CN105903292A - Oil drop filtering filler and high-efficient condensing oil gas recycling device - Google Patents
Oil drop filtering filler and high-efficient condensing oil gas recycling device Download PDFInfo
- Publication number
- CN105903292A CN105903292A CN201610518818.1A CN201610518818A CN105903292A CN 105903292 A CN105903292 A CN 105903292A CN 201610518818 A CN201610518818 A CN 201610518818A CN 105903292 A CN105903292 A CN 105903292A
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- CN
- China
- Prior art keywords
- oil
- filter packing
- oleophylic
- packing
- ceramic particle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/0001—Making filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/0027—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions
- B01D46/003—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions including coalescing means for the separation of liquid
- B01D46/0031—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions including coalescing means for the separation of liquid with collecting, draining means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/30—Particle separators, e.g. dust precipitators, using loose filtering material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
Abstract
The invention relates to the technical field of oil gas recycling and specifically relates to an oil drop filtering filler and a high-efficient condensing oil gas recycling device. The high-efficient condensing oil gas recycling device comprises a ceramic particle and is characterized in that the ceramic particle is of circular ball shape; a layer of oleophylic coating reagent is coated on the surface of the ceramic particle in circular ball shape; the oleophylic coating reagent comprises the following components by weight part: 30-40% of powder-shaped aluminosilicate, 3%-5% of quaternary ammonium salt, 8%-15% of inorganic binder and the balance of water. The high-efficient condensing oil gas recycling device has the beneficial effects that the oil drop filtering filler is coated with a layer of oleophylic coating reagent on the surface of the ceramic particle so as to absorb the oil drop from the oil gas, the oil drop is absorbed and gathered into liquid, the oil gas recovering device of the oil drop filtering filler is used for recovering the oil gas and the oil gas recycling device has the advantages of simple structure, convenience in maintenance and high recovery rate.
Description
Technical field
The present invention relates to Investigation of Petroleum Vapor Recovery Technology field, specifically a kind of oil droplet filter packing and high-efficiency condensation oil-gas recovery device.
Background technology
Along with the growth of vehicle guaranteeding organic quantity, the usage amount of gasoline is also sharply increasing, and produces in petrochemical industry, transports and store
During Deng, some liquid oil gas inevitable enters in air, causes oil product evaporating loss, to enterprise and society's band
Carrying out serious potential safety hazard, environmental pollution, energy waste and economic loss, therefore, one simply utilizes oil droplet filter packing
Make the oil droplet in oil gas be adsorbed by the oleophilic layer on filter packing surface during flowing through filter packing and pool drop and carry out oil
The method that gas reclaims seems particularly important.
Summary of the invention
For the problems referred to above, it is an object of the invention to provide a kind of oil droplet filter packing and high-efficiency condensation oil-gas recovery device, use
To solve above-mentioned technical problem.The oil droplet filter packing of the present invention uses can be effective at ceramic grain surface one layer of oleophylic paint of painting
Absorption oil gas in oil droplet, and then make oil droplet absorption pool liquid, and by using the petroleum vapor recovery of this oil droplet filter packing to set
For carrying out petroleum vapor recovery, this oil-gas recovery device has simple in construction, the advantage that the easy to maintenance and rate of recovery is high.
Technical scheme includes: a kind of oil droplet filter packing, and including ceramic particle, described ceramic particle is spheroidal,
One layer of oleophylic paint is scribbled on the surface of described spheroidal ceramic particle；Described oleophylic paint includes 30-40% according to percentage by weight
Powder shape aluminosilicate, the quaternary ammonium salt of 3%-5%, the inorganic binder of 8%-15%, the water of surplus.
Described quaternary ammonium salt is stearyl trimethyl ammonium chloride, VARISOFT TA100, octadecyl ammonium chloride and lecithin
In one.
Described inorganic binder is sodium silicate.Sodium silicate is easier to be combined with ceramic grain surface, strengthens paint at pottery
Adhesion strength on grain.
Technical scheme also includes: the preparation method of above-mentioned a kind of oil droplet filter packing, its preparation method includes following step
Rapid:
Step one: preparation surfacer, puts into powder shape aluminosilicate in water, disperses under normal temperature, adds quaternary ammonium salt and inorganic
Binding agent, stirs reactant liquor under 5 DEG C of-60 DEG C of normal pressures after fully dissolving, and obtains oleophylic paint after filtering；
Step 2: the oleophylic paint that step one prepares is coated in described ceramic grain surface uniformly；
Step 3: surface uniform application is crossed described ceramic particle heat drying at a temperature of 65-75 DEG C of oleophylic paint, obtains
Obtain ceramic particle oil droplet filter packing.
Described mixing time is 22-24 hour.
Described speed of agitator is 300rpm-400rpm.
The present invention be become oil loving silicate mixed sodium waterglass after former lyophilic powder shape aluminosilicate reacts with quaternary ammonium salt after
It is easier to bond with ceramic particle, forms a kind of stable oil droplet filter packing.
Technical scheme also includes: a kind of high-efficiency condensation oil-gas recovery device, including stuffing box, also includes claim
Oil droplet filter packing described in 1, is provided with the packing support net being obliquely installed, is provided with below described supporting network in the middle part of described stuffing box
The oil collection plate parallel with described supporting network, described oil collection plate is divided into being positioned at and half side on incline direction inclines without leakage of oil orifice plate and being positioned at
Band leakage of oil orifice plate half side under tilted direction, the parallel oil guide groove that is provided with in the downside of described oil collection plate, described oil guide groove and described collection
Forming air intake duct between oiled-plate method, the bottom of described oil guide groove and stuffing box sidewall junction are provided with drain tap, the top of described oil guide groove
Portion and described stuffing box sidewall junction are provided with oil and gas import, are provided with condenser between oil and gas import and stuffing box；Described supporting network
Being arranged above packing area, described oil droplet filter packing is positioned at described packing area, and packing area is arranged over top cover, in the middle part of described top cover
It is provided with exhaust outlet.
Described oil and gas import is provided with intake valve, and described drain tap is provided with tapping valve.
Described exhaust outlet is provided with spark arrester.During being possible to prevent petroleum vapor recovery, extraneous burning things which may cause a fire disaster is drawn by exhaust outlet entrance stuffing box
Play fire incident.
Described drain tap and a gasoline tank connect.
The invention has the beneficial effects as follows: the oil droplet filter packing of the present invention uses can at ceramic grain surface one layer of oleophylic paint of painting
Oil droplet in effective absorption oil gas, and then make oil droplet absorption pool liquid, and by using the oil gas of this oil droplet filter packing to return
Receiving unit carries out petroleum vapor recovery, and this oil-gas recovery device has simple in construction, the advantage that the easy to maintenance and rate of recovery is high.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of a kind of oil-gas recovery device utilizing oil droplet filter packing of the present invention.
In figure: 1 stuffing box, 2 supporting networks, 3 without leakage of oil orifice plate, 4 band leakage of oil orifice plates, and 5 oil guide groove, 6 air intake ducts, 7 let out
Hydraulic fluid port, 8 oil and gas imports, 9 top covers, 10 exhaust outlets, 11 spark arresters, 12 intake valves, 13 tapping valves, 14 oil droplets filter
Filler, 15 gasoline tanks.
Detailed description of the invention
Below in conjunction with Figure of description, the invention will be further described, so that advantages and features of the invention can be easier to by this
Artisans understand that of field, thus protection scope of the present invention is done apparent defining.
Embodiment 1, a kind of oil droplet filter packing, including ceramic particle, described ceramic particle is spheroidal, described ceramic particle
Particle diameter variable, for obtaining different porositys.One layer of oleophylic paint is scribbled on the surface of described spheroidal ceramic particle；Institute
State the powder shape aluminosilicate that oleophylic paint includes 30% according to percentage by weight, the VARISOFT TA100 of 3%, 8%
Sodium silicate, the water of surplus.
The preparation method of above-mentioned a kind of oil droplet filter packing, its preparation method comprises the following steps:
Step one: preparation surfacer, puts into powder shape aluminosilicate in water, disperses under normal temperature, add quaternary ammonium salt and sodium water
Glass, stirs reactant liquor 22 hours under 300rpm rotating speed under 20 DEG C of normal pressures after fully dissolving, obtains oleophylic after filtering
Paint；
Step 2: the oleophylic paint that step one prepares is coated in described ceramic grain surface uniformly；
Step 3: surface uniform application is crossed described ceramic particle heat drying at a temperature of 65 DEG C of oleophylic paint, it is thus achieved that pottery
Porcelain particle oil droplet filter packing.
As it is shown in figure 1, a kind of high-efficiency condensation oil-gas recovery device, including stuffing box 1, also include that above-mentioned a kind of oil droplet filters and fill out
A kind of oil droplet filter packing prepared by the preparation method of material, is provided with in the middle part of stuffing box 1 and is obliquely installed packing support net 2, supporting network 2
Lower section is provided with the oil collection plate parallel with supporting network 2, oil collection plate be divided into be positioned on incline direction half side without leakage of oil orifice plate 3 and position
Band leakage of oil orifice plate 4 half side under incline direction, the parallel oil guide groove 5 that is provided with, oil guide groove 5 and oil collection plate in the downside of oil collection plate
Between form air intake duct 6, be provided with drain tap 7 bottom the 5 of oil guide groove with stuffing box 1 sidewall junction, the top of oil guide groove 5 with
Stuffing box 1 sidewall junction is provided with oil and gas import 8, is provided with condenser (not shown) between oil and gas import 6 and stuffing box 1；
Supporting network 2 is arranged above packing area, and packing area is arranged over top cover 9, is provided with exhaust outlet 10, exhaust outlet 10 sets in the middle part of top cover 9
Having spark arrester 11, oil and gas import 8 to be provided with intake valve 12, drain tap 7 is provided with tapping valve 13, drain tap 7 and gasoline tank 15
Connect.
Embodiment 2, a kind of oil droplet filter packing, including ceramic particle, described ceramic particle is spheroidal, described ceramic particle
Particle diameter variable, for obtaining different porositys.One layer of oleophylic paint is scribbled on the surface of described spheroidal ceramic particle；Institute
State the powder shape aluminosilicate that oleophylic paint includes 40% according to percentage by weight, the VARISOFT TA100 of 5%, 15%
Sodium silicate, the water of surplus.
The preparation method of above-mentioned a kind of oil droplet filter packing, its preparation method comprises the following steps:
Step one: preparation surfacer, puts into powder shape aluminosilicate in water, disperses under normal temperature, add quaternary ammonium salt and sodium water
Glass, stirs reactant liquor 24 hours under 400rpm rotating speed under 100 DEG C of normal pressures after fully dissolving, obtains parent after filtering
Oil paint；
Step 2: the oleophylic paint that step one prepares is coated in described ceramic grain surface uniformly；
Step 3: surface uniform application is crossed described ceramic particle heat drying at a temperature of 75 DEG C of oleophylic paint, it is thus achieved that pottery
Porcelain particle oil droplet filter packing.
As it is shown in figure 1, a kind of high-efficiency condensation oil-gas recovery device, including stuffing box 1, also include that above-mentioned a kind of oil droplet filters and fill out
A kind of oil droplet filter packing prepared by the preparation method of material, is provided with in the middle part of stuffing box 1 and is obliquely installed packing support net 2, supporting network 2
Lower section is provided with the oil collection plate parallel with supporting network 2, oil collection plate be divided into be positioned on incline direction half side without leakage of oil orifice plate 3 and position
Band leakage of oil orifice plate 4 half side under incline direction, the parallel oil guide groove 5 that is provided with, oil guide groove 5 and oil collection plate in the downside of oil collection plate
Between form air intake duct 6, be provided with drain tap 7 bottom the 5 of oil guide groove with stuffing box 1 sidewall junction, the top of oil guide groove 5 with
Stuffing box 1 sidewall junction is provided with oil and gas import 8, is provided with condenser (not shown) between oil and gas import 6 and stuffing box 1；
Supporting network 2 is arranged above packing area, and packing area is arranged over top cover 9, is provided with exhaust outlet 10, exhaust outlet 10 sets in the middle part of top cover 9
Having spark arrester 11, oil and gas import 8 to be provided with intake valve 12, drain tap 7 is provided with tapping valve 13, drain tap 7 and gasoline tank 15
Connect.
For ease of the understanding of the present invention, the invention will be further described to use process below in conjunction with one:
Vaporizing oil-gas enters air intake duct 6 by oil and gas import 8, and sequentially passes through band leakage of oil orifice plate 4 and supporting network 2 enters packing area,
Tiny oil droplets in vaporizing oil-gas is travelling in the space that oil droplet filter packing 14 is formed, and the oleophylic on oil droplet filter packing 14 surface is coated with
Layer increases the probability of tiny oil droplets and oil droplet filter packing 14 collision so that tiny oil droplets can be easy at oil droplet filter packing
The surface spreading of 14 and attachment, finally congeal into bigger oil droplet coming off from oil droplet filter packing 14 surface, is dripped by supporting network 2
On oil collection plate, it flow on the slope on band leakage of oil orifice plate 4 due to gravity without the fluid on leakage of oil orifice plate 3, dripped by oil leaking hole
Fall in oil guide groove 6, finally discharge stuffing box 1 from drain tap 7 and enter gasoline tank 15.
The foregoing is only presently preferred embodiments of the present invention, be not whole embodiments of the present invention, not in order to limit this
Bright, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in this
Within bright protection domain.
In addition to technical characteristic described in specification, remaining technical characteristic is all known to a person skilled in the art technology, in order to highlight this
Bright innovative characteristics, above-mentioned technical characteristic does not repeats them here.
Claims (10)
1. an oil droplet filter packing, including ceramic particle, it is characterised in that described ceramic particle is spheroidal, at described circle
The surface of spherical ceramic particles scribbles one layer of oleophylic paint；Described oleophylic paint includes the powder shape of 30-40% according to percentage by weight
Aluminosilicate, the quaternary ammonium salt of 3%-5%, the inorganic binder of 8%-15%, the water of surplus.
A kind of oil droplet filter packing the most according to claim 1, it is characterised in that described quaternary ammonium salt is stearyl trimethyl
One in ammonium chloride, VARISOFT TA100, octadecyl ammonium chloride and lecithin.
A kind of oil droplet filter packing the most according to claim 1, it is characterised in that described inorganic binder is sodium silicate.
A kind of oil droplet filter packing the most according to claim 1, it is characterised in that preparation method comprises the following steps:
Step one: preparation surfacer, puts into powder shape aluminosilicate in water, disperses under normal temperature, add quaternary ammonium salt and sodium water
Glass, stirs reactant liquor under 5 DEG C of-60 DEG C of normal pressures after fully dissolving, and obtains oleophylic paint after filtering；
Step 2: the oleophylic paint that step one prepares is coated in described ceramic grain surface uniformly；
Step 3: surface uniform application is crossed described ceramic particle heat drying at a temperature of 65-75 DEG C of oleophylic paint, obtains
Obtain ceramic particle oil droplet filter packing.
The preparation method of a kind of oil droplet filter packing the most according to claim 4, it is characterised in that described mixing time is
22-24 hour.
The preparation method of a kind of oil droplet filter packing the most according to claim 4, it is characterised in that described speed of agitator is
300-400rpm。
7. a high-efficiency condensation oil-gas recovery device, including stuffing box, it is characterised in that also include the oil described in claim 1
Drip filter packing, be provided with the packing support net being obliquely installed in the middle part of described stuffing box, be provided with below described supporting network and described support
Net parallel oil collection plate, described oil collection plate be divided into be positioned on incline direction half side without leakage of oil orifice plate be positioned under incline direction
Half side band leakage of oil orifice plate, the parallel oil guide groove that is provided with, shape between described oil guide groove and described oil collection plate in the downside of described oil collection plate
Becoming air intake duct, the bottom of described oil guide groove and stuffing box sidewall junction to be provided with drain tap, the top of described oil guide groove is filled out with described
Hopper sidewall junction is provided with oil and gas import, is provided with condenser between oil and gas import and stuffing box；Described supporting network is arranged above filler
District, described oil droplet filter packing is positioned at described packing area, and packing area is arranged over top cover, is provided with exhaust outlet in the middle part of described top cover.
A kind of high-efficiency condensation oil-gas recovery device the most according to claim 7, it is characterised in that described oil and gas import is provided with
Intake valve, described drain tap is provided with tapping valve.
A kind of high-efficiency condensation oil-gas recovery device the most according to claim 7, it is characterised in that described exhaust outlet is provided with
Spark arrester.
A kind of high-efficiency condensation oil-gas recovery device the most according to claim 7, it is characterised in that described drain tap and one
Gasoline tank connects.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518818.1A CN105903292B (en) | 2016-07-01 | 2016-07-01 | A kind of oil droplet filter packing and high-efficiency condensation oil-gas recovery device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518818.1A CN105903292B (en) | 2016-07-01 | 2016-07-01 | A kind of oil droplet filter packing and high-efficiency condensation oil-gas recovery device |
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| Publication Number | Publication Date |
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| CN105903292A true CN105903292A (en) | 2016-08-31 |
| CN105903292B CN105903292B (en) | 2018-04-24 |
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Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2283512Y (en) * | 1997-01-22 | 1998-06-10 | 黄清福 | Air filter unit for freezing air drier |
| CN101081342A (en) * | 2007-07-04 | 2007-12-05 | 武汉理工大学 | Technics of preparing lipophilic porous ceramic filtering material |
| WO2009044965A1 (en) * | 2007-10-04 | 2009-04-09 | Chirolite Inc. | Lipophilic silicate functioning to remove foul smells and volatile organic compounds and method of preparing the same |
| WO2010076195A1 (en) * | 2008-12-15 | 2010-07-08 | Süd-Chemie AG | Method for processing waste water loaded with nitrogen |
| CN102728170A (en) * | 2012-05-28 | 2012-10-17 | 香港诺曼泰壹环保科技有限公司 | Flue gas purifying device |
| CN102826706A (en) * | 2012-09-28 | 2012-12-19 | 湖南科技大学 | Oilfield produced water treatment method and device |
| CN204058403U (en) * | 2014-06-26 | 2014-12-31 | 杨忠华 | A kind of marsh gas purifying equipment |
| CN104383719A (en) * | 2014-12-01 | 2015-03-04 | 东北石油大学 | Oil drop catcher of inverted fluidized bed |
| CN104524920A (en) * | 2014-12-24 | 2015-04-22 | 苏州绿科环保新材料有限公司 | Production method of lipophilic silicate |
| CN204745988U (en) * | 2015-06-11 | 2015-11-11 | 无锡顺达智能自动化工程股份有限公司 | Gas/water separator |
| CN204973394U (en) * | 2015-08-19 | 2016-01-20 | 威洁（石狮）中水回用技术有限公司 | Oiliness waste gas recovery equipment |
-
2016
- 2016-07-01 CN CN201610518818.1A patent/CN105903292B/en active Active
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2283512Y (en) * | 1997-01-22 | 1998-06-10 | 黄清福 | Air filter unit for freezing air drier |
| CN101081342A (en) * | 2007-07-04 | 2007-12-05 | 武汉理工大学 | Technics of preparing lipophilic porous ceramic filtering material |
| WO2009044965A1 (en) * | 2007-10-04 | 2009-04-09 | Chirolite Inc. | Lipophilic silicate functioning to remove foul smells and volatile organic compounds and method of preparing the same |
| WO2010076195A1 (en) * | 2008-12-15 | 2010-07-08 | Süd-Chemie AG | Method for processing waste water loaded with nitrogen |
| CN102728170A (en) * | 2012-05-28 | 2012-10-17 | 香港诺曼泰壹环保科技有限公司 | Flue gas purifying device |
| CN102826706A (en) * | 2012-09-28 | 2012-12-19 | 湖南科技大学 | Oilfield produced water treatment method and device |
| CN204058403U (en) * | 2014-06-26 | 2014-12-31 | 杨忠华 | A kind of marsh gas purifying equipment |
| CN104383719A (en) * | 2014-12-01 | 2015-03-04 | 东北石油大学 | Oil drop catcher of inverted fluidized bed |
| CN104524920A (en) * | 2014-12-24 | 2015-04-22 | 苏州绿科环保新材料有限公司 | Production method of lipophilic silicate |
| CN204745988U (en) * | 2015-06-11 | 2015-11-11 | 无锡顺达智能自动化工程股份有限公司 | Gas/water separator |
| CN204973394U (en) * | 2015-08-19 | 2016-01-20 | 威洁（石狮）中水回用技术有限公司 | Oiliness waste gas recovery equipment |
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| Publication number | Publication date |
|---|---|
| CN105903292B (en) | 2018-04-24 |
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