CN106032449A - Matt finishing varnish and preparation process thereof - Google Patents
Matt finishing varnish and preparation process thereof Download PDFInfo
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Abstract
The invention provides a matt finishing varnish and a preparation process thereof, and belongs to the field of stone-like coating materials, wherein the raw materials of the matt finishing varnish comprise, by weight, 25-40% of deionized water, 0-0.2% of a dispersing agent, 0.05-0.1% of a wetting agent, 2.5-6% of a matting material, 0.1-0.2% of an antifoaming agent, 50-65% of an emulsion, 2-5% of a film-forming auxiliary agent, 0.1-0.3% of a sterilization agent, 1-6% of an antifouling agent, and 0.2-0.5% of a thickening agent. The preparation process comprises: sequentially adding the raw materials to a material mixing barrel according to the formula to obtain a mixed material; and carrying out evacuation and gas bubble removing on the mixed material, and adding the thickening agent to obtain the matt finishing varnish. According to the present invention, with the matt finishing varnish, the contaminants can be easily removed, the occurrence of the rain mark can be avoided, and the hydrophilic self-cleaning effect can be achieved.
Description
Technical field
The present invention relates to stone-like coating field, particularly relate to a kind of dumb light finishing varnish and preparation technology thereof.
Background technology
Currently, imitative stone class coating (true mineral varnish, sliver paint etc.) is after spraying, and its surface is the thickest
Rough, after coating dumb light finishing varnish, both played the effect that should have of cover agent, and stone material can have been gone out in surface again
Texture surface, feels simplicity, low-key, generous sensation to people.And imitate the coating surface of stone class, granular sensation
More obvious, easily accumulate dust.
Existing finishing varnish is after emulsion film forming, and the polymer type coating majority of formation is hydrophobic film,
Owing to there are a lot of non-natural pollutant in air, the especially medium oil pollutant of atmosphere pollution gradually increase
Adding, they can adsorb the surface at the polymerization hydrophobic film of species, is difficult to be taken away by rain drop erosion, easily stays
Under ugly rainprint.
Summary of the invention
The present invention proposes a kind of dumb light finishing varnish and preparation technology thereof, solves above-mentioned existing dumb light cover clear
Paint easily adsorbs dust, problem the most easy to clean.
The technical scheme is that and be achieved in that:
A kind of dumb light finishing varnish, its raw material includes according to percentage by weight: deionized water 25-40%, dispersion
Agent 0-0.2%, wetting agent 0.05-0.1%, quenching matter 2.5-6%, defoamer 0.1-0.2%, emulsion 50-65%,
Coalescents 2-5%, antibacterial 0.1-0.3%, anti-fouling agent 1-6%, thickening agent 0.2-0.5%.
The invention still further relates to the preparation technology of above-mentioned dumb light finishing varnish, comprise the following steps: a, according to weight
Percentage ratio, is sequentially added into deionized water, dispersant, wetting agent in mixing tank, carries out stirring for the first time；
Add quenching matter, carry out second time and stir, then improve mixing speed, carry out third time and stir, make
The abundant wetting and dispersing of quenching matter；B, regulation rotating speed carry out the 4th stirring, and defoamer is joined step a
System in the middle of, until the invisible foam in surface；Sequentially add emulsion, coalescents, antibacterial, prevent
Dirty agent, adds while stirring, and regulation rotating speed carries out the 5th stirring；Obtain compound；C, by described mixing
After material evacuation bubble removing, add thickening agent while stirring, obtain described dumb light finishing varnish.
The invention have the benefit that
1, the present invention use type siloxane and derivant thereof as anti-fouling agent, it in the film forming procedure of coating
The hydroxy that surface is formed so that film has hydrophilic, and the oiliness pollutant in air are at hydrophilic film
Surface is not easy attachment, and rainwater has good wettability in hydrophilic film coated surface, it is easy to sprawl open form
Become moisture film, not only can easily take away pollutant, but also the generation of rainprint problem can be avoided, reach parent
Water automatically cleaning effect.
2, use general silica class flatting silica, after long-time storage, significantly precipitation can be produced, with it
Comparing, the quenching matter that the present invention uses is with hollow silica as carrier, does Lasaxing Oilfield on its surface,
The wax wrapped up is TPO, and its surface processes especially, easily disperses；Its density is at 0.95-1.05g/cm3
Between, can mix with the component such as water and emulsion, can not have significantly precipitation with even suspension wherein.
3, the dumb light finishing varnish that prepared by the present invention carries out following test, and its performance indications are as shown in table 1.
1) resistance to water-white test: the resistance to water-white important indicator being to check water-resistant coating energy of coating, water-tolerant is met
Water does not bleaches, and the resistance to water bad chance water capacity easily bleaches；The coating film coated is put in water the most after drying
Soak 2 hours and observe situation about bleaching.
2) the dumb light finishing varnish film prepared in embodiment is fully dried, carry out resistance to according to standard method
Aqueous, alkali resistance, acid rain resistant are tested, whether have before and after observing its test fade, rupture, foaming etc. abnormal
Situation.
3) use roller coat (or spraying), by the coatings of preparation at smooth aluminium foil surface, try in standard
Test maintenance 168h film forming under condition (temperature 23 ± 2 DEG C, relative humidity 50 ± 5%), i.e. obtain print；Will
Print carries out hydrophilic test, and method of testing is as follows:
1. initial hydrophilic test: use contact angle instrument to measure the water droplet contact when film coated surface is sprawled 30 seconds
Angle；
2. hydrophilic test after polluting: the print coated employing polluter (is advised in GB/T 9780-2005
Fixed test polluter), and polluter is configured to polluter suspension according in GB/T 9780-2005 8.1
Liquid, carries out pollution process according to 8.2.1.1 in GB/T 9780-2005 afterwards, after five circulations, tests water
Drop in contact angle when film coated surface is sprawled 30 seconds.
Table 1
| Project | Standard | Method | Result | Remarks |
| Resistance to water | GB/T 1733 | 96h | Without exception | |
| Alkali resistance | GB/T 9265 | 48h | Without exception | |
| Acid rain resistant is tested | GB/T 9274 | 48h | Without exception | |
| Water-whitening resistance | Said method 1 | 2h | Without exception | |
| Measurement of luster | Glossometer is tested | 60 degree of tests | 10-30Gu | Quenching matter is the most, and gloss is the least |
| Initial hydrophilic angle | Contact angle instrument | Said method is 1. | ≤10° | |
| Hydrophilic angle after pollution | Contact angle instrument | Said method is 2. | ≤25° |
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that retouched
The embodiment stated is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art obtained under not making creative work premise all its
His embodiment, broadly falls into the scope of protection of the invention.
Dumb light finishing varnish in embodiment, its raw material includes according to percentage by weight: deionized water 25-40%,
Dispersant 0-0.2%, wetting agent 0.05-0.1%, quenching matter 2.5-6%, defoamer 0.1-0.2%, emulsion
50-65%, coalescents 2-5%, antibacterial 0.1-0.3%, anti-fouling agent 1-6%, thickening agent 0.2-0.5%.
In embodiment, anti-fouling agent is type siloxane and derivant thereof, such as DOW CORNING DC193, vapour bar chemistry
IRGASURFTMHL560, Nantong mahatma weaves DF-121, the Chinese this chemistry Hans/Qs etc.；Delustring thing
Matter is with the silicon dioxide of hollow as carrier, wraps up TPO material on its surface, and TPO material is such as
Lu Borun chemical industry liquiMatt 6375, Midland, MI Matt920 etc.；Emulsion is that pure-acrylic emulsion is (such as Showa
Chemical industry AP4690, AP4765, TL-1143 or Ahmedabad richness RS-706T etc.), silicone acrylic emulsion is (as Ahmedabad is rich
RS-3788, RS-996AD, RS-996KD etc.) in one or both compound emulsion；Dispersant is ammonium salt
The dispersant of class, such as Dow Orotan1124, nopco SN-5027 etc.；Described wetting agent is without alkyl phenol
The wetting agent of polyoxyethylene ether compounds (being called for short APEO), such as Clariant LCN407, BasfWE 3111 etc.；Described coalescents be in alcohol ester 12, butyl carbitol one or both
Mixture；Described thickening agent is that polyurethanes thickening agent is (such as DOW RM-8W, Basf Rheovis
Pu1291, Basf Rheovis pu1191, SN-621N etc.), hydrophobically-modified alkali swelling class thickening agent is (such as Basf
Rheovis HS 1152, DOW ACRYSOL DR-73 etc.) in one or both mixture.
In embodiment, defoamer is the special defoamer of hydrophilic coating, such as Nippon Nopco Assistant Co., Ltd. SN-
Defoamer 327, Basf formstar A10, the bright icepro AGITAN A221 of Germany etc..Antibacterial in embodiment
For antibacterial commonly used in the art, such as THOR ACTICIDE EPW, THOR ACTICIDE HF, section's Lay
Grace CI15MV etc..
The invention still further relates to the preparation technology of above-mentioned dumb light finishing varnish, comprise the following steps:
A, according to percentage by weight, mixing tank is sequentially added into deionized water, dispersant, wetting agent, enters
Row stirring for the first time；Add quenching matter, carry out second time and stir, then improve mixing speed, carry out
Third time stirring, makes the abundant wetting and dispersing of quenching matter；
B, regulation rotating speed carry out the 4th stirring, are joined in the middle of the system of step a by defoamer, until table
The invisible foam in face；Sequentially add emulsion, coalescents, antibacterial, anti-fouling agent, add while stirring,
Regulation rotating speed carries out the 5th stirring；Obtain compound；
C, by after described compound evacuation bubble removing, add thickening agent while stirring, obtain described dumb light cover
Face varnish.
Preferably, in embodiment, the addition of raw material must be sequentially added in order, delustring thing the most easily occurs
The phenomenons such as matter dispersion is uneven, easily causing finishing varnish surface has little granule, affects apparent effect.
Preferably, the rotating speed of stirring is 100-200r/m for the first time, mixing time 5min；Second time stirring
Rotating speed is 100-200r/m, mixing time 10min；The rotating speed of third time stirring is 200-350r/m, during stirring
Between 25-30min；The rotating speed of the 4th stirring is 200-250r/m；The rotating speed of the 5th stirring is 300-350r/m,
Mixing time 15-25min.
Preferably, in step c, in vacuum, vacuum is-70～-80KPa, the time of evacuation
For 15-20 minute.
The proportioning of above-mentioned each raw material is different, may be constructed different embodiments, specific as follows.
Embodiment 1
A kind of dumb light finishing varnish, its raw material includes according to percentage by weight: deionized water 25%, wetting agent
0.1%, quenching matter 5%, defoamer 0.2%, emulsion 59%, coalescents 4%, antibacterial 0.2%,
Anti-fouling agent 6%, thickening agent 0.5%.
The preparation method of above-mentioned dumb light finishing varnish comprises the following steps:
A, according to percentage by weight, mixing tank is sequentially added into deionized water, dispersant, wetting agent, with
100-200r/m stirs 5min；Add quenching matter, stir 10min with 100-200r/m, wait delustring thing
After matter substantially moistening, then with 200-350r/m dispersed with stirring 25-30 minute, the abundant moistening of quenching matter is made to divide
Dissipate；
B, rotating speed is adjusted to 200-250r/m, defoamer is joined in the middle of the system of step a, until surface
Invisible foam；Sequentially add emulsion, coalescents, antibacterial, anti-fouling agent, add while stirring,
Continue to stir 15-25 minute with 300-350r/m；Obtain compound；
C, by after compound evacuation bubble removing, add thickening agent while stirring, obtain dumb light finishing varnish.
Dumb light finishing varnish prepared by the present embodiment, its performance indications are as shown in table 2.
Table 2
| Project | Standard | Method | Result | Remarks |
| Resistance to water | GB/T 1733 | 96h | Without exception | |
| Alkali resistance | GB/T 9265 | 48h | Without exception | |
| Acid rain resistant is tested | GB/T 9274 | 48h | Without exception | |
| Water-whitening resistance | Method 1 | 2h | Without exception | |
| Measurement of luster | Glossometer is tested | 60 degree of tests | 14Gu | Quenching matter is the most, and gloss is the least |
| Initial hydrophilic angle | Contact angle instrument | Method is 1. | 5° | |
| Hydrophilic angle after pollution | Contact angle instrument | Method is 2. | 18° |
Embodiment 2
A kind of dumb light finishing varnish, its raw material includes according to percentage by weight: deionized water 40.5%, dispersant
0.2%, wetting agent 0.1%, quenching matter 3.2%, defoamer 0.1%, emulsion 50%, coalescents 2.4%,
Antibacterial 0.1%, anti-fouling agent 3%, thickening agent 0.4%.
The preparation method of above-mentioned dumb light finishing varnish comprises the following steps:
A, according to percentage by weight, mixing tank is sequentially added into deionized water, dispersant, wetting agent, with
100-200r/m stirs 5min；Add quenching matter, stir 10min with 100-200r/m, wait delustring thing
After matter substantially moistening, then with 200-350r/m dispersed with stirring 25-30 minute, the abundant moistening of quenching matter is made to divide
Dissipate；
B, rotating speed is adjusted to 200-250r/m, defoamer is joined in the middle of the system of step a, until surface
Invisible foam；Sequentially add emulsion, coalescents, antibacterial, anti-fouling agent, add while stirring,
Continue to stir 15-25 minute with 300-350r/m；Obtain compound；
C, by after compound evacuation bubble removing, add thickening agent while stirring, obtain dumb light finishing varnish.
Dumb light finishing varnish prepared by the present embodiment, its performance indications are as shown in table 3.
Table 3
| Project | Standard | Method | Result | Remarks |
| Resistance to water | GB/T 1733 | 96h | Without exception | |
| Alkali resistance | GB/T 9265 | 48h | Without exception | |
| Acid rain resistant is tested | GB/T 9274 | 48h | Without exception | |
| Water-whitening resistance | Method 1 | 2h | Without exception | |
| Measurement of luster | Glossometer is tested | 60 degree of tests | 20Gu | Quenching matter is the most, and gloss is the least |
| Initial hydrophilic angle | Contact angle instrument | Method is 1. | 7° | |
| Hydrophilic angle after pollution | Contact angle instrument | Method is 2. | 21° |
Embodiment 3
A kind of dumb light finishing varnish, its raw material includes according to percentage by weight: deionized water 26%, wetting agent
0.1%, quenching matter 2.5%, defoamer 0.1%, emulsion 65%, coalescents 5%, antibacterial 0.1%,
Anti-fouling agent 1%, thickening agent 0.2%.
The preparation method of above-mentioned dumb light finishing varnish comprises the following steps:
A, according to percentage by weight, mixing tank is sequentially added into deionized water, dispersant, wetting agent, with
100-200r/m stirs 5min；Add quenching matter, stir 10min with 100-200r/m, wait delustring thing
After matter substantially moistening, then with 200-350r/m dispersed with stirring 25-30 minute, the abundant moistening of quenching matter is made to divide
Dissipate；
B, rotating speed is adjusted to 200-250r/m, defoamer is joined in the middle of the system of step a, until surface
Invisible foam；Sequentially add emulsion, coalescents, antibacterial, anti-fouling agent, add while stirring,
Continue to stir 15-25 minute with 300-350r/m；Obtain compound；
C, by after compound evacuation bubble removing, add thickening agent while stirring, obtain dumb light finishing varnish.
Dumb light finishing varnish prepared by the present embodiment, its performance indications are as shown in table 4.
Table 4
| Project | Standard | Method | Result | Remarks |
| Resistance to water | GB/T 1733 | 96h | Without exception | |
| Alkali resistance | GB/T 9265 | 48h | Without exception | |
| Acid rain resistant is tested | GB/T 9274 | 48h | Without exception | |
| Water-whitening resistance | Method 1 | 2h | Without exception | |
| Measurement of luster | Glossometer is tested | 60 degree of tests | 27Gu | Quenching matter is the most, and gloss is the least |
| Initial hydrophilic angle | Contact angle instrument | Method is 1. | 9° | |
| Hydrophilic angle after pollution | Contact angle instrument | Method is 2. | 25° |
Embodiment 4
A kind of dumb light finishing varnish, its raw material includes according to percentage by weight: deionized water 34%, dispersant
0.1%, wetting agent 0.05%, quenching matter 6%, defoamer 0.15%, emulsion 52%, coalescents 3.1%,
Antibacterial 0.3%, anti-fouling agent 4%, thickening agent 0.3%.
The preparation method of above-mentioned dumb light finishing varnish comprises the following steps:
A, according to percentage by weight, mixing tank is sequentially added into deionized water, dispersant, wetting agent, stirs
After mixing；Add quenching matter, continue stirring, after waiting quenching matter substantially moistening, heighten mixing speed again
Stirring, until the abundant wetting and dispersing of quenching matter；
Joining in the middle of the system of step a by defoamer while b, stirring, stirring is until the invisible bubble in surface
Foam；Sequentially add emulsion, coalescents, antibacterial, anti-fouling agent, add while stirring, finally heighten
Mixing speed stirs, and obtains compound；
C, by after compound evacuation bubble removing, add thickening agent while stirring, obtain dumb light finishing varnish.
Whipping process in embodiment operates with means commonly used in the art.
Dumb light finishing varnish prepared by the present embodiment, its performance indications are as shown in table 5.
Table 5
| Project | Standard | Method | Result | Remarks |
| Resistance to water | GB/T 1733 | 96h | Without exception | |
| Alkali resistance | GB/T 9265 | 48h | Without exception | |
| Acid rain resistant is tested | GB/T 9274 | 48h | Without exception | |
| Water-whitening resistance | Method 1 | 2h | Without exception | |
| Measurement of luster | Glossometer is tested | 60 degree of tests | 11Gu | Quenching matter is the most, and gloss is the least |
| Initial hydrophilic angle | Contact angle instrument | Method is 1. | 7° | |
| Hydrophilic angle after pollution | Contact angle instrument | Method is 2. | 22° |
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all at this
Within bright spirit and principle, any modification, equivalent substitution and improvement etc. made, should be included in this
Within bright protection domain.
Claims (10)
1. a dumb light finishing varnish, it is characterised in that its raw material includes according to percentage by weight: deionization
Water 25-40%, dispersant 0-0.2%, wetting agent 0.05-0.1%, quenching matter 2.5-6%, defoamer 0.1-0.2%,
Emulsion 50-65%, coalescents 2-5%, antibacterial 0.1-0.3%, anti-fouling agent 1-6%, thickening agent 0.2-0.5%.
Dumb light finishing varnish the most according to claim 1, it is characterised in that described anti-fouling agent is silicon
Oxygen alkanes and derivant thereof.
Dumb light finishing varnish the most according to claim 2, it is characterised in that described quenching matter be with
The silicon dioxide of hollow is carrier, its surface parcel TPO material.
Dumb light finishing varnish the most according to claim 3, it is characterised in that described emulsion is pure third breast
One or both compound emulsion in liquid, silicone acrylic emulsion.
Dumb light finishing varnish the most according to claim 4, it is characterised in that described dispersant is ammonium salt
The dispersant of class；Described wetting agent is the wetting agent without APEO；Described coalescents be alcohol ester 12,
One or both mixture in butyl carbitol；Described thickening agent is polyurethanes thickening agent, hydrophobically modified
One or both mixture in alkali swelling class thickening agent.
Dumb light finishing varnish the most according to claim 5, it is characterised in that
Its raw material includes according to percentage by weight: deionized water 25%, wetting agent 0.1%, quenching matter 5%,
Defoamer 0.2%, emulsion 59%, coalescents 4%, antibacterial 0.2%, anti-fouling agent 6%, thickening agent 0.5%；
Or,
Its raw material includes according to percentage by weight: deionized water 40.5%, dispersant 0.2%, wetting agent 0.1%,
Quenching matter 3.2%, defoamer 0.1%, emulsion 50%, coalescents 2.4%, antibacterial 0.1%, antifouling
Agent 3%, thickening agent 0.4%；Or,
Its raw material includes according to percentage by weight: deionized water 26%, wetting agent 0.1%, quenching matter 2.5%,
Defoamer 0.1%, emulsion 65%, coalescents 5%, antibacterial 0.1%, anti-fouling agent 1%, thickening agent 0.2%；
Or,
Its raw material includes according to percentage by weight: deionized water 34%, dispersant 0.1%, wetting agent 0.05%,
Quenching matter 6%, defoamer 0.15%, emulsion 52%, coalescents 3.1%, antibacterial 0.3%, antifouling
Agent 4%, thickening agent 0.3%.
7. the preparation technology of a dumb light finishing varnish, it is characterised in that comprise the following steps:
A, according to percentage by weight, be sequentially added in mixing tank deionized water 25-40%, dispersant 0-0.2%,
Wetting agent 0.05-0.1%, carries out stirring for the first time；Add quenching matter 2.5-6%, carry out second time and stir,
Then improve mixing speed, carry out third time and stir, make the abundant wetting and dispersing of quenching matter；
B, regulation rotating speed carry out the 4th stirring, join in the middle of the system of step a by defoamer 0.1-0.2%,
Until the invisible foam in surface；Sequentially add emulsion 50-65%, coalescents 2-5%, antibacterial 0.1-0.3%,
Anti-fouling agent 1-6%, adds while stirring, and regulation rotating speed carries out the 5th stirring；Obtain compound；
C, by after described compound evacuation bubble removing, add thickening agent 0.2-0.5% while stirring, obtain institute
State dumb light finishing varnish.
Preparation technology the most according to claim 7, it is characterised in that the rotating speed of stirring of described first time
For 100-200r/m, mixing time 5min；The rotating speed of described second time stirring is 100-200r/m, during stirring
Between 10min；The rotating speed of described third time stirring is 200-350r/m, mixing time 25-30min；Described 4th
The rotating speed of secondary stirring is 200-250r/m；The rotating speed of described 5th stirring is 300-350r/m, mixing time
15-25min；In step c, in vacuum, vacuum is-70～-80KPa, and the time of evacuation is
15-20min。
Preparation technology the most according to claim 7, it is characterised in that described anti-fouling agent is type siloxane
And derivant；Described quenching matter is with the silicon dioxide of hollow as carrier, wraps up polyolefin on its surface
Class material；Described emulsion is one or both compound emulsion in pure-acrylic emulsion, silicone acrylic emulsion；Described dispersion
Agent is the dispersant of ammonium salt class；Described wetting agent is the wetting agent without APEO；Described coalescents is alcohol
One or both mixture in ester 12, butyl carbitol；Described thickening agent be polyurethanes thickening agent,
One or both mixture in hydrophobically-modified alkali swelling class thickening agent.
Preparation technology the most according to claim 9, it is characterised in that
Its raw material includes according to percentage by weight: deionized water 25%, wetting agent 0.1%, quenching matter 5%,
Defoamer 0.2%, emulsion 59%, coalescents 4%, antibacterial 0.2%, anti-fouling agent 6%, thickening agent 0.5%；
Or,
Its raw material includes according to percentage by weight: deionized water 40.5%, dispersant 0.2%, wetting agent 0.1%,
Quenching matter 3.2%, defoamer 0.1%, emulsion 50%, coalescents 2.4%, antibacterial 0.1%, antifouling
Agent 3%, thickening agent 0.4%；Or,
Its raw material includes according to percentage by weight: deionized water 26%, wetting agent 0.1%, quenching matter 2.5%,
Defoamer 0.1%, emulsion 65%, coalescents 5%, antibacterial 0.1%, anti-fouling agent 1%, thickening agent 0.2%；
Or,
Its raw material includes according to percentage by weight: deionized water 34%, dispersant 0.1%, wetting agent 0.05%,
Quenching matter 6%, defoamer 0.15%, emulsion 52%, coalescents 3.1%, antibacterial 0.3%, antifouling
Agent 4%, thickening agent 0.3%.
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| CN106883700A (en) * | 2017-03-06 | 2017-06-23 | 河北晨阳工贸集团有限公司 | A kind of dumb light finishing varnish |
| CN110003746A (en) * | 2019-03-08 | 2019-07-12 | 合肥科天水性科技有限责任公司 | A kind of mono-component aqueous varnish of high rigidity and preparation method thereof |
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| CN106634354A (en) * | 2016-12-29 | 2017-05-10 | 成都富思特新材料有限公司 | Novel high-adhesive-dirt-resistance coating varnish, preparation method and construction method |
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| CN110845880B (en) * | 2019-08-15 | 2021-09-21 | 上海中大洁润丝实验室科技有限公司 | Protective varnish for screen printing plate |
| CN110724421A (en) * | 2019-10-26 | 2020-01-24 | 苏州大乘环保新材有限公司 | Water-based tile anti-slip cover and preparation method and application thereof |
| CN112521817A (en) * | 2020-12-11 | 2021-03-19 | 广东现代涂料科技有限公司 | Single-component matte clear finish paint and preparation method thereof |
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