CN105904526A - Manufacturing method of high-corrosion-resistance reconstructing material for outdoor use - Google Patents
Manufacturing method of high-corrosion-resistance reconstructing material for outdoor use Download PDFInfo
- Publication number
- CN105904526A CN105904526A CN201610511076.XA CN201610511076A CN105904526A CN 105904526 A CN105904526 A CN 105904526A CN 201610511076 A CN201610511076 A CN 201610511076A CN 105904526 A CN105904526 A CN 105904526A
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- Prior art keywords
- bamboo
- oil
- bundle
- corrosion resistant
- bamboo bundle
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27D—WORKING VENEER OR PLYWOOD
- B27D1/00—Joining wood veneer with any material; Forming articles thereby; Preparatory processing of surfaces to be joined, e.g. scoring
- B27D1/04—Joining wood veneer with any material; Forming articles thereby; Preparatory processing of surfaces to be joined, e.g. scoring to produce plywood or articles made therefrom; Plywood sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
Abstract
The invention discloses a manufacturing method of a high-corrosion-resistance reconstructing material for outdoor use. The process steps include that firstly, wood bundles, bamboo bundles or bamboo bundle pieces made in a ground manner serve as composition units, wherein the bamboo bundles or the bamboo bundle pieces need to be boiled in water or subjected to ultrasonic mould-proof treatment; secondly, the wood bundles, the bamboo bundles or the bamboo bundle pieces subjected to the above treatment are dried till the water content is 10% or below; thirdly, high-corrosion-resistance oil-soluble phenolic resin adhesives are applied to the dried wood bundles, bamboo bundles or bamboo bundle pieces, and the adhesive applying amount is 10% to 30%; fourthly, the wood bundles, the bamboo bundles or the bamboo bundle pieces subjected to adhesive application are drained off, form blanks and are pressed into the high-corrosion-resistance reconstructing material for outdoor use; and fifthly, after the pressed and formed high-corrosion-resistance reconstructing material is subjected to health maintenance treatment, later period machining can be performed, and secondary protective oil coating is not needed in use. The invention provides the manufacturing method of the oil-containing high-corrosion-resistance reconstructing material. The reconstructing material manufactured through the method is excellent in anti-mould, corrosion-resistant and aging-resistant performance, the product size stability is good, the manufacturing technology is simple, and the environment pollution is small.
Description
Technical field
The present invention relates to the manufacture method of a kind of outdoor use height corrosion resistant recombinant material, belong to building material technical field.
Background technology
Recombinant material is to stick other structure glue such as agent by rolling wood bundle, bamboo bundle or the bamboo bundle sheet made through applying water-soluble phenolic resin adhesive
After the new structure material again suppressed.Because the anisotropy of undersized log or dwarf bamboo is redistributed by it, remain
Wood, longitudinal high intensity of bamboo wood so that it is achieve clear superiority in structural material field.At present, recombinant material, especially bamboo matter
Recombinant material is mainly used as outdoor use floor and outdoor use furniture woods.This just requires that recombinant material has very well in outdoor hygrothermal environment
Antiseptic property.Therefore, the Component units such as bamboo bundle, wood bundle are carried out preservative treatment, composes recombinant material the most again, be instantly
One of recombinant material antiseptical main method.But, the waterborne-type preservation of wood bamboo wood not only has losing issue when application, right
Soil environment pollutes, and Component units surface can be caused interface pollution, affects the interface cohesion of itself and adhesive, enters
And reduce the outdoor ageing-resistant performance of recombinant material.In recent years, cosmolin is as a kind of good antiseptic treating agent, on recombinant material
Application also result in technical concern.Use immersion oil to process recombinant material Component units, then impose adhesive after removing oil and carry out
The research of glued manufacture recombinant material is the focus of technical concerns instantly.But, after bamboo bundle, the wood Component units immersion oil such as bundle, then enter
Row surface chemistry removing oil, not only complex process, and there is the secondary chemical contamination of oil removing conversion, simultaneously to again applying water
The interface cohesion of property phenolic resin adhesive has adverse effect.Recombinant material has high rotproofness and needs abundant rotproofness oil
Attachment, once removing oil, reduces the most again the antiseptic effect of oil.For situation above, the present invention uses the oil soluble of high corrosion resistant
Property phenolic resin adhesive be binding agent, with the Oleum Verniciae fordii of high corrosion resistant as medium, to construction unit dipping protection such as wood bundle, bamboo bundles
While oil, complete the glue-applying technique of Component units, eliminate the processing step of removing oil, and by Component units oil protective treatment with
Phenolic resin adhesive glue-applying technique has carried out technical integrated and innovation, can disposably produce the novel restructuring of high corrosion resistant
Material, simplifies production technology and decreases environmental pollution.
Summary of the invention
What the present invention proposed is a kind of with roll make wood bundle, bamboo bundle or bamboo bundle sheet as Component units, utilize the oil soluble of high corrosion resistant
Property phenolic resin adhesive makes the manufacture method of the outdoor use height corrosion resistant recombinant material of a kind of oil-containing.The recombinant material that this technology is made is resistance to
Water moisture-proof, anti-mildew resists rotten, and product size stability is high, can be not only used for the construction material of high intensity, it is also possible to as outdoor use
Floor, outdoor use moulding, plate for timber-construction protection wallboard etc..
The technical solution of the present invention comprises the technical steps that:
1) with roll make wood bundle, bamboo bundle or bamboo bundle sheet as Component units, wherein bamboo bundle or bamboo bundle sheet need to process through mildew-resistant；
2) wood bundle, bamboo bundle or the bamboo bundle sheet after above-mentioned process, is dried to moisture content less than 10%；
3) dried wood bundle, bamboo bundle or bamboo bundle sheet impose the oil-soluble phenolic resin adhesive of high corrosion resistant, resin added 10-30%；
4) wood bundle, bamboo bundle or the bamboo bundle sheet after applying glue is drained, assembly, be suppressed into the recombinant material of outdoor use height corrosion resistant；
5) after the high corrosion resistant recombinant material health preserving after compressing, post-production can be carried out, without carrying out secondary protection oil again during use
Cover with paint, lacquer, colour wash, etc..
6) step 1) described outdoor use height corrosion resistant recombinant material Component units in wood bundle be typically not required to carry out mildew-resistant process, bamboo bundle or
Bamboo bundle sheet, because then needing through decocting in water or supersound process containing the starch that easily goes mouldy, improves bamboo bundle or the mildew resistance of bamboo bundle sheet, bamboo bundle or
The sodium hydroxide that can add 0.5-2% mass fraction during bamboo bundle sheet decocting in water promotes starch removing, increases mildew resistance, and ultrasonic power controls
Below 1600W, ultrasonic weight-loss ratio is less than 3%.
7) step 2) described wood bundle, bamboo bundle, the drying means of bamboo bundle sheet can be conventional air dry be dried can also be oily be medium
Oil drying, wherein oil be medium be dried, the oil used is for mix or and oil-soluble with oil-soluble phenolic resin adhesive
The oil of phenolic resin adhesive is same oil, does not affect wood bundle, bamboo bundle, bamboo bundle sheet are executed with oil-soluble phenolic resin adhesive
Glue and gluing, temperature 50-90 DEG C of oil when oil is medium, immersion oil rate is less than 30%, dried moisture content less than 10%.
8) step 3) the oil-soluble phenolic resin adhesive that used of described outdoor use height corrosion resistant recombinant material is with Oleum Verniciae fordii for main dry
Property oil oil-soluble phenolic resin adhesive, Oleum Verniciae fordii can mix the Oleum Terebinthinae of 3-10%, Semen Ricini Water Oil Or Gas, for applying glue
Oil-soluble phenolic resin adhesive impregnation after solids content 20-35%, the alcohol-soluble phenolic resin that separately can add 0-10% is carried out
Applying glue, resin added 10-25%, applying glue after complete longitudinal assembly are blended.
9) step 4) pressure that the hot pressing of described outdoor use height corrosion resistant recombinant material is compressing is 2.0～5.0MPa, pressing time
1.0-1.3min/mm, pressed temperature is 115-250 DEG C, and when using cold forming heat cure molding, molding pressure is 30-70MPa, mould
In tool, solidified forming time is 40-60min/mm.
10) step 5) described outdoor use height corrosion resistant recombinant material, repressed after need health preserving more than 1 week, to balance in pressing process
Thermal stress and moisture gradient, when thickness specification is more than more than 15cm, conditioned time will be more than 2 weeks.
Detailed description of the invention
Embodiment 1: high corrosion resistant recombinant material restrainted by full wood
Step 1) it is dried rolling the wood bundle made to moisture content 8-10%；
Step 2) by dried wood bundle, to be immersed in solid content be in the 23-25% oil-soluble phenolic resin adhesive with Oleum Verniciae fordii as substrate, leaching
Glue amount controls at 15-18%, takes out, drain unnecessary fluid after reaching impregnation resin content；
Step 3) the wood bundle after impregnation is carried out being hot pressed into recombinant material by after complete longitudinal assembly, hot pressing pressure is 3.5-3.7MPa, pressurization
Time 1.1min/mm, pressed temperature is 150 DEG C；
Step 4) recombinant material hot pressing made is placed in the quenched room of damping and carries out health preserving, after health preserving can carry out sawing sanction etc. for more than 2 weeks
Processing.
Embodiment 2: full bamboo bundle is colded pressing high corrosion resistant recombinant material
Step 1) it is placed in rolling the bamboo bundle made in ultrasonic cleaning equipment, supersound process 30 minutes, ultrasonic power 1600W, super
Sound bath raio 1: 8, takes out bamboo bundle, is dried to moisture content 8-10% during bamboo Shu Chaosheng weight-loss ratio 1.5-2%；
Step 2) dried bamboo bundle is immersed in solid content is in the 23-25% oil-soluble phenolic resin adhesive with Oleum Verniciae fordii as substrate, leaching
Glue amount controls at 15-18%, takes out, drain unnecessary fluid after reaching impregnation resin content；
Step 3) the bamboo bundle after impregnation oils dissolubility phenolic resin adhesive is carried out cold forming heat cure by after complete longitudinal assembly in mould
Molding, molding pressure is 60-70MPa, and heat cure forming temperature is 150 DEG C, time 55min/mm；
Step 4) the full bamboo bunch recombining material being pressed into is placed in the quenched room of damping carries out health preserving, health preserving can carry out saw for more than 3 weeks and cut out
Deng post-treatment.
Embodiment 3: wood bundle bamboo bundle interlaminar hybrid height corrosion resistant recombinant material
Step 1) by rolling the wood bundle made, to be dried to moisture content 8% standby, it is placed in rolling the bamboo bundle made in ultrasonic cleaning equipment,
Supersound process 30 minutes, ultrasonic power 1600W, ultra sonic bath ratio 1: 8, take out bamboo bundle during bamboo Shu Chaosheng weight-loss ratio 1.5-2%, dry
Dry to moisture content 8-10%；
Step 2) by dried wood bundle, to be immersed in solid content respectively be the 23-25% oil-soluble phenolic resin glue with Oleum Verniciae fordii as substrate to bamboo bundle
In glutinous agent adhesive glue, impregnation resin content controls at 15-18%, takes out wood bundle, bamboo bundle, drain unnecessary fluid after reaching impregnation resin content,
Wood bundle and bamboo bundle are uniformly mixed according to 1: 3 mass ratio；
Step 3) oil-soluble phenolic resin glue will be soaked with after the wood bundle uniformly mixed and bamboo bundle hot-forming by carrying out after complete longitudinal assembly,
Hot pressing pressure is 4.0-4.5MPa, pressing time 1.0min/mm, pressed temperature is 150 DEG C；
Step 4) Bamboo-wood composite scrimber being pressed into is placed in the quenched room of damping carries out health preserving, health preserving can carry out sawing sanction etc. for more than 3 weeks
Post-treatment.
Embodiment 3: wood bundle bamboo bundle interlayer mixes high corrosion resistant recombinant material
Step 1) that wood bundle is dried to moisture content 8% is standby, and will roll bamboo bundle and be placed in ultrasonic cleaning equipment, supersound process 30 minutes,
Ultrasonic power 1600W, ultra sonic bath ratio 1: 8, takes out bamboo bundle, is dried to moisture content 8-10% during bamboo Shu Chaosheng weight-loss ratio 1.5-2%；
Step 2) by dried wood bundle, to be immersed in solid content respectively be the 23-25% oil-soluble phenolic resin glue with Oleum Verniciae fordii as substrate to bamboo bundle
In glutinous agent adhesive glue, impregnation resin content controls at 15-18%, takes out wood bundle, bamboo bundle, drain unnecessary fluid after reaching impregnation resin content；
Step 3) will be soaked with the upper and lower surface layer of the wooden Shu Zuowei recombinant material after oil-soluble phenolic resin glue, bamboo Shu Zuowei sandwich layer after impregnation,
Carry out interlayer according to top layer with core material 1: 3 mass ratio to mix, hot-forming by carrying out after complete longitudinal assembly, make with wood bundle
Interlayer for upper and lower surface mixes high corrosion resistant recombinant material, and hot pressing pressure is 3.5-3.7MPa, and pressing time, 1.0mim/mm, pressurizeed
Temperature is 160 DEG C；
Step 4) Bamboo-wood composite scrimber being pressed into is placed in the quenched room of damping carries out health preserving, health preserving can carry out sawing sanction etc. for more than 3 weeks
Post-treatment.
Claims (7)
1. a manufacture method for outdoor use height corrosion resistant recombinant material, its feature comprises the following steps that:
1) with roll make wood bundle, bamboo bundle or bamboo bundle sheet as Component units, wherein bamboo bundle or bamboo bundle sheet need to be through decocting in water or ultrasonic
Mildew-resistant processes；
2) wood bundle, bamboo bundle or the bamboo bundle sheet after above-mentioned process, is dried to moisture content less than 10%；
3) dried wood bundle, bamboo bundle or bamboo bundle sheet impose the oil-soluble phenolic resin adhesive of high corrosion resistant, resin added 10-30%；
4) by the wood bundle after applying glue, bamboo bundle or bamboo bundle sheet drains, assembly, it is suppressed into the recombinant material of outdoor use height corrosion resistant；
5), after compressing high corrosion resistant recombinant material health preserving, post-production can be carried out, without carrying out secondary protection oil painting again during use
Decorations.
2. according to the manufacture method of outdoor use height corrosion resistant recombinant material a kind of in claim 1, it is characterised in that: step 1) described room
In the Component units of external height corrosion resistant recombinant material, wood bundle is typically not required to carry out mildew-resistant process, bamboo bundle or bamboo bundle sheet and easily goes mouldy because containing
Starch need to can add 0.5-2% through decocting in water or supersound process when improving bamboo bundle or the mildew resistance of bamboo bundle sheet, bamboo bundle or bamboo bundle sheet decocting in water
The sodium hydroxide of mass fraction promotes starch removing, increases mildew resistance, and ultrasonic power controls at below 1600W, ultrasonic weight-loss ratio
Less than 3%.
3. according to the manufacture method of outdoor use height corrosion resistant recombinant material a kind of in claim 1, it is characterised in that: step 2) described wood
Bundle, bamboo bundle, the drying means of bamboo bundle sheet can be that conventional air dry is dried the oil drying that can also be oil for medium, and wherein oil is
Being dried of medium, the oil used is to mix with oil-soluble phenolic resin adhesive or be with the oil of oil-soluble phenolic resin adhesive
Same oil, does not affect wood bundle, bamboo bundle, bamboo bundle sheet and the applying glue of oil-soluble phenolic resin adhesive and gluing, and oil is done for medium
Time dry, the temperature of oil is 50-90 DEG C, and immersion oil rate is less than 30%, dried moisture content less than 10%.
4. according to the manufacture method of outdoor use height corrosion resistant recombinant material a kind of in claim 1, it is characterised in that: step 3) described room
The oil-soluble phenolic resin adhesive that external height corrosion resistant recombinant material is used be Oleum Verniciae fordii be the oil-soluble phenolic resin glue of main drying oil
Glutinous agent, can mix the Oleum Terebinthinae of 3-10%, Semen Ricini Water Oil Or Gas, for the oil-soluble phenolic resin adhesive of applying glue in Oleum Verniciae fordii
Solids content after impregnation is 20-35%, and the alcohol-soluble phenolic resin that separately can add 0-10% carries out applying glue, resin added are blended
10-25%, complete longitudinal assembly after applying glue.
5. according to the manufacture method of outdoor use height corrosion resistant recombinant material a kind of in claim 1, it is characterised in that: step 4) described room
The compressing pressure of external height corrosion resistant recombinant material hot pressing is 2.0～5.0MPa, pressing time 1.0-1.3min/mm, pressed temperature is
115-250 DEG C, when using cold forming heat cure molding, molding pressure is 30-70MPa, and mold curing molding time is
40-60min/mm。
6. according to the manufacture method of outdoor use height corrosion resistant recombinant material a kind of in claim 1, it is characterised in that: step 5) described room
External height corrosion resistant recombinant material, repressed after need health preserving more than 1 week, with balance in pressing process produce thermal stress and moisture content ladder
Degree, when thickness specification is more than more than 15cm, conditioned time will be more than 2 weeks.
The manufacture method of a kind of outdoor use height corrosion resistant recombinant material the most according to any one of claim 1 to 6, its feature exists
In: with roll make wood bundle, bamboo bundle or bamboo bundle sheet as Component units, use the oil-soluble phenolic resin adhesive pressure of high corrosion resistant
The high corrosion resistant recombinant material of system.Its assembly structure includes with Types Below: 1) with complete wooden high corrosion resistant that wood bundle is basic Component units
Recombinant material；2) with bamboo bundle or the full bamboo height corrosion resistant recombinant material of bamboo bundle sheet longitudinal assembly entirely；3) with uniform in wood bundle, bamboo bundle layer
The wooden bamboo height corrosion resistant recombinant material mixed；4) the bamboo high corrosion resistant weight of wood with bamboo bundle, the wood bundle layered distribution that mixes of interlayer as primary structure
Group material.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106863514A (en) * | 2017-02-21 | 2017-06-20 | 太尔化工（南京）有限公司 | Green persistently application and preparation method of the anticorrosive mildewproof phenolic resin on Recombined bamboo |
| CN106863512A (en) * | 2017-02-07 | 2017-06-20 | 南京林业大学 | The preparation method of outdoor timber recombinant material |
| CN107234696A (en) * | 2017-08-02 | 2017-10-10 | 国际竹藤中心 | A kind of bamboo（Wood）The preparation method of meal chopsticks laminated timber |
| CN107498666A (en) * | 2017-09-16 | 2017-12-22 | 蒋红卫 | Recombined bamboo processing technology |
| CN108162117A (en) * | 2017-12-31 | 2018-06-15 | 浙江省林业科学研究院 | A kind of manufacturing method of the termite-proof outdoor bamboo floor of efficient corrosion resisting |
| CN108340461A (en) * | 2018-03-02 | 2018-07-31 | 南京林业大学 | A kind of novel recombination is wooden to make method |
| CN111516071A (en) * | 2020-03-26 | 2020-08-11 | 南京林业大学 | Preparation method of corrosion-resistant mildew-proof recombined bamboo plate blank |
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| CN108162117A (en) * | 2017-12-31 | 2018-06-15 | 浙江省林业科学研究院 | A kind of manufacturing method of the termite-proof outdoor bamboo floor of efficient corrosion resisting |
| CN108340461A (en) * | 2018-03-02 | 2018-07-31 | 南京林业大学 | A kind of novel recombination is wooden to make method |
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| CN111516071A (en) * | 2020-03-26 | 2020-08-11 | 南京林业大学 | Preparation method of corrosion-resistant mildew-proof recombined bamboo plate blank |
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Application publication date: 20160831 |