CN105911222A - Metrological verification device for ammonia gas detector and metrological verification method thereof - Google Patents

Metrological verification device for ammonia gas detector and metrological verification method thereof Download PDF

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Publication number
CN105911222A
CN105911222A CN201610239318.4A CN201610239318A CN105911222A CN 105911222 A CN105911222 A CN 105911222A CN 201610239318 A CN201610239318 A CN 201610239318A CN 105911222 A CN105911222 A CN 105911222A
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CN
China
Prior art keywords
ammonia
concentration
calibrating device
ammonia detector
metering
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Pending
Application number
CN201610239318.4A
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Chinese (zh)
Inventor
孙健
李智平
王振
姜明
张贺
胡绪尧
朱亮
杨静怡
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China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
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China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
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Application filed by China Petroleum and Chemical Corp, Sinopec Qingdao Safety Engineering Institute filed Critical China Petroleum and Chemical Corp
Priority to CN201610239318.4A priority Critical patent/CN105911222A/en
Publication of CN105911222A publication Critical patent/CN105911222A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0006Calibrating gas analysers

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Combustion & Propulsion (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention relates to a metrological verification device for ammonia gas detector and a metrological verification method thereof. The verification device comprises a gas chamber for standard gas concentration to be measured. The gas chamber for standard gas concentration to be measured is respectively provided with a pure ammonia gas inlet, an ammonia gas inlet and a pure air inlet. The gas chamber for standard gas concentration to be measured is respectively connected to a flowmeter and a bypass flowmeter. The flowmeter is connected to an instrument for detection. The bypass flowmeter is connected to a vent nozzle. By the metrological verification device, various quantity-value transferring detection projects of an ammonia gas detector in the JJG1105-2015 'Ammonia Gas Detector' can be greatly completed.

Description

A kind of ammonia detector metering and calibrating device and measurement and examination method thereof
Technical field
The invention belongs to the measurement verification technical field of ammonia detector, be specifically related to a kind of ammonia Detector metering and calibrating device and measurement and examination method thereof.
Background technology
At present, ammonia detector is for detecting the electronic machine of ammonia concentration in environment.Have Can carry with, also have plenty of and be arranged on the fixed position being susceptible to ammonia leakage.Work as detection When in environment, the concentration of ammonia meets or exceeds preset alarming value, ammonia detector can send sound Light and vibrations alarm signal.It is widely used in all types of machine room of refrigerated warehouse, reality with the presence of ammonia Test room, ammonia is deposited warehouse etc. and is applied to the industrial site of ammonia, can effectively prevent poisoning, Explosion accident, ensures life, the safety of property.As a kind of measuring instrument, ammonia detector Never corresponding national verification code, also just never has the method for calibrating and sentences mark side Method.The transmission of quantity value of ammonia detector cannot be completed.All ammonia detector from producer The most just not having mechanism and method to go to evaluate whether after purchase can normally, works accurately.2015 In on April 30, in, State Administration for Quality Supervision and Inspection and Quarantine has issued JJG1105-2015 " ammonia Gas detector ", it is provided that every Testing index of ammonia detector and sentence mark method.To this end, Need a kind of ammonia detector metering and calibrating device so that it is can be good at Detection to the various transmission of quantity value of ammonia detector in JJG1105-2015 " ammonia detector " Project.
Summary of the invention
It is an object of the invention to provide a kind of ammonia detector metering and calibrating device so that it is can Well complete the various values to ammonia detector in JJG1105-2015 " ammonia detector " The detection project of transmission.
For achieving the above object, one aspect of the present invention provides a kind of ammonia detector measurement verification dress Put, including concentration Standard Gases air chamber to be measured, concentration Standard Gases air chamber to be measured is respectively equipped with ammonia Pure gas entrance, nitrogen inlet and pure air entrance, concentration Standard Gases air chamber to be measured respectively with stream Gauge is connected with bypass flow meter, and effusion meter is connected with standby test examination instrument, bypass flow meter with Drain is connected.
In above scheme preferably, ammonia pure gas entrance, nitrogen inlet and pure air enter Mouth is connected with first-class gauge, second gauge and the 3rd effusion meter respectively.
It may also be preferred that first-class gauge, second gauge and the 3rd effusion meter respectively with Concentration Standard Gases air chamber to be measured is connected.
It may also be preferred that ammonia detector metering and calibrating device also includes display part.
It may also be preferred that display part is arranged with liquid crystal display screen.
It may also be preferred that ammonia detector metering and calibrating device also includes Data Input Interface And data output interface.
It may also be preferred that ammonia detector metering and calibrating device also includes data processor.
Another aspect of the present invention provides the measurement verification of a kind of ammonia detector metering and calibrating device Method, uses the ammonia detector metering and calibrating device as above described in either a program, including following Three road air inlets of device are connected ammonia, nitrogen and pure air by step: the first step respectively, And have three effusion meters by connecting after three air inlets, three effusion meters be all connected to one to be measured Concentration Standard Gases air chamber, after the mixed air mixing of concentration Standard Gases air chamber to be measured, point two-way is the most defeated Going out to standby test examination instrument, another road is vented;Second step, is divided into liquid-crystal display section and includes two pieces Liquid crystal display screen, one piece is that the Standard Gases configuring respective concentration uses, and liquid crystal panel selects input ammonia The concentration of gas gas and the concentration of spirit, be simultaneously entered the Standard Gases concentration of the output of needs, be System, through automatically calculating the flow-rate ratio of ammonia and spirit, controls the pure gas of ammonia by numerical control Entrance and the first-class gauge of pure air entrance and the 3rd effusion meter, it is thus achieved that the concentration of needs Ammonia Standard Gases, another block liquid crystal display screen is used for recording and calculate the various data in verification process, And calculated feedback;3rd step, during the detection error of indication, the show value of the most standby test examination instrument Input second piece of screen, three display indicating values of typing same concentration so that system calculates automatically Go out the error of indication of this point, and it is the most qualified to be sentenced mark;4th step, the gas of three concentration After having led to, compare the size of three errors of indication, take maximum and compare with threshold value and then sentence Fixed qualified no;5th step, after inputting the concentration of six ventilations so that system is pressed according to repeatability Then determine that qualified no according to the computing formula result of calculation comparing with threshold value set;6th Step, carries stopwatch by system and sets response time parameter, start timing from ventilation, to stopping the supple of gas or steam Till, record duration of ventilation record, by calculate compare with threshold value then determine that qualified No.
In above scheme preferably, after the 6th step, by two pieces can touch liquid crystal display screen enters Row input and output, and data are printed by printer.
The ammonia detector metering and calibrating device of the present invention and measurement and examination method thereof, it can be very The good various values completed in JJG1105-2015 " ammonia detector " ammonia detector pass The detection project passed.
Accompanying drawing explanation
Fig. 1 is the structural representation of the ammonia detector metering and calibrating device of the present invention.
In figure, 1 is concentration Standard Gases air chamber to be measured, and 2 is ammonia pure gas entrance, and 3 is nitrogen Entrance, 4 is pure air entrance, and 5 is effusion meter, and 6 is bypass flow meter, and 7 is standby inspection instrument Device, 8 is drain.
Detailed description of the invention
In order to be more fully understood that the present invention, below in conjunction with specific embodiment, the present invention is made in detail Explanation.It is clear that the present invention can be carried out different modification and remodeling and without departing from rear attached power Profit requires the broader spirit and scope of the present invention limited.Therefore, following example have illustration Property and do not have conditional implication.
Embodiment:
A kind of ammonia detector metering and calibrating device, as it is shown in figure 1, include concentration standard to be measured Gas air chamber 1, concentration Standard Gases air chamber 1 to be measured is respectively equipped with ammonia pure gas entrance 2, nitrogen Entrance 3 and pure air entrance 4, concentration Standard Gases air chamber 1 to be measured respectively with effusion meter 5 and Bypass flow meter 6 is connected, and effusion meter 5 is connected with standby test examination instrument 7, bypass flow meter 6 It is connected with drain 8.
In the embodiment above, ammonia pure gas entrance 2, nitrogen inlet 3 and pure air entrance 4 are connected with first-class gauge, second gauge and the 3rd effusion meter respectively.
In the embodiment above, first-class gauge, second gauge and the 3rd effusion meter respectively with Concentration Standard Gases air chamber 1 to be measured is connected.
In the embodiment above, ammonia detector metering and calibrating device also includes display part.
In the embodiment above, display part is arranged with liquid crystal display screen.
In the embodiment above, ammonia detector metering and calibrating device also includes Data Input Interface And data output interface.
In the embodiment above, ammonia detector metering and calibrating device also includes data processor.
The ammonia detector metering and calibrating device of the present invention, its circuit connection section divides as shown in Figure 1 Carry out type selecting, connection, the measurement and examination method of the ammonia detector metering and calibrating device of the present invention, Use the ammonia detector metering and calibrating device as above described in either a program, comprise the following steps: Three road air inlets of device are connected ammonia, nitrogen and pure air by the first step respectively, and will Connect after three air inlets and have three effusion meters 5, three effusion meters 5 be all connected to one to be measured Concentration Standard Gases air chamber 1, after the mixed air mixing of concentration Standard Gases air chamber 1 to be measured, a point two-way divides Shu Chu not arrive standby test examination instrument 7, another road is vented;Second step, is divided into bag by liquid-crystal display section Including two pieces of liquid crystal display screens, one piece is that the Standard Gases configuring respective concentration uses, and liquid crystal panel selects The concentration of input ammonia gas and the concentration of spirit, the Standard Gases of the output being simultaneously entered needs is dense Degree, system, through automatically calculating the flow-rate ratio of ammonia and spirit, controls ammonia by numerical control Gas pure gas entrance 2 and the first-class gauge of pure air entrance 4 and the 3rd effusion meter, it is thus achieved that need The ammonia Standard Gases of the concentration wanted, another block liquid crystal display screen is used for recording and calculating in verification process Various data, and calculated feedback;3rd step, during the detection error of indication, the most standby inspection instrument Show value second piece of screen of input of device, three display indicating values of typing same concentration so that be System calculates the error of indication of this point automatically, and it is the most qualified to be sentenced mark;4th step, three After the gas of concentration has led to, compare the size of three errors of indication, take maximum and carry out with threshold value Relatively then determine that qualified no;5th step, after inputting the concentration of six ventilations so that system root Then determine that according to the computing formula result of calculation comparing with threshold value set according to repeatability Qualified no;6th step, carries stopwatch by system and sets response time parameter, from the beginning of ventilation Timing, to stopping the supple of gas or steam, record duration of ventilation record, compare with threshold value by calculating Then determine that qualified no.After 6th step, by two pieces can touch liquid crystal display screen carries out input and output, And data are printed by printer.Its data processing section, can be carried out on data processor " ammonia is examined for corresponding input/output function, the control of effusion meter and JJG1105-2015 Survey instrument " in computing formula and the threshold value of various parameters and sentence mark method.

Claims (9)

1. an ammonia detector metering and calibrating device, including concentration Standard Gases air chamber (1) to be measured, It is characterized in that: be respectively equipped with on concentration Standard Gases air chamber (1) to be measured ammonia pure gas entrance (2), Nitrogen inlet (3) and pure air entrance (4), concentration Standard Gases air chamber (1) to be measured is respectively It is connected with effusion meter (5) and bypass flow meter (6), effusion meter (5) and standby test examination instrument (7) being connected, bypass flow meter (6) is connected with drain (8).
2. ammonia detector metering and calibrating device as claimed in claim 1, it is characterised in that: Ammonia pure gas entrance (2), nitrogen inlet (3) and pure air entrance (4) connect respectively and set There are first-class gauge, second gauge and the 3rd effusion meter.
3. ammonia detector metering and calibrating device as claimed in claim 2, it is characterised in that: First-class gauge, second gauge and the 3rd effusion meter respectively with concentration Standard Gases air chamber to be measured (1) it is connected.
4. ammonia detector metering and calibrating device as claimed in claim 3, it is characterised in that: Ammonia detector metering and calibrating device also includes display part.
5. ammonia detector metering and calibrating device as claimed in claim 4, it is characterised in that: Display part is arranged with liquid crystal display screen.
6. the ammonia detector metering and calibrating device as according to any one of claim 1-5, its It is characterised by: ammonia detector metering and calibrating device also includes Data Input Interface and data output Interface.
7. ammonia detector metering and calibrating device as claimed in claim 6, it is characterised in that: Ammonia detector metering and calibrating device also includes data processor.
8. a measurement and examination method for ammonia detector metering and calibrating device, uses right such as to want Seek the ammonia detector metering and calibrating device according to any one of 1-7, comprise the following steps: the Three road air inlets of device are connected ammonia, nitrogen and pure air by step respectively, and by three Connecting after individual air inlet has three effusion meters (5), three effusion meters (5) to be all connected to one Concentration Standard Gases air chamber (1) to be measured, the mixed air mixing of concentration Standard Gases air chamber (1) to be measured A rear point two-way is respectively outputted to standby test examination instrument (7), and another road is vented;Second step, by liquid crystal Showing that part is divided into and include two pieces of liquid crystal display screens, one piece is that the Standard Gases configuring respective concentration uses, liquid Select concentration and the concentration of spirit of input ammonia gas in crystal panel, be simultaneously entered the defeated of needs The Standard Gases concentration gone out, system is through automatically calculating the flow-rate ratio of ammonia and spirit, logical Cross numerical control control ammonia pure gas entrance (2) and pure air entrance (4) first-class gauge with 3rd effusion meter, it is thus achieved that the ammonia Standard Gases of the concentration of needs, another block liquid crystal display screen is used for record With the various data calculated in verification process, and calculated feedback;3rd step, detects indicating value During error, show value second piece of screen of input of the most standby test examination instrument, the three of typing same concentration Secondary display indicating value so that system calculates the error of indication of this point automatically, and whether is sentenced mark Qualified;4th step, after the gas of three concentration has led to, compares the size of three errors of indication, Take maximum compare with threshold value then determine that qualified no;5th step, inputs six ventilations After concentration so that system according to repeatability according to set computing formula result of calculation and and threshold value Compare then determine that qualified no;6th step, carries stopwatch by system and sets response time Parameter, starts timing from ventilation, and to stopping the supple of gas or steam, record duration of ventilation record, by meter Calculate compare with threshold value then determine that qualified no.
9. the measurement verification side of ammonia detector metering and calibrating device as claimed in claim 8 Method, it is characterised in that: after the 6th step, by two pieces can touch liquid crystal display screen carries out input and output, And data are printed by printer.
CN201610239318.4A 2016-04-18 2016-04-18 Metrological verification device for ammonia gas detector and metrological verification method thereof Pending CN105911222A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107402287A (en) * 2017-09-01 2017-11-28 深圳小气科技有限公司 The calibration equipment and method of calibration of air quality detector
CN109307738A (en) * 2017-11-16 2019-02-05 中国石油化工股份有限公司 A kind of chlorine alarm calibration method and calibrating installation
CN111024892A (en) * 2019-11-25 2020-04-17 国网上海市电力公司 Inspection method of intelligent electric well lid gas monitoring device
CN111610337A (en) * 2020-05-20 2020-09-01 佳思德科技(深圳)有限公司 Alcohol detector calibrating device and method for displaying current calibration allowable error

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CN102445498A (en) * 2011-10-10 2012-05-09 上海科油石油仪器制造有限公司 Automatic calibration method of process chromatograph
CN203490209U (en) * 2013-10-23 2014-03-19 石建明 Calibrating device for harmful gas detection alarm of coal mine
CN205506797U (en) * 2016-04-18 2016-08-24 中国石油化工股份有限公司 Ammonia gas detection surveys appearance metrological verification device

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US6997347B2 (en) * 2003-07-02 2006-02-14 Industrial Scientific Corporation Apparatus and method for generating calibration gas
CN2689231Y (en) * 2003-07-23 2005-03-30 北京莱森电子技术有限公司 Standard gas intelligent proportioning apparatus
CN2741037Y (en) * 2004-01-03 2005-11-16 淮南矿业集团兴科计量技术服务有限责任公司 Testing house of harm gas monitoring instrument
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107402287A (en) * 2017-09-01 2017-11-28 深圳小气科技有限公司 The calibration equipment and method of calibration of air quality detector
CN109307738A (en) * 2017-11-16 2019-02-05 中国石油化工股份有限公司 A kind of chlorine alarm calibration method and calibrating installation
CN111024892A (en) * 2019-11-25 2020-04-17 国网上海市电力公司 Inspection method of intelligent electric well lid gas monitoring device
CN111610337A (en) * 2020-05-20 2020-09-01 佳思德科技(深圳)有限公司 Alcohol detector calibrating device and method for displaying current calibration allowable error

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Application publication date: 20160831