CN105954138A - Pole plate porosity measurement method - Google Patents

Pole plate porosity measurement method Download PDF

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Publication number
CN105954138A
CN105954138A CN201610272279.8A CN201610272279A CN105954138A CN 105954138 A CN105954138 A CN 105954138A CN 201610272279 A CN201610272279 A CN 201610272279A CN 105954138 A CN105954138 A CN 105954138A
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CN
China
Prior art keywords
pole plate
volume
water
measuring method
grid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610272279.8A
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Chinese (zh)
Inventor
杨云珍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chaowei Power Supply Co Ltd
Original Assignee
Chaowei Power Supply Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chaowei Power Supply Co Ltd filed Critical Chaowei Power Supply Co Ltd
Priority to CN201610272279.8A priority Critical patent/CN105954138A/en
Publication of CN105954138A publication Critical patent/CN105954138A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/02Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content

Abstract

The present invention relates to a pole plate porosity measurement method. The method comprises the steps of weighing a pole plate with active materials attached thereon as M1, measuring the volume of the pole plate as V1, weighing the pole plate as M2 after the pole plate is soaked for a period of time, calculating the volume of the active materials after absorbing water (wherein rho represents the water density), removing the wet active materials on the pole plate from the plate grid of the pole plate, measuring the volume of the plate grid as V3, and calculating. Based on the above method, the porosity of the pole plate can be accurately measured.

Description

A kind of pole plate porosity measuring method
Technical field
The present invention relates to a kind of pole plate porosity measuring method.
Background technology
The powder porous electrode that polar plate of lead acid storage battery active substance is made up of Hydrocerussitum (Ceruse), the porosity of porous electrode directly affects the performances such as the capacity of lead-acid accumulator, life-span.At present in lead-acid accumulator manufacture process, production is control paste density and water content finally to carry out the porosity of plate active material.It is very important that the porosity of the pole plate of final molding measures.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides a kind of pole plate porosity measuring method, comprise the following steps, to weigh to obtain weight M1 with the pole plate of active substance, measure described pole plate volume V1, weight M2 weighed after described pole plate is soaked a period of time, calculated activity material sucks the volume of water(p is the density of water), removes wet plate active material from the grid of pole plate, measures grid volume V3, calculates
Further, measuring described pole plate volume V1 is to put into aqueous solution storage vessel by pole plate, aqueous solution storage vessel communicates with graduated cylinder, graduated cylinder is identical with aqueous solution storage vessel liquid level, in graduated cylinder be connected a level sensing line on electronic balance display, when soaking during water put into by pole plate, in graduated cylinder, liquid level can rise, display body product V1 in electronic display 2.
Further, measuring grid volume V3 is to be removed by wet plate active material, processes the grid obtaining being dried, and puts into aqueous solution storage vessel, and graduated cylinder liquid level rises, and electronic display obtains volume number V3.
Further, when calculated activity material sucks the volume V2 of water, also include the step of temperature by thermometer measure water.
Further, described pole plate soaks a period of time is 2-3 hour.
By the method for the present invention, can accurate measuring pad porosity.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described.
The present invention relates to a kind of method measuring polar plate of lead acid storage battery porosity, comprise the following steps, first by with the pole plate of active substance scales/electronic balance weighing record, electronic display can directly display weight M1 dry weight.Aqueous solution storage vessel connects one has the graduated cylinder of exact scale to communicate, graduated cylinder is identical with aqueous solution storage vessel liquid level, in graduated cylinder be connected a level sensing line on electronic balance display, when soaking during water put into by pole plate, in graduated cylinder, liquid level can rise, can directly display volume milliliter number V1 in electronic display 2, this V1 is exactly the volume ml of pole plate.Pole plate will be weighed up and continue to put into immersion 2~4 hours in aqueous solution storage vessel, make the water suction of plate active material maximum saturation, after when pole plate immersion 2~4 is little, pole plate is carried unnecessary water has been drained, it is placed directly in hook upper 5 to weigh reading M2 weight in wet base, being connected displays temperature reading with electronic display with chronothermometer, water density at different temperatures is different, obtains density p water.So plate active material sucks the volume of waterBeing removed by wet plate active material, process the grid obtaining being dried, put into aqueous solution storage vessel, graduated cylinder liquid level rises, and electronic display obtains volume number V3, calculates
In present invention experiment, involved mass unit is a gram g, volume unit milliliter ml, density unit g/ml.The present invention uses Plethysmometry to measure pole plate porosity, easy can quickly measure pole plate porosity.

Claims (5)

1. a pole plate porosity measuring method, comprises the following steps, and is claimed by the pole plate with active substance Recuperation weight M1, measures described pole plate volume V1, weighs after described pole plate is soaked a period of time Weight M2, calculated activity material suck water volume(p is the density of water), Wet plate active material is removed from the grid of pole plate, measures grid volume V3, calculate pole
2. pole plate porosity measuring method as claimed in claim 1, it is characterised in that measure described Pole plate volume V1 is to put into aqueous solution storage vessel, aqueous solution storage vessel and amount by pole plate Cylinder communicates, and graduated cylinder is identical with aqueous solution storage vessel liquid level, with electronic balance display in graduated cylinder Piece level sensing line of upper connection, when soaking during water put into by pole plate, in graduated cylinder, liquid level can rise, Display body product V1 in electronic display 2.
3. pole plate porosity measuring method as claimed in claim 2, it is characterised in that measure grid Volume V3 is to be removed by wet plate active material, processes the grid obtaining being dried, puts into water-soluble Liquid storage vessel, graduated cylinder liquid level rises, electronic display obtains volume number V3.
4. the pole plate porosity measuring method as described in claim 1-3 any one, it is characterised in that When calculated activity material sucks the volume V2 of water, also include the temperature by thermometer measure water Step.
5. the pole plate porosity measuring method as described in claim 1-3 any one, it is characterised in that It is 2-3 hour that described pole plate soaks a period of time.
CN201610272279.8A 2016-04-27 2016-04-27 Pole plate porosity measurement method Pending CN105954138A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610272279.8A CN105954138A (en) 2016-04-27 2016-04-27 Pole plate porosity measurement method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610272279.8A CN105954138A (en) 2016-04-27 2016-04-27 Pole plate porosity measurement method

Publications (1)

Publication Number Publication Date
CN105954138A true CN105954138A (en) 2016-09-21

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610272279.8A Pending CN105954138A (en) 2016-04-27 2016-04-27 Pole plate porosity measurement method

Country Status (1)

Country Link
CN (1) CN105954138A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111413261A (en) * 2020-04-01 2020-07-14 浙江天能电池(江苏)有限公司 Method for detecting porosity of active substance of polar plate
CN113433024A (en) * 2021-06-01 2021-09-24 风帆有限责任公司 Method for detecting porosity of negative plate after formation of start-stop AGM battery
CN113758824A (en) * 2021-08-04 2021-12-07 超威电源集团有限公司 Method for testing porosity of green plate

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2504082B2 (en) * 1987-11-27 1996-06-05 新神戸電機株式会社 Manufacturing method of electrode plate for lead-acid battery
CN101420018A (en) * 2007-10-26 2009-04-29 比亚迪股份有限公司 Lithium ionic secondary cell barrier and preparation thereof
CN102646811A (en) * 2004-02-07 2012-08-22 株式会社Lg化学 Organic/inorganic composite porous layer-coated electrode and electrochemical device comprising the same
CN204115806U (en) * 2014-10-16 2015-01-21 风帆股份有限公司 The saturated wet pole plate volume measurement device of a kind of lead-acid accumulator
CN105241799A (en) * 2015-09-25 2016-01-13 超威电源有限公司 Polar plate porosity detection apparatus and polar plate porosity detection method
CN105322142A (en) * 2015-09-26 2016-02-10 河南新太行电源有限公司 Manufacturing method of positive plate of fiber-type cadmium-nickel storage battery

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2504082B2 (en) * 1987-11-27 1996-06-05 新神戸電機株式会社 Manufacturing method of electrode plate for lead-acid battery
CN102646811A (en) * 2004-02-07 2012-08-22 株式会社Lg化学 Organic/inorganic composite porous layer-coated electrode and electrochemical device comprising the same
CN101420018A (en) * 2007-10-26 2009-04-29 比亚迪股份有限公司 Lithium ionic secondary cell barrier and preparation thereof
CN204115806U (en) * 2014-10-16 2015-01-21 风帆股份有限公司 The saturated wet pole plate volume measurement device of a kind of lead-acid accumulator
CN105241799A (en) * 2015-09-25 2016-01-13 超威电源有限公司 Polar plate porosity detection apparatus and polar plate porosity detection method
CN105322142A (en) * 2015-09-26 2016-02-10 河南新太行电源有限公司 Manufacturing method of positive plate of fiber-type cadmium-nickel storage battery

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
R.E.科林斯: "《流体通过多孔材料的流动》", 31 August 1984, 石油工业出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111413261A (en) * 2020-04-01 2020-07-14 浙江天能电池(江苏)有限公司 Method for detecting porosity of active substance of polar plate
CN113433024A (en) * 2021-06-01 2021-09-24 风帆有限责任公司 Method for detecting porosity of negative plate after formation of start-stop AGM battery
CN113433024B (en) * 2021-06-01 2022-08-23 风帆有限责任公司 Method for detecting porosity of negative plate after formation of start-stop AGM battery
CN113758824A (en) * 2021-08-04 2021-12-07 超威电源集团有限公司 Method for testing porosity of green plate

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Application publication date: 20160921