CN105878128A - Silicon-free transparent shampoo containing humectant and preparing method of silicon-free transparent shampoo - Google Patents
Silicon-free transparent shampoo containing humectant and preparing method of silicon-free transparent shampoo Download PDFInfo
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- CN105878128A CN105878128A CN201610394139.8A CN201610394139A CN105878128A CN 105878128 A CN105878128 A CN 105878128A CN 201610394139 A CN201610394139 A CN 201610394139A CN 105878128 A CN105878128 A CN 105878128A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
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Abstract
The invention relates to a silicon-free transparent shampoo containing a humectant and a preparing method of the silicon-free transparent shampoo. The shampoo is prepared from, by mass, 10-15% of a main surfactant, 3.5-13% of an auxiliary surfactant, 0.25-3% of the humectant, 0.6-3% of a thickening and stabilizing agent, 4.5-20% of a conditioner, 1-4% of a grease applying agent, 0.5-2.5% of a solubilizing agent, 0.05-0.2% of a nutritional agent, 0.1-1% of fragrance, 0.1-1% of a viscosity modifier, 0.01-0.1% of a preservative and the balance deionized water. Compared with the prior art, the silicon-free transparent shampoo containing the humectant and the preparing method of the silicon-free transparent shampoo can effectively solve the problem of dryness and roughness in the hair washing process of silicon-free products and after hair washing, and have the advantages that the roughness is obviously relieved in the wet flushing process, higher smoothness is achieved in the washing process, and hair is moister after being dried.
Description
Technical field
The invention belongs to cosmetic field, relate to a kind of transparent shampoo without silicon containing wetting agent and preparation side thereof
Method.
Background technology
The effect of cleaning and maintaining hair is played in shampoo.Along with the increasing the weight of of air pollution, work rhythm continuous
Accelerate so that many people face scalp deionized water oil dysequilibrium, and hair color is intensely dark, lacks cordiality
Worry, therefore it is desirable to using the most healthy natural state of hair of reducing after shampoo.But current city
The shampoo of field upper more than 90% all contains silicone oil, i.e. polydimethylsiloxane, and this chemical substance is exactly a kind of
Softening agent, it can make hair smooth, but silicone oil is insoluble in deionized water, the perfume (or spice) that life-time service silicone oil is high
The various problems such as after ripple, silicone oil will be hoarded in hair surface, and hair may finally be caused to become sticky, the most fuel-displaced.
Therefore, occur successively without silicon series shampoo, but the most mostly deposit when hair washing and after hair washing without silicon shampoo
Dry and astringent in dry and astringent problem.
Summary of the invention
Defect that the purpose of the present invention is contemplated to overcome above-mentioned prior art to exist and provide the one can be effective
Solve when have one's hair wash without silicon product with have one's hair wash after the transparent shampoo without silicon containing wetting agent of dry and astringent problem and preparation thereof
Method.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content:
Described wetting agent is prepared by the component of following weight portion content:
The preparation employing following methods of described wetting agent:
By proportioning by after pantothenylol and laureth-7 citrate Hybrid Heating to 40 DEG C, add Curacao reed
Luxuriant growth leaf juice and glycine betaine, stir and can be prepared by this wetting agent.
Described primary surfactant is sodium laureth sulfate,
Described cosurfactant selects cocamido propyl betaine, decyl glucoside and lauroyl both sexes
Guanidine-acetic acid sodium mixes,
Described thickening stabilizing agent selects Coconut Fatty Acid Monoethanolamide and Polyethylene Glycol-120 methyl two oleic acid
Ester mixes,
Described conditioner selects 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon glue Hydroxyproyl Trimethyl
Ammonium chloride mixes,
Described tax fat agent is Polyethylene Glycol-7 glyceryl cocoate,
Described solubilizing agent is Polyethylene Glycol-40 castor oil hydrogenated,
Described nutrient is Prunus dulcis oil,
Described viscosity modifier is sodium chloride.
Preferably, this shampoo is prepared by the component of following mass percentage content:
Preferably, this shampoo is prepared by the component of following mass percentage content:
It is further preferred that this shampoo is prepared by the component of following mass percentage content:
Or, it is further preferred that this shampoo is prepared by the component of following mass percentage content:
The preparation method of the described transparent shampoo without silicon containing wetting agent, comprises the following steps:
(1) each component is taken by proportioning；
(2) thickening stabilizing agent is heated to 70-90 DEG C to be completely melt；
(3) by deionized water, primary surfactant and cosurfactant heated and stirred in agitated kettle；
(4) when temperature is warming up to 60-80 DEG C, conditioner is added；
(5) continue to be heated to temperature and rise to 80-98 DEG C, thickening stabilizing agent completely will be melted and add agitated kettle
In；
(6), after being sufficiently stirred for 5～65min, heating is stopped；
(7), when temperature is cooled to 50-70 DEG C, adds and mix nutrient and solubilizing agent completely；
(8) when continuing cool to 40-50 DEG C, be sequentially added into wetting agent, compose fat agent, essence, preservative and
Viscosity modifier, stops stirring after stirring 10-70min, obtains the described transparent shampoo without silicon containing wetting agent.
Preferably, this preparation method comprises the following steps:
(1) each component is taken by proportioning；
(2) thickening stabilizing agent is heated to 80 DEG C to be completely melt；
(3) by deionized water, primary surfactant and cosurfactant heated and stirred in agitated kettle；
(4) when temperature is warming up to 70 DEG C, conditioner is added；
(5) continue to be heated to temperature and rise to 90 DEG C, will melt in the agitated kettle of thickening stabilizing agent addition completely；
(6), after being sufficiently stirred for 35min, heating is stopped；
(7), when temperature is cooled to 60 DEG C, adds and mix nutrient and solubilizing agent completely；
(8), when continuing cool to 45 DEG C, it is sequentially added into wetting agent, composes fat agent, essence, preservative and glue
Degree regulator, stops stirring after stirring 40min, obtains the described transparent shampoo without silicon containing wetting agent.
The present invention adds multiple moisturizing ingredient, when can effectively solve to have one's hair wash without silicon product and hair washing after dry and astringent asking
Topic.Between wetting agent, compatibility is good, and property safe to the human body is good, and zest is little, it is possible to life-time service, and
The preparation process of this wetting agent and time this wetting agent is added in agitated kettle preparation shampoo all in gentle temperature
Carry out under degree, its effective ingredient will not be destroyed.Aloe Barbadensis Miller juice is Folium Aloe elite, containing abundant amino
Acid, vitamin and various mineral salt, it is possible to locking moisture, for very good moisturizer, can percdation,
Naturally balance skin acid-base value, it is possible to moisten scalp, the phenomenon that after reducing hair washing, dry scalp is felt nervous, with
Time it can be avoided that dry scalp, the oils and fats of supersecretion.Pantothenylol i.e. dexpanthenol, has lasting moisturizing
Function, prevents hair jag, impaired, increases the density of hair, improves the gloss of hair quality.Glycine betaine is water
The natural moisture absorption factor of dissolubility, has strong hygroscopicity, using the teaching of the invention it is possible to provide large quantity of moisture, makes hair and scalp protect
Hold moistening.Laureth-7 citrate being modified citric acid obtaining has long-acting moisture-keeping function,
It can reduce the moisture of skin transdermal loss of surfactant system, the barrier function of long-effective protection skin.
The wetting agent of the present invention is set about from many aspects, problem dry and astringent when solving to have one's hair wash without silicon product and after hair washing,
Hair is made more to add water profit, smooth.
Compared with prior art, the present invention not silicate-containing oil, by adding wetting agent, can effectively solve to produce without silicon
Problem dry and astringent during product hair washing and after hair washing.Wet when rushing astringent sense significantly reduce, more smooth during flushing, dry back
Sending out more add water profit, and product water white transparency, each component compatibility is good, and formula gentleness is non-stimulated, can be long-term
Use.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 10%, Polyethylene Glycol-7 glyceryl cocoate 1%, cocamido propyl betaine 2%,
Decyl glucoside 1%, Coconut Fatty Acid Monoethanolamide 0.5%, LAA 0.5%, wetting agent
0.25%, Polyethylene Glycol-120 methyl dioleate 0.1%, Prunus dulcis oil 0.05%, 5wt% polyquaternary amine
Salt-10 2%, Polyethylene Glycol-40 castor oil hydrogenated 0.5%, 2wt% hydroxypropyl melon glue Hydroxyproyl Trimethyl chlorine
Changing ammonium 2.5%, essence 0.1%, sodium chloride 0.1%, preservative 0.01%, surplus is water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 30 parts, and lauryl alcohol gathers
Ether-7 citrate 15 parts, glycine betaine 5 parts, 10 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 70 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 60 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 80 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 5min, stops heating.
6th step: when temperature is cooled to 50 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 40 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 10min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
Embodiment 2
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 15%, Polyethylene Glycol-7 glyceryl cocoate 4%, cocamido propyl betaine 6%,
Decyl glucoside 4%, Coconut Fatty Acid Monoethanolamide 2%, LAA 3%, wetting agent 3%,
Polyethylene Glycol-120 methyl dioleate 1%, Prunus dulcis oil 0.2%, 5wt% Polyquaternium-10 10%,
Polyethylene Glycol-40 castor oil hydrogenated 2.5%, 2wt% hydroxypropyl guar hydroxypropyltrimonium chloride 10%,
Essence 1%, sodium chloride 1%, preservative 0.1%, surplus is water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 50 parts, and lauryl alcohol gathers
Ether-7 citrate 35 parts, glycine betaine 25 parts, 30 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 90 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 80 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 98 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 65min, stops heating.
6th step: when temperature is cooled to 70 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 50 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 70min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
Embodiment 3
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 14.8%, Polyethylene Glycol-7 glyceryl cocoate 3.8%, cocamido propyl betaine
5.5%, decyl glucoside 3.5%, Coconut Fatty Acid Monoethanolamide 1.8%, LAA 2.8%,
Wetting agent 2.9%, Polyethylene Glycol-120 methyl dioleate 0.9%, Prunus dulcis oil 0.19%, 5wt%
Polyquaternium-10 9.5%, Polyethylene Glycol-40 castor oil hydrogenated 2.45%, 2wt% hydroxypropyl melon glue hydroxypropyl
Trimethyl ammonium chloride 9%, essence 0.95%, sodium chloride 0.96%, preservative 0.09%, surplus is water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 40 parts, and lauryl alcohol gathers
Ether-7 citrate 25 parts, glycine betaine 15 parts, 20 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 80 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 70 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 90 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 35min, stops heating.
6th step: when temperature is cooled to 60 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 45 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 40min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
Embodiment 4
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 12.5%, Polyethylene Glycol-7 glyceryl cocoate 2.5%, cocamidopropyl propyl amide Radix Betae
Alkali 5%, decyl glucoside 2.5%, Coconut Fatty Acid Monoethanolamide 1.25%, LAA 1.8%,
Wetting agent 1.65%, Polyethylene Glycol-120 methyl dioleate 0.55%, Prunus dulcis oil 0.125%,
5wt% Polyquaternium-10 6%, Polyethylene Glycol-40 castor oil hydrogenated 1.5%, 2wt% hydroxypropyl melon glue hydroxyl
Hydroxypropyltrimonium chloride 6.25%, essence 0.55%, sodium chloride 0.55%, preservative 0.055%, surplus
For water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 40 parts, and lauryl alcohol gathers
Ether-7 citrate 25 parts, glycine betaine 15 parts, 20 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 80 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 70 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 90 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 35min, stops heating.
6th step: when temperature is cooled to 60 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 45 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 40min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
Embodiment 5
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 12%, Polyethylene Glycol-7 glyceryl cocoate 2.2%, cocamido propyl betaine
4%, decyl glucoside 2.3%, Coconut Fatty Acid Monoethanolamide 1.2%, LAA 1.7%,
Wetting agent 1.6%, Polyethylene Glycol-120 methyl dioleate 0.5%, Prunus dulcis oil 0.12%, 5wt%
Polyquaternium-10 5.5%, Polyethylene Glycol-40 castor oil hydrogenated 1.4%, 2wt% hydroxypropyl melon glue hydroxypropyl
Trimethyl ammonium chloride 6%, essence 0.4%, sodium chloride 0.5%, preservative 0.052%, surplus is water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 40 parts, and lauryl alcohol gathers
Ether-7 citrate 25 parts, glycine betaine 15 parts, 20 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 80 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 70 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 90 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 35min, stops heating.
6th step: when temperature is cooled to 60 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 45 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 40min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
Comparative example 1
A kind of transparent shampoo without silicon without wetting agent, is made up of following content of starting materials: laureth sulphuric acid
Ester sodium 12.5%, Polyethylene Glycol-7 glyceryl cocoate 2.5%, cocamido propyl betaine 5%, decyl
Glucoside 2.5%, Coconut Fatty Acid Monoethanolamide 1.25%, LAA 1.8%, poly-second two
Alcohol-120 methyl dioleate 0.55%, Prunus dulcis oil 0.125%, 5wt% Polyquaternium-10 6%,
Polyethylene Glycol-40 castor oil hydrogenated 1.5%, 2wt% hydroxypropyl guar hydroxypropyltrimonium chloride
6.25%, essence 0.55%, sodium chloride 0.55%, preservative 0.055%, surplus is water.By said components
The transparent shampoo without silicon without wetting agent is i.e. obtained by the preparation method of embodiment 4.
Comparative example 2
A kind of transparent shampoo without silicon without wetting agent, is prepared by the component of following mass percentage content: the moon
Laureth sodium sulfovinate 12%, Polyethylene Glycol-7 glyceryl cocoate 2.2%, cocamidopropyl propyl amide Radix Betae
Alkali 4%, decyl glucoside 2.3%, Coconut Fatty Acid Monoethanolamide 1.2%, LAA 1.7%,
Wetting agent 1.6%, Polyethylene Glycol-120 methyl dioleate 0.5%, Prunus dulcis oil 0.12%, 5wt%
Polyquaternium-10 5.5%, Polyethylene Glycol-40 castor oil hydrogenated 1.4%, 2wt% hydroxypropyl melon glue hydroxypropyl
Trimethyl ammonium chloride 6%, essence 0.4%, sodium chloride 0.5%, preservative 0.052%, surplus is water.Will
Said components i.e. obtains the transparent shampoo without silicon without wetting agent by the preparation method of embodiment 5.
Embodiment 6
A kind of transparent shampoo without silicon containing wetting agent, is prepared by the component of following mass percentage content: Laurel
Alcohol polyethers sodium sulfovinate 10.5%, Polyethylene Glycol-7 glyceryl cocoate 1.2%, cocamido propyl betaine
2.5%, decyl glucoside 1.2%, Coconut Fatty Acid Monoethanolamide 0.6%, LAA 0.7%,
Wetting agent 0.3%, Polyethylene Glycol-120 methyl dioleate 0.11%, Prunus dulcis oil 0.06%, 5wt%
Polyquaternium-10 2.2%, Polyethylene Glycol-40 castor oil hydrogenated 0.55%, 2wt% hydroxypropyl melon glue hydroxypropyl
Trimethyl ammonium chloride 3%, essence 0.12%, sodium chloride 0.12%, preservative 0.015%, surplus is water.
The wetting agent of the present embodiment is prepared by the component of following weight portion content: pantothenylol 40 parts, and lauryl alcohol gathers
Ether-7 citrate 25 parts, glycine betaine 15 parts, 20 parts of Aloe Barbadensis Miller juice.
The preparation of this wetting agent uses following methods: pantothenylol and laureth-7 citrate are mixed by proportioning
After conjunction is heated to 40 DEG C, adds Aloe Barbadensis Miller juice and glycine betaine, stir and can be prepared by this wetting agent.
A kind of preparation method of the transparent shampoo without silicon containing wetting agent, the preparation process of the method is as follows:
The first step: by Coconut Fatty Acid Monoethanolamide, two oil phases of Polyethylene Glycol-120 methyl dioleate
It is heated to 80 DEG C to be completely dissolved.
Second step: by deionized water, sodium laureth sulfate, cocamido propyl betaine, Laurel
Acyl both sexes guanidine-acetic acid sodium and decyl glucoside heated and stirred in agitated kettle.
3rd step: when temperature rises to 70 DEG C, adds 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon
Glue hydroxypropyl-trimethyl ammonium chloride.
4th step: temperature rises to 90 DEG C, adds the oil phase dissolved in agitated kettle.
5th step: after being sufficiently stirred for 35min, stops heating.
6th step: when temperature is cooled to 60 DEG C, adds and mixes Prunus dulcis oil and Polyethylene Glycol-40 hydrogen completely
Change the transparency liquid of Oleum Ricini.
7th step: when being cooled to 45 DEG C, be sequentially added into wetting agent, Polyethylene Glycol-7 glyceryl cocoate,
Essence, preservative and sodium chloride, stop stirring after stirring 40min, obtains described saturating without silicon containing wetting agent
Bright shampoo.
Problem dry and astringent when the shampoo of the present invention can effectively solve to have one's hair wash without silicon product and after hair washing.Wet puckery when rushing
Sense significantly reduces, more smooth during flushing, dry rear hair more water profit, and product water white transparency, each component
Compatibility is good, and formula gentleness is non-stimulated, can life-time service.
The shampoo cleans hair that 50 triers use embodiment 1-5 and comparative example 1 and 2 to provide every day respectively,
Service condition is as follows:
Use the trier of shampoo of embodiment 1-5 after a procedure, compared with comparative example 1 and 2, wet when rushing
Astringent sense significantly reduces；During flushing more smooth；Hair more water profit after dry.
Claims (10)
1. the transparent shampoo without silicon containing wetting agent, it is characterised in that by following mass percentage content
Component prepare:
A kind of transparent shampoo without silicon containing wetting agent the most according to claim 1, it is characterised in that
Described wetting agent is prepared by the component of following weight portion content:
A kind of transparent shampoo without silicon containing wetting agent the most according to claim 2, it is characterised in that
The preparation employing following methods of described wetting agent:
By proportioning by after pantothenylol and laureth-7 citrate Hybrid Heating to 40 DEG C, add Curacao reed
Luxuriant growth leaf juice and glycine betaine, stir and can be prepared by this wetting agent.
4. according to a kind of transparent shampoo without silicon containing wetting agent described in claim 1, it is characterised in that
Described primary surfactant is sodium laureth sulfate,
Described cosurfactant selects cocamido propyl betaine, decyl glucoside and lauroyl both sexes
Guanidine-acetic acid sodium mixes,
Described thickening stabilizing agent selects Coconut Fatty Acid Monoethanolamide and Polyethylene Glycol-120 methyl two oleic acid
Ester mixes,
Described conditioner selects 5wt% Polyquaternium-10 and 2wt% hydroxypropyl melon glue Hydroxyproyl Trimethyl
Ammonium chloride mixes,
Described tax fat agent is Polyethylene Glycol-7 glyceryl cocoate,
Described solubilizing agent is Polyethylene Glycol-40 castor oil hydrogenated,
Described nutrient is Prunus dulcis oil,
Described viscosity modifier is sodium chloride.
5. according to a kind of transparent shampoo without silicon containing wetting agent described in claim 4, it is characterised in that by
The component of following mass percentage content prepares:
6. according to a kind of transparent shampoo without silicon containing wetting agent described in claim 5, it is characterised in that by
The component of following mass percentage content prepares:
7. according to a kind of transparent shampoo without silicon containing wetting agent described in claim 6, it is characterised in that by
The component of following mass percentage content prepares:
8. according to a kind of transparent shampoo without silicon containing wetting agent described in claim 6, it is characterised in that by
The component of following mass percentage content prepares:
9. the preparation method of the transparent shampoo without silicon containing wetting agent as claimed in claim 1, its feature exists
In, comprise the following steps:
(1) each component is taken by proportioning；
(2) thickening stabilizing agent is heated to 70-90 DEG C to be completely melt；
(3) by deionized water, primary surfactant and cosurfactant heated and stirred in agitated kettle；
(4) when temperature is warming up to 60-80 DEG C, conditioner is added；
(5) continue to be heated to temperature and rise to 80-98 DEG C, thickening stabilizing agent completely will be melted and add agitated kettle
In；
(6), after being sufficiently stirred for 5～65min, heating is stopped；
(7), when temperature is cooled to 50-70 DEG C, adds and mix nutrient and solubilizing agent completely；
(8) when continuing cool to 40-50 DEG C, be sequentially added into wetting agent, compose fat agent, essence, preservative and
Viscosity modifier, stops stirring after stirring 10-70min, obtains the described transparent shampoo without silicon containing wetting agent.
The preparation method of the transparent shampoo without silicon containing wetting agent the most according to claim 9, its feature
It is, comprises the following steps:
(1) each component is taken by proportioning；
(2) thickening stabilizing agent is heated to 80 DEG C to be completely melt；
(3) by deionized water, primary surfactant and cosurfactant heated and stirred in agitated kettle；
(4) when temperature is warming up to 70 DEG C, conditioner is added；
(5) continue to be heated to temperature and rise to 90 DEG C, will melt in the agitated kettle of thickening stabilizing agent addition completely；
(6), after being sufficiently stirred for 35min, heating is stopped；
(7), when temperature is cooled to 60 DEG C, adds and mix nutrient and solubilizing agent completely；
(8), when continuing cool to 45 DEG C, it is sequentially added into wetting agent, composes fat agent, essence, preservative and glue
Degree regulator, stops stirring after stirring 40min, obtains the described transparent shampoo without silicon containing wetting agent.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106176285A (en) * | 2016-08-25 | 2016-12-07 | 天津郁美净集团有限公司 | A kind of be applicable to that child uses have one's hair wash bath composition and preparation method thereof without silicon |
| CN106539714A (en) * | 2016-11-08 | 2017-03-29 | 宁夏艾伊生物工程研发有限公司 | A kind of special shampoo in colliery |
| CN107737026A (en) * | 2017-11-10 | 2018-02-27 | 广州神采化妆品有限公司 | A kind of emulsion with makeup removing effect |
| CN108904324A (en) * | 2018-09-14 | 2018-11-30 | 上海华银日用品有限公司 | A kind of high smoothness is without silicon shampoo and preparation method thereof |
| CN109646352A (en) * | 2019-01-10 | 2019-04-19 | 澳宝化妆品（惠州）有限公司 | A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract |
| CN110123721A (en) * | 2019-06-17 | 2019-08-16 | 医美生物科技(上海)有限公司 | A kind of shampoo compositions improving oiliness scalp |
| GB2595956B (en) * | 2020-04-21 | 2022-10-12 | Henkel Ag & Co Kgaa | Silicone-free leave-in hair serums comprising a modified polysaccharide and a plant based oil |
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| CN104921989A (en) * | 2015-06-12 | 2015-09-23 | 广州环亚化妆品科技有限公司 | Liquid shampoo without silicon oil and with hair caring effect and preparation method thereof |
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| CN104921989A (en) * | 2015-06-12 | 2015-09-23 | 广州环亚化妆品科技有限公司 | Liquid shampoo without silicon oil and with hair caring effect and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106176285A (en) * | 2016-08-25 | 2016-12-07 | 天津郁美净集团有限公司 | A kind of be applicable to that child uses have one's hair wash bath composition and preparation method thereof without silicon |
| CN106539714A (en) * | 2016-11-08 | 2017-03-29 | 宁夏艾伊生物工程研发有限公司 | A kind of special shampoo in colliery |
| CN107737026A (en) * | 2017-11-10 | 2018-02-27 | 广州神采化妆品有限公司 | A kind of emulsion with makeup removing effect |
| CN108904324A (en) * | 2018-09-14 | 2018-11-30 | 上海华银日用品有限公司 | A kind of high smoothness is without silicon shampoo and preparation method thereof |
| CN109646352A (en) * | 2019-01-10 | 2019-04-19 | 澳宝化妆品（惠州）有限公司 | A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract |
| CN110123721A (en) * | 2019-06-17 | 2019-08-16 | 医美生物科技(上海)有限公司 | A kind of shampoo compositions improving oiliness scalp |
| CN110123721B (en) * | 2019-06-17 | 2021-12-14 | 医美生物科技(上海)有限公司 | Shampoo composition for improving oily scalp |
| GB2595956B (en) * | 2020-04-21 | 2022-10-12 | Henkel Ag & Co Kgaa | Silicone-free leave-in hair serums comprising a modified polysaccharide and a plant based oil |
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