CN105995043A - Method for preparation of feeding additive from orange peel and lotus root dreg - Google Patents
Method for preparation of feeding additive from orange peel and lotus root dreg Download PDFInfo
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- CN105995043A CN105995043A CN201511019866.8A CN201511019866A CN105995043A CN 105995043 A CN105995043 A CN 105995043A CN 201511019866 A CN201511019866 A CN 201511019866A CN 105995043 A CN105995043 A CN 105995043A
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- citri tangerinae
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention discloses a method for preparation of a feeding immunopotentiator from orange peel and lotus root dreg as the main raw materials. The raw materials include, by weight, 12-14 parts of orange peel, 42-44 parts of lotus root dreg, 14-16 parts of bean dreg, 3.6-3.8 parts of Hylocereus undulates seed, 3.5-3.7 parts of dinobryon sertularia, 1.9 parts of carboxymethyl cellulose sodium, 1.3 parts of NaHSO3, and 2.5 parts of chitosan. The water content of the orange peel, lotus root dreg, dinobryon sertularia and Hylocereus undulates seed is 3-5%, and the water content of the bean dreg is 18-20%. The method consists of: mixing the five coarse powder in proportion, and mixing the mixture with an assistant evenly; then conducting grinding for 30min, and performing sieving with a 400-mesh sieve; carrying out treatment by a mechanochemical technology for 15min-30min according to the quality and humidity of the raw materials, thus obtaining a feeding immunopotentiator finished product. The method provided by the invention uses fruit and vegetable peel pomace and other production waste to produce the feeding immunopotentiator, significantly reduces the raw material production cost of the prior art, also recycles a lot of waste produced in food production, achieves low carbon production, and increases the added value of the product.
Description
Technical field
The invention belongs to field of feed, specifically refer to prepare for primary raw material feeding with Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag
The method of immunostimulant.
Background technology
China is live pig the first big producing country, but not makes the country prosperous, and reason is cultivation level and overall cultivation rule
Between mould incompatible.Owing to the aquaculture of China generally presents little and scattered, health and epidemic preventing working
It is difficult to put in place.The bottleneck problem of restriction industry development is the bacterial infection during pig-breeding, pathogenic bacterium
Often the pathogen such as the escherichia coli of zoonosis, not only affects aquaculture development, and threatens food
Safety.
Feeding antibiotic prevents and treats the history of aquaculture fowl bacterial disease existing decades, is considered for 20th century
The biotechnology that livestock and poultry breeding industry is the most prominent, numerous results of study shows, antibiotic can promote that animal is raw
Long, reduce sickness rate, mortality rate, improve the price of deed and carcase quality.Because antibiotic has price just
Preferably, instant effect, the feature such as easy to use, carry out huge economic benefit can to cultivation industrial belt.But just because of
This feature, the abuse of feeding antibiotic is the most universal.
In large-scale plant professional in the poultry farming of China and sideline production, raiser is also on a small scale
Depositing, cultivation relies on manpower to feed and nurse, and management level are relatively limited with sanitary condition ratio, though there being national legislation
Limit feeding antibiotic consumption, but part plant still excess tetracycline, soil that blindly use price is relatively low is mould
The broad ectrum antibiotic medicines such as element, chlortetracycline.After animal takes in above-mentioned medicine, it is enriched with in skeleton, in muscle
Also can extended residual, edible after cause the pathogen in human body to develop immunity to drugs, pass to disappear by health risk
Fei Zhe.
The common problem that the problem Ye Shi other countries that feeding antibiotic causes face, part European countries are
The measure that takes disables feeding growth promoting antibiotic.This measure of European countries can only reduce feeding antibiotic and pass
Passing the antibiotic resistance risk of people, the bacterial infection disease for prevention and control animal there is no help.1986
After year Sweden disables feeding antibacterial additives, the average raising 8 per ton of feed cost~11 dollars, cause poultry to be supported
Grow industry decline;After European Union's disabling part anti-bacteria agent for feeding, the pig farm of 50% is drastically gone up because of the mortality rate caused by diarrhoea
Rise, and food consumption increases, but poor growth.Scholar's statistics such as Viaene, the loss of every pig is close to 2
Dollar.In view of this present situation, exploitation has no side effect, does not develops immunity to drugs, the feed additive of noresidue,
Become the direction that various countries' research worker is made great efforts.Yolk antibody, probiotics, oligosaccharide, enzyme preparation, Tiny ecosystem
Preparation, active components of plants etc. all hold promise as feeding antibiotic succedaneum.Wherein, active components of plants
Because of its wide material sources, environmental protection, the feature such as safe and efficient, day by day become the focus of concern.
Active substance of plant has the multiple efficacies such as antibacterial, antiinflammatory, regulation immunity, but easily inactivates, suitable
Mouth property is poor;In producing reality, most Product Process are coarse, and product forms is single, difficult quality guarantee.
The present invention rely on Hunan Province fruit and vegerable cleaning processing engineering technology research center project (2015TP2022),
Orange juice born of the same parents clean production key technology study on the industrialization project (13CY028), orange juice born of the same parents' new product cleaning produces
Key technology Industrialization Projects (2015CK3031), Citrus sinensis Osbeck skin lesion of the scrotum clothing compound enzymic preparation produce key technology and turn
Change and demonstrative project (2014GB2D200228), the de-bitter machine of Pericarpium Citri tangerinae based on micro-cutting change-auxiliary agent interaction technology
Reason research project (14C1022), bean product process technologies provinces and cities build together applied basic research construction of base project
(2013TP4067), bean product process technology provinces and cities build together applied basic research construction of base project
(2013TP4068), quality comparison kinetic model and forecasting shelf life project in snack dried bean curd storage
(2014FJ4253), under etc. multiple fund projects are subsidized, seminar, through carrying out test of many times, obtains above-mentioned
Feeding immunostimulant.
Summary of the invention
It is an object of the invention to provide the method producing feeding immunostimulant with Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, carry simultaneously
For the product of the method gained, make full use of the garbage of processing of farm products, turn waste into wealth, promote aquaculture
Technology development.
Technical scheme is as follows:
The method producing feeding immunostimulant with Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, by Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, bean dregs, fire
Dragon fruit seed, garland bell jar algae are crushed to the coarse powder of 60~80 mesh respectively, by parts by weight of raw materials dispensing: Pericarpium Citri tangerinae 12~14
Part, Rhizoma Nelumbinis slag 42~44 parts, bean dregs 14~16 parts, dragon fruit seed 3.6~3.8 parts, garland bell jar algae 3.5~3.7
Part, auxiliary agent 8 parts;Auxiliary agent is by part 1.9 Carboxymethyl cellulose sodium, part 1.3NaHSO3,2.5 parts of chitosan structures
Become;Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, garland bell jar algae, dragon fruit seed water content 3~5%, bean dregs water content exists
18~20%;In described ratio, five kinds of coarse powder mixing are mixed with auxiliary agent again;Mechanochemistry method is used after mixing
Process, use high energy vibration mill to be processed, at cooling circulating water temperature 19-21 DEG C, frequency 16Hz, rod iron
Process 17-18min under the conditions of acceleration 8~9g, then shut down 3.5min, then with rod iron acceleration 6.7g at
Reason 12~13min, obtains feed additive finished product.
Optimization formula is: Pericarpium Citri tangerinae 13 parts, Rhizoma Nelumbinis slag 43 parts, 15 parts of bean dregs, dragon fruit seed 3.7 parts, flower
3.6 parts of ring bell jar algae, auxiliary agent 8 parts.
The application process of feeding immunostimulant, adds this by the weight ratio of 2~3% in live pig basal diet and exempts from
Epidemic disease reinforcing agent, it is thus achieved that rich in daidzein, soybean isoflavone, vitamin C, vitamin B, beta-carotene
Functional feed.
In formula, raw material part by weight is particularly significant, and reason is:
1. okara ratio particularity
Containing at least three kinds of antinutritional factor such as trypsin inhibitor, goitrin, haemoglutinins in bean dregs,
Addition is excessive, and during easily causing mechanico-chemical reaction, antinutritional factor inactivation is insufficient.
2. Rhizoma Nelumbinis slag ratio example particularity
Though containing immunostimulant such as vitamin C, vitamin B, polyphenol compound, peroxidase in Rhizoma Nelumbinis slag
Composition, but another importance is, and in Rhizoma Nelumbinis slag, contained active component can effectively reduce animal to Fructus Citri tangerinae in Pericarpium Citri tangerinae
Skin glycosides, tannin, limonin, the mycotoxin that may contain in bean dregs, contain in dragon fruit seed is thick fine
The impact that animal digestion is absorbed by the antinutritional factor such as dimension, is the buffering in formula, synergist.Garland bell jar
Algae, as the source of carotenoid, can improve immune level, can not be very few;But dimension contained therein is raw
If element A excess, also there is the risk producing negative effect.
3. Pericarpium Citri tangerinae ratio particularity
Pericarpium Citri tangerinae can increase palatability, can provide natural pigment, play the effect of phagostimulant in terms of color;
If but add too much, wherein the limonin of bitter taste affects palatability.
4. in five kinds of main components two-by-two between the particularity of ratio
Protein and the relative scale of vitamin B in Rhizoma Nelumbinis slag in bean dregs, in bean dregs, protein is special with Pericarpium Citri tangerinae
The relative scale of different composition Hesperidin, protein and the special composition β-Radix Dauci Sativae in garland bell jar algae in bean dregs
The relative scale of element, the ratio between these three groups of two kinds of compositions is substantially stationary.Reason is albumen in bean dregs
Matter has inclusion, slow release, water conservation, regulation mouthfeel in formula, strengthens the effect of palatability;Through this team
Early stage great many of experiments room and zoopery confirm, if bean dregs are less than normal with the ratio of other four kinds of components any one,
The active component in four kinds of components can be caused to be comprised insufficient, be exposed in gastric acid too early, and affect suitable
Mouth property, reduces feeding effect;If bigger than normal, then active component discharged slowly, DeGrain, produced economy
Waste, even 20% situation may affect the microorganism stable state of digestive tract back segment, cause animal digestion bad.
It addition, ratio between four kinds of main components in addition to bean dregs selected also has a particularity, herein without
Need to repeat, only one representative example of tool: containing carotenoid composition in Pericarpium Citri tangerinae, and in garland bell jar algae
Also containing analogous components, both proportional imbalances can cause adding generic ingredients excess, causes waste, even pair to be made
With.
The while of the present invention relates to 3 kinds of solid-state auxiliary agents, non-equal proportion, under high energy mechanical power effect with many plantations
Physical property raw material is jointly processed by, and multiple mechanico-chemical reaction the most necessarily occurs, and (this serial reaction is anti-between solid phase
Should, have essential distinction with the reaction in liquid system), cause the physics of vegetable raw material, chemistry, biological
The efficiently release of complicated change, beneficially bioactive ingredients can all occur and utilize.This concrete mechanism is also
Inventor team through repeatedly, many groups, multi-model test and propose first, without similar in domestic and international known technology
Report, those skilled in the art can not draw by rule of thumb or simply, and creativeness is that industry practitioner shows
And be clear to, meet the creativeness of Patent Law Article 22 third item defined.
To sum up, through repeatedly mixed extraction test with rat feeding experiment, Piglet feed test, become pig to feed,
And scale-up, obtain this special ratios.The ratio of any composition is too much or very few, all can be notable
Affect using effect, even result in the unbalance of this compound preparation, cause chain negative interaction, cause damage.
Present invention mechanical chemical technique processes Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, produces garbage with fruit and vegerable skin slag etc. and produces
Feeding immunostimulant, significantly reduces the raw material production cost of prior art, and will produce in food production
Raw a large amount of garbages recycle, it is achieved low-carbon (LC) produces, and increase added value of product.
(1) feed additive that the present invention provides uses in feedstuff for live pigs, and relatively prior art significantly reduces
Addition, has saved production cost, and improves the safety of raising, because low dosage adds greatly fall
Animal intestinal is easily produced by low Rhizoma Nelumbinis slag, garland bell jar algae, Pericarpium Citri tangerinae irritating composition (as tannin,
Limonin, colchicine etc.) potential risk;
(2) thickness of live pig gut epithelium tissue villus cell layer can be significantly improved;
(3) the quintessence oil constituents in Pericarpium Citri tangerinae has special aroma, can stimulate live pig appetite, press down and kill intestinal cause
The effect of pathogenic bacteria, thus the feed additive of present invention offer can improve the intestinal health situation of live pig, carries
High live pig production performance, feed conversion rate improves more than 3%;
(4) efficiency of feed utilization can be improved, to the palatability of feedstuff without any harmful effect;
(5) production technology of the present invention is simple, easy to use.
Detailed description of the invention
Embodiment is given below the present invention is elaborated.
Embodiment 1
The composition of raw materials of feeding immunostimulant is: Pericarpium Citri tangerinae 13 parts, Rhizoma Nelumbinis slag 43 parts, 15 parts of bean dregs, fire
Dragon fruit seed 3.7 parts, 3.6 parts of garland bell jar algae, auxiliary agent 8 parts.
Production method is, is processed by bean dregs miniature high-speed pulverizer, makes particle diameter reach 60 mesh, prepares bean
Slag coarse powder;By things such as the Rhizoma Nelumbinis slag being separately dried to water content 3%, garland bell jar algae, Pericarpium Citri tangerinae, dragon fruit seeds
Material, individually processes with miniature high-speed pulverizer respectively, makes particle diameter reach 60 mesh, prepares the thick of four kinds of materials
Powder;By formula proportion, five kinds of coarse powder are mixed;(auxiliary agent is by part 1.9 hydroxymethyl cellulose to add solid-state auxiliary agent again
Sodium, part 1.3NaHSO3,2.5 parts of chitosans are constituted) mix homogeneously;Use at mechanochemistry method after mixing
Reason, uses high energy vibration mill to be processed, and in cooling circulating water temperature 19-21 DEG C, frequency 16Hz, rod iron accelerates
Process 17-18min under the conditions of degree 8~9g, then shut down 3.5min, then with rod iron acceleration 6.7g process
12~13min, obtain feed additive finished product.
The application process of feeding immunostimulant is, the weight ratio interpolation pressing 2-3% in live pig basal diet should
Immunostimulant, is sufficiently mixed uniformly, obtains rich in daidzein, soybean isoflavone, vitamin C, dimension life
Element B, the functional feed of beta-carotene.
Embodiment 2
The composition of raw materials of feeding immunostimulant is: Pericarpium Citri tangerinae 12 parts, Rhizoma Nelumbinis slag 42 parts, 14 parts of bean dregs, fire
Dragon fruit seed 3.6 parts, 3.5 parts of garland bell jar algae, auxiliary agent 8 parts.
Production method and products application method are with embodiment 1.
Embodiment 3
The composition of raw materials of feeding immunostimulant is: Pericarpium Citri tangerinae 14 parts, Rhizoma Nelumbinis slag 44 parts, 16 parts of bean dregs, fire
Dragon fruit seed 3.8 parts, 3.7 parts of garland bell jar algae, auxiliary agent 8 parts.
Production method and products application method are with embodiment 1.
In order to check the effect of the present invention, in June, 2012 is carried out on Dong family of Daliang City of Liaoning Province ditch breeding pig farm
Following test:
Test material and method
It is added into adequate diet with the feeding immunostimulant of basis of embodiment 1~3 prescription, mixes with equal proportion simultaneously
Reference is carried out for comparison.Collection the following data:
1, rat challenge test: 30/group.Detect 1 μ g LPS (50 μ g/kg)+20mg D-GalN (1g/kg).
2, piglet experiment: 8/group, detection diarrhoea head number (counteracting toxic substances 5 × 1011E.coli K88), serum IgG
(g/L)。
3, pig experiment is become: 12/group, detecting 30 days body weight increase rate (%), Ea, EAC rosettes is formed
Rate (%), the apparent index of intestinal villus.Experimental result see table:
Separately, with 80 60-62kg American Duroc pig pigs as laboratory animal, it is divided into two groups, sets matched group respectively
(full price Dog ration) and test group (formula one) are tested.Result of the test shows: with matched group phase
Ratio, the diarrhea rate of test group significantly reduces, and Wall thickness of Small intestine significantly improves, IL-6 and IgA expresses and be respectively increased,
Feed conversion rate also significantly improves, and in live pig industrialized culture, average every day occurs situation ratio reducing aobvious
Writing, cost-effective and expenses more than 10%, effect is notable.
The present invention produces method and the product of feeding immunostimulant with Rhizoma Nelumbinis slag and Pericarpium Citri tangerinae, is widely used in supporting
The feed manufacturing on pig farm, cultivation.The present invention will provide a kind of for consumer of China and reduce feeding from beginning of production
Antibiotic amount, improves animal immune level, the product ensured food safety and issue-resolution.Fructus Citri tangerinae
The multiple peels such as skin, Rhizoma Nelumbinis slag are rich in polysaccharide and vitamin, it is possible to provide nutritional supplementation, strengthen animal immunizing power,
The more important thing is the carrier as active substance of plant and protective agent, improve palatability, make active substance of plant
Preparation process is difficult to disperse, after being administered orally, has slow release effect.
Claims (9)
1. Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag are the method that primary raw material prepares feeding immunostimulant, by Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag,
Bean dregs, dragon fruit seed, garland bell jar algae are crushed to the coarse powder of 60~80 mesh respectively, by parts by weight of raw materials dispensing:
Pericarpium Citri tangerinae 12~14 parts, Rhizoma Nelumbinis slag 42~44 parts, bean dregs 14~16 parts, dragon fruit seed 3.6~3.8 parts, garland bell jar algae
3.5~3.7 parts, auxiliary agent 8 parts;Auxiliary agent is by part 1.9 Carboxymethyl cellulose sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans
Constitute;Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, garland bell jar algae, dragon fruit seed water content 3~5%, bean dregs water content exists
18~20%;In described ratio, five kinds of coarse powder mixing are mixed with auxiliary agent again;Mechanochemistry method is used after mixing
Processing, use high energy vibration mill to be processed, in cooling circulating water temperature 19-21 DEG C, frequency 16Hz, rod iron adds
Process 17-18min under the conditions of speed 8~9g, then shut down 3.5min, then with rod iron acceleration 6.7g process
12~13min, obtain feed additive finished product.
Method the most according to claim 1, it is characterised in that by parts by weight of raw materials dispensing: Pericarpium Citri tangerinae 13 parts,
Rhizoma Nelumbinis slag 43 parts, 15 parts of bean dregs, dragon fruit seed 3.7 parts, 3.6 parts of garland bell jar algae, 1.9 hydroxylmethyl cellulose
Element sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
Method the most according to claim 1, it is characterised in that by parts by weight of raw materials dispensing: Pericarpium Citri tangerinae 12 parts,
Rhizoma Nelumbinis slag 42 parts, 14 parts of bean dregs, dragon fruit seed 3.6 parts, 3.5 parts of garland bell jar algae, 1.9 hydroxylmethyl cellulose
Element sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
Method the most according to claim 1, it is characterised in that by parts by weight of raw materials dispensing: Pericarpium Citri tangerinae 14 parts,
Rhizoma Nelumbinis slag 44 parts, 16 parts of bean dregs, dragon fruit seed 3.8 parts, 3.7 parts of garland bell jar algae, 1.9 hydroxylmethyl cellulose
Element sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
5. a feeding immunostimulant, raw material is by following weight portion dispensing: Pericarpium Citri tangerinae 12~14 parts, Rhizoma Nelumbinis slag 42~44
Part, bean dregs 14~16 parts, dragon fruit seed 3.6~3.8 parts, garland bell jar algae 3.5~3.7 parts, 1.9 hydroxymethyl cellulose
Sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans, Pericarpium Citri tangerinae, Rhizoma Nelumbinis slag, garland bell jar algae, dragon fruit seed aqueous
Amount is 3~5%, and bean dregs water content is 18~20%.
The feeding immunostimulant of one the most according to claim 5, it is characterised in that raw material dispensing by weight:
Pericarpium Citri tangerinae 13 parts, Rhizoma Nelumbinis slag 43 parts, 15 parts of bean dregs, dragon fruit seed 3.7 parts, 3.6 parts of garland bell jar algae, 1.9
Carboxymethyl cellulose sodium, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
Feeding immunostimulant the most according to claim 5, it is characterised in that raw material dispensing by weight: Fructus Citri tangerinae
Skin 12 parts, Rhizoma Nelumbinis slag 42 parts, 14 parts of bean dregs, dragon fruit seed 3.6 parts, 3.5 parts of garland bell jar algae, 1.9 hydroxyls
Sodium carboxymethylcellulose pyce, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
Feeding immunostimulant the most according to claim 5, it is characterised in that raw material dispensing by weight: Fructus Citri tangerinae
Skin 14 parts, Rhizoma Nelumbinis slag 44 parts, 16 parts of bean dregs, dragon fruit seed 3.8 parts, 3.7 parts of garland bell jar algae, 1.9 hydroxyls
Sodium carboxymethylcellulose pyce, 1.3 parts of NaHSO3, 2.5 parts of chitosans.
9. the application process of the arbitrary described feeding immunostimulant of claim 5-8, by 2~3% in live pig basal diet
Weight ratio add this immunostimulant, it is thus achieved that raw rich in daidzein, soybean isoflavone, vitamin C, dimension
Element B, the functional feed of beta-carotene.
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103734519A (en) * | 2013-12-24 | 2014-04-23 | 邵阳学院 | Method and product for producing forage immune enhancer by adopting soybean curb residue and orange peel |
CN103783329A (en) * | 2014-03-10 | 2014-05-14 | 邵阳学院 | Natural forage yolk toner produced by orange peels and flavedo and preparation method thereof |
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2015
- 2015-12-29 CN CN201511019866.8A patent/CN105995043A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103734519A (en) * | 2013-12-24 | 2014-04-23 | 邵阳学院 | Method and product for producing forage immune enhancer by adopting soybean curb residue and orange peel |
CN103783329A (en) * | 2014-03-10 | 2014-05-14 | 邵阳学院 | Natural forage yolk toner produced by orange peels and flavedo and preparation method thereof |
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Application publication date: 20161012 |