CN106018014A - High precision dilution sampling instrument - Google Patents

High precision dilution sampling instrument Download PDF

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Publication number
CN106018014A
CN106018014A CN201610627314.3A CN201610627314A CN106018014A CN 106018014 A CN106018014 A CN 106018014A CN 201610627314 A CN201610627314 A CN 201610627314A CN 106018014 A CN106018014 A CN 106018014A
Authority
CN
China
Prior art keywords
mass flow
valve
high accuracy
flow controller
sample gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610627314.3A
Other languages
Chinese (zh)
Inventor
王铁铮
张菲菲
王浩
李昌建
宁晓宇
张君
刘英会
经广欣
王金良
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Academy of Environmental Sciences
Original Assignee
Tianjin Academy of Environmental Sciences
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin Academy of Environmental Sciences filed Critical Tianjin Academy of Environmental Sciences
Priority to CN201610627314.3A priority Critical patent/CN106018014A/en
Publication of CN106018014A publication Critical patent/CN106018014A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/24Suction devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34Purifying; Cleaning
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38Diluting, dispersing or mixing samples
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D7/00Control of flow
    • G05D7/06Control of flow characterised by the use of electric means
    • G05D7/0617Control of flow characterised by the use of electric means specially adapted for fluid materials
    • G05D7/0629Control of flow characterised by the use of electric means specially adapted for fluid materials characterised by the type of regulator means
    • G05D7/0635Control of flow characterised by the use of electric means specially adapted for fluid materials characterised by the type of regulator means by action on throttling means
    • G05D7/0641Control of flow characterised by the use of electric means specially adapted for fluid materials characterised by the type of regulator means by action on throttling means using a plurality of throttling means
    • G05D7/0647Control of flow characterised by the use of electric means specially adapted for fluid materials characterised by the type of regulator means by action on throttling means using a plurality of throttling means the plurality of throttling means being arranged in series

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Automation & Control Theory (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention relates to a high precision dilution sampling instrument. A sampling probe is connected to a sample gas inlet, a calibration gas inlet is connected to a second one-way valve, the sample gas inlet is converged with the second one-way valve through a pipeline and is then connected to a first filter, then the first filter falls into two paths, one path is connected to a vacuum pump and a sample gas emptying port in order, and the other path is connected to a proportional valve, a second high precision mass flow controller and a Venturi tube in order, and the second high precision mass flow controller is also connected to a first high precision mass flow controller with different measuring range, a diluent gas inlet falls into two paths, one path is connected to a first pressure regulating valve and a first electromagnetic valve in order, and is then connected to one point on the pipeline between the proportional valve and the first filter, and the other path is connected to a second pressure regulating valve, a second filter and a second electromagnetic valve.

Description

A kind of high accuracy dilution sampling instrument
Technical field
The present invention relates to a kind of gas sampling apparatus technical field, particularly relate to a kind of high accuracy dilution sampling instrument.
Background technology
In recent years, China's atmospheric pollution is on the rise, and has become as the major issue faced by people, in polluter Foul gas is the important pollutant can not ignore, and the health for people causes serious threat, therefore to stench The emission monitoring of gas becomes a kind of necessary technology means.The foul gas concentration of general discharge is the highest, directly supervises Survey difficulty, it is necessary to gas dilution before sampling.But, general dilution sampling instrument dilution ratio single or Precision is inadequate.It is thus desirable to prior art is made improvement.
Summary of the invention
Present invention seek to address that the deficiencies in the prior art, and a kind of high accuracy dilution sampling instrument is provided.
The present invention for achieving the above object, by the following technical solutions:
Described a kind of high accuracy dilution sampling instrument, including sampling probe, sample gas inlet, calibration gas entrance, mixes Close gas exit, gaseous mixture evacuation port, vacuum pump, sample gas evacuation port, carrier gas entrance, it is characterised in that Also including the second check valve, controller, sampling probe is connected with sample gas inlet, calibration gas entrance and the second list Connecting to valve, sample gas inlet and the second check valve are connected after being collected by pipeline the first filter, the first mistake Being divided into two-way after filter, a road is sequentially connected with vacuum pump, sample gas evacuation port, and another road is sequentially connected with proportional Valve, the second high accuracy mass flow controller, Venturi tube, the second high accuracy mass flow controller is the most in parallel There is a first high accuracy mass flow controller different from its range, be divided into two-way after carrier gas entrance, a road It is connected with the first pressure regulator valve, the first electromagnetic valve in turn, on the pipeline subsequently and between proportioning valve, the first filter one Point connects, and another road is connected with the second pressure regulator valve, the second filter, the second electromagnetic valve in turn, subsequently by second Electromagnetic valve is divided into again two-way, and a road connects the first mass flow controller, is connected with Venturi tube subsequently, separately One tunnel is connected with the second mass flow controller, the first check valve in turn, Venturi tube, the going out of the first check valve Mouth collect by pipeline after connection have blender, blender be divided into again two-way respectively with gaseous mixture exit, mix Gas evacuation port connect, gaseous mixture exit connect have analytical tool, the second electromagnetic valve, the first electromagnetic valve, second Mass flow controller, the first mass flow controller, sampling probe, vacuum pump, proportioning valve, first high-precision Degree mass flow controller, the second high accuracy mass flow controller are connected with controller respectively.
Sampling probe is provided with coarse filtration net.
It is additionally provided with emission-control equipment after gaseous mixture evacuation port, sample gas evacuation port.
The invention has the beneficial effects as follows: adoption rate valve of the present invention and in parallel two high accuracy mass flows control Device can accurately regulate sample gas, uses mass flow controller to control carrier gas flow, so that dilution ratio can Adjust;Owing to high accuracy mass flow controller has temperature compensation function, use two parallel connections and range different Mass flow controller in high precision, compared with the mode of capillary tube and differential pressure transmitter parallel connection, flow is not by flue gas Temperature affects, and is greatly improved carrier gas flow control accuracy.
Accompanying drawing explanation
Fig. 1 is present configuration schematic diagram;
Fig. 2 is that the present invention ties control system schematic diagram.
In figure: 1-gaseous mixture exit;2-gaseous mixture evacuation port;3-blender;4-the first check valve;5- Two mass flow controllers;6-the second electromagnetic valve;7-the second filter;8-the second pressure regulator valve;9-first is high-precision Degree mass flow controller;10-the second high accuracy mass flow controller;11-the first mass flow controller; 12-Venturi tube;13-sampling probe;14-sample gas inlet;15-calibrates gas entrance;16-the second check valve; 17-the first pressure regulator valve;18-carrier gas entrance;19-sample gas evacuation port;20-vacuum pump;21-proportioning valve;22- First electromagnetic valve;23-the first filter;24-controller.
It is described in detail referring to the drawings below with reference to embodiments of the invention.
Detailed description of the invention
The invention will be further described below in conjunction with the accompanying drawings:
As depicted in figs. 1 and 2, a kind of high accuracy dilution sampling instrument, enter including sampling probe 13, sample gas Mouth 14, calibration gas entrance 15, gaseous mixture exit 1, gaseous mixture evacuation port 2, vacuum pump 20, sample gas Evacuation port 19, carrier gas entrance 18, it is characterised in that also include the second check valve 16, controller 24, adopt Sample probe 13 is connected with sample gas inlet 14, and calibration gas entrance 15 is connected with the second check valve 16, sample gas Entrance 14 is connected after being collected by pipeline with the second check valve 16 the first filter 23, the first filter 23 After be divided into two-way, a road is sequentially connected with vacuum pump 20, sample gas evacuation port 19, and another road is connected with ratio in turn Example valve the 21, second high accuracy mass flow controller 10, Venturi tube 12, the second high accuracy mass flow control Device 10 processed is also parallel with a first high accuracy mass flow controller 9 different from its range, carrier gas entrance Being divided into two-way after 18, a road is connected with first pressure regulator valve the 17, first electromagnetic valve 22 in turn, subsequently with proportioning valve 21, a little connect on the pipeline between the first filter 23, another road be connected with in turn the second pressure regulator valve 8, the Tow filtrator the 7, second electromagnetic valve 6, is divided into again two-way by the second electromagnetic valve 6 subsequently, and a road connects first Mass flow controller 11, is connected with Venturi tube 12 subsequently, and another road is connected with the second mass flow in turn Controller the 5, first check valve 4, the outlet of Venturi tube the 12, first check valve 4 is connected after being collected by pipeline Being connected to blender 3, blender 3 is divided into again two-way respectively with gaseous mixture exit 1, gaseous mixture evacuation port 2 even Connecing, gaseous mixture exit 1 connects analytical tool, second electromagnetic valve the 6, first electromagnetic valve the 22, second mass Flow controller the 5, first mass flow controller 11, sampling probe 13, vacuum pump 20, proportioning valve 21, First high accuracy mass flow controller 9, second high accuracy mass flow controller 10 respectively with controller 24 connect.
Sampling probe 13 is provided with coarse filtration net.
It is additionally provided with emission-control equipment after gaseous mixture evacuation port 2, sample gas evacuation port 19.
Invention has been described above, it is clear that the present invention implements and is not subject to the restrictions described above, only The method design of the present invention be have employed and the various improvement that carry out of technical scheme, or the most improved directly apply to Other occasion, all within protection scope of the present invention.

Claims (3)

1. a high accuracy dilution sampling instrument, including sampling probe (13), sample gas inlet (14), calibration Gas entrance (15), gaseous mixture exit (1), gaseous mixture evacuation port (2), vacuum pump (20), sample gas row Eat dishes without rice or wine (19), carrier gas entrance (18), it is characterised in that also include the second check valve (16), controller (24), sampling probe (13) is connected with sample gas inlet (14), and calibration gas entrance (15) is single with second Connecting to valve (16), sample gas inlet (14) is connected after being collected by pipeline with the second check valve (16) to be had First filter (23), the first filter is divided into two-way after (23), a road be sequentially connected with vacuum pump (20), Sample gas evacuation port (19), another road is connected with proportioning valve (21) in turn, the second high accuracy mass flow controls Device (10), Venturi tube (12), second high accuracy mass flow controller (10) be also parallel with one with its amount First high accuracy mass flow controller (9) of Cheng Butong, carrier gas entrance is divided into two-way after (18), a road It is connected with the first pressure regulator valve (17), the first electromagnetic valve (22) in turn, subsequently with proportioning valve (21), the first mistake A little connecting on pipeline between filter (23), another road is connected with the second pressure regulator valve (8), the second filtration in turn Device (7), the second electromagnetic valve (6), be divided into again two-way by the second electromagnetic valve (6) subsequently, and a road connects the One mass flow controller (11), is connected with Venturi tube (12) subsequently, and another road is connected with second in turn Mass flow controller (5), the first check valve (4), Venturi tube (12), the going out of the first check valve (4) After mouth collects by pipeline, connection has blender (3), blender (3) to be divided into again two-way to connect with gaseous mixture respectively Outlet (1), gaseous mixture evacuation port (2) connect, and gaseous mixture exit (1) connects analytical tool, and second Electromagnetic valve (6), the first electromagnetic valve (22), the second mass flow controller (5), the first mass flow control Device (11), sampling probe (13), vacuum pump (20), proportioning valve (21), the first high accuracy mass flow control Device processed (9), the second high accuracy mass flow controller (10) are connected with controller (24) respectively.
A kind of high accuracy dilution sampling instrument the most according to claim 1, it is characterised in that sampling probe (13) coarse filtration net it is provided with.
A kind of high accuracy dilution sampling instrument the most according to claim 1, it is characterised in that gaseous mixture is arranged Eat dishes without rice or wine (2), sample gas evacuation port is additionally provided with emission-control equipment after (19).
CN201610627314.3A 2016-07-29 2016-07-29 High precision dilution sampling instrument Pending CN106018014A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610627314.3A CN106018014A (en) 2016-07-29 2016-07-29 High precision dilution sampling instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610627314.3A CN106018014A (en) 2016-07-29 2016-07-29 High precision dilution sampling instrument

Publications (1)

Publication Number Publication Date
CN106018014A true CN106018014A (en) 2016-10-12

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610627314.3A Pending CN106018014A (en) 2016-07-29 2016-07-29 High precision dilution sampling instrument

Country Status (1)

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CN (1) CN106018014A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111879896A (en) * 2020-07-15 2020-11-03 北京市计量检测科学研究院(北京市能源计量监测中心) Odor measuring instrument, odor measuring method and device
CN112782357A (en) * 2020-12-22 2021-05-11 汉威科技集团股份有限公司 Automatic calibration method and device for gas sensor

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111879896A (en) * 2020-07-15 2020-11-03 北京市计量检测科学研究院(北京市能源计量监测中心) Odor measuring instrument, odor measuring method and device
CN112782357A (en) * 2020-12-22 2021-05-11 汉威科技集团股份有限公司 Automatic calibration method and device for gas sensor

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20161012

WD01 Invention patent application deemed withdrawn after publication