CN105908504A - Compound size for denim warp sizing and preparation method and application thereof - Google Patents
Compound size for denim warp sizing and preparation method and application thereof Download PDFInfo
- Publication number
- CN105908504A CN105908504A CN201610316921.8A CN201610316921A CN105908504A CN 105908504 A CN105908504 A CN 105908504A CN 201610316921 A CN201610316921 A CN 201610316921A CN 105908504 A CN105908504 A CN 105908504A
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- CN
- China
- Prior art keywords
- size
- warp sizing
- cowboy
- parts
- composite mortar
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/11—Starch or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a compound size for denim warp sizing and a preparation method and application thereof. The compound size for denim warp sizing is prepared from the following raw materials in parts by mass: 70 to 80 parts of starch size, 8 to 10 parts of PVA (Poly Vinyl Alcohol) size, 15 to 20 parts of acrylate size, 1 to 3 parts of wax sheets and plates, 1 to 3 parts of stabilizer, and 0.2 to 0.6 part of oxidant. The preparation method comprises the following steps: adding the starch size, the PVA size, the acrylate size, the wave sheets and plates, the stabilizer and the oxidant to a mixing tank in sequence in parts by mass, and uniformly mixing to obtain a finished product. Three major traditional sizes, namely the starch size, the PVA size and the acrylate size are compounded and are then added with an appropriate amount of oxidant and sterilizer. The size boiling time is short, the compound size has good film-forming property and a size film is pliable and tough, and wear-resistant. The preparation method is simple, high in production efficiency and relatively low in cost and has a good effect on denim warp sizing.
Description
Technical field
The present invention relates to technical field of textile, specifically a kind of cowboy's warp sizing composite mortar and its preparation method and application.
Background technology
The purpose of yarn sizing is to be coated with serous coat that is smooth, wear-resisting, pliable and tough and that have some strength on sliver surface, make fiber patch volt, reduce thread friction coefficient, slurries penetrate into yarn interior simultaneously, increase the adhesion between fiber, improve the tensile strength of yarn, to adapt to the friction in weaving process and tension force, reduce broken end, improve weaving efficiency.
The big spinning sizing agent of traditional three: starch size, PVA(polyvinyl alcohol) slurry, acrylic size, starch size is prone to degraded and has environment-friendly advantage, but owing to film phonograph strength is inadequate, fragility greatly, easily falls slurry, it is used alone the requirement being difficult to meet textile yarn starching, PVA slurry is unstable, easily layering, slurrying time are long, it is present in after desizing in slurries and is difficult to degrade, acrylic size is expensive due to cost of material, the most do not possesses superiority of effectiveness, and serous coat is too soft, there is the risk that moisture absorption is glued again.To this end, it is desirable to the composite mortar obtaining serous coat softness, high resilience and intensity height, anti-wear performance is good.
Summary of the invention
It is an object of the invention to provide a kind of pliable and tough, wear-resisting, preparation technology is simple, production efficiency is high, lower-cost cowboy's warp sizing composite mortar and its preparation method and application, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of cowboy's warp sizing composite mortar, is made up of according to the raw material of mass fraction following:
Starch size 70-80 part
PVA slurry 8-10 part
Acrylic acid class slurry 15-20 part
Wax disk(-sc) 1-3 part
Stabilizer 1-3 part
Oxidant 0.2-0.6 part.
As the further scheme of the present invention: described starch size is cassava modified starch, concentration be 6%, temperature be viscosity when 90 DEG C be 12-22mPa.s.
As the further scheme of the present invention: described PVA slurry model is PVA1799, concentration be 6%, temperature be viscosity when 90 DEG C be 22-28mPa.s.
As the further scheme of the present invention: described acrylic acid class slurry model is PSAA-I, concentration be 6%, temperature be viscosity when 90 DEG C be 10-30mPa.s.
As the further scheme of the present invention: described wax disk(-sc) model is QH-600.
As the further scheme of the present invention: described stabilizer is tertiary sodium phosphate.
As the further scheme of the present invention: described oxidant is potassium peroxydisulfate.
The preparation method of described cowboy's warp sizing composite mortar, by being added sequentially in blending tank according to the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant, mixes and gets product.
The application in cowboy's warp sizing material of the described composite mortar.
Compared with prior art, the invention has the beneficial effects as follows:
Starch size, PVA slurry, acrylic acid class slurry three great tradition slurry are combined by the present invention, add appropriate oxidant and stabilizer, and the mashing off time is short, slurries good film-forming property, serous coat is pliable and tough, wear-resisting, and preparation technology is simple, production efficiency is high, and cost is relatively low, and cowboy's warp sizing is had good effect.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, the preparation method of a kind of cowboy's warp sizing composite mortar, raw material composition mass fraction is: starch size 70 parts, 10 parts of PVA slurry, 20 parts of acrylic acid class slurry, wax disk(-sc) 1 part, stabilizer 1 part, 0.2 part of oxidant.
The preparation method of described cowboy's warp sizing composite mortar is: the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant is added sequentially in blending tank, mixes to obtain finished product.
Embodiment 2
In the embodiment of the present invention, the preparation method of a kind of cowboy's warp sizing composite mortar, raw material composition mass fraction is: starch size 75 parts, 9 parts of PVA slurry, 18 parts of acrylic acid class slurry, wax disk(-sc) 2 parts, stabilizer 2 parts, 0.4 part of oxidant.
The preparation method of described cowboy's warp sizing composite mortar is: the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant is added sequentially in blending tank, mixes to obtain finished product.
Embodiment 3
In the embodiment of the present invention, the preparation method of a kind of cowboy's warp sizing composite mortar, raw material composition mass fraction is: starch size 80 parts, 8 parts of PVA slurry, 15 parts of acrylic acid class slurry, wax disk(-sc) 3 parts, stabilizer 3 parts, 0.6 part of oxidant.
The preparation method of described cowboy's warp sizing composite mortar is: the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant is added sequentially in blending tank, mixes to obtain finished product.
Embodiment 4
In the embodiment of the present invention, a kind of cowboy's warp sizing composite mortar, it is made up of according to the raw material of mass fraction following: starch size 72 parts, 8 parts of PVA slurry, 17 parts of acrylic acid class slurry, wax disk(-sc) 2 parts, stabilizer 2 parts, 0.3 part of oxidant.
The preparation method of described cowboy's warp sizing composite mortar is: the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant is added sequentially in blending tank, mixes to obtain finished product.
Embodiment 5
In the embodiment of the present invention, a kind of cowboy's warp sizing composite mortar, it is made up of according to the raw material of mass fraction following: starch size 78 parts, 10 parts of PVA slurry, 19 parts of acrylic acid class slurry, wax disk(-sc) 2 parts, stabilizer 2 parts, 0.5 part of oxidant.
The preparation method of described cowboy's warp sizing composite mortar is: the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), stabilizer, oxidant is added sequentially in blending tank, mixes to obtain finished product.
In above example use starch size be cassava modified starch, concentration be 6%, temperature be viscosity when 90 DEG C be 12-22mPa.s.PVA slurry model is PVA1799, concentration be 6%, temperature be viscosity when 90 DEG C be 22-28mPa.s.Acrylic acid class slurry model is PSAA-I, concentration be 6%, temperature be viscosity when 90 DEG C be 10-30mPa.s.Wax disk(-sc) model is QH-600.Stabilizer is tertiary sodium phosphate.Oxidant is potassium peroxydisulfate.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing from the spirit or essential characteristics of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is limited by claims rather than described above, it is intended that all changes fallen in the implication of equivalency and scope of claim included in the present invention.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but the most each embodiment only comprises an independent technical scheme, this narrating mode of specification is only for clarity sake, specification should can also be formed, through appropriately combined, other embodiments that it will be appreciated by those skilled in the art that as an entirety, the technical scheme in each embodiment by those skilled in the art.
Claims (9)
1. cowboy's warp sizing composite mortar, it is characterised in that by the following raw material according to mass fraction
Composition:
Starch size 70-80 part
PVA slurry 8-10 part
Acrylic acid class slurry 15-20 part
Wax disk(-sc) 1-3 part
Stabilizer 1-3 part
Oxidant 0.2-0.6 part.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described shallow lake
Slurry material is cassava modified starch, concentration be 6%, temperature be viscosity when 90 DEG C be 12-22mPa.s.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described
PVA slurry model is PVA1799, concentration be 6%, temperature be viscosity when 90 DEG C be 22-28mPa.s.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described third
Diluted acid class slurry model is PSAA-I, concentration be 6%, temperature be viscosity when 90 DEG C be 10-30mPa.s.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described wax
Sheet model is QH-600.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described is steady
Determining agent is tertiary sodium phosphate.
Cowboy's warp sizing composite mortar the most according to claim 1, it is characterised in that described oxygen
Agent is potassium peroxydisulfate.
8. a preparation method for the cowboy's warp sizing composite mortar as described in claim 1-7 is arbitrary, its
It is characterised by, by according to the starch size of mass fraction, PVA slurry, acrylic acid class slurry, wax disk(-sc), steady
Determine agent, oxidant is added sequentially in blending tank, mixes and gets product.
9. the composite mortar as described in claim 1-7 is arbitrary application in cowboy's warp sizing material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610316921.8A CN105908504A (en) | 2016-05-13 | 2016-05-13 | Compound size for denim warp sizing and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610316921.8A CN105908504A (en) | 2016-05-13 | 2016-05-13 | Compound size for denim warp sizing and preparation method and application thereof |
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| Publication Number | Publication Date |
|---|---|
| CN105908504A true CN105908504A (en) | 2016-08-31 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610316921.8A Pending CN105908504A (en) | 2016-05-13 | 2016-05-13 | Compound size for denim warp sizing and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758317A (en) * | 2016-12-08 | 2017-05-31 | 武汉纺织大学 | A kind of cowboy's warp thread pigment dyeing starching integral process |
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|---|---|---|---|---|
| DE3724332A1 (en) * | 1987-07-23 | 1989-02-02 | Wacker Chemie Gmbh | Use of polyhydroxyl-containing polymers as sizing agents |
| EP0905301A1 (en) * | 1997-09-02 | 1999-03-31 | Chimitex S.A.R.L. | Size for the low temperature sizing system |
| CN101476244A (en) * | 2009-01-06 | 2009-07-08 | 东莞东美食品有限公司 | Environment-friendly type special combined slurry for jean |
| CN102002857A (en) * | 2010-12-15 | 2011-04-06 | 宏太（中国）有限公司 | Novel sizing agent for sizing terylene or terylene staple fiber |
| CN102936839A (en) * | 2012-11-26 | 2013-02-20 | 愉悦家纺有限公司 | Slashing method |
| CN103147209A (en) * | 2013-03-14 | 2013-06-12 | 江苏悦达纺织集团有限公司 | Stainless steel fiber radiation protection face fabric and fabrication method thereof |
| CN103510316A (en) * | 2013-10-17 | 2014-01-15 | 江苏联宏纺织有限公司 | Process for sizing high-count and high-density double-woven fabric |
| CN103643515A (en) * | 2013-12-30 | 2014-03-19 | 张海峰 | Textile size and preparation method thereof |
-
2016
- 2016-05-13 CN CN201610316921.8A patent/CN105908504A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3724332A1 (en) * | 1987-07-23 | 1989-02-02 | Wacker Chemie Gmbh | Use of polyhydroxyl-containing polymers as sizing agents |
| EP0905301A1 (en) * | 1997-09-02 | 1999-03-31 | Chimitex S.A.R.L. | Size for the low temperature sizing system |
| CN101476244A (en) * | 2009-01-06 | 2009-07-08 | 东莞东美食品有限公司 | Environment-friendly type special combined slurry for jean |
| CN102002857A (en) * | 2010-12-15 | 2011-04-06 | 宏太（中国）有限公司 | Novel sizing agent for sizing terylene or terylene staple fiber |
| CN102936839A (en) * | 2012-11-26 | 2013-02-20 | 愉悦家纺有限公司 | Slashing method |
| CN103147209A (en) * | 2013-03-14 | 2013-06-12 | 江苏悦达纺织集团有限公司 | Stainless steel fiber radiation protection face fabric and fabrication method thereof |
| CN103510316A (en) * | 2013-10-17 | 2014-01-15 | 江苏联宏纺织有限公司 | Process for sizing high-count and high-density double-woven fabric |
| CN103643515A (en) * | 2013-12-30 | 2014-03-19 | 张海峰 | Textile size and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 刘竹君等: "《牛仔布生成技术》", 31 January 2013, 东华大学出版社 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758317A (en) * | 2016-12-08 | 2017-05-31 | 武汉纺织大学 | A kind of cowboy's warp thread pigment dyeing starching integral process |
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Application publication date: 20160831 |