CN106047603A - Nano-molecular liquor and preparation method thereof - Google Patents

Nano-molecular liquor and preparation method thereof Download PDF

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Publication number
CN106047603A
CN106047603A CN201610677523.9A CN201610677523A CN106047603A CN 106047603 A CN106047603 A CN 106047603A CN 201610677523 A CN201610677523 A CN 201610677523A CN 106047603 A CN106047603 A CN 106047603A
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China
Prior art keywords
liquor
nano
wine
molecular
ice stone
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CN201610677523.9A
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Chinese (zh)
Inventor
张�林
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Chengde Jiulong Industrial Co Ltd
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Chengde Jiulong Industrial Co Ltd
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Priority to CN201610677523.9A priority Critical patent/CN106047603A/en
Publication of CN106047603A publication Critical patent/CN106047603A/en
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/22Ageing or ripening by storing, e.g. lagering of beer

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Toxicology (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

The invention discloses nano-molecular liquor and a preparation method thereof. A nano coating container is produced by spraying a coating and tourmaline onto an inner wall of a stainless steel container through a one-step high-pressure spray-coating technology. Luzhou-flavor high-quality liquor, which is regulated and filtered before, is stored in the nano coating container for 24 h, and then is filtered and regulated and is stored for 30 days to obtain the nano-molecular liquor. In the technical scheme, the common liquor is stored in the nano coating container to accelerate aging of the liquor and adsorb odors in the liquor, wherein molecules in the liquor are rearranged and recombined so that the liquor has a more mellow and soft taste. The nano-molecular liquor, compared with common liquor, has a more moderate and soft mouth feel, can avoid thirst after people drink the liquor, and is short in alcohol-effect-dispelling time.

Description

A kind of nano molecular wine and preparation method thereof
Technical field
The present invention relates to a kind of nano molecular wine and preparation method thereof.
Background technology
Rare ice stone is also called tourmaline, and mineralogist is referred to as tourmaline, it be by magnesium, ferrum, stannum, manganese, sodium, cobalt, silicon, Fluorine, copper, titanium, selenium and other trace elements and mineral composition, be a kind of permanent electric polar crystal material with pyroelectric effect.Strange ice Stone nano material has the light of brilliance, power, heat, electric absorption, the effect of catalytic decomposition, and its absorption affinity and extension are other materials Hundred times.Studying through the expert of numerous medical circles and show, when water is by rare ice stone nano material, that can kill in water is thin Bacterium, harmful substance in decomposition water, the abnormal flavour in absorption water, strengthen the gap width of hydrone, improve activation and the dissolving of water Degree, reduces the adhesive effect in water, makes water softening.
Summary of the invention
The technical problem to be solved is for the deficiencies in the prior art, and provides a kind of nano molecular The preparation method of wine, Chinese liquor stores in nano paint tank, can accelerate the aging of Chinese liquor, abnormal flavour in sorbing liquor, makes in Chinese liquor Constituent content change, make the more mellow cotton of wine body soft.
The two of the purpose of the present invention are to provide a kind of nano molecular wine being prepared from through said method, and this wine is than common Chinese liquor more coordinates, cotton soft, not xerostomia after drink, the relieving alcoholic intoxication time is fast.
To achieve these goals, the present invention adopts the following technical scheme that
The preparation method of a kind of nano molecular wine, it is characterised in that comprise the following steps:
(1) one-level debugging: using Luzhou-flavor high quality liquor that commercially available, alcoholic strength are 65~68 degree as base liquor, with employing Softening water, as softening water, is added in base liquor and base liquor is adjusted ethanol by the drinking water after reverse osmosis water purifier process Degree so that it is alcoholic strength drops to the required Chinese liquor number of degrees;
(2) single filter: the wine product obtained after step (1) being debugged filter with diatom filter after stirring;
(3) one-level storage: the wine product obtained after step (2) being filtered are placed in nano paint container, under normal temperature condition Sealed type storage 24h;
(4) cascade filtration: the wine product micro-porous filtration plate obtained after step (3) being stored filters;
(5) two grades of debugging: add amino sugar in the wine product obtained after step (4) filters, add in every 100g wine product 0.85-1.15mg amino sugar;
(6) two grades of storages: the wine product after step (5) being debugged are placed in another nano paint container, at normal temperature condition Lower seal is stored 30 days, and storage i.e. obtains nano molecular wine after terminating.
In technique scheme, in step (1), the described required Chinese liquor number of degrees are 33.6 degree, 36 degree, 42 degree or 52 Degree.
In technique scheme, the nano paint container described in step (3) and step (6) is to be prepared by following method :
1. after broken for rare ice stone, it is prepared as nano level rare ice stone powder;
2. by after paint heating to 50~85 DEG C, with the nanoscale rare ice stone powder described in step (1) according to 15~25:1 Weight ratio mix homogeneously;
3. mixture step 2. obtained carries out disposable high pressure painting to the inwall of liquor storage vessel, natural wind after spraying Do and within 10 days, i.e. obtain described nano paint container.
Preferably, step 1. described in nano level rare ice stone powder, its particle diameter is 0.1~100 nanometers.
Preferably, step 2. in, described coating is commercially available edible coating T99-30, including base material and firming agent, will After base material is heated to 75~85 DEG C, firming agent is heated to 50~70 DEG C, according to after the weight ratio mix homogeneously of 1:1 again with described Nano level rare ice stone powder mixes.
Preferably, step 2. in, weight ratio when described coating mixes with nanoscale rare ice stone powder is preferably 20:1.
Preferably, step 3. in, described liquor storage vessel is rustless steel container or ceramic vessel.
Preferably, step 3. in, described disposable high pressure painting, the pressure of its high pressure is 60~300kg/cm2
Preferably, step 3. in, when carrying out high pressure painting, the spray of the mixture of every kilogram of coating and nanoscale rare ice stone powder Being coated with the inwall of the liquor storage vessel of 20 square metres, the thickness of spraying is 0.4-0.7mm.
In technique scheme, described reverse osmosis water purifier, diatom filter, micro-porous filtration plate (bore dia 0.1~ 1mm) it is routine, commercial equipment, operates according to its operating process.
The present invention also provides for a kind of to nano molecular wine, is prepared from by said method.
The advantage of technical solution of the present invention is: common white spirit is stored in nano paint tank, can accelerate Chinese liquor Aging, abnormal flavour in sorbing liquor, make wine molecular rearrangement combine, make the more mellow cotton of wine body soft;The nano molecular being prepared from Wine, this wine more coordinates than common white spirit, cotton soft, and not xerostomia after drink, the relieving alcoholic intoxication time is fast.
Detailed description of the invention
Hereinafter the detailed description of the invention of technical solution of the present invention is described in detail, but the present invention is not limited in following description Hold:
In following example, described reverse osmosis water purifier, diatom filter, micro-porous filtration plate (bore dia 0.4mm) Being commercial equipment, one time high pressure painting uses high pressure airless spray equipment to complete.
Embodiment 1:
A kind of nano paint container, is prepared from by following method:
1. after being pulverized by rare ice stone, being prepared as rare ice stone powder with physical medium extractor, particle diameter is about 50-60nm;
2. the base material of edible coating T99-30 is heated to 80~85 DEG C, after firming agent is heated to 60~65 DEG C, according to 1:1 Weight ratio mix homogeneously after, the nanoscale rare ice stone powder obtained according to weight ratio and the step (1) of 20:1 is mixed homogeneously;
3. mixture step 2. obtained carries out disposable high pressure painting to the inwall of rustless steel container, and pressure is 100kg/cm2Left and right, the mixture of every kilogram of coating and nanoscale rare ice stone powder sprays the rustless steel container of 20 square metres Inwall, the thickness of spraying is 0.4-0.7mm;After spraying, natural air drying i.e. obtains described nano paint container for 10 days.
Embodiment 2:
A kind of nano paint container, preparation method is essentially identical with embodiment, except that, step 3. in for pottery The inwall of container carries out disposable high pressure painting, finally gives nano paint container.
Embodiment 3:
A kind of nano molecular wine, is prepared from by following method:
(1) one-level debugging: using commercially available, alcoholic strength be the Luzhou-flavor quality liquor of 65 degree as base liquor, to use reverse osmosis Softening water, as softening water, is added in base liquor and base liquor is adjusted alcoholic strength by the drinking water after water purifier softening so that it is Alcoholic strength is 33.6 degree;
(2) single filter: the wine product obtained after step (1) being debugged filter with diatom filter after stirring;
(3) one-level storage: the wine product obtained after step (2) being filtered are placed in the nano paint container that embodiment 1 obtains, 24h is stored at normal temperature condition lower seal;
(4) cascade filtration: the wine product micro-porous filtration plate obtained after step (3) being stored filters;
(5) two grades of debugging: add amino sugar in the wine product obtained after step (4) filters, add 1mg in every 100g wine product Amino sugar;
(6) two grades of storages: the wine product after step (5) being debugged are placed in the nano paint container that another embodiment 1 obtains In, to store 30 days at normal temperature condition lower seal, storage i.e. obtains nano molecular wine after terminating.
The nano molecular wine that base liquor and the present embodiment obtain, its sense organ and physical and chemical index are according to GB/T10781.1-2006 (top grade) examination criteria is carried out, and sanitary index detects according to the examination criteria of GB2757, and net content is according to the inspection of JJF1070 Mark standard detects, and amino sugar content detects according to the examination criteria of Q/JLJT0001S-2014, result such as table 1 institute Show:
Table 1: the base liquor of embodiment 1 and the various index of nano molecular wine
As shown in Table 1, through wine product prepared by the inventive method, indices complies fully with national standard, and, acetic acid second The parameters such as ester, ethyl hexanoate and amino sugar have raising in various degree, and acetic acid, methanol etc. affect mouthfeel, the parameter of the sense of taste has Reduction in various degree, vinosity is more mellow.
Embodiment 4:
A kind of nano molecular wine, preparation method is substantially the same manner as Example 3, except that, in step (3) and (6) Nano paint container is the nano paint container that embodiment 2 obtains, and obtains nano molecular wine.
The nano molecular wine that base liquor and the present embodiment obtain, its sense organ and physical and chemical index are according to GB/T10781.1-2006 (top grade) examination criteria is carried out, and sanitary index detects according to the examination criteria of GB2757, and net content is according to the inspection of JJF1070 Mark standard detects, and amino sugar content detects according to the examination criteria of Q/JLJT0001S-2014, result such as table 2 institute Show:
Table 2: the base liquor of embodiment 2 and the various index of nano molecular wine
As shown in Table 2, through wine product prepared by the inventive method, indices complies fully with national standard, and, acetic acid second The parameters such as ester, ethyl hexanoate and amino sugar have raising in various degree, and acetic acid, methanol etc. affect mouthfeel, the parameter of the sense of taste has Reduction in various degree, vinosity is more mellow.
Application Example
1000 consumers are uniformly divided into 10 groups according to the size of capacity for liquor, often organize 100 people, according to daily drink when everyone has dinner Wine method and drinking amount quote the wine product that the embodiment of the present invention 3 obtains, and add up the performance after drinking;Phase is drunk equally after second day The base liquor of the number of degrees commensurability, identical, adds up the performance after drinking, and result is as shown in table 3:
After drinking wine product and the corresponding base liquor of the embodiment of the present invention 3 respectively, survey result is as shown in table 3:
Table 3: the sensation after the drinking of different wine product and relieving alcoholic intoxication time
As shown in Table 3, the wine product that the inventive method obtains, cotton soft, not xerostomia after drink, the relieving alcoholic intoxication time is fast,
Examples detailed above simply for technology design and the technical characterstic of the present invention are described, can not limit the present invention's with this Protection domain.All equivalent transformations done according to the essence of the present invention or modification, all should contain in protection scope of the present invention Within.

Claims (10)

1. the preparation method of a nano molecular wine, it is characterised in that comprise the following steps:
(1) one-level debugging: using commercially available, alcoholic strength be the Luzhou-flavor high quality liquor of 65~68 degree as base liquor, to use reverse osmosis Softening water, as softening water, is added in base liquor and base liquor is adjusted alcoholic strength, make by the drinking water after water purifier processes thoroughly Its alcoholic strength drops to the required Chinese liquor number of degrees;
(2) single filter: the wine product obtained after step (1) being debugged filter with diatom filter after stirring;
(3) one-level storage: the wine product obtained after step (2) being filtered are placed in nano paint container, at normal temperature condition lower seal Storage 24h;
(4) cascade filtration: the wine product micro-porous filtration plate obtained after step (3) being stored filters;
(5) two grades of debugging: add amino sugar in the wine product obtained after step (4) filters, add 0.85-in every 100g wine product 1.15mg amino sugar;
(6) two grades of storages: the wine product after step (5) being debugged are placed in another nano paint container, close under normal temperature condition Envelope storage 30 days, storage i.e. obtains nano molecular wine after terminating.
Method the most according to claim 1, it is characterised in that the required Chinese liquor number of degrees described in step (1) are 33.6 degree, 36 degree, 42 degree or 52 degree.
Method the most according to claim 1, it is characterised in that the nano paint container described in step (3) and step (6) It is prepared from by following method:
1. after broken for rare ice stone, it is prepared as nano level rare ice stone powder;
2. by after paint heating to 50~85 DEG C, with the nanoscale rare ice stone powder described in step (1) according to 15~25:1 weight Amount compares mix homogeneously;
3. mixture step 2. obtained carries out disposable high pressure painting to the inwall of liquor storage vessel, natural air drying 10 after spraying It i.e. obtains described nano paint container.
Method the most according to claim 3, it is characterised in that step 1. described in nano level rare ice stone powder, its Particle diameter is 0.1~100 nanometers.
Method the most according to claim 3, it is characterised in that step 2. in, described coating is commercially available edible coating T99-30, including base material and firming agent, is heated to 75~85 DEG C, after firming agent is heated to 50~70 DEG C by base material, according to 1:1's Mix with described nano level rare ice stone powder again after weight ratio mix homogeneously.
Method the most according to claim 3, it is characterised in that step 2. in, described coating and nanoscale rare ice stone powder The weight ratio during mixing of end is 20:1.
Method the most according to claim 3, it is characterised in that step 3. in, described liquor storage vessel is rustless steel container Or ceramic vessel.
Method the most according to claim 3, it is characterised in that step 3. in, described disposable high pressure painting, its high pressure Pressure be 60~300kg/cm2
Method the most according to claim 3, it is characterised in that step 3. in, when carrying out high pressure painting, every kilogram of coating and The mixture of nanoscale rare ice stone powder sprays the inwall of the liquor storage vessel of 20 square metres, and the thickness of spraying is 0.4-0.7mm.
10. a nano molecular wine, it is characterised in that be prepared from by method described in any one of claim 1-8.
CN201610677523.9A 2016-08-17 2016-08-17 Nano-molecular liquor and preparation method thereof Pending CN106047603A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113308329A (en) * 2021-06-21 2021-08-27 内蒙古佘太酒业股份有限公司 Nano material and application of upper material tank thereof in white spirit aging
CN115925448A (en) * 2022-12-06 2023-04-07 河南海利未来生物药业有限公司 Ru porcelain for curing white spirit and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2637352Y (en) * 2003-06-14 2004-09-01 北京立高高新技术研究所 Nanometer wine quick ageing container
CN1616637A (en) * 2003-11-10 2005-05-18 北京立高高新技术研究所 Method for producing biological nano white spirit
CN1814740A (en) * 2005-12-07 2006-08-09 梁音 Method for purifying spirit liquor by nano-porcelain small balls
CN104961438A (en) * 2015-06-25 2015-10-07 福建省德化县瑞成陶瓷有限公司 Formula and preparation method for ceramic wine jar preform body capable of accelerating alcohol alcoholization

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2637352Y (en) * 2003-06-14 2004-09-01 北京立高高新技术研究所 Nanometer wine quick ageing container
CN1616637A (en) * 2003-11-10 2005-05-18 北京立高高新技术研究所 Method for producing biological nano white spirit
CN1814740A (en) * 2005-12-07 2006-08-09 梁音 Method for purifying spirit liquor by nano-porcelain small balls
CN104961438A (en) * 2015-06-25 2015-10-07 福建省德化县瑞成陶瓷有限公司 Formula and preparation method for ceramic wine jar preform body capable of accelerating alcohol alcoholization

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113308329A (en) * 2021-06-21 2021-08-27 内蒙古佘太酒业股份有限公司 Nano material and application of upper material tank thereof in white spirit aging
CN115925448A (en) * 2022-12-06 2023-04-07 河南海利未来生物药业有限公司 Ru porcelain for curing white spirit and preparation method thereof

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Application publication date: 20161026