CN105902456A

CN105902456A - Moisturizing and moistening mask containing wild apricots and eucommia and preparation method thereof

Info

Publication number: CN105902456A
Application number: CN201610515436.3A
Authority: CN
Inventors: 乌云塔娜; 朱绪春; 杜红岩; 李铁柱; 朱高浦; 赵罕
Original assignee: PAULOWNIA RESEARCH AND DEVELOPMENT CENTRE STATE FOREST BUREAU
Current assignee: PAULOWNIA RESEARCH AND DEVELOPMENT CENTRE STATE FOREST BUREAU
Priority date: 2016-07-02
Filing date: 2016-07-02
Publication date: 2016-08-31

Abstract

The invention discloses a moisturizing and moistening mask containing wild apricots and eucommia and a preparation method thereof. The mask comprises the following components: an emulsifying agent, a co-emulsifying agent, a skin moistening agent, a solvent, a thickening agent, a moisturizing agent, a preservative, a neutralizing agent, a skin conditioner and an aromatic. According to the invention, apricot oil and eucommia seed oil are effectively combined, so that the ageing resistance of the skin is greatly increased, the elasticity of the skin is kept, and the allergic reaction of the skin is effectively reduced; cherry blossom extract is added to serve as the moisturizing agent, and natural moisturizing ingredients are artificially synthesized into a moisturizing ingredient compound, so that the moisturizing time of the skin is greatly prolonged; and the cherry blossom extract contains cherry blossom pink baby, so that the skin can be further moistened.

Description

A kind of Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask and preparation method thereof

Technical field

The present invention relates to daily use chemicals product field.More particularly, to a kind of Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask and preparation side thereof Method.

Background technology

Along with progress and the fast development of science and technology of society, the problem such as environmental problem, operating pressure instead of purple gradually External exposure becomes the arch-criminal of injury people's skin.Healthy skin has smooth, full, the big key element of high resilience three.But, Environmental pollution, haze dust, computer radiate etc. make our skin of face be dried hydropenia, pore secretion unbalance, dull aging with And corse sweat pore etc.；Along with the growth at age, our skin of face can be made to relax, tarnish.These are for modern society For quality of life being required tighter people with beauty, it it is the insoluble difficult problem faced.

The ratio that cosmetics account in people's daily life is also come the biggest, and the kind of cosmetics gets more and more, function and pin Property is also come the strongest, as China's fastest-rising facial film of daily use chemicals industry, also become product that people seeking beauty increasingly favors it One.Facial film development speed is fast, and with its functional diversities more than kind, diversification of forms is all undivided.Relatively other are made up Product, facial film substantially can solve moisturizing, whitening, gentle oils and fats, antiallergic sense and anti-ageing skin Five problems of waiting for a long time simultaneously.Face Film has the various ways such as powder face pack, the membranaceous facial film of cream pack.

Facial film mainly plays skin nursing effect by three kinds of modes, is first package effect, when facial film covers in face During skin surface, make to be locally isolated between outside air and skin of face, suppress sebum secretion, stop sweat evaporation, improve face Portion's skin temperature, promotes the blood circulation of skin surface, makes the nutrition skin-protection composition in facial film preferably be absorbed.Secondly, Being water sorption, facial film can increase the concentration difference inside and outside keratodermatitis, makes the more moisture of skin absorption, and some are easy It is dissolved in the small-molecule substance of water.3rd, the viscous glutinous effect of absorption, when removing facial film, can be by skin surface and pore Dirt and metabolite are together removed, and make skin follicle unimpeded, keep skin clean, away from problems such as cysts.

Main flow facial film in the market, is the most also the effects such as leading moisturizing, whitening, skin protection, but the moisturizing of facial film Time is shorter, it is more difficult to reach the effect of skin care.

Summary of the invention

It is an object of the present invention to provide a kind of moistening effect good, the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisture saver mask of skin care simultaneously And preparation method thereof.

For reaching above-mentioned purpose, the present invention uses following technical proposals:

A kind of Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, is made up of following component: emulsifying agent, co-emulsifier, emollient, solvent, Thickening agent, wetting agent, preservative, nertralizer, skin conditioning agent and aromatic.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described emulsifying agent is the mixed of ceteareth-6 and olive oil acid esters Compound, the mass ratio of ceteareth-6 and olive oil acid esters is: 1:4～1, and described co-emulsifier is cetearyl alcohol.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described emollient is caprylic/capric triglyceride (GTCC), Palmic acid second The volume ratio of the own ester of base, vitamin E acetate, almond oil and the mixture of Eucommia Oil, almond oil and Eucommia Oil is 6～1:1.

Above-mentioned GTCC is commercially available prod, buys in Yu Xuan bio tech ltd, Guangzhou.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described solvent is water, and described thickening agent is carbomer, and described preservative is The mass ratio of phenyl phenol & ethylhexyl glycerol (PE9010) and methyl hydroxybenzoate, PE9010 and methyl hydroxybenzoate is 5～1: 1, described nertralizer is triethanolamine, and described aromatic is essence.

Above-mentioned PE9010 is commercially available prod, buys in Guangdong Zhong Peng Chemical Co., Ltd..

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described wetting agent is glycerol, propylene glycol and oriental cherry extract, described oriental cherry Extract is water, butanediol and the mixture of Sakura leaf extract, and the mass ratio of water, butanediol and Sakura leaf extract is: 15: 2.4:1.6, the extracting method of Sakura leaf extract is as follows: (1) Sakura leaf is dried, is ground into foam, obtains Sakura leaf foam；(2) use Ethanol or acetic acid ethyl dissolution Sakura leaf foam, heating and refluxing extraction 2～6 hours, concentrated extracting solution obtains crude extract 1；(3) by step (2) residue after extraction in decocting in water 5～12 hours, be concentrated to give crude extract 2；(3) crude extract 1 and crude extract 2 are mixed, With ethanol or acetic acid ethyl dissolution, it is heated to reflux 3～6 hours, is concentrated to give Sakura leaf extract.

Above-mentioned Fructus Pruni Cortex Eucommiae moisturizing mask, described skin conditioning agent includes that fragrant quick easypro, plant Shu Min agent and Radix Angelicae Sinensis carry Take thing mixture.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described fragrant quick relaxes for bisabolol and ginger-root extract, bisabolol and The mass ratio of ginger-root extract is 4:1, and the extracting method of ginger-root extract is as follows: (1) race dries, is ground into foam, obtains Race foam；(2) with ethanol or acetic acid ethyl dissolution race foam, heating and refluxing extraction 2～5 hours, concentrated extracting solution obtains crude extract 1；(3) by the residue after the extraction in step (2) decocting in water 5～10 hours, it is concentrated to give crude extract 2；(4) by crude extract 1 He Crude extract 2 mixes, and with ethanol or acetic acid ethyl dissolution, is heated to reflux 2～6 hours, is concentrated to give ginger-root extract；Described plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae extract, water, glycerol, sea The mass ratio of algae sugar, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae extract is: 25:3:1.3:0.8:1.2: 0.9, the extracting method of Radix Ophiopogonis extract is as follows: (1) Radix Ophiopogonis dries, is ground into foam, obtains foam Radix Ophiopogonis；(2) with ethanol or acetic acid Ethyl ester dissolves foam Radix Ophiopogonis, and heating and refluxing extraction 3～5 hours, concentrated extracting solution obtains crude extract 1；(3) by the extraction in step (2) After residue decocting in water 4～10 hours, be concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, by ethanol or second Acetoacetic ester dissolves, and is heated to reflux 2～5 hours, is concentrated to give Radix Ophiopogonis extract；The extracting method of Opuntia Streptacantha stem extract is such as Under: (1) Opuntia Streptacantha stem dries, is ground into foam, obtains Opuntia Streptacantha stem foam；(2) turn round with ethanol or acetic acid ethyl dissolution Thorn Cactus Pedicel foam, heating and refluxing extraction 3～8 hours, concentrated extracting solution obtains crude extract 1；(3) by after the extraction in step (2) Residue decocting in water 5～12 hours, be concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid Ethyl ester dissolves, and is heated to reflux 3～6 hours, is concentrated to give Opuntia Streptacantha stem extract；The extracting method of radix sophorae extract is such as Under: (1) radix sophorae dries, is ground into foam, obtains radix sophorae foam；(2) with ethanol or acetic acid ethyl dissolution radix sophorae foam, heat back Stream extracts 2～6 hours, and concentrated extracting solution obtains crude extract 1；(3) by little for the residue decocting in water 5～12 after the extraction in step (2) Time, it is concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid ethyl dissolution, be heated to reflux 3～ 6 hours, it is concentrated to give radix sophorae extract；, described Radix Angelicae Sinensis extract mixture is the mixing of water, butanediol and Radix Angelicae Sinensis extract Thing, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract is: 10:1.5:1.4, and the extracting method of Radix Angelicae Sinensis extract is as follows: (1) Radix Angelicae Sinensis dries, is ground into foam, obtains Radix Angelicae Sinensis foam；(2) with ethanol or acetic acid ethyl dissolution Radix Angelicae Sinensis foam, heating and refluxing extraction 4～ 6 hours, concentrated extracting solution obtained crude extract 1；(3) by the residue after the extraction in step (2) decocting in water 3～9 hours, it is concentrated to give Crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid ethyl dissolution, be heated to reflux 3～7 hours, concentrate Obtain Radix Angelicae Sinensis extract.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, described emulsifying agent is the mixed of ceteareth-6 and olive oil acid esters Compound, described co-emulsifier is cetearyl alcohol, and described emollient is GTCC, ethylhexyl palmitate, vitamin E acetate, almond oil With the mixture of Eucommia Oil, described solvent is water, and described thickening agent is carbomer, and described wetting agent is glycerol, propylene glycol and cherry Flower extract, described preservative is PE9010 and methyl hydroxybenzoate, and described nertralizer is triethanolamine, and described aromatic is essence, Described skin conditioning agent includes fragrant quick easypro, plant Shu Min agent and Radix Angelicae Sinensis extract mixture.

Above-mentioned Fructus Pruni Cortex Eucommiae moisturizing mask, including the component of following weight fraction: ceteareth-6 and Fructus Canarii albi The mixture 1.4～2.6% of oleate, cetearyl alcohol 0.05～0.16%, GTCC1.5～2.5%, ethylhexyl palmitate 1.5～2.5%, vitamin E acetate 0.25～0.35%, the mixture 0.4～0.6% of almond oil and Eucommia Oil, water 50～80%, Carbomer 0.04～0.15%, glycerol 4.5～5.6%, propylene glycol 4.5～5.6%, triethanolamine 0.04～0.15%, PE9010 and methyl hydroxybenzoate 0.29～0.51%, fragrant quick easypro 0.10～0.20%, plant Shu Min agent 0.15～0.25%, essence 0.01～0.03%, oriental cherry extract 0.05～0.15%, Radix Angelicae Sinensis extract mixture 0.05～0.15%.

Above-mentioned Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive The mixture 2% of olive oleate, cetearyl alcohol 0.1%, GTCC2%, ethylhexyl palmitate 2%, vitamin E acetate 0.3%, The mixture 0.5% of almond oil and Eucommia Oil, water 78.35%, carbomer 0.1%, glycerol 5%, propylene glycol 5%, triethanolamine 0.08%, PE9010 and methyl hydroxybenzoate 0.4%, fragrant quick easypro 0.15%, plant Shu Min agent 2%, essence 0.02%, oriental cherry extract 1%, Radix Angelicae Sinensis extract mixture 1%.

The preparation method of Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, comprises the steps:

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl The mixture of own ester, vitamin E acetate and almond oil and Eucommia Oil joins in emulsifying pot, is heated to 75 DEG C, and stirring is to the most molten Melt；

(2) water, carbomer, glycerol, propylene glycol and methyl hydroxybenzoate being joined in aqueous phase pot, be heated to 75 DEG C, stirring is extremely Mix homogeneously, and be completely dissolved；

(3) by the solution suction emulsifying pot in step (2), keeping pot inner pressure is 5～20 handkerchiefs, homogenizing 3min, cooling；

(4) raw material in step (3) is cooled to 60 DEG C add triethanolamine, PE9010 and fragrant quick relax, stir；

(5) raw material in step (4) is cooled to 45 DEG C of addition plant Shu Min agent, essence, oriental cherry extract and Radix Angelicae Sinensis carry Take thing mixture, stir；

(6) discharging after the raw material in step (5) being cooled to 40 DEG C, obtains Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask.

The preparation method of eucommia ulmoides seed oil of the present invention is as follows:

(1) supercritical CO is used₂Extraction process acquisition seed of bark of eucommia crude oil:

(1-1) seed of bark of eucommia supercritical CO₂The pre-treatment of extraction: seed of bark of eucommia is dried and pulverized 40 mesh sieves and obtains seed of bark of eucommia Powder, first seed of bark of eucommia powder is immersed in temperature be 50-60 DEG C, polyvinyl alcohol mass fraction be 2-4wt% poly-vinyl alcohol solution in 0.5-1 hour, seed of bark of eucommia powder soak while carry out supersound process, ultrasonic frequency is 35KMz, ultrasonic power be 260～ 400W, filters and is dried to obtain seed of bark of eucommia powder, and polyvinyl alcohol is polyvinyl alcohol 1788 or polyvinyl alcohol 1799；Poly-vinyl alcohol solution Preparation method is as follows: be soaked in by polyvinyl alcohol in the ethanol solution that ethanol mass fraction is 70-85wt% 12-24 hour, mistake Filter is dried, and is then joined by the polyvinyl alcohol obtained in the water of 50-60 DEG C, and heated and stirred i.e. obtains poly-vinyl alcohol solution in 1 hour

(1-2) seed of bark of eucommia powder supercritical CO₂Extraction: the seed of bark of eucommia powder obtained in step (1-1) is put in extraction kettle, Extraction process uses ethanol or ethanol volumetric concentration be 30～80% aqueous solution be entrainer, entrainer flow velocity is 1-3mL/ min；When being entrainer when using ethanol water, first the aqueous solution that ethanol volumetric concentration is 30% is passed through in extraction kettle, The most successively the aqueous solution that ethanol volumetric concentration is 40%, 50%, 60%, 70% and 80% is joined in extraction kettle, ethanol Aqueous solution that aqueous solution that volumetric concentration is 30%, ethanol volumetric concentration are 40%, ethanol volumetric concentration be 50% aqueous solution, Ethanol volumetric concentration be 60% aqueous solution, ethanol volumetric concentration be 70% aqueous solution and ethanol volumetric concentration be the water of 80% The ratio of the time that six kinds of ethanol waters of solution are passed through extraction kettle is: 2:3:1:1:1:2；Extracting pressure is 25～35MPa, extraction Temperature is 45～50 DEG C, and extraction time is 1.5～2.5h, and separating pressure is 6～7MPa, and separation temperature is 45～50 DEG C, obtains Seed of bark of eucommia crude oil；

(2) refine of seed of bark of eucommia crude oil, specifically comprises the following steps that

(2-1) being placed in heating tank by seed of bark of eucommia crude oil, be warming up to 60～70 DEG C, adding weight is seed of bark of eucommia crude oil weight 0.05-0.25wt ‰, concentration are the phosphoric acid of 80-90wt%, react 45～55min；

(2-2) the seed of bark of eucommia crude oil in heating tank is proceeded in outer tank, add the alkali liquor prepared in advance immediately, pour into Alkali liquor at the uniform velocity stirs on one side, and mixing speed is 40～50 turns/min, reacts 10～15min, settles 4～6h；

In this step: alkali liquor is NaOH solution, NaOH solution is 3:1～5:1/mL:g with the ratio of seed of bark of eucommia crude oil；Alkali Changing temperature is 70～80 DEG C；

In this step: total alkali consumption calculates according to the following steps:

A. theoretical caustic dosage N:N=7.13 × 10^-4× AV × Q, Q are Kg/h for oil flow, unit, and AV is seed of bark of eucommia crude oil Acid number, unit be mgNaOH/g；

B. phosphoric acid alkali consumption NP: owing to the addition of phosphoric acid in the degumming of this technique, therefore alkali liquor interpolation is considered as neutralising phosphoric acid consumption Alkali number；NP=1.22 × W, W are H₃PO₄Addition, unit are Kg/h, and the amount of phosphoric acid is pure phosphoric acid amount here；

C. excess alkali quantity NC: excess alkali is the 0.25～0.5wt% of oil mass, NC=Q × 25%, and Q for oil flow, unit is Kg/h；

Actual caustic soda amount NS: due to the Caustic soda purity on market, therefore should be according to its NaOH actual content when calculating Convert: the NaOH percentage composition of actual caustic soda amount NS=(N+NP+NC)/commercially available alkali；

(2-3) taking supernatant, adding NaCl mass fraction is the NaCl solution of 0.5-1.5wt%, NaCl solution addition For seed of bark of eucommia crude oil weight 5-15wt%, at the uniform velocity stir, rotating speed 40～50 turns/min, settle 2h；

(2-4) taking supernatant, be 0.06～0.095Mpa in vacuum, temperature is dried under conditions of being 90～110 DEG C；

(2-5) entering bleacher, in bleacher, vacuum is 0.06～0.095Mpa, and temperature is 90～110 DEG C, toward decolouring Tank adds seed of bark of eucommia crude oil and weighs the food grade active hargil of 2～4wt%, react 45～55min；

(2-6) open circulated filter system, be circulated filtration, clarifying to seed of bark of eucommia crude oil；

(2-7) entering in deodorizing tower, in deodorizing tower, vacuum is 0.0002MPa, temperature be 100～240 DEG C of reactions 3～ 5h；

In this step: deodorizing tower is to use physical refining tower, fatty acid supplementary set device to be applied in combination and carry out physical deacidification deodorize；

(2-8) being naturally cooling to 100～170 DEG C, water flowing is accelerated to be cooled to room temperature；

(2-9) it is polished filtering by bag filter, bestows the pressure of 4kg, filter, obtain seed of bark of eucommia refined oil；

In this step: in bag filter the material of filter bag film be polyphenylene sulfide fibre, polyimides, aramid fiber or One in polytetrafluoroethylene fibre；

In this step: in bag filter, the aperture size of filter bag film is 0.2～0.9nm.

The preparation method of mountain almond oil of the present invention is as follows:

(1) the de-bitter pre-treatment of Semen pruni armeniacae:

(1-1) Semen pruni armeniacae hulling machine shelling, first machine screening, then artificial screening obtains the Semen pruni armeniacae that shells；

(1-2) Semen pruni armeniacae is poured in 90～100 DEG C of hot water 60～120s, proceed to 4～10 DEG C of cold water impinging cooling 2～ 5min；

(1-3) being poured into by Semen pruni armeniacae in stripping machine and peel, first machine screening, then artificial screening obtains Prunus armeniaca L.var.ansu Maxim. of peeling Core；

(1-4) decortication Semen pruni armeniacae is poured in 90～100 DEG C of hot water carry out four times soak, in immersion process, water temperature is the coldest But；Soak 2～4h for the first time, rinse with tap water after pulling out；Second time soaks 10～12h, rinses with tap water after pulling out；The Soak 2～4h, rinse with tap water after pulling out for three times；Soak 2～4h, rinse with tap water after pulling out for 4th time；

(1-5) Semen pruni armeniacae of de-hardship is poured in drying pool, at 60～70 DEG C, air blast or microwave drying；During microwave drying, The frequency using microwave drying is 2000～2400MHz, power 1500～2800W, and the thickness of the bed of material is 6～7cm；

(2) mountain almond oil extraction refine:

(2-1) pretreatment after Semen pruni armeniacae takes off hardship: Semen pruni armeniacae was pulverized 50 mesh sieves and obtains Semen pruni armeniacae powder, soaks Semen pruni armeniacae powder Steep temperature be 50-60 DEG C, polyvinyl alcohol mass fraction be 2-4wt%, Polyethylene Glycol mass fraction be the poly-second of 5-10wt% In enol-polyglycol solution 0.5-1 hour, Semen pruni armeniacae powder carried out supersound process while soaking, and ultrasonic frequency is 35KHz, ultrasonic power is 260～400W, filters and is dried to obtain Semen pruni armeniacae powder, and polyvinyl alcohol is polyvinyl alcohol 1788 or poly-second Enol 1799, Polyethylene Glycol is polyethylene glycol 200, PEG400 or Macrogol 600；

The preparation method of polyvinyl alcohol-polyethylene glycol solution is as follows: it is 70-that polyvinyl alcohol is soaked in ethanol mass fraction In the ethanol solution of 85wt% 12-24 hour, filtering drying, then the polyvinyl alcohol obtained is joined in the water of 50-60 DEG C, Heated and stirred obtains poly-vinyl alcohol solution in 1 hour, obtains polyvinyl alcohol-polyethylene glycol molten after then adding Polyethylene Glycol stirring and dissolving Liquid；

(2-2) low temperature squeezes mountain almond oil: expressing process uses pure physical squeezing, and temperature controls between 35～55 DEG C, Solid-liquid is carried out the isolated Semen pruni armeniacae dregs of rice and supernatant；The Semen pruni armeniacae dregs of rice are joined in the water of its quality 3-6 times, utilize microwave Reactor controls the temperature 55 of material～60 DEG C, and being added thereto to account for Semen pruni armeniacae dregs of rice mass fraction is 0.055～0.065wt% Compound enzyme, enzymolysis 60～80min, it is centrifuged to obtain thick Semen pruni armeniacae crude oil, the frequency of microwave reactor is 2500～3000MHz, power 1600～2500W；Compound enzyme includes that the mass ratio of protease and cellulase, protease and cellulase is 1:3～2:5；Egg The mass ratio that white enzyme includes neutral protease and alkaline protease, neutral protease and alkaline protease is 1:1～2:3；

(2-3) mountain almond oil refine:

(2-3-1) supernatant and thick Semen pruni armeniacae crude oil are mixed, obtain Semen pruni armeniacae crude oil；

(2-3-2) Semen pruni armeniacae crude oil is warming up to 60～70 DEG C, adds Semen pruni armeniacae crude oil weight 0.05-0.15wt%, concentration For the phosphoric acid of 75-95wt%, react 25～35min；

(2-3-3) take the supernatant obtained in step (2-3-2), add the water of Semen pruni armeniacae crude oil weight 5-15wt%, at the uniform velocity Stirring, rotating speed is 40～50 turns/min, settles 2h；

(2-3-4) take the supernatant obtained in step (2-3-3), vacuum be 0.06～0.095Mpa, temperature be 90 ～be dried under conditions of 110 DEG C；

(2-3-5) enter bleacher, in bleacher vacuum be 0.06～0.095Mpa, temperature be 90～110 DEG C, add The food grade active hargil of Semen pruni armeniacae crude oil weight 2wt%～4wt%, reacts 25～35min；

(2-3-6) open circulated filter system, be circulated filtration, clarifying to filter liquor；

(2-3-7) enter in deodorizing tower, in deodorizing tower vacuum be 0.0002MPa, temperature be 100～240 DEG C, react 2 ～4h；

(2-3-8) being naturally cooling to 100～170 DEG C, water flowing is accelerated to be cooled to room temperature；

(2-3-9) it is polished filtering by bag filter, gives the pressure of 4kg, filter, obtain Semen pruni armeniacae Refined oil.

Beneficial effects of the present invention is as follows:

(1) rich in V in almond oil_A、V_E、V_D3、V_PIt is effective antioxidant and life Deng multivitamin, vitamin A and E Thing free radical scavenger, can effectively prevent skin aging, keep skin elasticity, make skin maintain vigour；

(2) rich in unsaturated fatty acid in eucommia ulmoides seed oil, wherein the content of alpha linolenic acid is up to more than 60%, is that human body must Needing fatty acid, it can promote skin growth, prevents skin aging, keeps skin elasticity, reduces skin allergy.

(3) almond oil and eucommia ulmoides seed oil are effectively combined by the present invention, substantially increase the ageing resistace of skin, make skin Keep elasticity, effectively reduce the anaphylactic reaction of skin simultaneously；

(4) interpolation oriental cherry extract is as wetting agent, by being combined, greatly by natural moisture preserving composition synthetic moisturizing ingredient The big moisture preserving time extending skin, and rich in the light red element of oriental cherry in oriental cherry extract, skin can be made more moist.

Detailed description of the invention

In order to be illustrated more clearly that the present invention, below in conjunction with preferred embodiment, the present invention is described further.Ability Field technique personnel should be appreciated that following specifically described content is illustrative and be not restrictive, and should not limit this with this The protection domain of invention.

Part I: the preparation of eucommia ulmoides seed oil

A kind of eucommia ulmoides seed oil extracts refinery practice, comprises the steps:

(1) supercritical CO is used₂Extraction process obtains seed of bark of eucommia crude oil.

(1-1) seed of bark of eucommia supercritical CO₂The pre-treatment of extraction: seed of bark of eucommia is dried and pulverized 40 mesh sieves and obtains seed of bark of eucommia Powder, first seed of bark of eucommia powder is immersed in temperature be 55 DEG C, polyvinyl alcohol mass fraction be 3wt% poly-vinyl alcohol solution in 1 hour, Seed of bark of eucommia powder carries out supersound process while soaking, and ultrasonic frequency is 35KMz, and ultrasonic power is 350W, filters and is dried Seed of bark of eucommia powder, polyvinyl alcohol is polyvinyl alcohol 1788 or polyvinyl alcohol 1799；The preparation method of poly-vinyl alcohol solution is as follows: will be poly- Vinyl alcohol is soaked in the ethanol solution that ethanol mass fraction is 80wt% 12 hours, filtering drying, the poly-second that then will obtain Enol joins in the water of 55 DEG C, and heated and stirred i.e. obtains poly-vinyl alcohol solution in 1 hour；

(1-2) seed of bark of eucommia powder supercritical CO₂Extraction: the seed of bark of eucommia powder obtained in step (1-1) is put in extraction kettle, Extraction process uses ethanol or ethanol volumetric concentration be 30～80% aqueous solution be entrainer, entrainer flow velocity is 1-3mL/ min；When being entrainer when using ethanol water, first the aqueous solution that ethanol volumetric concentration is 30% is passed through in extraction kettle, The most successively the aqueous solution that ethanol volumetric concentration is 40%, 50%, 60%, 70% and 80% is joined in extraction kettle, ethanol Aqueous solution that aqueous solution that volumetric concentration is 30%, ethanol volumetric concentration are 40%, ethanol volumetric concentration be 50% aqueous solution, Ethanol volumetric concentration be 60% aqueous solution, ethanol volumetric concentration be 70% aqueous solution and ethanol volumetric concentration be the water of 80% The ratio of the time that six kinds of ethanol waters of solution are passed through extraction kettle is: 2:3:1:1:1:2；I.e.: always extraction time is the situation of 2h Under, aqueous solution, ethanol volumetric concentration that aqueous solution that ethanol volumetric concentration is 30%, ethanol volumetric concentration are 40% are 50% Aqueous solution, ethanol volumetric concentration be 60% aqueous solution, ethanol volumetric concentration be 70% aqueous solution and ethanol volumetric concentration be Six kinds of ethanol waters of the aqueous solution of 80% each lead into the time span in extraction kettle successively and are: 24min, 36min, 12min, 12min、12min、24min；Extracting pressure is 25MPa, and extraction temperature is 45 DEG C, and extraction time is 1.5h, and separating pressure is 6MPa, separation temperature is 45 DEG C, obtains seed of bark of eucommia crude oil.

(2) seed of bark of eucommia crude oil refine.

(2-1) being placed in heating tank by seed of bark of eucommia crude oil, be warming up to 60 DEG C, adding weight is seed of bark of eucommia crude oil weight 0.05wt ‰, concentration are the phosphoric acid of 80wt%, react 45min.

(2-2) the seed of bark of eucommia crude oil in heating tank is proceeded in outer tank, add the aqueous slkali prepared in advance immediately, predominate Entering alkali liquor at the uniform velocity to stir on one side, mixing speed is 40 turns/min, reacts 10min, settles 4h.

Alkali liquor is NaOH solution, and NaOH solution is 3:1mL/g with the ratio of seed of bark of eucommia crude oil；Alkalization temperature is 70 DEG C.Always Alkali consumption calculates according to the following steps:

A. theoretical caustic dosage N:N=7.13 × 10^-4× AV × Q, Q are Kg/h for oil flow, unit, and AV is seed of bark of eucommia crude oil Acid number, unit be mgNaOH/g.

B. phosphoric acid alkali consumption NP: owing to the addition of phosphoric acid in the degumming of this technique, therefore alkali liquor interpolation is considered as neutralising phosphoric acid consumption Alkali number；NP=1.22 × W, W are H₃PO₄Addition, unit are Kg/h, and the amount of phosphoric acid is pure phosphoric acid amount here.

C. excess alkali quantity NC: excess alkali is the 0.5wt% of oil mass, NC=Q × 50%, and Q is Kg/h for oil flow, unit.

Actual caustic soda amount NS: due to the Caustic soda purity on market, therefore should be according to its NaOH actual content when calculating Convert: the NaOH percentage composition of actual caustic soda amount NS=(N+NP+NC)/commercially available alkali.

(2-3) taking supernatant, adding NaCl mass fraction is the NaCl solution of 0.5wt%, and NaCl solution addition is Du Secondary seed crude oil weight 5wt%, at the uniform velocity stirs, 40 turns/min of rotating speed, settles 2h.

(2-4) take supernatant, vacuum be 0.06Mpa, temperature be 90 DEG C under conditions of be dried.

(2-5) enter bleacher, in bleacher vacuum be 0.06Mpa, temperature be 90 DEG C, toward bleacher in addition the Cortex Eucommiae The food grade active hargil of seed crude oil weight 2wt%, reacts 45min.

(2-6) open circulated filter system, be circulated filtration, clarifying to seed of bark of eucommia crude oil.

(2-7) enter in deodorizing tower, in deodorizing tower vacuum be 0.0002MPa, temperature be 120 DEG C, react 3h；Deodorizing tower It is to use physical refining tower and fatty acid supplementary set device to be applied in combination and carry out physical deacidification deodorize.

(2-8) being naturally cooling to 100 DEG C, water flowing is accelerated to be cooled to room temperature.

(2-9) carry out polishing by bag filter to filter, and gave the pressure of 4kg, filter, obtain seed of bark of eucommia essence Oil refining；In bag filter, the material of filter bag film is polyphenylene sulfide fibre；The aperture size of filter bag film in bag filter For 0.2nm.

Palmic acid, stearic acid, oleic acid, the content of linoleic acid plus linolenic acid and Folium Persicae coral in the seed of bark of eucommia refined oil obtained The coral glycosides proportion of goods damageds are as shown in table 1-1；The seed of bark of eucommia refined oil physicochemical property obtained is as shown in table 1-2.

The aucubin proportion of goods damageds=(aucubin in the quality seed of bark of eucommia refined oil of aucubin in seed of bark of eucommia Quality) quality * 100% of aucubin in/seed of bark of eucommia, aucubin content (mg/100g) and Du in seed of bark of eucommia In secondary seed refined oil, aucubin content (mg/100g) all uses detection method well known in the prior art.

The seed of bark of eucommia refined oil fatty acid that table 1-1 obtains forms and content

Note: the seed of bark of eucommia crude oil aerial shelf-life is less than three months.

The seed of bark of eucommia refined oil physicochemical property that table 1-2 obtains

* it is crude oil and the refined oil of corresponding embodiment extraction

The preparation of Part II mountain almond oil

A kind of mountain almond oil extracts refinery practice, comprises the steps:

(1) the de-bitter pre-treatment of Semen pruni armeniacae.

(1-2) Semen pruni armeniacae is poured 120s in 100 DEG C of hot water into, proceed to 10 DEG C of cold water impinging cooling 5min；

(1-4) decortication Semen pruni armeniacae is poured in 100 DEG C of hot water carry out four times soak, water temperature natural cooling in immersion process； Soak 4h for the first time, rinse with tap water after pulling out；Second time soaks 12h, rinses with tap water after pulling out；Third time is soaked 4h, rinses with tap water after pulling out；Soak 4h, rinse with tap water after pulling out for 4th time；

(1-5) pouring in drying pool by the Semen pruni armeniacae of de-hardship, at 70 DEG C, microwave drying, the frequency of microwave drying is 2400MHz, power 2500W, the thickness of the bed of material is 6cm.

(2) mountain almond oil extracts refine.

Mountain almond oil extracts refine and includes that low temperature pressing extracts mountain almond oil and mountain almond oil refine；

(2-1) pretreatment after Semen pruni armeniacae takes off hardship: before low temperature pressing extracts mountain almond oil, first Semen pruni armeniacae was pulverized 50 mesh sieves obtain Semen pruni armeniacae powder, Semen pruni armeniacae powder is immersed in temperature be 60 DEG C, polyvinyl alcohol mass fraction be 3wt%, Polyethylene Glycol Mass fraction be 10wt% polyvinyl alcohol-polyethylene glycol solution in 1 hour, Semen pruni armeniacae powder soak while carry out ultrasonic place Reason, ultrasonic power is 350W, supersonic frequency 40KHz, filters and is dried to obtain Semen pruni armeniacae powder, and polyvinyl alcohol is polyvinyl alcohol 1799, Polyethylene Glycol is PEG400；

The preparation method of polyvinyl alcohol-polyethylene glycol solution is as follows: polyvinyl alcohol 1799 is soaked in ethanol mass fraction For in the ethanol solution of 85wt% 12 hours, filtering drying, then the polyvinyl alcohol obtained is joined in the water of 60 DEG C, heating Stir 1 hour to obtain poly-vinyl alcohol solution, obtain polyvinyl alcohol-polyethylene glycol after then adding PEG400 stirring and dissolving molten Liquid；

(2-2) during low temperature pressing extracts mountain almond oil step: expressing process uses pure physical squeezing, and temperature controls 55 DEG C, solid-liquid is carried out the isolated Semen pruni armeniacae dregs of rice and supernatant.Then Semen pruni armeniacae dregs of rice post processing is carried out: joined by the Semen pruni armeniacae dregs of rice In the water of its quality 4 times, utilizing microwave reactor to control the temperature 60 C of material, the frequency of microwave reactor is 3000MHz, merit Rate 2500W, then to be added thereto to account for Semen pruni armeniacae dregs of rice mass fraction be the compound enzyme of 0.065wt%, enzymolysis 80min, slightly centrifugal Semen pruni armeniacae crude oil；Compound enzyme includes that the mass ratio of protease and cellulase, protease and cellulase is 1:3；Protease bag The mass ratio including neutral protease and alkaline protease, neutral protease and alkaline protease is 2:3.

(2-3) mountain almond oil refine:

(2-3-1) supernatant obtained in and the mixing of thick Semen pruni armeniacae crude oil, obtain Semen pruni armeniacae crude oil；

(2-3-2) Semen pruni armeniacae crude oil being warming up to 70 DEG C, addition Semen pruni armeniacae crude oil weight 0.15wt%, concentration are 80wt%'s Phosphoric acid, reacts 35min；

(2-3-3) take the supernatant obtained in step (2-3-2), add the water of Semen pruni armeniacae crude oil weight 15wt%, at the uniform velocity stir Mixing, rotating speed is 50 turns/min, settles 2h；

(2-3-4) take the supernatant obtained in step (2-3-3), vacuum be 0.095Mpa, temperature be the bar of 90 DEG C It is dried under part；

(2-3-5) enter bleacher, in bleacher vacuum be 0.095Mpa, temperature be 90 DEG C, add Semen pruni armeniacae crude oil The food grade active hargil of weight 4wt%, reacts 35min；

(2-3-7) enter in deodorizing tower, in deodorizing tower vacuum be 0.0002MPa, temperature be 110 DEG C, react 2h；

(2-3-8) being naturally cooling to 100 DEG C, water flowing is accelerated to be cooled to room temperature；

Gained Semen pruni armeniacae refined oil fatty acid composition, content analysis and physicochemical property are as shown in table 2-1 and table 2-2.

Table 2-1 Semen pruni armeniacae refined oil fatty acid composition and content analysis

Composition	Content
		Palmic acid	3.55wt%
Palmitoleic acid	0.61wt%
		Stearic acid	0.87wt%
Oleic acid	66.91wt%
		Linoleic acid	27.71wt%
Alpha linolenic acid	0.11wt%
		Mountain almond oil extraction ratio	79.76wt%
The vitamin E proportion of goods damageds	1.83wt%
		V_D3The proportion of goods damageds	2.10wt%

Table 2-2 Semen pruni armeniacae refined oil physicochemical property

The preparation of Part III Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask

Mountain almond oil and eucommia ulmoides seed oil used by this part use the eucommia ulmoides seed oil and second prepared by above-mentioned Part I The mountain almond oil of part preparation.

Embodiment 1

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive oil The mixture 2.3% (mass ratio of ceteareth-6 and olive oil acid esters is 1:3) of acid esters, cetearyl alcohol 0.12%, GTCC2.3%, ethylhexyl palmitate 1.9%, vitamin E acetate 0.30%, the mixture (Fructus Pruni of almond oil and Eucommia Oil The volume ratio of core oil and Eucommia Oil is 3:1) 0.6%, water 81%, carbomer 0.15%, glycerol 4.7%, propylene glycol 5.4%, three Ethanolamine 0.08%, PE9010 and methyl hydroxybenzoate (PE9010 and methyl hydroxybenzoate mass ratio are 3:1) 0.42%, fragrant quick easypro 0.20% (the fragrant quick mass ratio relaxed for bisabolol and ginger-root extract, bisabolol and ginger-root extract is 4:1), plant (plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae in Shu Min agent 0.21% Extract, the mass ratio of water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae extract is: 25:3:1.3:0.8:1.2:0.9), essence 0.02%, (oriental cherry extract is water, butanediol and oriental cherry to oriental cherry extract 0.15% The mixture of leaf extract, the mass ratio of water, butanediol and Sakura leaf extract is: 15:2.4:1.6), and Radix Angelicae Sinensis extract mixes (Radix Angelicae Sinensis extract mixture is the mixture of water, butanediol and Radix Angelicae Sinensis extract, and water, butanediol and Radix Angelicae Sinensis extract for thing 0.15% The ratio mass ratio of thing is: 10:1.5:1.4).

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl The mixture (volume ratio of almond oil and Eucommia Oil is 3:1) of own ester, vitamin E acetate and almond oil and Eucommia Oil joins emulsifying In pot, being heated to 75 DEG C, stirring is to the most melted；

(3) by the solution suction emulsifying pot in step (2), keeping pot inner pressure is 18 handkerchiefs, homogenizing 3min, cooling；

In the preparation process of Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, the extracting method of each extract is as follows:

The extracting method of Sakura leaf extract is as follows: (1) Sakura leaf is dried, is ground into foam, obtains Sakura leaf foam；(2) use Ethanol dissolves Sakura leaf foam, and heating and refluxing extraction 4 hours, concentrated extracting solution obtains crude extract 1；(3) after step (2) being extracted Residue decocting in water 8 hours, is concentrated to give crude extract 2；(3) crude extract 1 and crude extract 2 are mixed, with acetic acid ethyl dissolution, heating Reflux 5 hours, be concentrated to give Sakura leaf extract.

The extracting method of ginger-root extract is as follows: (1) race dries, is ground into foam, obtains race foam；(2) acetic acid second is used Ester dissolves race foam, and heating and refluxing extraction 3 hours, concentrated extracting solution obtains crude extract 1；(3) residue after extracting in step (2) With decocting in water 6 hours, it is concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with acetic acid ethyl dissolution, be heated to reflux 3 hours, it is concentrated to give ginger-root extract.

The extracting method of Radix Ophiopogonis extract is as follows: (1) Radix Ophiopogonis dries, is ground into foam, obtains foam Radix Ophiopogonis；(2) molten with ethanol Solving foam Radix Ophiopogonis, heating and refluxing extraction 5 hours, concentrated extracting solution obtains crude extract 1；(3) the residue water after extracting in step (2) Boil 7 hours, be concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with acetic acid ethyl dissolution, be heated to reflux 4 little Time, it is concentrated to give Radix Ophiopogonis extract.

The extracting method of Opuntia Streptacantha stem extract is as follows: (1) Opuntia Streptacantha stem dries, is ground into foam, is turned round Thorn Cactus Pedicel foam；(2) with acetic acid ethyl dissolution Opuntia Streptacantha stem foam, heating and refluxing extraction 5 hours, concentrated extracting solution obtains slightly Extractum 1；(3) by the decocting in water 8 hours of the residue after the extraction in step (2), it is concentrated to give crude extract 2；(4) by crude extract 1 He Crude extract 2 mixes, and dissolves with ethanol, is heated to reflux 6 hours, is concentrated to give Opuntia Streptacantha stem extract.

The extracting method of radix sophorae extract is as follows: (1) radix sophorae dries, is ground into foam, obtains radix sophorae foam；(2) use The mixed solution (volume ratio of ethanol and ethyl acetate is 3:1) of ethanol and ethyl acetate dissolves radix sophorae foam, is heated to reflux carrying Taking 3 hours, concentrated extracting solution obtains crude extract 1；(3) by the decocting in water 7 hours of the residue after the extraction in step (2), it is concentrated to give Crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, dissolve with ethanol, be heated to reflux 5 hours, be concentrated to give radix sophorae and extract Thing.

The extracting method of Radix Angelicae Sinensis extract is as follows: (1) Radix Angelicae Sinensis dries, is ground into foam, obtains Radix Angelicae Sinensis foam；(2) molten with ethanol Solving Radix Angelicae Sinensis foam, heating and refluxing extraction 5 hours, concentrated extracting solution obtains crude extract 1；(3) residue after the extraction in step (2) is used Decocting in water 4 hours, is concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, dissolve with ethanol, be heated to reflux 5 hours, It is concentrated to give Radix Angelicae Sinensis extract.

Embodiment 2

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive oil The mixture 1.4% (mass ratio of ceteareth-6 and olive oil acid esters is 1:3) of acid esters, cetearyl alcohol 0.08%, GTCC1.7%, ethylhexyl palmitate 1.5%, vitamin E acetate 0.25%, the mixture (Fructus Pruni of almond oil and Eucommia Oil The volume ratio of core oil and Eucommia Oil is 5:1) 0.4%, water 84%, carbomer 0.09%, glycerol 4.8%, propylene glycol 4.7%, three Ethanolamine 0.05%, PE9010 and methyl hydroxybenzoate (PE9010 and methyl hydroxybenzoate mass ratio are 2:1) 0.50%, fragrant quick easypro (fragrant The quick mass ratio relaxed for bisabolol and ginger-root extract, bisabolol and ginger-root extract is 4:1) 0.16%, plant is relaxed Quick dose (plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae extract, The mass ratio of water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae extract is: 25:3: 1.3:0.8:1.2:0.9) 0.19%, essence 0.03%, (Radix Angelicae Sinensis extract mixture is Radix Angelicae Sinensis extract mixture 0.15% The mixture of water, butanediol and Radix Angelicae Sinensis extract, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract is: 10:1.5: 1.4)。

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl The mixture (volume ratio of almond oil and Eucommia Oil is 5:1) of own ester, vitamin E acetate and almond oil and Eucommia Oil joins emulsifying In pot, being heated to 75 DEG C, stirring is to the most melted；

(3) by the solution suction emulsifying pot in step (2), keeping pot inner pressure is 14 handkerchiefs, homogenizing 3min, cooling；

(5) raw material in step (4) is cooled to 45 DEG C and adds plant Shu Min agent, essence and Radix Angelicae Sinensis extract mixture, Stir；

Embodiment 3

Prunus armeniaca L.var.ansu Maxim. moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive oil acid esters Mixture 2.3% (mass ratio of ceteareth-6 and olive oil acid esters is 1:3), cetearyl alcohol 0.12%, GTCC2.3%, ethylhexyl palmitate 1.9%, vitamin E acetate 0.30%, almond oil 0.6%, water 81%, carbomer 0.15%, Glycerol 4.7%, propylene glycol 5.4%, triethanolamine 0.08%, PE9010 and methyl hydroxybenzoate (PE9010 and methyl hydroxybenzoate quality it Than being 3:1) 0.52%, fragrant quick relax 0.20% and (fragrant quick relax for bisabolol and ginger-root extract, bisabolol and ginger-root extract Mass ratio be 4:1), (plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, torsion thorn for plant Shu Min agent 0.11% Cactus Pedicel extract and radix sophorae extract, water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and hardship The mass ratio of ginseng root extract is: 25:3:1.3:0.8:1.2:0.9), essence 0.02%, (oriental cherry carries oriental cherry extract 0.15% Taking thing is water, butanediol and the mixture of Sakura leaf extract, and the mass ratio of water, butanediol and Sakura leaf extract is: 15: 2.4:1.6), (Radix Angelicae Sinensis extract mixture is the mixing of water, butanediol and Radix Angelicae Sinensis extract for Radix Angelicae Sinensis extract mixture 0.15% Thing, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract is: 10:1.5:1.4).

The preparation method of Prunus armeniaca L.var.ansu Maxim. moisturizing mask, comprises the steps:

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl Own ester, vitamin E acetate and almond oil join in emulsifying pot, are heated to 75 DEG C, and stirring is to the most melted；

(6) discharging after the raw material in step (5) being cooled to 40 DEG C, obtains Prunus armeniaca L.var.ansu Maxim. moisturizing mask.

Embodiment 4

Cortex Eucommiae moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive oil acid esters Mixture 2.3% (mass ratio of ceteareth-6 and olive oil acid esters is 1:3), cetearyl alcohol 0.12%, GTCC2.3%, ethylhexyl palmitate 1.9%, vitamin E acetate 0.30%, Eucommia Oil 0.6%, water 81%, carbomer 0.15%, Glycerol 4.7%, propylene glycol 5.4%, triethanolamine 0.08%, PE9010 and methyl hydroxybenzoate (PE9010 and methyl hydroxybenzoate quality it Than being 3:1) 0.42%, fragrant quick relax 0.20% and (fragrant quick relax for bisabolol and ginger-root extract, bisabolol and ginger-root extract Mass ratio be 4:1), (plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, torsion thorn for plant Shu Min agent 0.21% Cactus Pedicel extract and radix sophorae extract, water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and hardship The mass ratio of ginseng root extract is: 25:3:1.3:0.8:1.2:0.9), essence 0.02%, (oriental cherry carries oriental cherry extract 0.15% Taking thing is water, butanediol and the mixture of Sakura leaf extract, and the mass ratio of water, butanediol and Sakura leaf extract is: 15: 2.4:1.6), (Radix Angelicae Sinensis extract mixture is the mixing of water, butanediol and Radix Angelicae Sinensis extract for Radix Angelicae Sinensis extract mixture 0.15% Thing, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract is: 10:1.5:1.4).

The preparation method of Cortex Eucommiae moisturizing mask, comprises the steps:

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl Own ester, vitamin E acetate and Eucommia Oil join in emulsifying pot, are heated to 75 DEG C, and stirring is to the most melted；

(6) discharging after the raw material in step (5) being cooled to 40 DEG C, obtains Cortex Eucommiae moisturizing mask.

Embodiment 5

Moisturizing mask, including the component of following weight fraction: ceteareth-6 and olive oil acid esters mixed Compound 2.3% (mass ratio of ceteareth-6 and olive oil acid esters is 1:3), cetearyl alcohol 0.12%, GTCC2.3%, ethylhexyl palmitate 1.9%, vitamin E acetate 0.30%, water 81.73%, carbomer 0.15%, glycerol 4.7%, propylene glycol 5.4%, triethanolamine 0.08%, (PE9010 and methyl hydroxybenzoate mass ratio are for PE9010 and methyl hydroxybenzoate 3:1) 0.44%, fragrant quick 0.20% (the fragrant quick matter relaxed for bisabolol and ginger-root extract, bisabolol and ginger-root extract of relaxing The ratio of amount is 4:1), (plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, torsion thorn celestial being in plant Shu Min agent 0.21% Palm stem extract and radix sophorae extract, water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and radix sophorae The mass ratio of extract is: 25:3:1.3:0.8:1.2:0.9), essence 0.02%, Radix Angelicae Sinensis extract mixture 0.15% (Radix Angelicae Sinensis Extract mixtures is the mixture of water, butanediol and Radix Angelicae Sinensis extract, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract For: 10:1.5:1.4).

The preparation method of moisturizing mask, comprises the steps:

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, GTCC, palm acid ethyl Own ester, vitamin E acetate join in emulsifying pot, are heated to 75 DEG C, and stirring is to the most melted；

(6) discharging after the raw material in step (5) being cooled to 40 DEG C, obtains moisturizing mask.

The impact of skin moisture-keeping moisturizing effect is tested by embodiment 1～5:

Subject Population is divided into 5 groups, and each group of people uses the moisturizing mask of embodiment 1～5 respectively.

Before smearing mask, experimenter uses identical soap or handwashing liquid cleaning arm, chooses 3 × 3cm²Size area 5 pieces of regions as test position, carry out water content test.The most respectively the facial film of embodiment 1～5 is spread upon experimenter's On the back of the hand, through 2h, 4h, 8h, 16h, test the water content of skin respectively.

Each time period, detect at every experimenter's test zone moisture of skin tester (production of Taiwan CBS Corp.) The water-retention value at test position, is repeated 5 times respectively, draws meansigma methods.

The moisture content of skin of embodiment 1～5 is as shown in the table:

The measurement result of moisture preserving time shows, embodiments of the invention 1 are for the addition of oriental cherry extract and Prunus armeniaca L.var.ansu Maxim./Du simultaneously The Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask of secondary oil, after smearing 16h, moisture of skin increments is 15.87mmv, and embodiment 2 is not for add Adding the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask of oriental cherry extract, after smearing 16h, moisture of skin increments is 7.15mmv, by implementing Example 1 and 2 contrasts it can be seen that oriental cherry extract significantly extends the moistening effect of skin.Embodiment 3 is without Eucommia Oil Prunus armeniaca L.var.ansu Maxim. moisturizing mask, after smearing 16h, moisture of skin increments is 13.44mmv；Embodiment 4 is without almond oil Cortex Eucommiae moisturizing mask, after smearing 16h, moisture of skin increments is 10.99mmv, have embodiment 1,3 and 4 it can be seen that Individually add the moisture preserving time of oriental cherry extract less than adding oriental cherry extract and the facial film moisture preserving time of Prunus armeniaca L.var.ansu Maxim./Eucommia Oil simultaneously Long.

And embodiment 5 is without oriental cherry extract and the facial film of Prunus armeniaca L.var.ansu Maxim./Eucommia Oil, after smearing 16h, moisture of skin increases Dosage is 4.06mmv, this shows that the present invention is by adding oriental cherry extract and the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing of Prunus armeniaca L.var.ansu Maxim./Eucommia Oil Moisten the moistening effect of facial film apparently higher than without oriental cherry extract and the facial film of Prunus armeniaca L.var.ansu Maxim./Eucommia Oil.

In sum, the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask of the present invention can effectively extend moisturizing, makes skin high resilience, Make skin smooth moisten simultaneously.

The repeatedly irritation test of embodiment 1～5:

The Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask of embodiment 1～5 is carried out repeatedly irritation test.Testing conditions and knot Fruit is as follows:

1. testing agency's title: certain Entry-Exit Inspection and Quarantine Bureau's inspection and quarantine complex art center；

2. inspected time: 2016.04.19；

3. detection foundation: " cosmetics health specification " (version in 2007)；

4. detection method and result:

4.1 tested material

4.2 animals and feeding environment

4.3 test method

Repeatedly irritation test is carried out according to " cosmetics health specification " (version in 2007)；

Being cut by hair spinal column both sides, laboratory animal back before Shi Yan, unhairing scope is respectively 3cm × 3cm, surface covered 2.5cm×2.5cm。

Taking tested material 0.5mL to be coated on the skin of side, opposite side painting normal saline, as comparison, applies 1 time, even every day Continuous coating 14d.From the beginning of second day, it is coated with cropping before application every time, removes residual tested material with normal saline.Observe after one hour Result.

4.4 result of the test

There is not erythema and edema in matched group in 1-14 days, by comparing with matched group, embodiment 1～5 is at 1- Erythema and edema did not the most occur in 14 days, illustrates that the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask prepared by the present invention is nontoxic, to skin There is no zest.

Obviously, the above embodiment of the present invention is only for clearly demonstrating example of the present invention, and is not right The restriction of embodiments of the present invention, for those of ordinary skill in the field, the most also may be used To make other changes in different forms, cannot all of embodiment be given exhaustive here, every belong to this What bright technical scheme was extended out obviously changes or changes the row still in protection scope of the present invention.

Claims

1. a Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, it is characterised in that be made up of following component: emulsifying agent, co-emulsifier, skin moistening Agent, solvent, thickening agent, wetting agent, preservative, nertralizer, skin conditioning agent and aromatic.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 1, it is characterised in that described emulsifying agent is cetearyl alcohol Alcohol polyethers-6 and the mixture of olive oil acid esters, the mass ratio of ceteareth-6 and olive oil acid esters is: 1:4～1, institute Stating co-emulsifier is cetearyl alcohol.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 1, it is characterised in that described emollient is octanoic acid/last of the ten Heavenly stems Acid glycerol three ester, ethylhexyl palmitate, vitamin E acetate, almond oil and the body of the mixture of Eucommia Oil, almond oil and Eucommia Oil Long-pending ratio is 6～1:1.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 1, it is characterised in that described solvent is water, described increasing Thick dose is carbomer, and described preservative is phenyl phenol & ethylhexyl glycerol and methyl hydroxybenzoate, phenyl phenol & ethyl The mass ratio of hexyl glycerol and methyl hydroxybenzoate is 5～1:1, and described nertralizer is triethanolamine, and described aromatic is essence.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 1, it is characterised in that described wetting agent be glycerol, third Glycol and oriental cherry extract, described oriental cherry extract is water, butanediol and the mixture of Sakura leaf extract, water, butanediol and The mass ratio of Sakura leaf extract is: 15:2.4:1.6, and the extracting method of Sakura leaf extract is as follows: (1) Sakura leaf is dried, powder It is broken into foam, obtains Sakura leaf foam；(2) with ethanol or acetic acid ethyl dissolution Sakura leaf foam, heating and refluxing extraction 2～6 hours, concentrate Extracting solution obtains crude extract 1；(3) by the residue after middle for step (2) extraction decocting in water 5～12 hours, it is concentrated to give crude extract 2；(3) Crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid ethyl dissolution, is heated to reflux 3～6 hours, is concentrated to give Sakura leaf and carries Take thing；Described skin conditioning agent includes fragrant quick easypro, plant Shu Min agent and Radix Angelicae Sinensis extract mixture.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 5, it is characterised in that described fragrant quick relax for bisabolol With the mass ratio of ginger-root extract, bisabolol and ginger-root extract is 4:1, the extracting method of ginger-root extract is as follows: (1) Race dries, is ground into foam, obtains race foam；(2) with ethanol or acetic acid ethyl dissolution race foam, heating and refluxing extraction 2～5 is little Time, concentrated extracting solution obtains crude extract 1；(3) by the residue after middle for step (2) extraction decocting in water 5～10 hours, it is concentrated to give thick leaching Cream 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid ethyl dissolution, be heated to reflux 2～6 hours, be concentrated to give Ginger-root extract；Described plant Shu Min agent is water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and Radix Sophorae Flavescentis Root extract, water, glycerol, trehalose, Radix Ophiopogonis extract, Opuntia Streptacantha stem extract and the mass ratio of radix sophorae extract For: 25:3:1.3:0.8:1.2:0.9, the extracting method of Radix Ophiopogonis extract is as follows: (1) Radix Ophiopogonis dries, is ground into foam, obtains wheat Winter foam；(2) with ethanol or acetic acid ethyl dissolution foam Radix Ophiopogonis, heating and refluxing extraction 3～5 hours, concentrated extracting solution obtains crude extract 1； (3) by the residue after middle for step (2) extraction decocting in water 4～10 hours, it is concentrated to give crude extract 2；(4) by crude extract 1 and thick leaching Cream 2 mixes, and with ethanol or acetic acid ethyl dissolution, is heated to reflux 2～5 hours, is concentrated to give Radix Ophiopogonis extract；Opuntia Streptacantha stem The extracting method of extract is as follows: (1) Opuntia Streptacantha stem dries, is ground into foam, obtains Opuntia Streptacantha stem foam；(2) second is used Alcohol or acetic acid ethyl dissolution Opuntia Streptacantha stem foam, heating and refluxing extraction 3～8 hours, concentrated extracting solution obtains crude extract 1；(3) will The residue after extraction in step (2) decocting in water 5～12 hours, be concentrated to give crude extract 2；(4) by crude extract 1 and crude extract 2 Mixing, with ethanol or acetic acid ethyl dissolution, is heated to reflux 3～6 hours, is concentrated to give Opuntia Streptacantha stem extract；Radix sophorae The extracting method of extract is as follows: (1) radix sophorae dries, is ground into foam, obtains radix sophorae foam；(2) by ethanol or ethyl acetate Dissolving radix sophorae foam, heating and refluxing extraction 2～6 hours, concentrated extracting solution obtains crude extract 1；(3) by after the extraction in step (2) Residue decocting in water 5～12 hours, be concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid Ethyl ester dissolves, and is heated to reflux 3～6 hours, is concentrated to give radix sophorae extract；Described Radix Angelicae Sinensis extract mixture is water, fourth two Alcohol and the mixture of Radix Angelicae Sinensis extract, the ratio mass ratio of water, butanediol and Radix Angelicae Sinensis extract is: 10:1.5:1.4, Radix Angelicae Sinensis carries The extracting method taking thing is as follows: (1) Radix Angelicae Sinensis dries, is ground into foam, obtains Radix Angelicae Sinensis foam；(2) work as with ethanol or acetic acid ethyl dissolution Gui Mo, heating and refluxing extraction 4～6 hours, concentrated extracting solution obtains crude extract 1；(3) residue after the extraction in step (2) is used Decocting in water 3～9 hours, be concentrated to give crude extract 2；(4) crude extract 1 and crude extract 2 are mixed, with ethanol or acetic acid ethyl dissolution, It is heated to reflux 3～7 hours, is concentrated to give Radix Angelicae Sinensis extract.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 1, it is characterised in that described emulsifying agent is cetearyl alcohol Alcohol polyethers-6 and the mixture of olive oil acid esters, described co-emulsifier is cetearyl alcohol, and described emollient is that caprylic/capric is sweet Oil three esters, ethylhexyl palmitate, vitamin E acetate, almond oil and the mixture of Eucommia Oil, described solvent is water, described thickening agent For carbomer, described wetting agent is glycerol, propylene glycol and oriental cherry extract, and described preservative is phenyl phenol & ethylhexyl Glycerol and methyl hydroxybenzoate, described nertralizer is triethanolamine, and described aromatic is essence, and described skin conditioning agent includes fragrant quick Relax, plant Shu Min agent and Radix Angelicae Sinensis extract mixture.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 7, it is characterised in that include the group of following weight fraction Point: the mixture 1.4～2.6% of ceteareth-6 and olive oil acid esters, cetearyl alcohol 0.05～0.16%, pungent Acid/tricaprin 1.5～2.5%, ethylhexyl palmitate 1.5～2.5%, vitamin E acetate 0.25～0.35%, Semen Armeniacae Amarum Oil and the mixture 0.4～0.6% of Eucommia Oil, water 50～80%, carbomer 0.04～0.15%, glycerol 4.5～5.6%, third Glycol 4.5～5.6%, triethanolamine 0.04～0.15%, phenyl phenol & ethylhexyl glycerol and methyl hydroxybenzoate 0.29～ 0.51%, fragrant quick easypro 0.10～0.20%, plant Shu Min agent 0.15～0.25%, essence 0.01～0.03%, oriental cherry extract 0.05～0.15%, Radix Angelicae Sinensis extract mixture 0.05～0.15%.

Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask the most according to claim 8, it is characterised in that include the group of following weight fraction Point: the mixture 2% of ceteareth-6 and olive oil acid esters, cetearyl alcohol 0.1%, caprylic/capric triglyceride 2%, ethylhexyl palmitate 2%, vitamin E acetate 0.3%, the mixture 0.5% of almond oil and Eucommia Oil, water 78.35%, card Ripple nurse 0.1%, glycerol 5%, propylene glycol 5%, methyl hydroxybenzoate 0.1%, triethanolamine 0.08%, phenyl phenol & ethylhexyl Glycerol and methyl hydroxybenzoate 0.3%, fragrant quick easypro 0.15%, plant Shu Min agent 2%, essence 0.02%, oriental cherry extract 1%, when Return extract mixtures 1%.

10. utilize the method that the Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask described in claim 8 prepares Prunus armeniaca L.var.ansu Maxim. Cortex Eucommiae moisturizing mask, It is characterized in that, comprise the steps:

(1) by ceteareth-6 and the mixture of olive oil acid esters, cetearyl alcohol, caprylic/capric triglyceride, palm fibre The mixture of palmitic acid acid Octyl Nitrite, vitamin E acetate and almond oil and Eucommia Oil joins in emulsifying pot, is heated to 75 DEG C, and stirring is extremely The most melted；

(2) water, carbomer, glycerol, propylene glycol and methyl hydroxybenzoate being joined in aqueous phase pot, be heated to 75 DEG C, stirring is to mixing Uniformly, and be completely dissolved；

(4) raw material in step (3) is cooled to 60 DEG C and adds triethanolamine, phenyl phenol & ethylhexyl glycerol and fragrant Quick easypro, stir；

(5) raw material in step (4) is cooled to 45 DEG C and adds plant Shu Min agent, essence, oriental cherry extract and Radix Angelicae Sinensis extract Mixture, stirs；