CN105995346A - Preparation method of plateau highland barley water - Google Patents
Preparation method of plateau highland barley water Download PDFInfo
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- CN105995346A CN105995346A CN201610381086.6A CN201610381086A CN105995346A CN 105995346 A CN105995346 A CN 105995346A CN 201610381086 A CN201610381086 A CN 201610381086A CN 105995346 A CN105995346 A CN 105995346A
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- avenae nudae
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 146
- 235000007340 Hordeum vulgare Nutrition 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 240000005979 Hordeum vulgare Species 0.000 title claims 3
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 49
- 239000011265 semifinished product Substances 0.000 claims abstract description 35
- 230000001954 sterilising effect Effects 0.000 claims abstract description 32
- 238000000605 extraction Methods 0.000 claims abstract description 31
- 239000000047 product Substances 0.000 claims abstract description 28
- 238000003756 stirring Methods 0.000 claims abstract description 28
- 239000006228 supernatant Substances 0.000 claims abstract description 26
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000004382 Amylase Substances 0.000 claims abstract description 13
- 102000013142 Amylases Human genes 0.000 claims abstract description 13
- 108010065511 Amylases Proteins 0.000 claims abstract description 13
- 235000019418 amylase Nutrition 0.000 claims abstract description 13
- 238000011049 filling Methods 0.000 claims abstract description 7
- 238000001694 spray drying Methods 0.000 claims abstract 2
- 210000000582 semen Anatomy 0.000 claims description 159
- 239000000284 extract Substances 0.000 claims description 23
- 240000004784 Cymbopogon citratus Species 0.000 claims description 20
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims description 20
- 230000002787 reinforcement Effects 0.000 claims description 17
- 238000004659 sterilization and disinfection Methods 0.000 claims description 17
- 229920002307 Dextran Polymers 0.000 claims description 14
- 239000012528 membrane Substances 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 12
- 239000000919 ceramic Substances 0.000 claims description 12
- 238000000265 homogenisation Methods 0.000 claims description 12
- 108090000623 proteins and genes Proteins 0.000 claims description 12
- 102000004169 proteins and genes Human genes 0.000 claims description 12
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 10
- 235000013305 food Nutrition 0.000 claims description 9
- 239000000796 flavoring agent Substances 0.000 claims description 8
- 235000019634 flavors Nutrition 0.000 claims description 8
- 235000015203 fruit juice Nutrition 0.000 claims description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 4
- 206010013911 Dysgeusia Diseases 0.000 claims description 2
- 108090000790 Enzymes Proteins 0.000 claims description 2
- 102000004190 Enzymes Human genes 0.000 claims description 2
- 230000002572 peristaltic effect Effects 0.000 claims description 2
- 241000209219 Hordeum Species 0.000 abstract description 25
- 108010059892 Cellulase Proteins 0.000 abstract description 11
- 229940106157 cellulase Drugs 0.000 abstract description 11
- 238000002137 ultrasound extraction Methods 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 5
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 abstract description 3
- 229920002498 Beta-glucan Polymers 0.000 abstract description 3
- 229940069780 barley extract Drugs 0.000 abstract 3
- 239000011259 mixed solution Substances 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 10
- 229910052708 sodium Inorganic materials 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- 235000021028 berry Nutrition 0.000 description 6
- 230000036541 health Effects 0.000 description 4
- 241001093152 Mangifera Species 0.000 description 3
- 240000000851 Vaccinium corymbosum Species 0.000 description 3
- 235000003095 Vaccinium corymbosum Nutrition 0.000 description 3
- 235000017537 Vaccinium myrtillus Nutrition 0.000 description 3
- 235000021014 blueberries Nutrition 0.000 description 3
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000015205 orange juice Nutrition 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 210000002421 cell wall Anatomy 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 239000003651 drinking water Substances 0.000 description 2
- 235000020188 drinking water Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000007705 chemical test Methods 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229940088598 enzyme Drugs 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to a preparation method of plateau highland barley water. The method comprises the following steps of (1) mixing crushed highland barley with water in proportion, and adjusting a pH value so as to obtain a mixed solution; (2) sequentially adding amylase and cellulase to the mixed solution, and performing ultrasonic extraction or heating extraction in water bath so as to obtain an extracting solution; (3) adjusting the pH value of the extracting solution, and performing filtration so as to obtain supernatant; (4) performing ultrafiltration on the supernatant, and performing spray drying so as to obtain a highland barley extract which is rich in crude fibers and highland barley beta-glucan; (5) heating pure water, adding the highland barley extract to the heated pure water, and stirring the highland barley extract and the heated pure water so as to obtain semi-finished products of the plateau highland barley water; and (6) homogenizing, the semi-finished products of the plateau highland barley water, sterilizing the homogenized products, and filling the sterilizing products so as to obtain the plateau highland barley water with primary taste, or performing taste blending on the, semi-finished products of the plateau highland barley water, homogenizing the blended products, sterilizing the homogenized products, and filling the sterilized products so as to obtain the plateau highland barley water. Through the adoption of the preparation method disclosed by the invention, the purpose of high-efficiently utilizing the effective components of highland barley can be achieved.
Description
Technical field
The present invention relates to Semen avenae nudae deep process technology field, particularly relate to the preparation method of plateau Semen avenae nudae water.
Background technology
Semen avenae nudae has abundant nutritive value and prominent health preserving effect.In the Qinghai-Tibet Platean of severe cold region, why it is no lack of
Centenarian, this is undivided with often food Semen avenae nudae.
Beta glucan in Semen avenae nudae is a kind of Natural linear non-starch polysaccharides(nsp), is the main one-tenth of hullessbarley seed Formation of Endosperm Cell Walls
Point, account for about the 75% of cell wall dry weight.It has been investigated that, it has blood fat reducing, cholesterol reducing, regulation blood glucose, improves immunity
Power and through U.S. FDA certification have prevention cardiovascular disease effect.The beta glucan content of Semen avenae nudae is higher than other paddy
Thing, but due to Semen avenae nudae coarse mouthfeel, and eating method is complex, therefore Semen avenae nudae class commercially available prod is difficult to be esthetically acceptable to the consumers,
Therefore the human body demand to Semen avenae nudae Middle nutrition composition cannot be met.And conventional culinary mode exists obtaining Semen avenae nudae effective ingredient
Difficulty.
Now, the drinking water of high-quality has been subjected to the concern of consumer, and people increasingly note while make-up water source
The health of weight drinking water, the water drinking high-quality has become as the consumption concept of a kind of health, fashion.
At present, the domestic pertinent literature and patent having no that its technological process, technological parameter etc. studied by plateau Semen avenae nudae water.
Summary of the invention
The technical problem to be solved is to provide a kind of plateau Semen avenae nudae water efficiently utilizing Semen avenae nudae effective ingredient
Preparation method.
For solving the problems referred to above, the preparation method of plateau of the present invention Semen avenae nudae water, comprise the following steps:
(1) after the Semen avenae nudae being crushed to 30 ~ 80 mesh being mixed according to the ratio of 1kg:15 ~ 25L with water, use mass concentration be 85 ~
The sodium bicarbonate regulation pH value of 95%, to 11, obtains mixed liquor；
(2), in described mixed liquor, it is sequentially added into the fibre of the amylase of 0.30 ~ 0.50g, 0.35 ~ 0.50g by 1000mL mixed liquor
Dimension element enzyme, then extracts through supersound extraction or heating in water bath, obtains extracting solution；
The most described extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 85 ~ 95% to 4.5, place mistake after 10 ~ 14h in 4 DEG C
Filter off except the protein in solution, obtain supernatant；
(4), after described supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing；
(5), after pure water being heated to 60 ~ 70 DEG C, pure water as described in every 100mL adds Semen avenae nudae extract described in 0.06 ~ 0.10g, and
Use reinforcement agitator to stir 20 ~ 40min with the rotating speed of 100 ~ 200r/min, obtain plateau Semen avenae nudae water semi-finished product；
(6), by described plateau Semen avenae nudae water semi-finished product through homogeneous, sterilization filling, obtain original flavor plateau Semen avenae nudae water；Or described plateau is blue or green
Highland barley water semi-finished product, after taste hooks and adjusts, obtain Semen avenae nudae filter liquor or fruity Semen avenae nudae aquatic products, this Semen avenae nudae filter liquor or fruity Semen avenae nudae
Aquatic products, through homogenizing, sterilization filling, obtain plateau Semen avenae nudae water.
Described step (1) in sodium bicarbonate be food stage.
Described step (2) in ultrasonic extraction conditions refer to temperature be 55 ~ 65 DEG C, frequency be 35 ~ 45 kHz, extraction time be
15~25min。
Described step (2) in heating in water bath extraction conditions refer to temperature be 60 ~ 70 DEG C, extraction time be 2 ~ 4 h.
The condition of described step (4) middle ultrafiltration refers to that ultrafiltration pressure is 0.6 ~ 0.8MPa, and ultrafiltrate temperature is 25 ~ 35 DEG C, ultrafiltration
Film Ceramics ultrafilter membrane.
The described step (4) middle condition being spray-dried refers to that inlet temperature is 160 ~ 170 DEG C, and leaving air temp is 75 ~ 85 DEG C,
Fan speed is 60.0Hz, and peristaltic pump rotating speed is 650 ~ 750mL/h, striker time 0.5 ~ 1.5s, striker interval 1 ~ 3s.
Described step (6) middle Semen avenae nudae filter liquor refers to described plateau Semen avenae nudae water semi-finished product heating in water bath to 60 ~ 70 DEG C, presses
Semen avenae nudae extract solution described in every 100mL adds 0.01 ~ 0.03g food stage lemon grass (Cymbopogon citratus), and use reinforcement agitator with 100 ~
Filter described lemon grass (Cymbopogon citratus) after the rotating speed stirring 6 ~ 10min of 200r/min and get final product.
Described step (6) middle fruity Semen avenae nudae aquatic products refer to add the concentration of 5 ~ 10% in the Semen avenae nudae water semi-finished product of described plateau
Fruit juice, or add ten thousand/fruity flavor to 5/10000ths in the Semen avenae nudae water semi-finished product of described plateau, formulated and get final product.
Described step (6) middle processing condition refers to that homogenization pressure is 50 ~ 80MPa, and temperature is 25 ~ 35 DEG C.
Described step (6) middle sterilising conditions refers to that temperature is 90 ~ 120 DEG C, and sterilization time is 4 ~ 8min.
The present invention compared with prior art has the advantage that
1, rich in Semen avenae nudae dietary fiber and highland barley Beta-dextran in Semen avenae nudae aquatic products of the present invention, it is a to there is certain health care functions
The product of property；Meanwhile, Semen avenae nudae is combined by invention product with water, traditional " eating Semen avenae nudae " is changed into " drinking Semen avenae nudae ", more has
It is beneficial to human body and to the efficient absorption of effective ingredient in Semen avenae nudae water and utilizes (seeing table 1).
Table 1 Semen avenae nudae water physical and chemical test data
2, the present invention uses ultrafiltration and drying process with atomizing to combine to a certain extent to improve highland barley Beta-dextran extraction ratio, change
It is apt to extract quality.
3, this novel highland barley product of present invention exploitation, has expanded Naked Barley from Qinghai-Tibet Plateau in China process deeply industry chain, is conducive to
Improve Semen avenae nudae added value, along with the market development degree of corn activated water product continues to increase, Semen avenae nudae fishery market potentiality
Huge.
Detailed description of the invention
The preparation method of embodiment 1 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:15L with water by the Semen avenae nudae being crushed to 30 mesh, using mass concentration is the bicarbonate of 85%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.30g, 0.350g by 1000mL mixed liquor, so
By supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 55 DEG C, frequency be 35 kHz, extraction time be 15min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 85% to 4.5, place to filter after 10h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.6MPa, and ultrafiltrate temperature is 25 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 160 DEG C, and leaving air temp is 75 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 650mL/h, striker time 0.5s, striker interval 1s.
(5), after pure water being heated to 60 DEG C, add 0.06g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 20min with the rotating speed of 100r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6), by plateau Semen avenae nudae water semi-finished product through homogeneous, sterilization filling, obtain original flavor plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 50MPa, and temperature is 25 DEG C.
Sterilising conditions refers to that temperature is 90 DEG C, and sterilization time is 8min.
The preparation method of embodiment 2 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:25L with water by the Semen avenae nudae being crushed to 80 mesh, using mass concentration is the bicarbonate of 95%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.50g, 0.50g by 1000mL mixed liquor, then
Through supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 65 DEG C, frequency be 45 kHz, extraction time be 25min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 95% to 4.5, place to filter after 14h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.8MPa, and ultrafiltrate temperature is 35 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 170 DEG C, and leaving air temp is 85 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 750mL/h, striker time 1.5s, striker interval 3s.
(5), after pure water being heated to 70 DEG C, add 0.10g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 40min with the rotating speed of 200r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6), by plateau Semen avenae nudae water semi-finished product heating in water bath to 60 DEG C, add 0.01g food by every 100mL Semen avenae nudae extract solution
Grade lemon grass (Cymbopogon citratus), and use reinforcement agitator to filter lemon grass (Cymbopogon citratus) after stirring 6min with the rotating speed of 100r/min, obtain the filter of Semen avenae nudae water
Liquid, this sterilized fill of Semen avenae nudae filter liquor, obtain plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 80MPa, and temperature is 35 DEG C.
Sterilising conditions refers to that temperature is 120 DEG C, and sterilization time is 4min.
The preparation method of embodiment 3 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:20L with water by the Semen avenae nudae being crushed to 40 mesh, using mass concentration is the bicarbonate of 90%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.40g, 0.40g by 1000mL mixed liquor, then
Through supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 60 DEG C, frequency be 40 kHz, extraction time be 20min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 90% to 4.5, place to filter after 12h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.7MPa, and ultrafiltrate temperature is 30 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 165 DEG C, and leaving air temp is 80 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 700mL/h, striker time 1s, striker interval 2s.
(5), after pure water being heated to 65 DEG C, add 0.08g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 30min with the rotating speed of 150r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6), by plateau Semen avenae nudae water semi-finished product heating in water bath to 70 DEG C, add 0.03g food by every 100mL Semen avenae nudae extract solution
Grade lemon grass (Cymbopogon citratus), and use reinforcement agitator to filter lemon grass (Cymbopogon citratus) after stirring 10min with the rotating speed of 200r/min, obtain the filter of Semen avenae nudae water
Liquid, this sterilized fill of Semen avenae nudae filter liquor, obtain plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 60MPa, and temperature is 30 DEG C.
Sterilising conditions refers to that temperature is 100 DEG C, and sterilization time is 6min.
The preparation method of embodiment 4 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:15L with water by the Semen avenae nudae being crushed to 50 mesh, using mass concentration is the bicarbonate of 85%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.35g, 0.45g by 1000mL mixed liquor, then
Extract through heating in water bath, obtain extracting solution.
Wherein: heating in water bath extraction conditions refer to temperature be 60 DEG C, extraction time be 2 h.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 85% to 4.5, place to filter after 10h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.6MPa, and ultrafiltrate temperature is 25 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 160 DEG C, and leaving air temp is 75 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 650mL/h, striker time 0.5s, striker interval 1s.
(5), after pure water being heated to 60 DEG C, add 0.06g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 20min with the rotating speed of 100r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6), by plateau Semen avenae nudae water semi-finished product heating in water bath to 65 DEG C, add 0.02g food by every 100mL Semen avenae nudae extract solution
Grade lemon grass (Cymbopogon citratus), and use reinforcement agitator to filter lemon grass (Cymbopogon citratus) after stirring 8min with the rotating speed of 150r/min, obtain the filter of Semen avenae nudae water
Liquid, this sterilized fill of Semen avenae nudae filter liquor, obtain plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 70MPa, and temperature is 25 DEG C.
Sterilising conditions refers to that temperature is 110 DEG C, and sterilization time is 5min.
The preparation method of embodiment 5 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:25L with water by the Semen avenae nudae being crushed to 60 mesh, using mass concentration is the bicarbonate of 95%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.45g, 0.45g by 1000mL mixed liquor, then
Extract through heating in water bath, obtain extracting solution.
Wherein: heating in water bath extraction conditions refer to temperature be 70 DEG C, extraction time be 4 h.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 95% to 4.5, place to filter after 14h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.8MPa, and ultrafiltrate temperature is 35 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 170 DEG C, and leaving air temp is 85 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 750mL/h, striker time 1.5s, striker interval 3s.
(5), after pure water being heated to 70 DEG C, add 0.10g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 40min with the rotating speed of 200r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6) add in the Semen avenae nudae water semi-finished product of plateau 5% Sucus Mali pumilae or Fructus Citri Limoniae juice or Sucus Mangiferae indicae, orange juice, blue berry,
The concentrated fruit juice such as Fructus Rubi berry, the formulated fruity Semen avenae nudae aquatic products that obtain, this fruity sterilized fill of Semen avenae nudae aquatic products, obtain high
Former Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 50MPa, and temperature is 25 DEG C.
Sterilising conditions refers to that temperature is 90 DEG C, and sterilization time is 8min.
The preparation method of embodiment 6 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:20L with water by the Semen avenae nudae being crushed to 80 mesh, using mass concentration is the bicarbonate of 95%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.50g, 0.50g by 1000mL mixed liquor, then
Extract through supersound extraction or heating in water bath, obtain extracting solution.
Wherein: heating in water bath extraction conditions refer to temperature be 65 DEG C, extraction time be 3 h.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 95% to 4.5, place to filter after 12h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.6MPa, and ultrafiltrate temperature is 25 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 160 DEG C, and leaving air temp is 75 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 650mL/h, striker time 0.5s, striker interval 1s.
(5), after pure water being heated to 65 DEG C, add 0.08g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 30min with the rotating speed of 150r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6) add in the Semen avenae nudae water semi-finished product of plateau 10% Sucus Mali pumilae or Fructus Citri Limoniae juice or Sucus Mangiferae indicae, orange juice, blue berry,
The concentrated fruit juice such as Fructus Rubi berry, the formulated fruity Semen avenae nudae aquatic products that obtain, this fruity sterilized fill of Semen avenae nudae aquatic products, obtain high
Former Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 80MPa, and temperature is 35 DEG C.
Sterilising conditions refers to that temperature is 120 DEG C, and sterilization time is 4min.
The preparation method of embodiment 7 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:25L with water by the Semen avenae nudae being crushed to 60 mesh, using mass concentration is the bicarbonate of 95%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.45g, 0.45g by 1000mL mixed liquor, then
Extract through heating in water bath, obtain extracting solution.
Wherein: heating in water bath extraction conditions refer to temperature be 70 DEG C, extraction time be 4 h.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 95% to 4.5, place to filter after 14h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.8MPa, and ultrafiltrate temperature is 35 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 170 DEG C, and leaving air temp is 85 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 750mL/h, striker time 1.5s, striker interval 3s.
(5), after pure water being heated to 70 DEG C, add 0.10g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 40min with the rotating speed of 200r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6) add in the Semen avenae nudae water semi-finished product of plateau 8% Sucus Mali pumilae or Fructus Citri Limoniae juice or Sucus Mangiferae indicae, orange juice, blue berry,
The concentrated fruit juice such as Fructus Rubi berry, the formulated fruity Semen avenae nudae aquatic products that obtain, this fruity sterilized fill of Semen avenae nudae aquatic products, obtain high
Former Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 70MPa, and temperature is 30 DEG C.
Sterilising conditions refers to that temperature is 100 DEG C, and sterilization time is 6min.
The preparation method of embodiment 8 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:20L with water by the Semen avenae nudae being crushed to 40 mesh, using mass concentration is the bicarbonate of 90%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.40g, 0.40g by 1000mL mixed liquor, then
Through supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 60 DEG C, frequency be 40 kHz, extraction time be 20min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 90% to 4.5, place to filter after 12h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.7MPa, and ultrafiltrate temperature is 30 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 165 DEG C, and leaving air temp is 80 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 700mL/h, striker time 1s, striker interval 2s.
(5), after pure water being heated to 65 DEG C, add 0.08g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 30min with the rotating speed of 150r/min, obtains plateau Semen avenae nudae water semi-finished product.
In the Semen avenae nudae water semi-finished product of plateau add ten thousand/ Fructus Mali pumilae or Fructus Citri Limoniae, Fructus Mangifera Indicae, orange, Fructus Crataegi, berry etc.
Fruity flavor, obtains fruity Semen avenae nudae aquatic products, this fruity sterilized fill of Semen avenae nudae aquatic products, obtains plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 60MPa, and temperature is 30 DEG C.
Sterilising conditions refers to that temperature is 100 DEG C, and sterilization time is 6min.
The preparation method of embodiment 9 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:25L with water by the Semen avenae nudae being crushed to 80 mesh, using mass concentration is the bicarbonate of 95%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.50g, 0.50g by 1000mL mixed liquor, then
Through supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 65 DEG C, frequency be 45 kHz, extraction time be 25min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 95% to 4.5, place to filter after 14h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.8MPa, and ultrafiltrate temperature is 35 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 170 DEG C, and leaving air temp is 85 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 750mL/h, striker time 1.5s, striker interval 3s.
(5), after pure water being heated to 70 DEG C, add 0.10g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 40min with the rotating speed of 200r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6) in the Semen avenae nudae water semi-finished product of plateau, add Fructus Mali pumilae or Fructus Citri Limoniae, Fructus Mangifera Indicae, orange, Fructus Crataegi, the berry etc. of 5/10000ths
Fruity flavor, obtains fruity Semen avenae nudae aquatic products, this fruity sterilized fill of Semen avenae nudae aquatic products, obtains plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 80MPa, and temperature is 35 DEG C.
Sterilising conditions refers to that temperature is 120 DEG C, and sterilization time is 4min.
The preparation method of embodiment 10 plateau Semen avenae nudae water, comprises the following steps:
(1), after being mixed according to the ratio of 1kg:15L with water by the Semen avenae nudae being crushed to 30 mesh, using mass concentration is the bicarbonate of 85%
Sodium regulation pH value, to 11, obtains mixed liquor.
(2), in mixed liquor, it is sequentially added into the cellulase of the amylase of 0.30g, 0.350g by 1000mL mixed liquor, so
By supersound extraction, obtain extracting solution.
Wherein: ultrasonic extraction conditions refer to temperature be 55 DEG C, frequency be 35 kHz, extraction time be 15min.
Extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 85% to 4.5, place to filter after 10h in 4 DEG C and remove
Protein in solution, obtains supernatant.
(4), after supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing.
Wherein: the condition of ultrafiltration refers to that ultrafiltration pressure is 0.6MPa, and ultrafiltrate temperature is 25 DEG C, ultrafilter membrane Ceramics ultrafiltration
Film.
The condition being spray-dried refers to that inlet temperature is 160 DEG C, and leaving air temp is 75 DEG C, and fan speed is 60.0Hz, compacted
Dynamic revolution speed is 650mL/h, striker time 0.5s, striker interval 1s.
(5), after pure water being heated to 60 DEG C, add 0.06g Semen avenae nudae extract by every 100mL pure water, and use reinforcement to stir
Device stirs 20min with the rotating speed of 100r/min, obtains plateau Semen avenae nudae water semi-finished product.
(6) in the Semen avenae nudae water semi-finished product of plateau, add Fructus Mali pumilae or Fructus Citri Limoniae, Fructus Mangifera Indicae, orange, Fructus Crataegi, the berry etc. of 3/10000ths
Fruity flavor, obtains fruity Semen avenae nudae aquatic products, this fruity sterilized fill of Semen avenae nudae aquatic products, obtains plateau Semen avenae nudae water.
Wherein: processing condition refers to that homogenization pressure is 50MPa, and temperature is 25 DEG C.
Sterilising conditions refers to that temperature is 90 DEG C, and sterilization time is 8min.
In above-described embodiment 1 ~ 10, sodium bicarbonate is food stage.
Claims (10)
1. the preparation method of plateau Semen avenae nudae water, comprises the following steps:
(1) after the Semen avenae nudae being crushed to 30 ~ 80 mesh being mixed according to the ratio of 1kg:15 ~ 25L with water, use mass concentration be 85 ~
The sodium bicarbonate regulation pH value of 95%, to 11, obtains mixed liquor；
(2), in described mixed liquor, it is sequentially added into the fibre of the amylase of 0.30 ~ 0.50g, 0.35 ~ 0.50g by 1000mL mixed liquor
Dimension element enzyme, then extracts through supersound extraction or heating in water bath, obtains extracting solution；
The most described extracting solution use mass concentration be the Fructus Citri Limoniae acid for adjusting pH value of 85 ~ 95% to 4.5, place mistake after 10 ~ 14h in 4 DEG C
Filter off except the protein in solution, obtain supernatant；
(4), after described supernatant being carried out ultrafiltration, the spray-dried prepared Semen avenae nudae rich in crude fibre and highland barley Beta-dextran is extracted
Thing；
(5), after pure water being heated to 60 ~ 70 DEG C, pure water as described in every 100mL adds Semen avenae nudae extract described in 0.06 ~ 0.10g, and
Use reinforcement agitator to stir 20 ~ 40min with the rotating speed of 100 ~ 200r/min, obtain plateau Semen avenae nudae water semi-finished product；
(6), by described plateau Semen avenae nudae water semi-finished product through homogeneous, sterilization filling, obtain original flavor plateau Semen avenae nudae water；Or described plateau is blue or green
Highland barley water semi-finished product, after taste hooks and adjusts, obtain Semen avenae nudae filter liquor or fruity Semen avenae nudae aquatic products, this Semen avenae nudae filter liquor or fruity Semen avenae nudae
Aquatic products, through homogenizing, sterilization filling, obtain plateau Semen avenae nudae water.
2. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (1) in sodium bicarbonate
For food stage.
3. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (2) middle supersound extraction bar
Part refer to temperature be 55 ~ 65 DEG C, frequency be 35 ~ 45 kHz, extraction time be 15 ~ 25min.
4. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (2) middle heating in water bath carries
The condition of taking refer to temperature be 60 ~ 70 DEG C, extraction time be 2 ~ 4 h.
5. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: the condition of described step (4) middle ultrafiltration
Referring to that ultrafiltration pressure is 0.6 ~ 0.8MPa, ultrafiltrate temperature is 25 ~ 35 DEG C, ultrafilter membrane Ceramics ultrafilter membrane.
6. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (4) middle spray drying
Condition refers to that inlet temperature is 160 ~ 170 DEG C, and leaving air temp is 75 ~ 85 DEG C, and fan speed is 60.0Hz, and peristaltic pump rotating speed is
650 ~ 750mL/h, striker time 0.5 ~ 1.5s, striker interval 1 ~ 3s.
7. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (6) middle Semen avenae nudae filter liquor
Referring to described plateau Semen avenae nudae water semi-finished product heating in water bath to 60 ~ 70 DEG C, as described in every 100mL, Semen avenae nudae extract solution adds
0.01 ~ 0.03g food stage lemon grass (Cymbopogon citratus), and use reinforcement agitator to filter after stirring 6 ~ 10min with the rotating speed of 100 ~ 200r/min
Described lemon grass (Cymbopogon citratus) and get final product.
8. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (6) middle fruity Semen avenae nudae water
Product refers to add the concentrated fruit juice of 5 ~ 10% in the Semen avenae nudae water semi-finished product of described plateau, or at described plateau Semen avenae nudae water semi-finished product
The fruity flavor of middle addition ten thousand/to 5/10000ths, formulated and get final product.
9. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (6) middle processing condition is
Finger homogenization pressure is 50 ~ 80MPa, and temperature is 25 ~ 35 DEG C.
10. the preparation method of plateau as claimed in claim 1 Semen avenae nudae water, it is characterised in that: described step (6) middle sterilising conditions
Referring to that temperature is 90 ~ 120 DEG C, sterilization time is 4 ~ 8min.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112079938A (en) * | 2020-08-18 | 2020-12-15 | 周银根 | Highland barley polysaccharide extraction method, highland barley polysaccharide extract and application thereof |
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