CN105963227B - A kind of preparation method and applications of 3D facial masks solution - Google Patents

A kind of preparation method and applications of 3D facial masks solution Download PDF

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CN105963227B
CN105963227B CN201610440217.3A CN201610440217A CN105963227B CN 105963227 B CN105963227 B CN 105963227B CN 201610440217 A CN201610440217 A CN 201610440217A CN 105963227 B CN105963227 B CN 105963227B
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parts
solution
facial masks
green tea
verbena officinalis
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CN105963227A (en
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陈松彬
易萍
倪彦艳
张爱萍
刘杰森
吴纯玲
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Guangdong Cooway Biological Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8129Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/925Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y70/00Materials specially adapted for additive manufacturing

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Abstract

The present invention provides a kind of preparation method and applications of 3D facial masks solution, belongs to cosmetics preparation field.Although 3D facial masks start commercially to emerge in large numbers in the prior art, the real solution research and development progress for being used for 3D facial masks is very slow, the present invention is intended to provide a kind of preparation method and applications of 3D facial masks solution, described facial mask solution is prepared by following raw material:40 50 parts of Verbena officinalis plant essence liquid, 0.01 3 parts of shitosan, 26 parts of honey, 46 parts of water-soluble lanolin, 10 20 parts of green tea extractive liquor, 35 parts of ginsenoside, 35 parts of glycine, 13 parts of vitamin E, 24 parts of polyvinyl alcohol.The 3D facial masks for preparing can significantly improve keratoderma water content and the percutaneous water loss of skin of face, with good application prospect.

Description

A kind of preparation method and applications of 3D facial masks solution
Technical field
The present invention relates to a kind of preparation method and applications of 3D facial masks solution, belong to cosmetics preparation field.
Background technology
Facial mask market has turned into that China's daily use chemicals industry is fastest-rising one of to segment market at present.Ground according to Nelson's retail Study carefully data, up to 78.5 hundred million yuans (similarly hereinafter), continuous 3 years annual compound growth rates surpass Chinese facial mask market sale scale in 2012 21.9% is crossed, facial mask market will continue mad growth within 2014, it is contemplated that sales volume the most conservative will be up to 30,000,000,000 by 2015 Unit.Facial mask sale in 2013 occupies the 3rd in Cosmetic Market, accounts for the 16.3% of market sale total value.Data display, 2012 13.9 hundred million yuan of Watson facial mask sales volume, is 11% in the sale accounting of Watson, and by 2013, its facial mask sales volume reached 1700000000 yuan, increase by 22% on a year-on-year basis.The facial mask category gross sales amount of Taobao in 2013 is up to 2,200,000,000 yuan, wherein frivolous stealthy silk face Film sales volume is 10.2 hundred million yuan, accounting 46.69%.
The development speed of facial mask it is closely bound up with its effect soon.Facial mask can simultaneously solve the big problem of skin 5:Moisturizing, Whitening, oil-control, antiallergic sense and anti-aging.And everyday skincare is often just for subproblem therein comprehensively, it is impossible to quickly change Kind skin condition.Facial mask is temporarily isolating air and the pollution in the external world using the of short duration time for being covered in face, improves skin temperature With expansion pore, promote sweat gland secretion and metabolism, skin oxygen content is increased.Moisture in facial mask penetrates into skin cutin Layer, makes it become soft, increases elasticity;Gumminess composition or powdered absorbent in facial mask can stick in skin surface and pore Dirt, metabolic waste and excessive grease etc., and by its thorough removing.
The principle of facial mask is exactly that air and the pollution in the external world are temporarily isolating using the of short duration time for being covered in face, is improved Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, the oxygen content of skin is increased, and is conducive to skin The product of epidermal cell metabolism and the oil substances of accumulation are excluded, the moisture in facial mask penetrates into the cutin of skin epidermis Layer, skin becomes soft, and light is flexible naturally for skin.Facial mask is a kind of carrier of face beautifying health keeping product, is applied in 15-30 on the face Minute, institute's nutrient-containing is slowly absorbed by the skin supplement with adjustment.
French Sisley is released in March, 2010 and adopts bright flesh clay mask in a wink.Kaolin and mica are with the addition of in formula Solid powder, can remove impurity and grease on the face;Polysorbate -60 and the smooth isostearate of sorb as emulsifying agent, with High molecular polymer compounding use, improves the suspension stability of solid powder.In addition carrot elite, Portugal are also added in formula Grape folic acid China, wild rose elite, rosemary and chamomile essential oil isoreactivity material, with the dark yellow effect of the removal colour of skin.
Laneige brand releases a daily strawberry yoghurt pack, Yoghourt in January, 2012 in China under love jasmine group of South Korea Be combined together for the concept of food and cosmetics well by outward appearance and strawberry odor type, is received significant attention after listing.The facial mask In with the addition of butter fruit resin and Bai Mang flower seed oils, there is provided the nutriment needed for skin.Formula has used natural botanical source Emulsifying agent, such as tristerin, Glyceryl stearate citrate, sucrose and sucrose palmitate, with good outward appearance And quality.
The U of Chinese utility model patent CN 202959257 disclose the three-dimensional closely connected facial masks of high-tension 3D, and it mainly includes face Film layer, described face mask layer is a three-dimensional entirety facial mask, facial mask layer surface according to the streamlined design of shape of face of people, nostril, Opening is designed with mouth and eyes.Wherein 3D facial masks more meet human face's curve and depression projection, viscose glue and blend polyester Facial mask material, it is possible to which help is lifted, the effect of consolidation skin, and it is ventilative comfortable;Skin uniform force, accumulates with skin contact Reach more than 95%;Essence utilization rate is high, and common 2D facial masks absorption affinity is small, and easily slime flux causes to waste Essence everywhere.
The A of Chinese invention patent application CN 105326744 disclose a kind of abalone facial mask preparation method, and it is with abalone as former Material is obtained abalone hydrolyzate, is equipped with the Chinese medicine extract that almond, Poria cocos, cucumber, peppermint, green tea, peach blossom, rose are raw material, The facial mask solution for adding honey to be mixed to prepare, then Face film towel is soaked in facial mask solution, then Vacuum Package is made.Its Play the work(of beauty in prescription altogether with abalone hydrolyzate, Chinese medicine extract, honey, each component compatibility complements one another, brings out the best in each other.
The A of Chinese invention patent application CN 104721061 disclose a kind of preparation method of 3D facial masks and its 3D of preparation Facial mask.The method includes:Scanning skin of face, obtains skin condition and surface image;Three-dimensional mold is set up according to surface image; Facial mask solution is printed to three-dimensional mold according to skin condition, obtains 3D facial masks;Facial mask solution includes:Water, film forming agent, plasticising Agent, surfactant and functional components.It is experimentally confirmed that using the facial mask solution in present invention offer preparation method after printing Can fast filming, film forming thin and thick be suitable, physicochemical property does not occur substantially change before and after printing, and tensile resistance is stronger, does not send out The excessive adhesion phenomenon of life.
The content of the invention
Although 3D facial masks start commercially to emerge in large numbers in the prior art, the real solution research and development progress for being used for 3D facial masks It is very slow, the present invention is intended to provide a kind of preparation method and applications of 3D facial masks solution
What above-mentioned technique effect of the present invention was obtained by following technical proposals:
A kind of 3D facial masks solution, it is prepared by following raw material:40-50 parts of Verbena officinalis plant essence liquid, shitosan 0.01-3 parts, honey 2-6 parts, water-soluble lanolin 4-6 parts, green tea extractive liquor 10-20 parts, ginsenoside 3-5 parts, glycine 3- 5 parts, vitamin E 1-3 parts, polyvinyl alcohol 2-4 parts.
The preparation method of wherein described Verbena officinalis plant essence liquid is:After Verbena officinalis clean dry, 6-8 times of horsewhip is used The ethanol water soak extraction of herbaceous stem amount 70%, Extracting temperature obtains an extract solution for 2-3 hours for 60~80 DEG C of extractions, to filter 4-6 times of 80% ethanol water of volume is added to extract in slag 1-2 hours, Extracting temperature is 50~60 DEG C, is filtrated to get secondary Filtrate, merging filtrate and to adding the papain of enzyme activity >=600,000 units to stand 8-10 hours in filtrate, addition is The 0.2-0.5% of filtrate volume, you can obtain Verbena officinalis plant essence liquid.
The preparation method of green tea extractive liquor is:Green tea 20-30 parts, rose 3-5 parts is taken, after centella 4-6 parts is cleaned and dry The purified water soak extraction of 6-8 times of volume of its quality is added, controls Extracting temperature to be obtained within 0.5-1.5 hours for 50~60 DEG C of extractions Extract solution, to adding the 4-6 times of purified water of volume to extract in filter residue 1-2 hours, Extracting temperature is 50~60 DEG C, is filtered To secondary filtrate, merging filtrate is that can obtain green tea extractive liquor.
Applicant has been carried out further preferably always according to the cosmetic result of the 3D facial mask solution for preparing to its prescription, its Described in 3D facial masks solution prepared by following raw material:45 parts of Verbena officinalis plant essence liquid, 1.2 parts of shitosan, honey 4 Part, 5 parts of water-soluble lanolin, 15 parts of green tea extractive liquor, 4 parts of ginsenoside, 4 parts of glycine, 2 parts of vitamin E, polyvinyl alcohol 3 Part.More preferably, the affinity with skin is more excellent, and substantially anti-without allergy for the whitening effect of the facial mask solution obtained by the formula Should.
Present invention also offers a kind of preparation method of above-mentioned 3D facial masks solution, it specifically includes following steps:
1) Verbena officinalis plant essence liquid and green tea extractive liquor are prepared according to above-mentioned technique;
2) after mixing Verbena officinalis plant essence liquid and green tea extractive liquor in proportion, add thereto after being heated to 60-70 DEG C Enter shitosan, water-soluble lanolin and polyvinyl alcohol, temperature is cooled to less than 40 DEG C after filtering while hot, be added thereto to honeybee Honey, glycine, vitamin E and ginsenoside, obtain final product.
The present invention is also claimed the 3D facial masks prepared by above-mentioned facial mask solution.The preparation side of described 3D facial masks Method, it is characterised in that scan user's skin of face first, obtains skin condition and surface image, then according to surface image Three-dimensional mold is set up, facial mask solution is printed to three-dimensional mold according to skin condition, 3D facial masks are obtained final product.
3D facial masks solution of the present invention and its 3D facial masks for preparing, compared with prior art with following technology Effect:
1st, had using keratoderma water content after the 3D facial masks described in embodiment of the present invention 1-5 and significantly risen, made More long with the time, improvement is more obvious, and the improvement of the particularly facial mask corresponding to embodiment 2 is optimal.Comparative example 1- pairs Ratio 5 also has a certain upgrade effect to keratoderma water content, but its improvement is nothing like embodiment of the present invention 1- 5, component has significant collaboration in terms of keratoderma water content is improved during this shows 3D facial masks solution of the present invention Effect.
2nd, under being had significantly using the 3D facial mask percutaneous water losses of rear face skin described in embodiment of the present invention 1-5 Drop, use time is more long, and improvement is more obvious, and the improvement of the particularly facial mask corresponding to embodiment 2 is optimal.Comparative example 1- comparative examples 5 also have a certain upgrade effect to keratoderma water content, but its improvement is nothing like implementation of the present invention Example 1-5, component is reducing the percutaneous water loss of skin of face with significant during this shows 3D facial masks solution of the present invention Synergy.
3rd, facial mask solution anaphylaxis of the present invention is low, and to skin without any stimulation, its formula is simple, and very It is adapted to make 3D facial masks, with good application prospect.
Specific embodiment
The present invention is further described below by way of specific embodiment, but it limits patent of the invention never in any form Protection domain.
Embodiment 1
A kind of 3D facial masks solution, it is prepared by following raw material:40 parts of Verbena officinalis plant essence liquid, shitosan 0.01 Part, 2 parts of honey, 4 parts of water-soluble lanolin, 10 parts of green tea extractive liquor, 3 parts of ginsenoside, 3 parts of glycine, 1 part of vitamin E, 2 parts of polyvinyl alcohol.
Preparation technology:
1) preparation method of Verbena officinalis plant essence liquid is:After Verbena officinalis clean dry, 6 times of Verbena officinalis quality 70% are used Ethanol water soak extraction, Extracting temperature obtains an extract solution for 2 hours for 60 DEG C of extractions, to 4 times of volumes of addition in filter residue 80% ethanol water extract 1 hour, Extracting temperature is 50 DEG C, is filtrated to get secondary filtrate, merging filtrate and in filtrate The papain of enzyme activity >=600,000 units is added to stand 8-10 hours, addition is the 0.2% of filtrate volume, you can obtained Verbena officinalis plant essence liquid.
2) preparation method of green tea extractive liquor is:20 parts of green tea, 3 parts of rose are taken, 4 parts of centella is cleaned after drying and adds it The purified water soak extraction of 6 times of volumes of quality, controls Extracting temperature to obtain within 0.5 hour an extract solution for 50 DEG C of extractions, to filter 4 times of purified waters of volume are added to extract in slag 1 hour, Extracting temperature is 50 DEG C, is filtrated to get secondary filtrate, merging filtrate Obtain green tea extractive liquor.
3) after mixing Verbena officinalis plant essence liquid and green tea extractive liquor in proportion, shell is added thereto to after being heated to 60 DEG C Glycan, water-soluble lanolin and polyvinyl alcohol, less than 40 DEG C are cooled to after filtering while hot by temperature, be added thereto to honey, Glycine, vitamin E and ginsenoside, obtain final product.
Embodiment 2
A kind of 3D facial masks solution, it is prepared by following raw material:45 parts of Verbena officinalis plant essence liquid, shitosan 1.2 Part, 4 parts of honey, 5 parts of water-soluble lanolin, 15 parts of green tea extractive liquor, 4 parts of ginsenoside, 4 parts of glycine, 2 parts of vitamin E, 3 parts of polyvinyl alcohol.
Preparation technology:
1) preparation method of Verbena officinalis plant essence liquid is:After Verbena officinalis clean dry, 7 times of Verbena officinalis quality 70% are used Ethanol water soak extraction, Extracting temperature obtains an extract solution for 2.5 hours for 70 DEG C of extractions, to 5 times of bodies of addition in filter residue Long-pending 80% ethanol water is extracted 1.5 hours, and Extracting temperature is 55 DEG C, is filtrated to get secondary filtrate, merging filtrate and to filter The papain of enzyme activity >=600,000 units is added to stand 9 hours in liquid, addition is the 0.4% of filtrate volume, you can To Verbena officinalis plant essence liquid.
2) preparation method of green tea extractive liquor is:25 parts of green tea, 4 parts of rose are taken, 5 parts of centella is cleaned after drying and adds it The purified water soak extraction of 7 times of volumes of quality, controls Extracting temperature to obtain within 1 hour an extract solution for 55 DEG C of extractions, to filter residue Middle to add 5 times of purified waters of volume to extract 1.5 hours, Extracting temperature is 55 DEG C, is filtrated to get secondary filtrate, merging filtrate Obtain green tea extractive liquor.
3) after mixing Verbena officinalis plant essence liquid and green tea extractive liquor in proportion, shell is added thereto to after being heated to 65 DEG C Glycan, water-soluble lanolin and polyvinyl alcohol, less than 40 DEG C are cooled to after filtering while hot by temperature, be added thereto to honey, Glycine, vitamin E and ginsenoside, obtain final product.
Embodiment 3
A kind of 3D facial masks solution, it is prepared by following raw material:50 parts of Verbena officinalis plant essence liquid, 1 part of shitosan, 6 parts of honey, 6 parts of water-soluble lanolin, 20 parts of green tea extractive liquor, 5 parts of ginsenoside, 5 parts of glycine, 3 parts of vitamin E, poly- second 4 parts of enol.
Preparation technology:
1) preparation method of Verbena officinalis plant essence liquid is:After Verbena officinalis clean dry, 8 times of Verbena officinalis quality 70% are used Ethanol water soak extraction, Extracting temperature obtains an extract solution for 3 hours for 80 DEG C of extractions, to 6 times of volumes of addition in filter residue 80% ethanol water extract 2 hours, Extracting temperature is 60 DEG C, is filtrated to get secondary filtrate, merging filtrate and in filtrate The papain of enzyme activity >=600,000 units is added to stand 10 hours, addition is the 0.5% of filtrate volume, you can obtain horse Whip grass plant essence liquid.
2) preparation method of green tea extractive liquor is:30 parts of green tea, 5 parts of rose are taken, 6 parts of centella is cleaned after drying and adds it The purified water soak extraction of 8 times of volumes of quality, controls Extracting temperature to obtain within 1.5 hours an extract solution for 60 DEG C of extractions, to filter 6 times of purified waters of volume are added to extract in slag 2 hours, Extracting temperature is 60 DEG C, is filtrated to get secondary filtrate, merging filtrate Obtain green tea extractive liquor.
3) after mixing Verbena officinalis plant essence liquid and green tea extractive liquor in proportion, shell is added thereto to after being heated to 70 DEG C Glycan, water-soluble lanolin and polyvinyl alcohol, less than 40 DEG C are cooled to after filtering while hot by temperature, be added thereto to honey, Glycine, vitamin E and ginsenoside, obtain final product.
Embodiment 4
A kind of 3D facial masks solution, it is prepared by following raw material:40 parts of Verbena officinalis plant essence liquid, 2 parts of shitosan, 5 parts of honey, 6 parts of water-soluble lanolin, 10 parts of green tea extractive liquor, 5 parts of ginsenoside, 3 parts of glycine, 3 parts of vitamin E, poly- second 2 parts of enol.
Preparation technology is with embodiment 1.
Embodiment 5
A kind of 3D facial masks solution, it is prepared by following raw material:50 parts of Verbena officinalis plant essence liquid, shitosan 2.5 Part, 3 parts of honey, 4 parts of water-soluble lanolin, 20 parts of green tea extractive liquor, 3 parts of ginsenoside, 5 parts of glycine, 1 part of vitamin E, 4 parts of polyvinyl alcohol.
Preparation technology is with embodiment 2.
Comparative example 1:
In addition in facial mask solution without Verbena officinalis plant essence liquid, other prescriptions and preparation technology are with embodiment 2.
Comparative example 2:
In addition in facial mask solution without green tea extractive liquor, other prescriptions and preparation technology are with embodiment 2.
Comparative example 3:
In addition in facial mask solution without ginsenoside, other prescriptions and preparation technology are with embodiment 2.
Comparative example 4:
Except not in addition to chitosan-containing, other prescriptions and preparation technology are with embodiment 2 in facial mask solution.
Comparative example 5
In facial mask solution Verbena officinalis plant essence liquid without papain outside, other prescriptions and the same embodiment of preparation technology 2。
The efficacy assessments of the 3D facial masks prepared by the facial mask solution of the present invention of embodiment 6
Subject is chosen using obtaining 3D facial masks, every group of subject's morning prepared by above-described embodiment 1-5 and comparative example 1-5 It is late each using once, determining using the keratoderma water content in facial mask 6 weeks and the percutaneous water loss of skin of face, determine Method is as follows:1. keratoderma moisture measurement (moisture content of skin):Left and right cheek position angle is measured using moisture tester Matter layer water content, measurement is averaged for 4 times;2. the percutaneous water loss of skin of face (TEWL values) measurement:Use moisture of skin stream Commit a breach of etiquette, the measurement left and right percutaneous water loss of face, measurement is averaged for 2 times;Measurement result is as shown in the table.
The keratoderma water content efficacy assessments of the 3D facial masks prepared by the facial mask solution of the present invention of table 1
0 week (A.U) 2 weeks (A.U) 4 weeks (A.U) 6 weeks (A.U)
Embodiment 1 49.4±1.6 54.6±1.7 61.2±1.6 74.6±1.8
Embodiment 2 49.2±1.3 56.4±1.9 62.8±1.9 75.4±1.9
Embodiment 3 49.3±1.6 54.3±1.8 59.8±1.8 70.8±2.2
Embodiment 4 49.7±1.5 54.5±1.6 58.6±2.1 71.6±1.5
Embodiment 5 48.9±1.4 55.1±2.1 59.4±1.6 72.5±1.9
Comparative example 1 49.1±1.2 51.2±2.2 52.3±2.2 54.6±1.5
Comparative example 2 49.0±1.4 50.6±1.6 56.1±1.7 57.4±1.5
Comparative example 3 49.5±1.1 51.3±1.5 53.5±1.5 54.4±1.4
Comparative example 4 49.2±1.5 49.8±1.7 52.9±1.5 55.4±1.7
Comparative example 5 49.4±1.5 51.2±1.6 53.4±1.4 54.6±1.5
As can be seen from Table 1, had significantly using keratoderma water content after the 3D facial masks described in embodiment of the present invention 1-5 The rising of degree, use time is more long, and improvement is more obvious, and the improvement of the particularly facial mask corresponding to embodiment 2 is optimal. Comparative example 1- comparative examples 5 also have a certain upgrade effect to keratoderma water content, but its improvement is nothing like this hair Bright embodiment 1-5, component has in terms of keratoderma water content is improved during this shows 3D facial masks solution of the present invention Significant synergy.
The percutaneous water loss measurement of skin of face of the facial mask solution of the present invention of table 2
As can be seen from Table 2, had using the 3D facial mask percutaneous water losses of rear face skin described in embodiment of the present invention 1-5 Significantly decline, use time is more long, improvement is more obvious, particularly the improvement of the facial mask corresponding to embodiment 2 Most preferably.Comparative example 1- comparative examples 5 also have a certain upgrade effect to keratoderma water content, but its improvement is nothing like Embodiment of the present invention 1-5, component is reducing the percutaneous water loss of skin of face during this shows 3D facial masks solution of the present invention With significant synergy.

Claims (3)

1. a kind of 3D facial masks solution, it is prepared by following raw material:Verbena officinalis plant essence liquid 40-50 weight portions, shell gathers Sugared 0.01-3 weight portions, honey 2-6 weight portions, water-soluble lanolin 4-6 weight portions, green tea extractive liquor 10-20 weight portions, ginseng Saponin(e 3-5 weight portions, glycine 3-5 weight portions, the weight portion of vitamin e1-3, polyvinyl alcohol 2-4 weight portions;
The preparation method of described Verbena officinalis plant essence liquid is:After Verbena officinalis clean dry, 6-8 times of Verbena officinalis quality is used 70% ethanol water soak extraction, Extracting temperature obtains an extract solution for 2-3 hours for 60~80 DEG C of extractions, adds in filter residue Enter 4-6 times of 80% ethanol water of volume to extract 1-2 hours, Extracting temperature is 50~60 DEG C, is filtrated to get secondary filtrate, is closed And filtrate and in filtrate add enzyme activity >=600,000 units papain stand 8-10 hours, addition is filtrate volume 0.2-0.5%, you can obtain Verbena officinalis plant essence liquid;
The preparation method of described green tea extractive liquor is:Take green tea 20-30 weight portions, rose 3-5 weight portions, centella 4-6 weights Amount part cleans the purified water soak extraction that 6-8 times of volume of its quality is added after drying, and it is 50~60 DEG C of extractions to control Extracting temperature An extract solution is obtained within 0.5-1.5 hours, to adding the 4-6 times of purified water of volume to extract in filter residue 1-2 hours, Extracting temperature is 50~60 DEG C, secondary filtrate is filtrated to get, merging filtrate is that can obtain green tea extractive liquor;
The preparation method of the 3D facial masks solution specifically includes following steps:
1) Verbena officinalis plant essence liquid and green tea extractive liquor are prepared respectively;
2) after mixing Verbena officinalis plant essence liquid and green tea extractive liquor in proportion, shell is added thereto to after being heated to 60-70 DEG C Glycan, water-soluble lanolin and polyvinyl alcohol, less than 40 DEG C are cooled to after filtering while hot by temperature, be added thereto to honey, Glycine, vitamin E and ginsenoside, obtain final product.
2. 3D facial masks solution according to claim 1, it is characterised in that described 3D facial masks solution is by following raw material system It is standby to obtain:The weight portion of Verbena officinalis plant essence liquid 45, the weight portion of shitosan 1.2, the weight portion of honey 4, the weight of water-soluble lanolin 5 Part, the weight portion of green tea extractive liquor 15, the weight portion of ginsenoside 4, the weight portion of glycine 4, vitamin E2 weight portion, polyvinyl alcohol 3 Weight portion.
3. the 3D facial masks that a kind of facial mask solution as described in claim 1 is prepared.
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Publication number Priority date Publication date Assignee Title
CN101336876A (en) * 2008-06-06 2009-01-07 庄建玲 Skin care product with moisture-keeping function
CN102885747A (en) * 2011-07-22 2013-01-23 方樱翰 Black bean powder ageing-resistant facial mask
CN104721061A (en) * 2015-02-10 2015-06-24 广州赛莱拉干细胞科技股份有限公司 Method for manufacturing 3D facial mask and 3D facial mask manufactured through method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101336876A (en) * 2008-06-06 2009-01-07 庄建玲 Skin care product with moisture-keeping function
CN102885747A (en) * 2011-07-22 2013-01-23 方樱翰 Black bean powder ageing-resistant facial mask
CN104721061A (en) * 2015-02-10 2015-06-24 广州赛莱拉干细胞科技股份有限公司 Method for manufacturing 3D facial mask and 3D facial mask manufactured through method

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