CN105973781A - Stress-chemical coupling visualization testing system for laminated salt rock - Google Patents

Stress-chemical coupling visualization testing system for laminated salt rock Download PDF

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Publication number
CN105973781A
CN105973781A CN201610270252.5A CN201610270252A CN105973781A CN 105973781 A CN105973781 A CN 105973781A CN 201610270252 A CN201610270252 A CN 201610270252A CN 105973781 A CN105973781 A CN 105973781A
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China
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tubulose body
chemical solution
stress
confined pressure
temperature sensor
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陈结
刘伟
康燕飞
姜德义
彭辉华
卢丹
周建坤
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Chongqing University
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Chongqing University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N17/00Investigating resistance of materials to the weather, to corrosion, or to light

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Environmental Sciences (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a stress-chemical coupling visualization testing system for a laminated salt rock, wherein the testing system includes a specimen clamp holder, an axial chemical solution adding system, a confining pressure loading system and a magnetic resonance imaging system; the clamp holder comprises a tubular machine body, an upper plug, a lower plug, an upper jacking head, a lower jacking head, a tubular sealing sleeve, a heating layer and the like. The testing system can easily control and adjust the pressure and temperature of a chemical solution, and the confining pressure and the environment temperature of a specimen during testing, and then a seepage path and permeability amount of petroleum in a bedding zone are subjected to visualized analysis under a certain confining pressure condition of the laminated salt rock in virtue of the magnetic resonance imaging system; different degrees of corrosion effects are generated because a liquid solution is infiltrated into the salt rock or an interlayer along cracks after a surrounding rock is cracked and damaged under stress action, the surrounding rock is weakened, new cracks are promoted to generate the coupling superposition effect, and the bedding stress-chemical coupling effect and permeability in a salt cave oil storage process is revealed.

Description

The stress of alternating layers rock salt-chemical Coupling Visualization system
Technical field
The present invention relates to testing equipment, study rock salt long-term creep under multi-scenarios method effect particularly to a kind of Testing equipment.
Background technology
Oil is as the blood of industry, in occupation of very important status in national economy.Once there is oil Crisis, will cause the serious consequence such as economic recession, social unrest.China from reform and opening-up since economy always Keeping high speed development, the demand for oil also grows with each passing day.According to CNPC's group economy technical research " domestic and international gas industries development report " that institute issues for 2016 is pointed out, China's oil consumption in 2015 Being 5.43 billion cubic meters, external dependence degree is up to 60.6%.China's oil-production capacity wretched insufficiency, it is necessary to big Amount depends on import.But, external oil interdependency is the highest, and China's oil market is affected by international environment The biggest, energy potential collision hazard is the most prominent, if the politics in the world, the unfavorable situation such as economic and military Under the influence of, it is possible to there is the serious consequences such as oil shortage even oil crisis.
In the morning on October 23rd, 2015, " the 3rd salt cave utilizes international symposium " holds in Beijing, meeting On from more than 100 name experts and scholars Chinese, German, French, Austrian around the " economy of salt cave resource Exploitation and technical security " theme carried out academic discuss and exchange of technology, and wherein salt cave oil storage, salt cave are comprehensive The advanced problems such as utilization cause scholar's extensive concern.In meeting, China Salt Industry Co. president-Li Yao refers to by force Go out, " although there is abundant rock salt resources in China, but the salt cave quantity being utilized at present is the most few, As technical method science is correct, salt cave utilizes can provide crude oil, product oil, natural gas and some Industry Wastes The preferable memory space of material, but as method is the most proper, either during exploitation, or at bank During use, a potential safety hazard will be become.”
Utilize many interlayers salt cave to carry out the material storages such as crude oil and must take into the chemical solutions such as the oil phase with country rock Interaction relation.It is big, during particularly note is adopted that salt cavern underground storage buried depth makes greatly to store hydrostatic oil pressure Bigger pressure reduction change can accelerate Rock Damage, and the chemical erosion bad effect of oil/salt, makes underground in addition The environment of bank is more complicated, is more difficult to predict to its safe condition.Accordingly, it would be desirable to the corresponding examination of exploitation Experiment device research salt cave crude oil note adopts the stress-chemical Coupling effect of process casing reason, it is achieved steady to country rock Qualitative analysis and prediction.
Summary of the invention
In view of this, it is an object of the invention to provide the stress-chemical Coupling Visualization of a kind of alternating layers rock salt System, to simulate the interaction environment of the chemical solutions such as oil and country rock, the research salt cave crude oil note process of adopting is enclosed Stress-chemical Coupling the effect of rock stratum reason, it is achieved stability analysis and the prediction to country rock.
The stress of alternating layers rock salt of the present invention-chemical Coupling Visualization system, including specimen holder device, axially Chemical solution add-on system, confined pressure loading system and nuclear magnetic resonance imaging system;
Described clamper includes tubulose body, the two ends pore of described tubulose body is arranged upper plug head and under Plug, the end of described tubulose body is additionally provided with the lower end cap of fixing lower end cap and fixes seat, described on Plug is positioned on one end of tubulose body and is provided with top end, and described lower end cap is positioned at tubulose body It is provided with lower top on one end, between top end and lower top, is provided with test specimen;
Described tubulose body also includes the tubular seals glue that two ends are connected on upper plug head and lower end cap Set, described top end, lower top and test specimen are positioned in tubular seals gum cover;
It is provided with zone of heating on the inner tubal wall of described tubulose body, the outer tube wall of tubulose body is provided with guarantor Temperature layer, the space between described zone of heating and tubular seals set is confined pressure room, and described tubulose body is arranged There is the first temperature sensor of detection confined pressure indoor temperature, the two ends of tubulose body are respectively arranged with and enclose Pressure chamber connection confined pressure oil-feed pore and confined pressure emptying pore, the oil-out of described confined pressure loading system with enclose It is pressed into oil pipe hole to connect, outside described heat-insulation layer, is cased with the malcoils of nuclear magnetic resonance imaging system;
Two ends on described test specimen are provided with the chemical solution passage axially extended, and described upper plug head sets Being equipped with upper liquid inlet pipe hole channel attached with chemical solution on test specimen, institute's lower end cap and lower end cap are fixed on seat It is provided with lower liquid inlet pipe hole channel attached with chemical solution on test specimen;Described upper liquid inlet pipe hole and lower feed liquor Pore liquid outlet with axial chemical solution add-on system respectively is connected.
Further, described axial chemical solution add-on system includes chemical solution container and being arranged on of inlet Learn the compression pump in solution container, the liquid outlet lateral line of described compression pump is disposed with effusion meter, Second temperature sensor, the first heater having auto-regulating temp, three-temperature sensor, the first pressure transducer With the 4th temperature sensor, the pipeline between described pressure transducer and the 4th temperature sensor is provided with First arm, described first arm connects and has vacuum pump, the liquid outlet side of described 4th temperature sensor It is provided with the second arm on pipeline, described second arm is provided with manual switch valve.
Further, described confined pressure loading system includes confined pressure pump, and the liquid outlet lateral line of described confined pressure pump sets It is equipped with the second heater having auto-regulating temp, the 5th temperature sensor and the second pressure transducer.
Further, described zone of heating is spiral heat exchange tube or the ring set of band annular liquid storage cylinder, described tubulose body On be provided with the deep fat that adds that the ring set with spiral heat exchange tube or band annular liquid storage cylinder is connected and enter pore and heating Pore discharged by oil.
Beneficial effects of the present invention:
The stress of alternating layers rock salt of the present invention-chemical Coupling Visualization system, the chemical solution at two ends on its test specimen Liquid passage can be blind hole, it is also possible to for the through hole of coaxial communication, can need to select according to test;Test Time chemical solution passage in be full of solution, and the pressure of solution, temperature can by axial chemical solution add system Tracking saves, in conjunction with the confined pressure power suffered by confined pressure loading system regulation test specimen and the temperature residing for zone of heating regulation test specimen Environment, it is possible to simulation petroleum storage process height hydrostatic oil pressure and note oil recovery process;Relend and help nuclear magnetic resonance, NMR As system, can visual analyzing alternating layers rock salt under the conditions of certain confined pressure, oil layer reason band percolation path and Infiltration capacity.Therefore, this pilot system has taken into full account that salt cave is storing oil process, and cavity country rock is subject to simultaneously The common effect of crustal stress, crude oil medium osmosis corrosion;Salt after the corrosion of this pilot system energy relative analysis crude oil solution The deformation characteristic of rock, strength characteristics and fine sight architectural feature thereof, and monitor crucial ion concentration in chemical solution Changing Pattern, inquire into rock salt sample oiling corrosive effect.This pilot system can be simulated when country rock is at stress After the lower crack and damage of effect, liquid solution penetrates into the corrosion work produced rock salt or interlayer in various degree along crack With, weaken country rock, promote that new crack produces this coupling synergistic effect, disclose salt cave oil storage process layer reason Stress-chemical Coupling effect and permeability.
Accompanying drawing explanation
Fig. 1 is the structural representation of the stress-chemical Coupling Visualization system of alternating layers rock salt of the present invention;
Fig. 2 is the sectional structure schematic diagram of P portion clamper in Fig. 1.
Detailed description of the invention
The invention will be further described with embodiment below in conjunction with the accompanying drawings.
As it can be seen, the stress of the present embodiment alternating layers rock salt-chemical Coupling Visualization system, including test specimen Clamper, axial chemical solution add-on system, confined pressure loading system and nuclear magnetic resonance imaging system;
Described clamper includes tubulose body 1, arranges upper plug head 2 in the two ends pore of described tubulose body With lower end cap 3, the lower end cap that the end of described tubulose body is additionally provided with fixing lower end cap fixes seat 4, Described upper plug head is positioned on one end of tubulose body and is provided with top end 5, and described lower end cap is positioned at tubulose device It is provided with lower top 6 on internal one end, between top end and lower top, is provided with test specimen 7;
Described tubulose body also includes the tubular seals set 8 that two ends are connected on upper plug head and lower end cap, Described top end, lower top and test specimen are positioned in tubular seals set, and the tubular seals set in the present embodiment is logical Cross clip 36 to be connected with plug, connect simple and convenient;
It is provided with zone of heating 9 on the inner tubal wall of described tubulose body, the outer tube wall of tubulose body is provided with guarantor Temperature layer 10, the space between described zone of heating and tubular seals set is confined pressure room 11, on described tubulose body It is provided with the first temperature sensor 12 of detection confined pressure indoor temperature, the two ends of tubulose body are respectively provided with There is the confined pressure oil-feed pore 13 and confined pressure emptying pore 14 connected with confined pressure room, described confined pressure loading system Oil-out is connected with confined pressure oil-feed pore, is cased with the nuclear-magnetism of nuclear magnetic resonance imaging system altogether outside described heat-insulation layer Shake coil 15;
The two ends of described test specimen are provided with the chemical solution passage axially extended, as it is shown in figure 1, this reality The chemical solution passage executing two ends on test specimen in example can be blind hole, described upper plug head is provided with on test specimen The channel attached upper liquid inlet pipe hole 16 of chemical solution, institute's lower end cap and lower end cap are fixed and are provided with on seat and try The channel attached lower liquid inlet pipe hole 17 of chemical solution on part;Described upper liquid inlet pipe hole and lower liquid inlet pipe hole are respectively It is connected with the liquid outlet of axial chemical solution add-on system.
The stress of the present embodiment alternating layers rock salt-chemical Coupling Visualization system, the chemistry at two ends on its test specimen Solution channel can be blind hole, and in different tests, on test specimen, the chemical solution passage at two ends can also be certainly The through hole of coaxial communication, can need to select according to test;Solution it is full of in chemical solution passage during test, and The pressure of solution, temperature can be regulated by axial chemical solution add-on system, regulate in conjunction with confined pressure loading system Confined pressure power suffered by test specimen and zone of heating regulation temperature environment residing for test specimen, it is possible to simulation petroleum storage process is high Hydrostatic oil pressure and note oil recovery process;Relend and help nuclear magnetic resonance imaging system, can visual analyzing alternating layers rock salt Under the conditions of certain confined pressure, oil manages percolation path and the infiltration capacity of band at layer.Therefore, this pilot system is abundant Considering salt cave and storing oil process, cavity country rock jointly by crustal stress, the corrosion of crude oil medium osmosis simultaneously Effect;The deformation characteristic of rock salt, strength characteristics and micro-after the corrosion of this pilot system energy relative analysis crude oil solution Microscopical structure feature, and monitor the Changing Pattern of crucial ion concentration in chemical solution, inquire into the oil of rock salt sample Chemical attack effect.This pilot system can be simulated when country rock is under stress effect after crack and damage, liquid solution edge Crack is penetrated into and rock salt or interlayer is produced corrosiveness in various degree, weakens country rock, promotes that new crack produces This coupling synergistic effect, discloses stress-chemical Coupling effect and the permeability of salt cave oil storage process layer reason.
In the present embodiment, described axial chemical solution add-on system includes chemical solution container 18 and inlet The compression pump 19 being arranged in chemical solution container, the liquid outlet lateral line of described compression pump sets gradually There are effusion meter the 20, second temperature sensor the 21, first heater having auto-regulating temp 22, three-temperature sensor 23, the first pressure transducer 24 and the 4th temperature sensor 25, described pressure transducer and the 4th temperature pass Being provided with the first arm 26 on pipeline between sensor, described first arm connects vacuum pump 27, institute State and on the liquid outlet lateral line of the 4th temperature sensor, be provided with the second arm 28, described second arm sets It is equipped with manual switch valve 29.
Axial chemical solution add-on system in the present embodiment can easily regulate the chemical solution entering test specimen Pressure and temperature, controlling test is simple.
In the present embodiment, described confined pressure loading system includes confined pressure pump 30, the liquid outlet side of described confined pressure pump The second heater having auto-regulating temp the 31, the 5th temperature sensor 32 and the second pressure transducer it is provided with on pipeline 33。
Confined pressure loading system in the present embodiment can easily regulate enter confined pressure room pressure oil pressure and Temperature, controlling test is simple.
In the present embodiment, described zone of heating 9 is spiral heat exchange tube, and zone of heating is also the most in different embodiments Can be ring set or other structure of band annular liquid storage cylinder, described tubulose body is provided with and spiral heat exchange tube The deep fat that adds connected enters pore 34 and adds deep fat discharge pipe hole 35;Zone of heating simple in construction, easily implements.
Finally illustrate, above example only in order to technical scheme to be described and unrestricted, although With reference to preferred embodiment, the present invention is described in detail, it will be understood by those within the art that, Technical scheme can be modified or equivalent, without deviating from technical solution of the present invention Objective and scope, it all should be contained in the middle of scope of the presently claimed invention.

Claims (4)

1. the stress of an alternating layers rock salt-chemical Coupling Visualization system, it is characterised in that: include examination Part clamper, axial chemical solution add-on system, confined pressure loading system and nuclear magnetic resonance imaging system;
Described clamper includes tubulose body, the two ends pore of described tubulose body is arranged upper plug head and under Plug, the end of described tubulose body is additionally provided with the lower end cap of fixing lower end cap and fixes seat, described on Plug is positioned on one end of tubulose body and is provided with top end, and described lower end cap is positioned at tubulose body It is provided with lower top on one end, between top end and lower top, is provided with test specimen;
Described tubulose body also includes the tubular seals set that two ends are connected on upper plug head and lower end cap, Described top end, lower top and test specimen are positioned in tubular seals set;
It is provided with zone of heating on the inner tubal wall of described tubulose body, the outer tube wall of tubulose body is provided with guarantor Temperature layer, the space between described zone of heating and tubular seals set is confined pressure room, and described tubulose body is arranged There is the first temperature sensor of detection confined pressure indoor temperature, the two ends of tubulose body are respectively arranged with and enclose Pressure chamber connection confined pressure oil-feed pore and confined pressure emptying pore, the oil-out of described confined pressure loading system with enclose It is pressed into oil pipe hole to connect, outside described heat-insulation layer, is cased with the malcoils of nuclear magnetic resonance imaging system;
The two ends of described test specimen are provided with the chemical solution passage axially extended, and described upper plug head is arranged Having upper liquid inlet pipe hole channel attached with chemical solution on test specimen, institute's lower end cap and lower end cap are fixed and are set on seat It is equipped with lower liquid inlet pipe hole channel attached with chemical solution on test specimen;Described upper liquid inlet pipe hole and lower feed tube Hole liquid outlet with axial chemical solution add-on system respectively is connected.
The stress of alternating layers rock salt the most according to claim 1-chemical Coupling Visualization system, it is special Levy and be: described axial chemical solution add-on system includes that chemical solution container and inlet are arranged on chemistry Compression pump in solution container, the liquid outlet lateral line of described compression pump is disposed with effusion meter, Two temperature sensors, the first heater having auto-regulating temp, three-temperature sensor, the first pressure transducer and 4th temperature sensor, the pipeline between described pressure transducer and the 4th temperature sensor is provided with One arm, described first arm connects and has vacuum pump, the liquid outlet side pipe of described 4th temperature sensor It is provided with the second arm on road, described second arm is provided with manual switch valve.
The stress of alternating layers rock salt the most according to claim 1-chemical Coupling Visualization system, it is special Levy and be: described confined pressure loading system includes confined pressure pump, the liquid outlet lateral line of described confined pressure pump is arranged There are the second heater having auto-regulating temp, the 5th temperature sensor and the second pressure transducer.
The stress of alternating layers rock salt the most according to claim 1-chemical Coupling Visualization system, it is special Levy and be: described zone of heating is spiral heat exchange tube or the ring set of band annular liquid storage cylinder, on described tubulose body It is provided with the deep fat that adds that the ring set with spiral heat exchange tube or band annular liquid storage cylinder is connected enter pore and add deep fat Discharge pore.
CN201610270252.5A 2016-04-27 2016-04-27 Stress-chemical coupling visualization testing system for laminated salt rock Pending CN105973781A (en)

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CN106404548A (en) * 2016-10-31 2017-02-15 重庆大学 Method for visually analyzing crack propagation under hydraulic fracturing effect
CN107894392A (en) * 2017-12-20 2018-04-10 山东大学 Bolted discontinuous rock anchors the research system and method for Corrosion mechanism under sea water intrusion
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CN110805440A (en) * 2019-11-26 2020-02-18 西南石油大学 Visual agent injection physical model for high-temperature high-pressure fracture-cavity oil reservoir
CN112432891A (en) * 2020-10-21 2021-03-02 西安理工大学 Roller compacted concrete corrosion real-time monitoring device and method capable of considering hydraulic pressure action

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CN107894392B (en) * 2017-12-20 2023-08-25 山东大学 Research system and method for anchoring corrosion mechanism of anchored jointed rock mass under seawater corrosion
CN110096824A (en) * 2019-05-08 2019-08-06 中国科学院武汉岩土力学研究所 Salt cave storage tank farm method for estimating stability
CN110805440A (en) * 2019-11-26 2020-02-18 西南石油大学 Visual agent injection physical model for high-temperature high-pressure fracture-cavity oil reservoir
CN112432891A (en) * 2020-10-21 2021-03-02 西安理工大学 Roller compacted concrete corrosion real-time monitoring device and method capable of considering hydraulic pressure action

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Application publication date: 20160928