gel former, thickener, dispersing agent, mineralizer, water;Preparation method includes: the vegetation water of the parts by weight, filler to be added in the water of the parts by weight, and creeping chill nucleating agent, gel former, thickener, dispersing agent, the mineralizer of the parts by weight is added in stirring, stirs, and forms uniform sticky mixed liquor;Mixed liquor obtained is subjected to negative pressure leaching by filter membrane, obtained smoke filtrate forms spherical gel particles through cooling and solidifying, the as described creeping chill gel rubber material.The creeping chill gel rubber material that the present invention is prepared has good application and prospect in preparing disposable sanitary articles.
Description
Technical field
The present invention relates to absorption pad fields, and in particular to a kind of creeping chill gel rubber material and the preparation method and application thereof.
Background technique
The materials such as disposable sanitary articles, including sanitary napkin, paper diaper, panty liner, incontinence pad, especially require material to have
There are good gas permeability, salubrious property, comfort, water imbibition etc..Current such amenities common problem is: because producing
Product thermal coefficient is low, and the dredging of body local heat is unsmooth, causes the symptoms such as sultry, red and swollen part, erythema, inflammation, cannot give people
Body brings good using body-sensing.There is part disposal sanitary article using cool feeling substances such as peppermints, since thermal coefficient is excessively high,
Cause body local excessively cool, women, children, the old and the weak's use will cause uncomfortable, resistance decrease.
Since resistance is weaker during women constitution is weaker and feminine menstrual, airtight, sultry amenities can be led
Cause the generation of the diseases such as gynaecological imflammation.Mainly use Western medicine oral the treatment of gynecological disease etc. at present square with drug suppository etc.
Method treatment, but this method treatment cost is big, it is easy to recur, therefore, using the feminine hygiene articles containing traditional Chinese medicine ingredients to treatment
Gynecological disease has good effect, but the amenities containing traditional Chinese medicine ingredients is generally with Chinese traditional powder or traditional Chinese medicine extraction at present
Directly as the inner core material of health product, this health product directly contacts with female private part object form, easily causes women negative
Portion's acid-base imbalance, to cause physically weak, cold body.The symptoms such as irregular menstruation.Therefore, using traditional Chinese medicine ingredients as disposable hygienic
When the core material of product, it should be noted that the product form of traditional Chinese medicine ingredients is with, product to the cold-storage capacity of heat transmission and product of human body
The stability of effect.
Chinese patent CN201210565788.1 discloses a kind of Chinese medicine antibacterial sanitary napkin, containing according to the following weight percentages
The functional material of preparation: polyamines polyol 3%~7%, sorbitol 4%~9%, Hinokitiol 5%~10%, kuh-seng 2%~
5%, Cortex Phellodendri 1%~3%, Radix Angelicae Sinensis 2%~5%, the root of Dahurain angelica 5%~10%, frutus cnidii 5%~10%, honeysuckle 25%~30%
With folium artemisiae argyi 20%~25%.But the patent, using Chinese medicine extract to be sprayed on sanitary napkin, this method makes female private part
With Chinese medical extract is upright contacts, directly stimulated, malleable female private part pH value makes female private part acid-base imbalance, more
It is encroached on vulnerable to external flora.
Chinese patent CN201310695849.0 discloses a kind of feminine napkin, including surface layer, internal layer, side and back
Glue fills effective component traditional Chinese medicine powder parts by weight: 14 parts of kuh-seng, 20 parts of motherwort, 25 parts of honeysuckle, thin in sanitary napkin internal layer
8 parts of lotus, 6 parts of oriental wormwood, 12 parts of rhizoma atractylodis, 10 parts, 5 parts of tourmaline powder of radix saposhnikoviae.But the patent is defended using the preparation of Chinese traditional powder form
Raw towel, the easy quick release of drug effect, it is difficult to guarantee the quality of product, and easily cause female body uncomfortable.
It is a kind of suitable for disposable sanitary articles, especially sanitary napkin, paper diaper, panty liner, mistake therefore, it is necessary to prepare
The creeping chill material for prohibiting the fields such as pad makes human body have good comfortable, salubrious body-sensing, and product form is stablized, and connects with human body
When touching, body-sensing is comfortable, has no adverse effects, and has good efficacy to gynaecological imflammation.
Summary of the invention
The present invention is in view of the above-mentioned problems, provide a kind of creeping chill gel rubber material and the preparation method and application thereof.
The present invention solve the above problems used by technical solution be: a kind of creeping chill gel rubber material, creeping chill gel rubber material by
100 parts of vegetation water, 5 parts~15 parts of filler, 4 parts~10 parts of creeping chill nucleating agent, 3 parts~5 parts of gel former, 1 part of thickener~
3 parts, 2 parts~4 parts of dispersing agent, 1 part~3 parts of mineralizer, 30 parts~50 parts of water be prepared;
Wherein, vegetation water be aloe liquid, Bitter Melon Juice, cucurbit juice, lucid asparagus liquid, motherwort juice, sweet basil liquid, Rhizoma Atractylodis Macrocephalae juice, when
Return juice, rough gentian grass juice factor any one or more of;Filler is that starch, hyaluronic acid, pentosan are any one or more of;Creeping chill
Nucleating agent is that kapur, purple perilla, folium isatidis, sweet wormwood, cassia seed, the fruit of glossy privet, Fructus Corni, Rhizoma Chuanxiong are any one or more of;It is solidifying
Glue forming agent is any one of zinc oxide, aluminium chloride, zinc chloride or two kinds;Thickener is sodium alginate, appointing in ferric sulfate
It is one or two kinds of;Dispersing agent is any one of Sodium Polyacrylate, single monoglyceride or two kinds;Mineralizer is copper sulphate, chlorination
Any one of copper or two kinds.
Further, creeping chill nucleating agent are as follows: the graininess powder that average grain diameter is 1 μm~3 μm.
Another goal of the invention of the invention is to provide a kind of preparation method of above-mentioned creeping chill gel rubber material, including following
Step:
Step 1 the vegetation water of the parts by weight, filler is added in the water of the parts by weight, is heated to 40 DEG C~60
DEG C, 30min~60min is stirred, 70 DEG C~90 DEG C is continuously heating to, creeping chill nucleating agent, the gel-forming of the parts by weight is added
Agent, thickener, dispersing agent, mineralizer stir 20min~40min, form uniform sticky mixed liquor;
Mixed liquor made from step 1 is carried out negative pressure leaching by the filter membrane that aperture is 3 μm~8 μm, obtained by step 2
Smoke filtrate through cooling and solidifying form spherical gel particles, the as described creeping chill gel rubber material.
Further, in step 1, the range of viscosities of mixed liquor is 2000mPas~4000mPas.
Further, in step 2, the vacuum degree of negative pressure is 0.8MPa~1.6MPa.
Further, in step 2, temperature range when cooling is 0 DEG C~5 DEG C.
Another goal of the invention of the invention is to provide a kind of above-mentioned creeping chill gel rubber material and is preparing disposable sanitary articles
In application, specifically: the creeping chill gel rubber material being prepared is arranged on base material, is carried out using skin-material
Cladding, carries out the cementing core material to get disposable sanitary articles of hot pressing with hot melt adhesive.
Further, disposable sanitary articles include: any one of sanitary napkin, paper diaper, panty liner, incontinence pad.
Further, base material are as follows: polypropylene, polyethylene, any material in polyethylene terephthalate
The non-woven fabrics being prepared.
Further, skin-material by: cotton fibre material is prepared.
The invention has the advantages that
1. the creeping chill gel rubber material that the present invention is prepared is prepared using vegetation water, property is uniform, stablizes, environmental protection,
It is non-stimulated;
2. the present invention is using the disposable sanitary articles of creeping chill gel rubber material preparation, thermal coefficient is moderate, and air penetrability is good,
It has no stimulation, to human body with salubrious, comfortable body-sensing, and contains traditional Chinese medicine ingredients, facilitate the growth for inhibiting microorganism;
3. the present invention has well hemorrhoid and gynaecological imflammation using the disposable sanitary articles of creeping chill gel rubber material preparation
Curative effect;
4. the preparation method of what the present invention used prepare creeping chill gel rubber material is easy, easily operated, production is advantageously reduced
Cost, thus scale volume production.
Specific embodiment
The embodiment of the present invention is described in detail below, but what the present invention can be defined by the claims and cover
Multitude of different ways is implemented.
Embodiment 1
A kind of creeping chill gel rubber material, by 50 parts of Bitter Melon Juice, 50 parts of cucurbit juice, 5 parts of starch, 2 parts of kapur, 2 parts of purple perilla, oxygen
Change 3 parts of zinc, 1 part of sodium alginate, 2 parts of Sodium Polyacrylate, 1 part of copper sulphate, 30 parts of water be prepared;
Wherein Bitter Melon Juice is that balsam pear is pruned to crust and interior seed, juice made of being squeezed;Cucurbit juice is to prune cucurbit
Crust and interior seed, juice made of being squeezed;Wherein kapur is the graininess powder that average grain diameter is 1 μm;Purple perilla is average
The graininess powder that partial size is 1 μm.
Embodiment 2
A kind of creeping chill gel rubber material, by 60 parts of aloe liquid, 20 parts of motherwort juice, 20 parts of sweet basil liquid, 15 parts of hyaluronic acid, big
3 parts of leafiness, 4 parts of sweet wormwood, 3 parts of cassia seed, 5 parts of aluminium chloride, 3 parts of ferric sulfate, single 4 parts of monoglyceride, 3 parts of copper chloride, 50 parts of water
It is prepared;
Wherein aloe liquid is juice made of squeezing fresh aloe;Motherwort juice is will be made of the squeezing of new fresh leonurus
Juice;Sweet basil liquid is juice made of being squeezed sweet basil;Wherein folium isatidis is the graininess powder that average grain diameter is 3 μm;It is green
Wormwood artemisia is the graininess powder that average grain diameter is 3 μm;Cassia seed is the graininess powder that average grain diameter is 3 μm.
Embodiment 3
A kind of creeping chill gel rubber material, by 100 parts of motherwort juice, 10 parts of pentosan, 3 parts of the fruit of glossy privet, 2 parts of Fructus Corni, Rhizoma Chuanxiong 2
Part, 4 parts of zinc chloride, sodium alginate, 1 part, 1 part of ferric sulfate, 2 parts of Sodium Polyacrylate, single 1 part of monoglyceride, 2 parts of copper sulphate, water
40 parts are prepared;
Wherein motherwort juice is by juice made of the squeezing of new fresh leonurus;It is 2 μm that wherein the fruit of glossy privet, which is average grain diameter,
Graininess powder;Fructus Corni is the graininess powder that average grain diameter is 2 μm;Rhizoma Chuanxiong is the graininess powder that average grain diameter is 2 μm.
Embodiment 4
A kind of creeping chill gel rubber material, by 30 parts of Rhizoma Atractylodis Macrocephalae juice, 30 parts of Radix Angelicae Sinensis juice, 40 parts of rough gentian grass juice factor, 1 part of starch, hyalomitome
Sour 3 parts, 3 parts of pentosan, 2 parts of kapur, 2 parts of the fruit of glossy privet, 1 part of Rhizoma Chuanxiong, 2 parts of zinc oxide, 1.5 parts of aluminium chloride, sodium alginate
1.5 parts, 1.2 parts of Sodium Polyacrylate, single 1.3 parts of monoglyceride, 1.5 parts of copper chloride, 35 parts of water be prepared;
Wherein Rhizoma Atractylodis Macrocephalae juice is juice made of squeezing Rhizoma Atractylodis Macrocephalae;Radix Angelicae Sinensis juice is juice made of squeezing Radix Angelicae Sinensis;Radix gentianae
Juice is juice made of being squeezed fresh radix gentianae;Wherein kapur is the graininess powder that average grain diameter is 1 μm;The fruit of glossy privet
The graininess powder for being 1 μm for average grain diameter;Rhizoma Chuanxiong is the graininess powder that average grain diameter is 3 μm.
Embodiment 5
A kind of creeping chill gel rubber material, by 50 parts of lucid asparagus liquid, 50 parts of aloe liquid, 6 parts of starch, 6 parts of hyaluronic acid, purple perilla 2
Part, 4 parts of cassia seed, 2 parts of Fructus Corni, 1 part of aluminium chloride, 3.5 parts of zinc chloride, 2.5 parts of ferric sulfate, 2.5 parts of Sodium Polyacrylate, list
1 part of monoglyceride, 1 part of copper sulphate, 1.5 parts of copper chloride, 45 parts of water be prepared;
Wherein lucid asparagus liquid is by juice made of the squeezing of fresh lucid asparagus;Aloe liquid is made of squeezing fresh aloe
Juice;Wherein purple perilla is the graininess powder that average grain diameter is 3 μm;Cassia seed is the graininess powder that average grain diameter is 2 μm;
Fructus Corni is the graininess powder that average grain diameter is 2 μm.
Embodiment 6
A kind of creeping chill gel rubber material, by 80 parts of aloe liquid, 20 parts of Rhizoma Atractylodis Macrocephalae juice, 3 parts of hyaluronic acid, 2 parts of pentosan, sweet wormwood
10 parts, 4 parts of zinc oxide, 1 part of zinc chloride, 0.6 part of sodium alginate, 0.4 part of ferric sulfate, 3 parts of Sodium Polyacrylate, 0.5 part of copper sulphate,
1 part of copper chloride, 40 parts of water be prepared;
Wherein aloe liquid is juice made of squeezing fresh aloe;Rhizoma Atractylodis Macrocephalae juice is juice made of squeezing Rhizoma Atractylodis Macrocephalae;Its
Middle sweet wormwood is the graininess powder that average grain diameter is 2.5 μm.
Embodiment 7
A kind of preparation method of creeping chill gel rubber material, comprising the following steps:
Step 1 the vegetation water of the parts by weight, filler is added in the water of the parts by weight, is heated to 40 DEG C, is turning
Speed stirs 30min under conditions of being 500r/min, is continuously heating to 70 DEG C, creeping chill nucleating agent, the gel of the parts by weight is added
Forming agent, thickener, dispersing agent, mineralizer first stir 5min under conditions of revolving speed is 80r/min, then improve revolving speed extremely
600r/min stirs 15min, forms the mixed liquor that uniform sticky range of viscosities is 2000mPas;
Step 2, the filter membrane for being 3 μm by aperture by mixed liquor made from step 1, in the item that vacuum degree is 0.8MPa
Negative pressure leaching is carried out under part, obtained smoke filtrate forms spherical gel particles through cooling and solidifying, the as described creeping chill gel rubber material.
Temperature range when wherein cooling down is 0 DEG C.
Embodiment 8
A kind of preparation method of creeping chill gel rubber material, comprising the following steps:
Step 1 the vegetation water of the parts by weight, filler is added in the water of the parts by weight, is heated to 60 DEG C, is turning
Speed stirs 60min under conditions of being 400r/min, is continuously heating to 90 DEG C, creeping chill nucleating agent, the gel of the parts by weight is added
Forming agent, thickener, dispersing agent, mineralizer first stir 10min under conditions of revolving speed is 70r/min, then improve revolving speed extremely
700r/min stirs 30min, forms the mixed liquor that uniform sticky range of viscosities is 4000mPas;
Step 2, the filter membrane for being 8 μm by aperture by mixed liquor made from step 1, in the item that vacuum degree is 1.6MPa
Negative pressure leaching is carried out under part, obtained smoke filtrate forms spherical gel particles through cooling and solidifying, the as described creeping chill gel rubber material.
Temperature range when wherein cooling down is 5 DEG C.
Embodiment 9
A kind of preparation method of creeping chill gel rubber material, comprising the following steps:
Step 1 the vegetation water of the parts by weight, filler is added in the water of the parts by weight, is heated to 50 DEG C, is turning
Speed stirs 45min under conditions of being 450r/min, is continuously heating to 80 DEG C, creeping chill nucleating agent, the gel of the parts by weight is added
Forming agent, thickener, dispersing agent, mineralizer first stir 8min under conditions of revolving speed is 75r/min, then improve revolving speed extremely
650r/min stirs 22min, forms the mixed liquor that uniform sticky range of viscosities is 3000mPas;
Step 2, the filter membrane for being 5 μm by aperture by mixed liquor made from step 1, in the item that vacuum degree is 1.2MPa
Negative pressure leaching is carried out under part, obtained smoke filtrate forms spherical gel particles through cooling and solidifying, the as described creeping chill gel rubber material.
Temperature range when wherein cooling down is 2 DEG C.
Embodiment 10
The creeping chill gel rubber material being prepared is arranged on polyethylene nonwoven base material, uses cotton fiber material
Expect that the skin-material being prepared is coated, carries out the cementing core material to get sanitary napkin of hot pressing with hot melt adhesive.
Embodiment 11
The creeping chill gel rubber material being prepared is arranged on polypropylene non-woven fabric base material, uses cotton fiber material
Expect that the skin-material being prepared is coated, carries out the cementing core material to get paper diaper of hot pressing with hot melt adhesive.
Embodiment 12
The creeping chill gel rubber material being prepared is spread on polyethylene terephthalate nonwoven fabric base bottom material
Row, coated using the skin-material that cotton fibre material is prepared, and it is cementing to get incontinence pad to carry out hot pressing with hot melt adhesive
Core material.
Embodiment 13
The creeping chill gel rubber material being prepared is arranged on polyethylene nonwoven base material, uses cotton fiber material
Expect that the skin-material being prepared is coated, carries out the cementing core material to get panty liner of hot pressing with hot melt adhesive.
Experimental example 1
The creeping chill gel rubber material that Examples 1 to 9 is prepared, is respectively labeled as 1~sample of sample 9, test to sample 1~
The thermal coefficient of sample 9, test result are as shown in table 1.Wherein thermal coefficient is tested using ASTM-D5470 method.
The performance test results of 1 creeping chill gel rubber material of table
Experimental example 2
The effect of sanitary napkin that testing example 10 is prepared is when treating hemorrhoid.
Choose women hemorrhoid patients 40, patient age be 20 years old~45 years old, the course of disease 0.5 year~5 years, 1 before patient assessment
Week does not carry out associated medication therapies, and patient is randomly divided into control group (20), test group (20), and wherein control group is using normal
Rule treatment, test group are assisted conventional therapy, after 7 days, are referred to inspection and anus microscopy through outpatient service anus using the sanitary napkin being prepared
It looks into, its curative effect is assessed, assessment result is as shown in table 2.
Drug effect compares before and after 2 medication of table
Experimental example 3
The panty liner that the sanitary napkin and embodiment 13 that testing example 10 is prepared are prepared is in treatment gynaecology's disease
The effect of when sick.Choose gynaecological imflammation patient 60, patient age be 20 years old~45 years old, the course of disease 0.5 year~2 years, patient assessment
Do not carry out within first 1 week associated medication therapies, patient is randomly divided into control group (20), test group (40), wherein control group not into
Row drug therapy, test group 1 (20) use the sanitary napkin being prepared, and test group 2 (20) use the health being prepared
Protection pad.The curative effect of cervicitis, vaginitis, vulvitis, several gynaecological imflammations of pruritus vulvue is counted after 14 days, statistics knot
Fruit is as shown in table 3.
Exclusion criteria: (1) crissum, rectum and colonic operation patient;(2) Patients with Fecal Incontinence;(3) gestation, acute abdomen, disappear
Change gastrointestinal hemorrhage patient;(4) severe cardiovascular disease patient;(5) endometriosis, gynecologic tumor;(6) serious liver kidney
Illness, diabetic.
Curative effect determinate standard
(1) cure: patient's lower abdominal pain, pendant, which rise to feel, to disappear, and secretion is reduced, and physical examination and laboratory check and be no different
Often, ultrasound diagnosis prompt does not find the Radiologic imagings such as mass, hydrops;
(2) effective: patient's lower abdominal pain, falling inflation sense disappear or significant mitigation, physical examination and laboratory examination results
It is obviously improved, mass, hydrops significantly reduce (1/2 or more) or disappear in ultrasound diagnosis prompt pelvic cavity;
(3) effectively: patient's lower abdominal pain, falling inflation sense mitigation, physical examination and laboratory examination results make moderate progress, B
It is super to check that mass, hydrops are reduced less than 1/2 in prompt pelvic cavity;
(4) invalid: the pretherapy and post-treatment clinical symptoms of patient, physical examination, laboratory check, ultrasound diagnosis is without substantially changeing very
To exacerbation.
Total effective rate=cure rate+obvious effective rate+effective percentage.
3 curative effect statistical result of table
Group | It cures | It is effective | Effectively | In vain | Total effective rate |
Test group 1 | 5 (25%) | 6 (30%) | 6 (30%) | 3 (15%) | 85% |
Test group 2 | 3 (15%) | 5 (25%) | 6 (30%) | 6 (30%) | 70% |
Control group | 0 (0%) | 1 (5%) | 2 (10%) | 17 (85%) | 15% |
These are only the preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of creeping chill gel rubber material, which is characterized in that the creeping chill gel rubber material is by 100 parts of vegetation water, filler 5 parts~15
Part, 4 parts~10 parts of creeping chill nucleating agent, 3 parts~5 parts of gel former, 1 part~3 parts of thickener, 2 parts of dispersing agent~4 parts, mineralising
1 part~3 parts of agent, 30 parts~50 parts of water be prepared;
Wherein, the vegetation water be aloe liquid, Bitter Melon Juice, cucurbit juice, lucid asparagus liquid, motherwort juice, sweet basil liquid, Rhizoma Atractylodis Macrocephalae juice, when
Return juice, rough gentian grass juice factor any one or more of;
The filler is that starch, hyaluronic acid, pentosan are any one or more of;
The creeping chill nucleating agent is kapur, purple perilla, folium isatidis, sweet wormwood, cassia seed, the fruit of glossy privet, Fructus Corni, any in Rhizoma Chuanxiong
Kind is a variety of;
The gel former is any one of zinc oxide, aluminium chloride, zinc chloride or two kinds;
The thickener is any one of sodium alginate, ferric sulfate or two kinds;
The dispersing agent is any one of Sodium Polyacrylate, single monoglyceride or two kinds;
The mineralizer is any one of copper sulphate, copper chloride or two kinds;The preparation method of the creeping chill gel rubber material, including
Following steps:
Step 1 the vegetation water of the parts by weight, filler is added in the water of the parts by weight, is heated to 40 DEG C~60 DEG C, stirs
30min~60min is mixed, is continuously heating to 70 DEG C~90 DEG C, creeping chill nucleating agent, the gel former, increasing of the parts by weight is added
Thick dose, dispersing agent, mineralizer stir 20min~40min, form uniform sticky mixed liquor;
Mixed liquor made from step 1 is carried out negative pressure leaching, obtained pumping by the filter membrane that aperture is 3 μm~8 μm by step 2
Filtrate forms spherical gel particles through cooling and solidifying, the as described creeping chill gel rubber material.
2. creeping chill gel rubber material according to claim 1, which is characterized in that the creeping chill nucleating agent are as follows: average grain diameter 1
μm~3 μm of graininess powder.
3. creeping chill gel rubber material according to claim 1, which is characterized in that in step 1, the viscosity model of the mixed liquor
It encloses for 2000mPas~4000mPas.
4. creeping chill gel rubber material according to claim 1, which is characterized in that in step 2, the vacuum degree of the negative pressure is
0.8MPa~1.6MPa.
5. creeping chill gel rubber material according to claim 1, which is characterized in that the temperature model in step 2, when described cooling
Enclose is 0 DEG C~5 DEG C.
6. a kind of creeping chill gel rubber material according to any one of claims 1 to 5 is in preparing disposable sanitary articles
Using, specifically: the creeping chill gel rubber material being prepared is arranged on base material, is wrapped using skin-material
It covers, carries out the cementing core material to get disposable sanitary articles of hot pressing with hot melt adhesive.
7. application according to claim 6, which is characterized in that the disposable sanitary articles include: sanitary napkin, paper urine
Any one of trousers, panty liner, incontinence pad.
8. application according to claim 6, which is characterized in that the base material are as follows: polypropylene, gathers to benzene polyethylene
The non-woven fabrics that any material in naphthalate is prepared.
9. application according to claim 6, which is characterized in that the skin-material by: cotton fibre material is prepared.
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CN107997245B (en) * | 2018-01-22 | 2019-06-21 | 浙江夏舒生物科技有限公司 | A kind of underwear plant cool feeling material and its preparation process |
CN108245701A (en) * | 2018-01-22 | 2018-07-06 | 浙江夏舒生物科技有限公司 | A kind of preparation process of amenities plant aloe extract gel rubber material |
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CN101184513A (en) * | 2004-12-13 | 2008-05-21 | 东南医疗技术有限公司 | Agents for controlling biological fluids and methods of use thereof |
CN103550819A (en) * | 2013-10-31 | 2014-02-05 | 天津市中科健新材料技术有限公司 | Absorbable product |
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ATE327778T1 (en) * | 2001-04-17 | 2006-06-15 | Procter & Gamble | REFRESHING COMPOSITIONS |
EP1250941A1 (en) * | 2001-04-17 | 2002-10-23 | The Procter & Gamble Company | Articles comprising a mint odor-free cooling agent |
CA2716125A1 (en) * | 2008-02-22 | 2009-08-27 | The Procter & Gamble Company | Absorbent article comprising lotion composition comprising a cooling agent |
CN104096259B (en) * | 2014-07-18 | 2016-05-25 | 天津信氏达科技发展有限公司 | A kind of cool feeling delivering compositions and application thereof |
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CN101184513A (en) * | 2004-12-13 | 2008-05-21 | 东南医疗技术有限公司 | Agents for controlling biological fluids and methods of use thereof |
CN103550819A (en) * | 2013-10-31 | 2014-02-05 | 天津市中科健新材料技术有限公司 | Absorbable product |
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