CN106018612A - 一种环境与食品中多种内分泌干扰物的检测分析方法 - Google Patents
一种环境与食品中多种内分泌干扰物的检测分析方法 Download PDFInfo
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- CN106018612A CN106018612A CN201610466428.4A CN201610466428A CN106018612A CN 106018612 A CN106018612 A CN 106018612A CN 201610466428 A CN201610466428 A CN 201610466428A CN 106018612 A CN106018612 A CN 106018612A
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
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- G01N2030/067—Preparation by reaction, e.g. derivatising the sample
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CN201610466428.4A CN106018612B (zh) | 2016-06-24 | 2016-06-24 | 一种环境与食品中多种内分泌干扰物的检测分析方法 |
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CN201610466428.4A CN106018612B (zh) | 2016-06-24 | 2016-06-24 | 一种环境与食品中多种内分泌干扰物的检测分析方法 |
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CN106018612B CN106018612B (zh) | 2018-10-12 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107976504A (zh) * | 2017-12-07 | 2018-05-01 | 北京工业大学 | 一种厌氧颗粒污泥中***含量的检测方法 |
CN109001311A (zh) * | 2018-06-29 | 2018-12-14 | 浙江省海洋水产研究所 | 一种水产品中内外源性***的液相色谱串联质谱检测方法 |
CN109298151A (zh) * | 2018-09-27 | 2019-02-01 | 江苏雅信昆成检测科技有限公司 | 一种能识别多种环境内分泌干扰物的检测方法 |
WO2019037665A1 (zh) * | 2017-08-22 | 2019-02-28 | 杭州谱景柏泰科技有限公司 | 芳香族化合物的检测方法及试剂盒 |
CN113740455A (zh) * | 2021-09-03 | 2021-12-03 | 广东省中鼎检测技术有限公司 | 一种测试消费品中2,2-二(4-羟基苯基)丁烷的检测方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007019180A2 (en) * | 2005-08-04 | 2007-02-15 | Science & Technology Corporation @ Unm | Compounds for binding to eralpha/beta and gpr30, methods of treating disease states and conditions mediated through these receptors and identification thereof |
CN103185762A (zh) * | 2011-12-29 | 2013-07-03 | 复旦大学 | 一种分析测定食品中多种内分泌干扰物的方法 |
CN104297377A (zh) * | 2014-10-24 | 2015-01-21 | 曲阜师范大学 | 一种植物甾醇的检测分析方法 |
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2016
- 2016-06-24 CN CN201610466428.4A patent/CN106018612B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007019180A2 (en) * | 2005-08-04 | 2007-02-15 | Science & Technology Corporation @ Unm | Compounds for binding to eralpha/beta and gpr30, methods of treating disease states and conditions mediated through these receptors and identification thereof |
CN103185762A (zh) * | 2011-12-29 | 2013-07-03 | 复旦大学 | 一种分析测定食品中多种内分泌干扰物的方法 |
CN104297377A (zh) * | 2014-10-24 | 2015-01-21 | 曲阜师范大学 | 一种植物甾醇的检测分析方法 |
Non-Patent Citations (3)
Title |
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P.J.M. KWAKMAN等: "Liquid chromatographic determination of oestradiol in serum by pre-column derivatization with dansyl chloride or laryl chloride and peroxyoxalate chemiluminescence detection", 《JOURNAL OF PHARMACEUTICAL & BIOMEDICAL ANALYSIS》 * |
XIAN-EN ZHAO等: "Dual ultrasonic-assisted dispersive liquid–liquid microextraction coupled with microwave-assisted derivatization for simultaneous determination of 20(S)-protopanaxadiol and 20(S)-protopanaxatriol by ultra high performance liquid chromatography", 《JOURNAL OF CHROMATOGRAPHY A》 * |
赵先恩等: "罗丹明B衍生化超高效液相色谱三重四极杆质谱高灵敏测定人参二醇", 《分析化学》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019037665A1 (zh) * | 2017-08-22 | 2019-02-28 | 杭州谱景柏泰科技有限公司 | 芳香族化合物的检测方法及试剂盒 |
CN107976504A (zh) * | 2017-12-07 | 2018-05-01 | 北京工业大学 | 一种厌氧颗粒污泥中***含量的检测方法 |
CN109001311A (zh) * | 2018-06-29 | 2018-12-14 | 浙江省海洋水产研究所 | 一种水产品中内外源性***的液相色谱串联质谱检测方法 |
CN109298151A (zh) * | 2018-09-27 | 2019-02-01 | 江苏雅信昆成检测科技有限公司 | 一种能识别多种环境内分泌干扰物的检测方法 |
CN113740455A (zh) * | 2021-09-03 | 2021-12-03 | 广东省中鼎检测技术有限公司 | 一种测试消费品中2,2-二(4-羟基苯基)丁烷的检测方法 |
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CN106018612B (zh) | 2018-10-12 |
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Inventor after: Zhu Shuyun Inventor after: Wei Na Inventor after: Wang Renjun Inventor after: Yan Ping Inventor after: Wang Yuhua Inventor after: He Yongrui Inventor after: Song Cuihua Inventor after: Zhao Xianen Inventor after: You Jinmao Inventor before: Zhao Xianen Inventor before: Wei Na Inventor before: Wang Renjun Inventor before: Yan Ping Inventor before: Wang Yuhua Inventor before: He Yongrui Inventor before: Song Cuihua Inventor before: Zhu Shuyun Inventor before: You Jinmao |
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