CN105925177A - Water-based organic and inorganic hybrid high-temperature-resistant paint and preparing method thereof - Google Patents
Water-based organic and inorganic hybrid high-temperature-resistant paint and preparing method thereof Download PDFInfo
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- CN105925177A CN105925177A CN201610315853.3A CN201610315853A CN105925177A CN 105925177 A CN105925177 A CN 105925177A CN 201610315853 A CN201610315853 A CN 201610315853A CN 105925177 A CN105925177 A CN 105925177A
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- temperature resistant
- film forming
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
- C09D5/103—Anti-corrosive paints containing metal dust containing Al
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
- C09D5/106—Anti-corrosive paints containing metal dust containing Zn
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses water-based organic and inorganic hybrid high-temperature-resistant paint. The paint is prepared from, by mass, 40-45% of main film forming matter, 10-13% of auxiliary film forming matter, 1-2% of high-temperature-resisting corrosion inhibitor, 2-5% of low-melting-point glass dust, 3-5% of anticorrosion filler, 1-3% of sodium silicate, 20-25% of water and 10-13% of ethyl alcohol. Raw material source is extensive, preparing process is simple, production and use are safe and free of pollution, and the paint is novel environment-friendly paint. Tests prove that the paint has high temperature resistance and corrosion resistance, and the defect of poor temperature resistance of existing water-based paint is effectively overcome. The invention further discloses preparing and using methods of the water-based organic and inorganic hybrid high-temperature-resistant paint.
Description
Technical field
The invention belongs to chemical industry fire-resistant anticorrosion paint technical field, be specifically related to a kind of aqueous organic inorganic hybridization high-temperature resistant coating
And preparation method thereof.
Background technology
Along with economic fast development, global environment occurs in that unprecedented crisis, deteriorates to control the continuation of global environment,
Corresponding laws and regulations have all been formulated to limit the discharge of harmful substance in countries in the world.The appearance of these restricted laws and regulations and reality
Execute, be a deathblow for traditional solvent-borne coatings industry.Therefore the succedaneum finding traditional solvent-borne coating is carved not
Rong Huan.Water paint is one as the coating with water as dispersant and replaces the best selection of solvent based coating, but aqueous at present
High temperature resistant, the antiseptic property of coating also have no small difference with traditional solvent-borne coating, and the correlated performance improving water paint is to send out
The emphasis direction of exhibition.In numerous water paints, water based silicone coating obtains the great attention of numerous scholar and businessman.
Due to the development of World Economics, more severe to the use environment of metal material, the ring of some high temperature height corrosion
In border, metal damage is serious, causes huge economic loss.Severe just because of metal material Service Environment, protects it
Coating it is also proposed higher requirement, and under high temperature height etch state, the aqueous coating of long service is few, general heat-resisting painting
Layer is extremely difficult to the high temperature of 400 DEG C.Although the most universal high-temperature resistant coating has certain heat resistance, but its
Corrosion Protection is very poor, often loses its resistance to elevated temperatures, lose more than gain while improving corrosion resistance.So raising water
Property coating high temperature resistant, corrosion resistance be that current technical field of coatings is badly in need of the emphasis paid close attention to and the difficult problem captured.
Summary of the invention:
The invention aims to solve problem and the defect that prior art exists, it is provided that a kind of resistance to height of aqueous organic inorganic hybridization
Thermo-paint and preparation method thereof.
The technical staff being engaged in coating research and development and preparation both knows about, though aqueous organic coating has good adhesive force, chemically-resistant medicine
Moral character, acidproof, alkali resistance, but it is difficult to the high temperature of resistance to more than 400 DEG C.And though aqueous inorganic coating has good thermostability,
High temperature resistant up to more than 800 DEG C, but its bad mechanical property, poor adhesive force, it is difficult in metal surface film forming alone.And aqueous
Polysiloxane coating materials has good resistance to elevated temperatures, if coordinating glass powder with low melting point that the temperature tolerance of its coating can be made to carry further
High；If coordinate traditional anticorrosive packing just the most durothermic can have good anticorrosion ability having again simultaneously.
Based on the above, the present invention is to be combined with the Common advantages of organic coating and inorganic coating, by the side of organic inorganic hybridization
Method, can obtain the highest crosslink density by organic crosslinking film forming, effectively completely cut off the contact of corrosive medium and base material,
And coordinating anticorrosive packing and Zn powder and Al powder so that coating can have preferable Corrosion Protection.Aqueous organic coating adds
Enter glass powder with low melting point, make coating have the most high temperature resistant, decay resistance.
The present invention efficiently solves the defect of water paint non-refractory, makes the heatproof of water paint reach more than 700 DEG C, simultaneously
Anticorrosive packing is added so that it is Corrosion Protection is the most well improved by using.
For reaching above-mentioned target, the technical solution used in the present invention is:
A kind of aqueous organic inorganic hybridization high-temperature resistant coating, by mass percentage by component: main film forming substance be 40～45%, auxiliary
Furtherance membrane substance be 10～13%, high temperature resistant corrosion inhibitor is 1～2%, glass powder with low melting point 2～5%, anticorrosive packing be 3～5%, silicon
Acid sodium be 1～3%, water be 20～25%, ethanol be 10～13% composition.
Wherein said main film forming substance is the mixture of diacrylate and MTMS, and its mixing quality ratio is
Diacrylate: MTMS=1:1.5, its structural formula is:
CH3-Si(OR)3
Wherein, L is alkyl, C1～C10, R is methyl；
Described auxiliary film forming matter is titanate esters, 2-(Acryloyloxy)ethanol and the mixture to hexichol trimethoxy silane, and it mixes
Conjunction mass ratio is titanate esters: 2-(Acryloyloxy)ethanol: to hexichol trimethoxy silane=1:2:2, and its structure of matter formula is:
Ti(OR)4
Wherein, R is methyl.
Described glass powder with low melting point is by mass percentage by Al2O3Content is 5%, and ZnO content is 27%, B2O3Content
It is 30%, P2O5Content is 19%, and BaO content is 5%, and CaO content is 7%, and SrO content is 2%, and content of MgO is
5% composition.
The structural formula of described high temperature resistant corrosion inhibitor is:
Wherein, R is methyl.
Described anticorrosive packing is the mixture of zinc powder and aluminium powder, and its mixing quality is than for zinc powder: aluminium powder=1:1.
The preparation method of a kind of aqueous organic inorganic hybridization high-temperature resistant coating, comprises the steps:
1, according to mass percent by the main film forming substance in proportioning component, glass powder with low melting point, high temperature resistant corrosion inhibitor, silicic acid
Sodium, anticorrosive packing, water and the mixing of 1/2 ethanol, stirring, obtain component A slip, and room temperature is placed；
2, according to mass percent by the auxiliary film forming matter in proportioning component and remaining 1/2 ethanol, mixing, stirring is all
Even, obtain B component homogenate, room temperature stands, and seals and preserves.
The using method of a kind of aqueous organic inorganic hybridization high-temperature resistant coating, comprises the concrete steps that:
The B component that component A step (1) in above-mentioned preparation method obtained and step (2) obtain mixes, stirring
Uniformly, then brush, again at 130 DEG C of maintenance 1h after solidification 1h at 30 DEG C.
Compared with prior art, have the feature that and beneficial effect are mainly the present invention:
1, use the method for organic inorganic hybridization to prepare water paint, by adding appropriate exotic material, significantly improve water
The resistance to elevated temperatures of property coating, after testing, coating heatproof reaches more than 700 DEG C.
2, by using interpolation anticorrosive packing, i.e. it is aided with zinc powder and aluminium powder, significantly improves the Corrosion Protection of coating.
3, raw material sources are extensive, and preparation technology is simple, produces and uses process safety pollution-free, are a kind of novel environment friendly coating.
Detailed description of the invention:
Below in conjunction with specific embodiment, the present invention is expanded on further.Should be understood that these embodiments are merely to illustrate rather than limit
The scope of the present invention processed.In addition, it is to be understood that after having read the content that the present invention lectures, those skilled in the art can be to this
Invention makes various changes or modifications, and these equivalent form of values fall within the application depended on claims limited range equally.
Embodiment 1
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application
1, according to mass percent by the main film forming substance in proportioning component, high temperature resistant filler, high temperature resistant corrosion inhibitor, catalyst,
Anticorrosive packing, water, 1/2 ethanol mixing, stirring, obtain component A slip, room temperature is placed.
2, according to mass percent by the auxiliary film forming matter in proportioning component and remaining 1/2 ethanol mixing, stirring, B is obtained
Component is homogenized, and room temperature stands, and seals and preserves.
When 3, using, component A and B component are fully mixed, then application, at 30 DEG C, solidify 1h, then at 130 DEG C
Maintenance 1h.
Three, beneficial effect
The present embodiment gained coating is coated on cold-rolled steel sheet, and through experiment and detection, corrosion does not occurs in coating salt spray resistance experiment 300h
Focus, adhesive force 2 grades, coating heatproof reaches 350 DEG C.
Embodiment 2
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, corruption does not occurs in coating salt spray resistance experiment 350h
Erosion focus, adhesion 1 grade, coating heatproof reaches 400 DEG C.
Embodiment 3
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, corruption does not occurs in coating salt spray resistance experiment 400h
Erosion focus, adhesion 1 grade, coating heatproof is up to 450 DEG C.
Embodiment 4
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, corruption does not occurs in coating salt spray resistance experiment 450h
Erosion focus, adhesion 1 grade, coating heatproof is up to 460 DEG C.
Embodiment 5
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, corruption does not occurs in coating salt spray resistance experiment 500h
Erosion focus, adhesion 1 grade, coating heatproof is up to 480 DEG C.
Embodiment 6
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, corruption does not occurs in coating salt spray resistance experiment 500h
Erosion focus, adhesion 1 grade, coating heatproof is up to 700 DEG C.
Embodiment 7
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, the experiment of coating salt spray resistance does not goes out up to 480h
Now corroding focus, adhesion 1 grade, coating heatproof is up to 600 DEG C.
Embodiment 8
One, the formula of compositions
1, prepare main film forming substance, auxiliary film forming matter, glass powder with low melting point, high temperature resistant corrosion inhibitor the most respectively, prevent
The mixture of rotten pigment.
2, each constituent content of compositions formulated by mass percentage:
Two, preparation and application is with embodiment 1
Three, beneficial effect
The present embodiment resulting composition is coated on cold-rolled steel sheet, and through experiment and detection, the experiment of coating salt spray resistance does not goes out up to 480h
Now corroding focus, adhesion 1 grade, coating heatproof is up to 550 DEG C.
The above is only the preferred embodiment of the present invention, it should be pointed out that: to those of ordinary skill in the art,
Without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should be regarded as the present invention
Protection domain.
Claims (6)
1. an aqueous organic inorganic hybridization high-temperature resistant coating, it is characterised in that by mass percentage by component: main
Film forming matter be 40～45%, auxiliary film forming matter be 10～13%, high temperature resistant corrosion inhibitor be 1～2%, low-melting glass
Powder 2～5%, anticorrosive packing be 3～5%, sodium silicate be 1～3%, water be 20～25%, ethanol be 10～13% composition,
Wherein said main film forming substance is the mixture of diacrylate and MTMS, and its mixing quality ratio is
Diacrylate: MTMS=1:1.5, its structural formula is:
CH3-Si(OR)3
Wherein, L is alkyl, C1～C10, R is methyl；
Described auxiliary film forming matter is titanate esters, 2-(Acryloyloxy)ethanol and the mixture to hexichol trimethoxy silane,
Its mixing quality ratio is for titanate esters: 2-(Acryloyloxy)ethanol: to hexichol trimethoxy silane=1:2:2, its structure of matter formula
For:
Ti(OR)4
Wherein, R is methyl.
A kind of aqueous organic inorganic hybridization high-temperature resistant coating the most according to claim 1, it is characterised in that institute
The glass powder with low melting point stated is by mass percentage by Al2O3Content is 5%, and ZnO content is 27%, B2O3Content is
30%, P2O5Content is 19%, and BaO content is 5%, and CaO content is 7%, and SrO content is 2%, and MgO contains
Amount is 5% composition.
A kind of aqueous organic inorganic hybridization high-temperature resistant coating the most according to claim 1, it is characterised in that institute
The structural formula of the high temperature resistant corrosion inhibitor stated is:
Wherein, R is methyl.
A kind of aqueous organic inorganic hybridization high-temperature resistant coating the most according to claim 1, it is characterised in that described
The mixture that anticorrosive packing is zinc powder and aluminium powder, its mixing quality is than for zinc powder: aluminium powder=1:1.
5. the preparation side according to the aqueous organic inorganic hybridization high-temperature resistant coating described in any one of Claims 1-4
Method, it is characterised in that comprise the steps:
(1) according to mass percent by the main film forming substance in proportioning component, glass powder with low melting point, high temperature resistant inhibition
Agent, sodium silicate, anticorrosive packing, water and the mixing of 1/2 ethanol, stirring, obtain component A slip, and room temperature is placed；
(2) according to mass percent by the auxiliary film forming matter in proportioning component and remaining 1/2 ethanol, mix,
Stirring, obtain B component homogenate, room temperature stands, and seals and preserves.
6. the user according to the aqueous organic inorganic hybridization high-temperature resistant coating described in any one of Claims 1-4
Method, it is characterised in that comprise the concrete steps that: during use, the component A that claim 5 step (1) is obtained and step
(2) B component obtained mixes, and stirs, then application, again at 130 DEG C after solidification 1h at 30 DEG C
Maintenance 1h.
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Cited By (4)
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| CN107057420A (en) * | 2016-12-29 | 2017-08-18 | 广州凯耀资产管理有限公司 | Inorganic slim expansion fire-resistant coating for steel structure and preparation method thereof |
| CN110746849A (en) * | 2019-10-17 | 2020-02-04 | 江苏科技大学 | Hydrogen sulfide corrosion-resistant water-based coating composition and preparation method and application thereof |
| CN110819185A (en) * | 2019-10-24 | 2020-02-21 | 常州市武进新邦涂料有限公司 | XB-S-water-soluble high-reflection photovoltaic backboard glass paint and application scheme thereof |
| CN111793434A (en) * | 2020-07-01 | 2020-10-20 | 安徽新大陆特种涂料有限责任公司 | Preparation method of high-temperature-resistant ceramic anticorrosive heat-insulating coating |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110746849B (en) * | 2019-10-17 | 2021-08-10 | 江苏科技大学 | Hydrogen sulfide corrosion-resistant water-based coating composition and preparation method and application thereof |
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| CN111793434A (en) * | 2020-07-01 | 2020-10-20 | 安徽新大陆特种涂料有限责任公司 | Preparation method of high-temperature-resistant ceramic anticorrosive heat-insulating coating |
| CN111793434B (en) * | 2020-07-01 | 2021-09-07 | 安徽新大陆特种涂料有限责任公司 | Preparation method of high-temperature-resistant ceramic anticorrosive heat-insulating coating |
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| Publication number | Publication date |
|---|---|
| CN105925177B (en) | 2019-06-21 |
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Effective date of registration: 20191112 Address after: 201417, Shanghai chemical industry zone, Fengxian District, Chu Hua Road, No. 369 Patentee after: Peter Chemical (Shanghai) Co., Ltd. Address before: Meng Xi Road 212003 Zhenjiang city of Jiangsu province Jingkou District No. 2 Patentee before: Jiangsu University of Science and Technology |