CN105902825A - Processing method of dendrobium characteristic decoction pieces - Google Patents
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- CN105902825A CN105902825A CN201610231367.3A CN201610231367A CN105902825A CN 105902825 A CN105902825 A CN 105902825A CN 201610231367 A CN201610231367 A CN 201610231367A CN 105902825 A CN105902825 A CN 105902825A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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Abstract
Belonging to the technical field of traditional Chinese medicine processing, the invention discloses a processing method of dendrobium characteristic decoction pieces. The method includes the steps of: 1) taking fresh dendrobium strips, conducting precooling washing, then putting the dendrobium strips in a high pressure resistant ethylene propylene rubber bag, and conducting sealing; 2) putting the ethylene propylene rubber bag loaded with the fresh strips into a cold water holding ultrahigh-pressure container, and carrying out pressurization and pressure maintaining; 3) taking out the fresh dendrobium strips subjected to high pressure in step 2), sucking dry the surface moisture, and placing the fresh strips in a freeze dryer cold trap to perform quick-freezing; 4) subjecting the quick-frozen fresh dendrobium strips of step 3) to vacuum sublimation; 5) beveling the fresh dendrobium strips into slices; 6) placing the slices obtained in step 5) into a cold trap to perform quick-freezing; 7) freeze-drying the quick-frozen dendrobium slices according to a set process; and 8) acquiring the dendrobium characteristic decoction pieces. The method provided by the invention can effectively improve the dissolution rate and dissolution speed of polysaccharide and dendrobine in hot water, and enhances the medicinal value and health care efficacy of dendrobium. A vacuum freeze-drying technology is employed for freeze-drying, and obviously prolongs the shelf life of the dendrobium characteristic decoction pieces.
Description
Technical field
The processing method that the present invention relates to a kind of Herba Dendrobii characteristic decoction pieces, is specifically related to one and utilizes supertension and lyophilizing work
The method of skill processing Herba Dendrobii characteristic decoction pieces (wafer thin), belongs to technical field of agricultural product process.
Background technology
Herba Dendrobii, one of orchid, as valuable medical material, it is distributed mainly on Tropical Asian and subtropical zone, Australia is big
Leah and Pacific Islands.In China, major part is distributed in the ground such as southwest, south China, Taiwan.As medical material or food
Material, its source mostly is the fresh or dry stem of the orchid family herbaceos perennial Dendrobium nobile and Herba Dendrobii；Herba Dendrobii is made
For the valuable ingredients of traditional Chinese medicine, there is reinforcing stomach reg fluid, drive solution deficiency-heat, the benefit essence curative effect such as reinforcing YIN-essence.Containing substantial amounts of stone in Herba Dendrobii
Dry measure used in former times alkali and polysaccharide slime formers matter；Wherein, dendrobine has certain pain relieving antipyretic effect, similar to phenacetin but more weak；
Dendrobium polysaccharide energy enhancing human body immunity function, and there is anti-tumor activity.
From late 1950s, Domestic Scientific Research personnel start from protection of resources, Sustainable Development and Utilization etc.
Aspect research Herba Dendrobii, having realized Herba Dendrobii from tissue cultured seedling factorial praluction, extensive standardized cultivation construction of base etc. is
Row link breaks through, it is achieved that Herba Dendrobii sustainable use and industrialization.This human world of Herba Dendrobii Herba mesonae chinensis, has been enter into ordinary hundred
The dining table of surname man, for the health service of ordinary people.But there is active substance dissolution rate in existing Herba Dendrobii dry products
The problems such as low, dissolution quick-freezing is slow, have impact on Herba Dendrobii medical value and health value, also result in Dendrobium Plants utilization rate
Low.Therefore, dendrobe fresh product is processed, improves its active substance dissolution rate when bubble drink to greatest extent
And dissolution efficiency, become the new problem of its industrial upgrading and sustainable development.
Summary of the invention
The technical problem to be solved in the present invention is the processing method proposing a kind of Herba Dendrobii characteristic decoction pieces (wafer thin), can
It is effectively improved dendrobium polysaccharide and the dendrobine dissolution rate when bubble drink and dissolution efficiency, strengthens the medicinal of Herba Dendrobii product
It is worth and health value.
For solve above-mentioned technical problem of the present invention, the present invention by the following technical solutions:
The processing method of a kind of Herba Dendrobii characteristic decoction pieces, comprises the steps:
1) take the fresh bar of Herba Dendrobii, clean, be placed in high pressure resistant polystyrene bag, sealing, standby；
2) by step 1) in put in ultrahigh pressure vessel equipped with the polystyrene bag of the fresh bar of Herba Dendrobii, pressurization, pressurize；
3) by step 2) in the fresh bar of supertension Herba Dendrobii take out, blot surface moisture, be placed in quick-freezing in freeze dryer cold-trap；
4) by step 3) in the good fresh bar of Herba Dendrobii of pre-freeze move to rapidly above cold-trap chamber, by the technique distillation set；
5) by step 4) the fresh bar of Herba Dendrobii takes out after quick-freezing, is mitered into thin slice；
6) by step 5) gained thin slice is placed in quick-freezing in cold-trap；
7) by step 6) in quick-freezing Herba Dendrobii thin slice move to rapidly above cold-trap chamber, by set technique lyophilizing；
8) by step 7) taking-up of Herba Dendrobii fresh bar characteristic decoction pieces, packaging.
As improvement, described step 1) in Herba Dendrobii fresh bar cold water wash, and load containing cold water high pressure resistant poly-
In third vinyl bag.
As improvement, described step 2) applied in pressure be 300～500MPa, the dwell time is 20s～1
min。
As improvement, described step 3) in fast freezing conditions be: layer thickness is 10～30mm, is down to stone in temperature
Freezing more than 1h is continued after dry measure used in former times eutectic point.
As improvement, step 4) in sublimation condition be :-10～-5 DEG C of dry more than 2h.
As improvement, step 5) in the fresh bar of Herba Dendrobii be cut into 1～2mm thin slice by the oblique angle of 10～20 °.
As improvement, step 6) in Herba Dendrobii thin slice fast freezing conditions be: layer thickness is 10～30mm, temperature drop
More than 1h is maintained to eutectic point.
As improvement, step 7) in the lyophilizing technique that sets of Herba Dendrobii thin slice as :-10～-5 DEG C of dry more than 2h,
10～15 DEG C of dry more than 2h, 30～35 DEG C of dry more than 2h.
As improvement, step 8) in the Herba Dendrobii of lyophilizing take out in the container loading polystyrene plastics bag or sealing,
Sealing preservation.
The beneficial effects of the present invention is:
After ultra high pressure treatment, active substance dendrobium polysaccharide and the stripping quantity of dendrobine and dissolution in Herba Dendrobii characteristic decoction pieces
Speed all dramatically increases at hot water bubble drink.
Detailed description of the invention
Following embodiment is to further illustrate using as the explaination to the technology of the present invention content for present invention,
But the flesh and blood of the present invention is not limited in described in following embodiment, those of ordinary skill in the art can and should
When know any simple change based on true spirit or replace all should belong to protection model of the presently claimed invention
Enclose.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces, comprises the steps:
1) dendrobe fresh product is taken, defoliation, take fresh bar, after cleaning with cold water, load high pressure resistant poly-third second filling cold water
In alkene bag, sealing；
2) in ultrahigh pressure vessel load cold water, put into step 1) in the polystyrene bag equipped with the fresh bar of Herba Dendrobii,
It is forced into 300～500MPa, and pressurize 20s～1min, pressure release；
3) by step 2) in the fresh bar of supertension Herba Dendrobii take out, blot surface moisture, be placed in freeze dryer cold-trap, paving
Material thickness is 10～30mm, opens compressor, after quick freezing temperature is down to Herba Dendrobii eutectic point, continue freezing 1h with
On；
4) by step 3) the fresh bar of middling speed lardite dry measure used in former times takes out, and moves to rapidly above freeze dryer cold-trap chamber, in-10～-5 DEG C
It is dried more than 2h；
5) by step 4) in the fresh bar of Herba Dendrobii take out, be cut into 1～2mm thin slice by the corner cut of 10～20 °；
6) by step 5) in Herba Dendrobii thin slice move in the cold well of freeze dryer, layer thickness is 10～30mm, and startup is frozen
Dry machine, temperature maintains more than 1h after being down to eutectic point；
7) by step 6) middling speed lardite dry measure used in former times thin slice moves to rapidly above freeze dryer cold-trap chamber, it is dried in-10～-5 DEG C
More than 2h, 10～15 DEG C of dry more than 2h, 30～35 DEG C of dry more than 2h；
8) by step 7) in Herba Dendrobii thin slice take out in the container loading polystyrene plastics bag or sealing, sealing preservation.
The present invention uses the pressure bar fresh to Herba Dendrobii of 300～500MPa to carry out processing 20s～1min, can destroy stone
Adhesion between the matter structure of dry measure used in former times and active substance, hence it is evident that increase the dissolution when hot water bubble drink of dendrobium polysaccharide and dendrobine
Speed and dissolution efficiency.
Supertension and Vacuum Freezing & Drying Technology are combined processing Herba Dendrobii characteristic decoction pieces, the Herba Dendrobii of gained by the present invention
Characteristic decoction pieces long shelf-life, color and luster is fresh.
Embodiment one
As a example by Herba Dendrobii, specifically comprise the following steps that
1) iron-sheet dendrobe fresh product is taken, defoliation, take fresh bar, after cleaning with cold water, load and fill the high pressure resistant poly-of cold water
In third vinyl bag, sealing；
2) in ultrahigh pressure vessel, load cold water, put into step 1) in equipped with the polystyrene bag of the fresh bar of Herba Dendrobii,
It is forced into 400MPa, pressurize 20s, pressure release；
3) by step 2) in ultra high pressure treatment the fresh bar of Herba Dendrobii take out, blot surface moisture, be placed in freeze dryer
Cold well in, layer thickness is 10mm, opens compressor, after freeze temperature is down to Herba Dendrobii eutectic point,
Continue freezing 1h；
4) by step 3) in the fresh bar of quick-freezing Herba Dendrobii take out, move to rapidly above freeze dryer cold-trap chamber, in-10 DEG C
It is dried 2h；
5) by step 4) in the fresh bar of Herba Dendrobii take out, be cut into 1mm thin slice by the corner cut of 10 °；
6) by step 5) in Herba Dendrobii thin slice move in the cold well of freeze dryer, layer thickness is 30mm, and startup is frozen
Dry machine, maintains 1h after reaching eutectic point；
7) by step 6) in quick-freezing Herba Dendrobii thin slice move to rapidly above freeze dryer cold-trap chamber, in-10 DEG C be dried
2h, 10 DEG C of dry 2h, 30 DEG C of dry 2h；
8) by step 7) in the Herba Dendrobii thin slice of lyophilizing take out in the container loading polystyrene plastics bag or sealing,
Sealing preservation.
The result preparing Herba Dendrobii characteristic decoction pieces is as shown in table 1.
Polysaccharide and dendrobine dissolution efficiency in 100 DEG C of hot water in table 1 Herba Dendrobii characteristic decoction pieces
* P < 0.01, difference is the most notable compared with hot dry products
Embodiment two
As a example by Herba Dendrobii, specifically comprise the following steps that
1) iron-sheet dendrobe fresh product is taken, defoliation, take fresh bar, clean with cold water, load and fill high pressure resistant poly-the third of cold water
In vinyl bag, sealing；
2) in ultrahigh pressure vessel, load cold water, put into step 1) in equipped with the polystyrene bag of the fresh bar of Herba Dendrobii,
After being forced into 500MPa, pressurize 1min, pressure release；
3) by step 2) in the fresh bar of supertension Herba Dendrobii take out, blot surface moisture, be placed in the cold well of freeze dryer
In, layer thickness is 30mm, opens compressor, continues freezing 3h after quick freezing temperature is down to eutectic point；
4) by step 3) in quick-freezing Herba Dendrobii take out, move to rapidly above freeze dryer cold-trap chamber, in-5 DEG C do
Dry 4h；
5) by step 4) in the fresh bar of Herba Dendrobii take out, be cut into the thin slice of about 2mm by the oblique angle of 20 °；
6) by step 5) in Herba Dendrobii thin slice move in the cold well of freeze dryer, layer thickness is 10mm, opens pressure
Contracting machine, continues freezing 2h after quick freezing temperature is down to eutectic point；
7) by step 6) in Herba Dendrobii wafer thin move to above freeze dryer cold-trap chamber, in-5 DEG C of dry 2h, 15 DEG C
It is dried 3h, 35 DEG C of dry 4h；
8) by step 7) in the Herba Dendrobii thin slice of lyophilizing take out, load polystyrene plastics bag or the container of sealing
In, sealing preservation.
The result preparing Herba Dendrobii characteristic decoction pieces is as shown in table 2.
Polysaccharide and dendrobine dissolution efficiency in 100 DEG C of hot water in table 2 Herba Dendrobii characteristic decoction pieces
* P < 0.01, difference is the most notable compared with hot dry products
Embodiment three
As a example by Herba Dendrobii, specifically comprise the following steps that
1) iron-sheet dendrobe fresh product is taken, defoliation, take fresh bar, clean with cold water, load and fill high pressure resistant poly-the third of cold water
In vinyl bag, sealing；
2) in ultrahigh pressure vessel, load cold water, put into step 1) in equipped with the polystyrene bag of the fresh bar of Herba Dendrobii,
After being forced into 300MPa, pressurize 40s, pressure release；
3) by step 2) in the fresh bar of supertension Herba Dendrobii take out, blot surface moisture, be placed in the cold well of freeze dryer
In, layer thickness is 15mm, opens compressor, continues freezing 2h after quick freezing temperature is down to eutectic point；
4) by step 3) in quick-freezing Herba Dendrobii take out, move to rapidly above freeze dryer cold-trap chamber, in-5 DEG C do
Dry 3h；
5) by step 4) in the fresh bar of Herba Dendrobii take out, be cut into the thin slice of about 1.5mm by the oblique angle of 15 °；
6) by step 5) in Herba Dendrobii thin slice move in the cold well of freeze dryer, layer thickness is 15mm, opens pressure
Contracting machine, continues freezing 1.5h after quick freezing temperature is down to eutectic point；
7) by step 6) in Herba Dendrobii wafer thin move to above freeze dryer cold-trap chamber, in-10 DEG C of dry 3h, 10 DEG C
It is dried 2h, 33 DEG C of dry 2h；
8) by step 7) in the Herba Dendrobii thin slice of lyophilizing take out, load polystyrene plastics bag or the container of sealing
In, sealing preservation.
The result preparing Herba Dendrobii characteristic decoction pieces is as shown in table 3.
Polysaccharide and dendrobine dissolution efficiency in 100 DEG C of hot water in table 3 Herba Dendrobii characteristic decoction pieces
* P < 0.01, difference is the most notable compared with hot dry products
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and
Without departing from the spirit or essential characteristics of the present invention, it is possible to realize the present invention in other specific forms.
Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, this
The scope of invention is limited by claims rather than described above, it is intended that by the equivalent in claim that falls
All changes in the implication of important document and scope are included in the present invention.
Claims (9)
1. the processing method of a Herba Dendrobii characteristic decoction pieces, it is characterised in that comprise the steps:
1) take the fresh bar of Herba Dendrobii, clean, be placed in high pressure resistant polystyrene bag, sealing, standby；
2) polystyrene bag equipped with the fresh bar of Herba Dendrobii in step 1) is put in ultrahigh pressure vessel, pressurization, pressurize；
3) by step 2) in the fresh bar of supertension Herba Dendrobii take out, blot surface moisture, be placed in quick-freezing in freeze dryer cold-trap；
4) the fresh bar of Herba Dendrobii that pre-freeze in step 3) is good is moved to rapidly above cold-trap chamber, by the technique distillation set；
5) the fresh bar of Herba Dendrobii after step 4) quick-freezing is taken out, be mitered into thin slice；
6) step 5) gained thin slice is placed in quick-freezing in cold-trap；
7) the quick-freezing Herba Dendrobii thin slice in step 6) is moved to rapidly above cold-trap chamber, by the technique lyophilizing set；
8) fresh for step 7) Herba Dendrobii bar characteristic decoction pieces is taken out, packaging.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that the Herba Dendrobii fresh bar cold water wash in described step 1), and load in the high pressure resistant polystyrene bag containing cold water.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that described step 2) applied in pressure be 300～500 MPa, the dwell time is 20
S～1 min.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that in described step 3), fast freezing conditions is: layer thickness is 10 ~ 30 mm, continues freezing 1 more than h after temperature is down to Herba Dendrobii eutectic point.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that in step 4), sublimation condition is :-10 ~-5 DEG C are dried 2 more than h.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that in step 5), the fresh bar of Herba Dendrobii is cut into 1 ~ 2 mm thin slice by the oblique angle of 10 ~ 20 °.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that in step 6), Herba Dendrobii thin slice fast freezing conditions is: layer thickness is 10 ~ 30 mm, maintains 1 more than h after temperature is down to eutectic point.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that the lyophilizing technique that in step 7), Herba Dendrobii thin slice sets as :-10 ~-5 DEG C be dried 2 more than h, 10 ~ 15
DEG C be dried 2 more than h, 30 ~ 35 DEG C be dried 2 more than h.
The processing method of a kind of Herba Dendrobii characteristic decoction pieces the most as claimed in claim 1, it is characterised in that the Herba Dendrobii of lyophilizing in step 8) takes out in the container loading polystyrene plastics bag or sealing, sealing preservation.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106692703A (en) * | 2017-03-17 | 2017-05-24 | 贵州健瑞安药业有限公司 | Preparation method of dendrobium freeze-dried powder |
| CN107753751A (en) * | 2017-09-27 | 2018-03-06 | 霍山县长冲中药材开发有限公司 | A kind of processing method of stem of noble dendrobium medicine materical crude slice |
| CN108992585A (en) * | 2018-09-14 | 2018-12-14 | 滁州学院 | A kind of processing method of dendrobium nobile fresh medicine lozenge |
| CN108991331A (en) * | 2018-06-27 | 2018-12-14 | 广西驰胜农业科技有限公司 | A kind of dendrobium candidum medicine materical crude slice and its preparation method and application |
| CN109105587A (en) * | 2017-06-22 | 2019-01-01 | 广西壮族自治区中医药研究院 | The tea bag and preparation method thereof of effect is relieved fatigue with strengthen immunity |
| CN109105779A (en) * | 2017-06-22 | 2019-01-01 | 广西壮族自治区中医药研究院 | A kind of preparation method of Noni fruit freeze-drying dried fruit |
| CN110559395A (en) * | 2019-09-12 | 2019-12-13 | 厦门涌泉科技有限公司 | Preparation method of dendrobium instant freeze-dried block |
| CN111426149A (en) * | 2020-03-27 | 2020-07-17 | 广西农业职业技术学院 | Dendrobium officinale freeze-drying method |
| CN114306513A (en) * | 2021-11-30 | 2022-04-12 | 安徽省双辉生物科技有限公司 | Production process of low-oxidation dried dendrobium |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106692703A (en) * | 2017-03-17 | 2017-05-24 | 贵州健瑞安药业有限公司 | Preparation method of dendrobium freeze-dried powder |
| CN109105587A (en) * | 2017-06-22 | 2019-01-01 | 广西壮族自治区中医药研究院 | The tea bag and preparation method thereof of effect is relieved fatigue with strengthen immunity |
| CN109105779A (en) * | 2017-06-22 | 2019-01-01 | 广西壮族自治区中医药研究院 | A kind of preparation method of Noni fruit freeze-drying dried fruit |
| CN107753751A (en) * | 2017-09-27 | 2018-03-06 | 霍山县长冲中药材开发有限公司 | A kind of processing method of stem of noble dendrobium medicine materical crude slice |
| CN108991331A (en) * | 2018-06-27 | 2018-12-14 | 广西驰胜农业科技有限公司 | A kind of dendrobium candidum medicine materical crude slice and its preparation method and application |
| CN108992585A (en) * | 2018-09-14 | 2018-12-14 | 滁州学院 | A kind of processing method of dendrobium nobile fresh medicine lozenge |
| CN110559395A (en) * | 2019-09-12 | 2019-12-13 | 厦门涌泉科技有限公司 | Preparation method of dendrobium instant freeze-dried block |
| CN110559395B (en) * | 2019-09-12 | 2022-02-08 | 厦门涌泉科技有限公司 | Preparation method of dendrobium instant freeze-dried block |
| CN111426149A (en) * | 2020-03-27 | 2020-07-17 | 广西农业职业技术学院 | Dendrobium officinale freeze-drying method |
| CN114306513A (en) * | 2021-11-30 | 2022-04-12 | 安徽省双辉生物科技有限公司 | Production process of low-oxidation dried dendrobium |
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