CN106010238A - Preparation method of antirust paint for power distribution cabinet - Google Patents
Preparation method of antirust paint for power distribution cabinet Download PDFInfo
- Publication number
- CN106010238A CN106010238A CN201610392828.5A CN201610392828A CN106010238A CN 106010238 A CN106010238 A CN 106010238A CN 201610392828 A CN201610392828 A CN 201610392828A CN 106010238 A CN106010238 A CN 106010238A
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- preparation
- antirust paint
- power distribution
- distribution cabinet
- resin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D187/00—Coating compositions based on unspecified macromolecular compounds, obtained otherwise than by polymerisation reactions only involving unsaturated carbon-to-carbon bonds
- C09D187/005—Block or graft polymers not provided for in groups C09D101/00 - C09D185/04
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G83/00—Macromolecular compounds not provided for in groups C08G2/00 - C08G81/00
- C08G83/001—Macromolecular compounds containing organic and inorganic sequences, e.g. organic polymers grafted onto silica
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to a preparation method of a metal antirust paint, and in particular, relates to the preparation method for the antirust paint for a power distribution cabinet, wherein the method comprises the following steps: (1) adding chlorinated rubber, a film-forming auxiliary agent, a filler, a paint film self-cleaning agent and a defoaming agent into an ethyl acetate solution, heating to 40-50 DEG C, carrying out ultrasonic dispersion, adding inositol hexaphosphate and dipropylene glycol dibenzoate, and stirring for 20-30 min; (2) rising the temperature to 50-60 DEG C, adding modified alkyd resin, fluorocarbon resin and glass resin, and stirring for 40-50 min; and (3) adding a leveling agent, stirring, and dispersing to obtain the antirust paint. The prepared antirust paint has the advantages of wide use scope, high adhesive force, excellent weatherability, high hardness after curing, good wear resistance, no discoloring, no wrinkling, difficult peeling, sun-scorching and rain-drenching resistance, good decoration, and excellent anti-rust and self-cleaning effects; and the preparation method is simple, low in cost, and suitable for mass production.
Description
Technical field
The present invention relates to a kind of metallic anti-rust paint, be specifically related to the preparation side of a kind of antirust paint for power distribution cabinet
Method.
Background technology
The effect of power distribution cabinet is that distribution controls to be assigned to electric energy each load position, and in short circuit, mistake
Power-off protection is carried out when carrying and leak electricity.The frequent species of power distribution cabinet has the board-like power distribution cabinet of stationary plane, protection to join
Electricity cabinet, drawer-type distribution box and power and lighting power distribution cabinet etc..At present, on market, the power distribution cabinet of 80% is all to use
This material of cold-rolled steel sheet is made, the power distribution cabinet of this kind of section bar matter, reliable in quality, low price, at present should
The most extensive with obtaining.The work under bad environment of transformation cabinet, is in natural environment for a long time, bear wind, frost, rain,
Snow, high temperature, severe cold, chemical attack etc., under the effect of these extraneous factors, its performance is it would appear that bad
Changing, this is by the safe operation of serious threat to power equipment.We are generally in the surface-coated one layer of power transformation box
Antirust paint reaches the function of the aspect such as high temperature resistant, cold-resistant, ageing-resistant, antirust.
Antirust paint is a kind of chemistry protecting metal surfaces from air, sea water etc. or the painting of electrochemical corrosion
Material.It is broadly divided into physical property and the big class of chemically antirust paint two.The former suitably joins by pigment and paint vehicle,
Form the intrusion with prevention corrosive substance of the fine and close paint film, such as iron oxide red, aluminium powder, graphite antirust paint etc.;After
Person presses down rust effect, such as Plumbum preparatium, zinc chromate anti-rust paint etc. by the chemistry of rust resisting pigment.Antirust paint has antirust because of it
Effect and looked at by people parent, but at present the noxious substance contained by antirust paint the most on the market is numerous, generally exists
Weather resistance is the best, easy to fall off, inadaptable complicated, adverse circumstances.
Summary of the invention
For solving above-mentioned technical problem, it is an object of the invention to provide the system of a kind of antirust paint for power distribution cabinet
Preparation Method.
The present invention adopts the following technical scheme that
The preparation method of a kind of antirust paint for power distribution cabinet, comprises the following steps:
(1) chlorinated rubber, coalescents, filler, paint film automatically cleaning agent, defoamer are joined acetic acid second
In ester solution, it is heated to 40-50 DEG C, ultrasonic disperse 30-40min, add inositol hexaphosphate and dipropylene glycol
Dibenzoate, under 600~800r/min speed conditions, stirs 20~30min;
(2) by step (1) liter high-temperature to 50-60 DEG C, modified alkyd resin, fluorocarbon resin, glass are added
Glass resin, under 600~1000r/min speed conditions, stirs 40~50min;
(3) levelling agent, under 600~800r/min speed conditions, dispersed with stirring 10~20min are added;Mixed
It is added to grinding machine for grinding after closing uniformly be uniformly dispersed, is filtrated to get the material that fineness is 30-45 μm, bag
Fill;
Wherein, each component composition is calculated as with parts by weight: inositol hexaphosphate 5-10 part, dipropylene glycol hexichol
Formic acid esters 3-5 part, chlorinated rubber 1-3 part, modified alkyd resin 20-25 part, coalescents 15-20 part,
Filler 15-20 part, fluorocarbon resin 10-15 part, glass resin 5-10 part, paint film automatically cleaning agent 1-3 part, disappear
Infusion 1-3 part, levelling agent 3-5 part, ethyl acetate surplus.
Specifically, described modified alkyd resin is prepared as follows: (1) is the guarantor of drying nitrogen gas
Protect down, by 20-25 part trimethylolpropane, 20-25 part 1,2-PD, 10-15 part maleic anhydride, positive silicon
Acetoacetic ester 10-15 part, styrene 3-5 part joins the four-hole boiling flask equipped with motor stirrer and oil water separator
In, it is uniformly mixed;(2) in step (1), add 0.1-0.2 part Lithium hydrate and 0.1-0.5 part resists
Oxidant 1010, slowly liter high-temperature is to 200-220 DEG C, when system acid number is 50-55mg KOH/g,
Stop heating;(4) reduction temperature is to 120 DEG C, adds 5-8 part propylene-glycol ethyl ether and stirs, and continues to reduce
Temperature, to 60 DEG C, adds 5-10 part diethanolamine reaction 0.5-1h, obtains silica microsphere modified alkyd tree
Fat.
Specifically, described coalescents, including the following component of parts by weight:
Polyvinyl butyral resin 15-20 part, precipitated calcium carbonate 5-10 part, white carbon black 3-5 part, Pulvis Talci 5-10
Part, attapulgite clay 10-15 part, organobentonite 5-10 part, cyclomethicone 3-5 part, acetic acid second
Ester surplus.
Specifically, described filler, including the following component of parts by weight:
Acrylic resin 15-20 part, vinyl bis-stearamides 0.5-1.5 part, Kaolin 5-10 part, sulphuric acid
Barium 5-10 part, metal mixture 40-50 part, anti-settling agent 1-3 part, ethyl acetate surplus.
Specifically, described metal mixture be chromium oxide, zinc powder, antimony oxide in mass ratio
1:(0.5-1): (1-2) forms.
Specifically, described anti-settling agent is anionic anti-settling agent.It is preferably the 118 of Wuxi moral space chemical industry to prevent
Heavy agent.
Specifically, described paint film automatically cleaning agent is hydrophilizing agent, it is possible to the effective pollution removing coating surface
Thing, optional model C P1000;Defoamer is modified polysiloxanes, optional model H52-3;Levelling agent is
Fluorin modified crylic acid ester, optional model A-1377.
Beneficial effects of the present invention:
(1) silica microsphere modified alkyd resin prepared by the present invention, introduces resin by silicon dioxide molecules
In strand, can improve the adhesive force of alkyd resin and hardness, paint film smooth, pliability is good;And
And silicon dioxide microsphere utilizes the hole between microsphere, can effectively absorb sound wave, there is the function of noise elimination.
(2) the antirust paint range of the present invention is wide, and adhesive force is high, and weatherability is excellent, hardness after solidification
Height, wearability is good, and invariant color is wrinkle resistant, is difficult to peel off.
(3) auxiliary agent that the present invention adds has good dispersion, does not assembles, and the most sun-resistant drenches with rain, and decorates
Property good, there is the antirust and automatically cleaning effect of excellence, use the time long, reduce the expense of later period maintenance.
(4) preparation method of the present invention is simple, and raw material is easy to get, low cost, is suitable for large-scale production.
Detailed description of the invention
In order to make the object of the invention, technical scheme and advantage clearer, below in conjunction with example, to this
Invention is described in further detail.
Embodiment 1
The preparation method of a kind of antirust paint for power distribution cabinet, comprises the following steps:
(1) chlorinated rubber, coalescents, filler, paint film automatically cleaning agent, defoamer are joined acetic acid second
In ester solution, it is heated to 40-50 DEG C, ultrasonic disperse 30-40min, add inositol hexaphosphate and dipropylene glycol
Dibenzoate, under 600~800r/min speed conditions, stirs 20~30min;
(2) by step (1) liter high-temperature to 50-60 DEG C, modified alkyd resin, fluorocarbon resin, glass are added
Glass resin, under 600~1000r/min speed conditions, stirs 40~50min;
(3) levelling agent, under 600~800r/min speed conditions, dispersed with stirring 10~20min are added;Mixed
It is added to grinding machine for grinding after closing uniformly be uniformly dispersed, is filtrated to get the material that fineness is 30-45 μm, bag
Fill;
Wherein, each component composition is calculated as with parts by weight: inositol hexaphosphate 5-10 part, dipropylene glycol hexichol
Formic acid esters 3-5 part, chlorinated rubber 1-3 part, modified alkyd resin 20-25 part, coalescents 15-20 part,
Filler 15-20 part, fluorocarbon resin 10-15 part, glass resin 5-10 part, paint film automatically cleaning agent 1-3 part, disappear
Infusion 1-3 part, levelling agent 3-5 part, ethyl acetate surplus.
Wherein, modified alkyd resin is prepared as follows: (1), will under the protection of drying nitrogen gas
20-25 part trimethylolpropane, 20-25 part 1,2-PD, 10-15 part maleic anhydride, tetraethyl orthosilicate 10-15
Part, styrene 3-5 part joins in the four-hole boiling flask equipped with motor stirrer and oil water separator, stirring mixing
Uniformly;(2) in step (1), 0.1-0.2 part Lithium hydrate and 0.1-0.5 part antioxidant 1010 are added,
Slowly liter high-temperature is to 200-220 DEG C, when system acid number is 50-55mg KOH/g, stops heating;(4)
Reduce temperature to 120 DEG C, add 5-8 part propylene-glycol ethyl ether stir, continue reduce temperature to 60 DEG C,
Add 5-10 part diethanolamine reaction 0.5-1h, obtain silica microsphere modified alkyd resin.
Wherein, coalescents includes the following component of parts by weight:
Polyvinyl butyral resin 15-20 part, precipitated calcium carbonate 5-10 part, white carbon black 3-5 part, Pulvis Talci 5-10
Part, attapulgite clay 10-15 part, organobentonite 5-10 part, cyclomethicone 3-5 part, acetic acid second
Ester surplus.Coalescents proportioning in above each compositional range all can meet demand.
Preparation method is precipitated calcium carbonate, white carbon black, Pulvis Talci, attapulgite clay, organobentonite to be added
In ethyl acetate, grinding distribution, then, add polyvinyl butyral resin and cyclomethicone, heat up
To 40-50 DEG C, stirring reaction 1-2h, to obtain final product.
Wherein, filler includes the following component of parts by weight:
Acrylic resin 15-20 part, vinyl bis-stearamides 0.5-1.5 part, Kaolin 5-10 part, sulphuric acid
Barium 5-10 part, chromium oxide, zinc powder, antimony oxide 1:(0.5-1 in mass ratio): the metal mixed that (1-2) forms
Thing 40-50 part, anti-settling agent 1-3 part, ethyl acetate surplus.
Filler proportioning in above each compositional range all can meet demand.
Its preparation method is to add in ethyl acetate by Kaolin, barium sulfate, Pulvis Talci, metal mixture,
Grinding distribution, then, adds acrylic resin, vinyl bis-stearamides and anti-settling agent, is warming up to
40-50 DEG C, stirring reaction 1-2h, to obtain final product.
Embodiment 2-6 is substantially the same manner as Example 1, and difference is table 1
Table 1
By above-mentioned formula gained antirust paint film performance such as table 2
Table 2
With the above-mentioned desirable embodiment according to the present invention for enlightenment, by above-mentioned description, related work
Personnel can carry out various change and amendment completely in the range of without departing from this invention technological thought.
The content that the technical scope of this invention is not limited in description, it is necessary to according to right
Determine its technical scope.
Claims (7)
1. the preparation method for the antirust paint of power distribution cabinet, it is characterised in that comprise the following steps:
(1) chlorinated rubber, coalescents, filler, paint film automatically cleaning agent, defoamer are joined acetic acid second
In ester solution, it is heated to 40-50 DEG C, ultrasonic disperse 30-40min, add inositol hexaphosphate and dipropylene glycol
Dibenzoate, under 600~800r/min speed conditions, stirs 20~30min;
(2) by step (1) liter high-temperature to 50-60 DEG C, modified alkyd resin, fluorocarbon resin, glass are added
Glass resin, under 600~1000r/min speed conditions, stirs 40~50min;
(3) levelling agent, under 600~800r/min speed conditions, dispersed with stirring 10~20min are added;Mixed
It is added to grinding machine for grinding after closing uniformly be uniformly dispersed, is filtrated to get the material that fineness is 30-45 μm, bag
Fill;
Wherein, each component composition is calculated as with parts by weight: inositol hexaphosphate 5-10 part, dipropylene glycol hexichol
Formic acid esters 3-5 part, chlorinated rubber 1-3 part, modified alkyd resin 20-25 part, coalescents 15-20 part,
Filler 15-20 part, fluorocarbon resin 10-15 part, glass resin 5-10 part, paint film automatically cleaning agent 1-3 part, disappear
Infusion 1-3 part, levelling agent 3-5 part, ethyl acetate surplus.
2. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 1, it is characterised in that
Described modified alkyd resin is prepared as follows: (1) under the protection of drying nitrogen gas, by 20-25
Part trimethylolpropane, 20-25 part 1,2-PD, 10-15 part maleic anhydride, tetraethyl orthosilicate 10-15
Part, styrene 3-5 part joins in the four-hole boiling flask equipped with motor stirrer and oil water separator, stirring mixing
Uniformly;(2) in step (1), 0.1-0.2 part Lithium hydrate and 0.1-0.5 part antioxidant 1010 are added,
Slowly liter high-temperature is to 200-220 DEG C, when system acid number is 50-55mg KOH/g, stops heating;(3)
Reduce temperature to 120 DEG C, add 5-8 part propylene-glycol ethyl ether stir, continue reduce temperature to 60 DEG C,
Add 5-10 part diethanolamine reaction 0.5-1h, obtain silica microsphere modified alkyd resin.
3. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 1, it is characterised in that
Described coalescents, including the following component of parts by weight:
Polyvinyl butyral resin 15-20 part, precipitated calcium carbonate 5-10 part, white carbon black 3-5 part, Pulvis Talci 5-10
Part, attapulgite clay 10-15 part, organobentonite 5-10 part, cyclomethicone 3-5 part, acetic acid second
Ester surplus.
4. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 1, it is characterised in that
Described filler, including the following component of parts by weight:
Acrylic resin 15-20 part, vinyl bis-stearamides 0.5-1.5 part, Kaolin 5-10 part, sulphuric acid
Barium 5-10 part, metal mixture 40-50 part, anti-settling agent 1-3 part, ethyl acetate surplus.
5. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 4, it is characterised in that
Described metal mixture is chromium oxide, zinc powder, antimony oxide 1:(0.5-1 in mass ratio): (1-2) forms.
6. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 4, it is characterised in that
Described anti-settling agent is anionic anti-settling agent.
7. by the preparation method of a kind of antirust paint for power distribution cabinet described in claim 1, it is characterised in that
Described paint film automatically cleaning agent is hydrophilizing agent;Defoamer is modified polysiloxanes;Levelling agent is fluorine richness third
Olefin(e) acid ester.
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CN201610392828.5A CN106010238A (en) | 2016-06-05 | 2016-06-05 | Preparation method of antirust paint for power distribution cabinet |
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CN201610392828.5A CN106010238A (en) | 2016-06-05 | 2016-06-05 | Preparation method of antirust paint for power distribution cabinet |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108395770A (en) * | 2018-02-10 | 2018-08-14 | 南京林业大学 | A kind of antiseptic and hydrophilic coating and preparation method thereof of chloride containing natural rubber |
CN108610684A (en) * | 2016-12-02 | 2018-10-02 | 张记飞 | A kind of preparation process of antirust paint for distribution box |
Citations (4)
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CN101613546A (en) * | 2008-06-24 | 2009-12-30 | 邹文和 | A kind of environment-friendly rust sealed base paint |
CN102174291A (en) * | 2011-02-11 | 2011-09-07 | 中国电力科学研究院 | Organosilicon-modified alkyd resin paint composite and preparation method thereof |
CN103509451A (en) * | 2013-09-10 | 2014-01-15 | 马鞍山市金韩涂料制造有限公司 | Alkyd resin antirust paint used on vessel bottom , and preparation method thereof |
CN105622908A (en) * | 2014-11-28 | 2016-06-01 | 合众(佛山)化工有限公司 | Preparation method of nano-SiO2 modified alkyd resin |
-
2016
- 2016-06-05 CN CN201610392828.5A patent/CN106010238A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101613546A (en) * | 2008-06-24 | 2009-12-30 | 邹文和 | A kind of environment-friendly rust sealed base paint |
CN102174291A (en) * | 2011-02-11 | 2011-09-07 | 中国电力科学研究院 | Organosilicon-modified alkyd resin paint composite and preparation method thereof |
CN103509451A (en) * | 2013-09-10 | 2014-01-15 | 马鞍山市金韩涂料制造有限公司 | Alkyd resin antirust paint used on vessel bottom , and preparation method thereof |
CN105622908A (en) * | 2014-11-28 | 2016-06-01 | 合众(佛山)化工有限公司 | Preparation method of nano-SiO2 modified alkyd resin |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108610684A (en) * | 2016-12-02 | 2018-10-02 | 张记飞 | A kind of preparation process of antirust paint for distribution box |
CN108395770A (en) * | 2018-02-10 | 2018-08-14 | 南京林业大学 | A kind of antiseptic and hydrophilic coating and preparation method thereof of chloride containing natural rubber |
CN108395770B (en) * | 2018-02-10 | 2020-05-12 | 南京林业大学 | Anticorrosive hydrophilic coating containing chlorinated natural rubber and preparation method thereof |
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Application publication date: 20161012 |