CN105839420A - Preparation method of sustained-release fragrant fabric - Google Patents
Preparation method of sustained-release fragrant fabric Download PDFInfo
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- CN105839420A CN105839420A CN201510024110.6A CN201510024110A CN105839420A CN 105839420 A CN105839420 A CN 105839420A CN 201510024110 A CN201510024110 A CN 201510024110A CN 105839420 A CN105839420 A CN 105839420A
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Abstract
The invention discloses a preparation method of a sustained-release fragrant fabric. The preparation method comprises the steps of: (1) putting a 200-300nm porous mineral material (sepiolite, Xixia county Jinxiang mining limited liability company) in a high-speed mixer and performing beating to prepare a suspension slurry; adding natural aromatic substances into the suspension slurry in the high-speed mixer, and carrying out dewatering, drying, drying and grinding treatment to obtain load aromatic powder with a water content of less than 10%; (2) feeding mixing equipment with the grinded load aromatic powder and polyester fiber plain sheet by a single-screw feeder and carrying out mixing treatment, then sending the mixed materials into melt spinning equipment to conduct melting and spinning, then conducting consolidation forming in acid bath, and then carrying out drafting, washing, desulfurization, bleaching, oiling, dehydration, cutting and drying, thus obtaining aromatic fiber; (3) blending the aromatic fiber with cotton to obtain long-acting aromatic yarn; (4) performing weaving treatment; and (5) carrying out after-finishing treatment on the woven fabric. The fabric prepared by the method provided by the invention has fragrance lasting for more than two years, and can be washable by over 20 times.
Description
Technical field
The present invention relates to the preparation method of a kind of textile fabric, particularly to a kind of long-acting slow-release fragrance fabric
Preparation method.
Background technology
Along with the concern of functional product is got more and more by everybody in recent years, continuous along with living standards of the people
Improving, functional being also intended to of home textile product is asked more and more higher, common fabric can not meet consumer
Demand, aromatics fabric is seasonable and gives birth to, and receives pursuing of more and more people in recent years, but fragrance
Persistency is always the core of people's research and development, is also difficult point；Prior art is typically all and uses binding agent to carry
Rise fabric fragrance longevity, but its persistency is comparatively short.
Summary of the invention
The technical problem to be solved in the present invention is to provide one to be had and persistently discharges perfume container, can make fragrance
Fabric fragrance effectively discharges, and does not affect the system of a kind of long-acting slow-release fragrance fabric of the serviceability of fabric simultaneously
Preparation Method.
For reaching above-mentioned purpose, technical scheme is as follows:
A kind of preparation method of long-acting slow-release fragrance fabric；Described preparation method includes following preparation process:
(1) preparation of aroma loaded powder body, by porous mineral materials, (meerschaum, Xixia County's auspicious mining industry of gold has
Limit responsible company) it is ground to 200-300nm, put in homogenizer, add water and stir, high-speed stirred
Machine carries out making beating operation, makes the suspension slurry that concentration is 1%～10%；Natural aromatic substance is milled into
Superfine powder, and join in the suspension slurry in homogenizer, adjust the pH value of reaction system to 5～
7, room temperature reaction controlled at 2～3 hours；Then selection is centrifugal or suspension slurry is dehydrated by filter method
Process；Then the gains after dehydration are dried at a temperature of less than 80 DEG C, be dried after drying
Process obtains aroma loaded powder body, and baking temperature is 140～180 DEG C, and drying time is 40～80min, dry
It is ground after dry, aroma loaded powder body is ground to 200-300nm, obtain water content bearing less than 10%
Carry fragrance powder body；
(2) prepared by fragrant fiber, and the aroma loaded powder body after grinding is by single screw feeders feeding one
In mixing apparatus, polyester fiber plain film is fed in this mixing apparatus, at this by single screw rod feeding machine simultaneously
After aroma loaded powder body in mixing apparatus and polyester fiber plain film mix homogeneously, send in apparatus for melt spinning
After melted, spray webbing, enter acid bath coagulation forming, then through drawing-off, washing, desulfurization, bleach, oil, de-
Water, cut off, dry and make fragrant fiber；
(3) preparation of long-acting fragrance yarn, long-acting fragrance yarn uses fragrant fiber and cotton to carry out blending,
Blending rate is 30% fragrant fiber, and 70% is cotton；
(4) preparation of long-acting slow-release fragrance fabric, organizine and tram all select long-acting fragrance yarn, then
Put in loom and weave cotton cloth；
(5) Final finishing of long-acting slow-release fragrance fabric processes, and is padded by long-acting slow-release fragrance fabric compounding
In solution, and pick-up is 70%；Finally carrying out drying and processing, temperature during drying is 120-150 DEG C,
Time is 40-60s.
In one embodiment of the invention, to be contained within the aromatic micro-capsule of 15-20g/L whole for described combination solution
The nano adhesive NANO-PU of reason agent BAYSCENT (open up receive chemistry) and 10-15g/L (in spinning
Work).
In one embodiment of the invention, described natural aromatic substance is jasmine, lavandula angustifolia or Flos Rosae Rugosae.
In one embodiment of the invention, the mass percent of described superfine powder accounts for suspension slurry
10-20%.
By technique scheme, the invention has the beneficial effects as follows:
The present invention uses load technology to be carried on porous mineral materials by fragrance powder body, reapplies polyester fine
A kind of fiber with persistently release fragrance is prepared, in order to strengthen the fragrance of fragrance and hold on the spining technology of dimension
Property for a long time, selects natural aromatic microcapsule dressing agent to compound nano adhesive on last phase tidying up, the most both ensured
Fragrance also has good feel simultaneously, and sustainable more than 2 years of its fragrance is water-fastness more than 20 times, this
A little technology all in the past can not be compared.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect,
The present invention is further elucidated below.
Embodiment 1
The invention discloses the preparation method of a kind of long-acting slow-release fragrance fabric；This preparation method includes making as follows
Standby step:
(1) preparation of aroma loaded powder body, by porous mineral materials, (meerschaum, Xixia County's auspicious mining industry of gold has
Limit responsible company) it is ground to 200-300nm, put in homogenizer, add water and stir, high-speed stirred
Machine carries out making beating operation, makes the suspension slurry that concentration is 1%～10%；Natural aromatic substance (is included jasmine
The XIANGFEN such as jasmine, lavandula angustifolia, Flos Rosae Rugosae, Dongguan Wan Te Chemical Co., Ltd.) it is milled into superfine powder, will be relatively
The aromatic substance superfine powder of suspension slurry mass ratio 10-20% joins the suspension slurry in homogenizer
In, the pH value of adjustment reaction system is to 5, and room temperature reaction controlled at 2 hours；Then select centrifugal or filter
Method carries out processed to suspension slurry；Gains after processed are entered at a temperature of less than 80 DEG C
Row is dried, and carries out dried and obtain aroma loaded powder body after drying, and temperature during dried is 140 DEG C,
Drying time is 40min, is ground after drying, and aroma loaded powder body is ground to 200-300nm,
To the water content aroma loaded powder body less than 10%；
(2) prepared by fragrant fiber, and the aroma loaded powder body after grinding is by single screw feeders feeding one
In mixing apparatus, polyester fiber plain film is fed in this mixing apparatus, at this by single screw rod feeding machine simultaneously
After aroma loaded powder body in mixing apparatus and polyester fiber plain film mix homogeneously, send in apparatus for melt spinning
After melted, spray webbing, enter acid bath coagulation forming, then through drawing-off, washing, desulfurization, bleach, oil, de-
Water, cut off, dry and make fragrant fiber；
(3) preparation of long-acting fragrance yarn, long-acting fragrance yarn uses fragrant fiber and cotton to carry out blending,
Blending rate is 30% fragrant fiber, and 70% is cotton；The preparation of this yarn not only has good fragrance, becomes simultaneously
This is relatively low；
(4) preparation of long-acting slow-release fragrance fabric, organizine and tram all select long-acting fragrance yarn, then
Put in loom and weave cotton cloth；
(5) Final finishing of long-acting slow-release fragrance fabric processes, and is padded by long-acting slow-release fragrance fabric compounding
In solution, combination solution is contained within the aromatic micro-capsule finishing agent BAYSCENT (open up receive chemistry) of 15g/L
With the nano adhesive NANO-PU of 10g/L (in spin chemical industry)；And pick-up is 70%；Finally dry
Dry-cure, temperature during drying is 120 DEG C, and the time is 40s；Final finishing processes and improves fabric thick flavor
Degree and the persistency of fragrance, have good feel simultaneously.
Embodiment 2
The invention discloses the preparation method of a kind of long-acting slow-release fragrance fabric；This preparation method includes making as follows
Standby step:
(1) preparation of aroma loaded powder body, by porous mineral materials, (meerschaum, Xixia County's auspicious mining industry of gold has
Limit responsible company) it is ground to 200-300nm, put in homogenizer, add water and stir, high-speed stirred
Machine carries out making beating operation, makes the suspension slurry that concentration is 1%～10%；Natural aromatic substance (is included jasmine
The XIANGFEN such as jasmine, lavandula angustifolia, Flos Rosae Rugosae, Dongguan Wan Te Chemical Co., Ltd.) it is milled into superfine powder, will be relatively
The aromatic substance superfine powder of suspension slurry mass ratio 10-20% joins the suspension slurry in homogenizer
In, the pH value of adjustment reaction system is to 6, and room temperature reaction controlled at 2.5 hours；Then centrifugal or mistake is selected
Filtering method carries out processed to suspension slurry；By the gains after processed at a temperature of less than 80 DEG C
Drying, carry out dried and obtain aroma loaded powder body after drying, temperature during dried is
160 DEG C, drying time is 60min, is ground after drying, and aroma loaded powder body is ground to 200-300nm,
Obtain the water content aroma loaded powder body less than 10%；
(2) prepared by fragrant fiber, and the aroma loaded powder body after grinding is by single screw feeders feeding one
In mixing apparatus, polyester fiber plain film is fed in this mixing apparatus, at this by single screw rod feeding machine simultaneously
After aroma loaded powder body in mixing apparatus and polyester fiber plain film mix homogeneously, send in apparatus for melt spinning
After melted, spray webbing, enter acid bath coagulation forming, then through drawing-off, washing, desulfurization, bleach, oil, de-
Water, cut off, dry and make fragrant fiber；
(3) preparation of long-acting fragrance yarn, long-acting fragrance yarn uses fragrant fiber and cotton to carry out blending,
Blending rate is 30% fragrant fiber, and 70% is cotton；The preparation of this yarn not only has good fragrance, becomes simultaneously
This is relatively low；
(4) preparation of long-acting slow-release fragrance fabric, organizine and tram all select long-acting fragrance yarn, then
Put in loom and weave cotton cloth；
(5) Final finishing of long-acting slow-release fragrance fabric processes, and is padded by long-acting slow-release fragrance fabric compounding
In solution, combination solution is contained within the aromatic micro-capsule finishing agent BAYSCENT (open up receive chemistry) of 18g/L
With the nano adhesive NANO-PU of 12g/L (in spin chemical industry)；And pick-up is 70%；Finally dry
Dry-cure, temperature during drying is 135 DEG C, and the time is 50s；Final finishing processes and improves fabric thick flavor
Degree and the persistency of fragrance, have good feel simultaneously.
Embodiment 3
The invention discloses the preparation method of a kind of long-acting slow-release fragrance fabric；This preparation method includes making as follows
Standby step:
(1) preparation of aroma loaded powder body, by porous mineral materials, (meerschaum, Xixia County's auspicious mining industry of gold has
Limit responsible company) it is ground to 200-300nm, put in homogenizer, add water and stir, high-speed stirred
Machine carries out making beating operation, makes the suspension slurry that concentration is 1%～10%；Natural aromatic substance (is included jasmine
The XIANGFEN such as jasmine, lavandula angustifolia, Flos Rosae Rugosae, Dongguan Wan Te Chemical Co., Ltd.) it is milled into superfine powder, will be relatively
The aromatic substance superfine powder of suspension slurry mass ratio 10-20% also joins the suspension slurry in homogenizer
In liquid, the pH value of adjustment reaction system is to 7, and room temperature reaction controlled at 3 hours；Then centrifugal or mistake is selected
Filtering method carries out processed to suspension slurry；By the gains after processed at a temperature of less than 80 DEG C
Drying, carry out dried and obtain aroma loaded powder body after drying, temperature during dried is
180 DEG C, drying time is 80min, is ground after drying, and aroma loaded powder body is ground to 200-300nm,
Obtain the water content aroma loaded powder body less than 10%；
(2) prepared by fragrant fiber, and the aroma loaded powder body after grinding is by single screw feeders feeding one
In mixing apparatus, polyester fiber plain film is fed in this mixing apparatus, at this by single screw rod feeding machine simultaneously
After aroma loaded powder body in mixing apparatus and polyester fiber plain film mix homogeneously, send in apparatus for melt spinning
After melted, spray webbing, enter acid bath coagulation forming, then through drawing-off, washing, desulfurization, bleach, oil, de-
Water, cut off, dry and make fragrant fiber；
(3) preparation of long-acting fragrance yarn, long-acting fragrance yarn uses fragrant fiber and cotton to carry out blending,
Blending rate is 30% fragrant fiber, and 70% is cotton；The preparation of this yarn not only has good fragrance, becomes simultaneously
This is relatively low；
(4) preparation of long-acting slow-release fragrance fabric, organizine and tram all select long-acting fragrance yarn, then
Put in loom and weave cotton cloth；
(5) Final finishing of long-acting slow-release fragrance fabric processes, and is padded by long-acting slow-release fragrance fabric compounding
In solution, combination solution is contained within the aromatic micro-capsule finishing agent BAYSCENT (open up receive chemistry) of 20g/L
With the nano adhesive NANO-PU of 15g/L (in spin chemical industry)；And pick-up is 70%；Finally dry
Dry-cure, temperature during drying is 150 DEG C, and the time is 60s；Final finishing processes and improves fabric thick flavor
Degree and the persistency of fragrance, have good feel simultaneously.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.The industry
Skilled person will appreciate that, the present invention is not restricted to the described embodiments, in above-described embodiment and description
The principle that the present invention is simply described described, without departing from the spirit and scope of the present invention, the present invention
Also having various changes and modifications, these changes and improvements both fall within scope of the claimed invention.This
The claimed scope of invention is defined by appending claims and equivalent thereof.
Claims (4)
1. the preparation method of a long-acting slow-release fragrance fabric；It is characterized in that: described preparation method include as
Lower preparation process:
(1) preparation of aroma loaded powder body, by porous mineral materials, (meerschaum, Xixia County's auspicious mining industry of gold has
Limit responsible company) it is ground to 200-300nm, put in homogenizer, add water and stir, high-speed stirred
Machine carries out making beating operation, makes the suspension slurry that concentration is 1%～10%；Natural aromatic substance is milled into
Superfine powder, and join in the suspension slurry in homogenizer, adjust the pH value of reaction system to 5～
7, room temperature reaction controlled at 2～3 hours；Then selection is centrifugal or suspension slurry is dehydrated by filter method
Process；Then the gains after dehydration are dried at a temperature of less than 80 DEG C, be dried after drying
Process obtains aroma loaded powder body, and baking temperature is 140～180 DEG C, and drying time is 40～80min, dry
It is ground after dry, aroma loaded powder body is ground to 200-300nm, obtain water content bearing less than 10%
Carry fragrance powder body；
(2) prepared by fragrant fiber, and the aroma loaded powder body after grinding is by single screw feeders feeding one
In mixing apparatus, polyester fiber plain film is fed in this mixing apparatus, at this by single screw rod feeding machine simultaneously
After aroma loaded powder body in mixing apparatus and polyester fiber plain film mix homogeneously, send in apparatus for melt spinning
After melted, spray webbing, enter acid bath coagulation forming, then through drawing-off, washing, desulfurization, bleach, oil, de-
Water, cut off, dry and make fragrant fiber；
(3) preparation of long-acting fragrance yarn, long-acting fragrance yarn uses fragrant fiber and cotton to carry out blending,
Blending rate is 30% fragrant fiber, and 70% is cotton；
(4) preparation of long-acting slow-release fragrance fabric, organizine and tram all select long-acting fragrance yarn, then
Put in loom and weave cotton cloth；
(5) Final finishing of long-acting slow-release fragrance fabric processes, and is padded by long-acting slow-release fragrance fabric compounding
In solution, and pick-up is 70%；Finally carrying out drying and processing, temperature during drying is 120-150 DEG C,
Time is 40-60s.
The preparation method of a kind of long-acting slow-release fragrance fabric the most according to claim 1, its feature exists
In: described combination solution is contained within the aromatic micro-capsule finishing agent BAYSCENT of 15-20g/L and (opens up receiving
Learn) and the nano adhesive NANO-PU (in spin chemical industry) of 10-15g/L.
The preparation method of a kind of long-acting slow-release fragrance fabric the most according to claim 1, its feature exists
In: described natural aromatic substance is jasmine, lavandula angustifolia or Flos Rosae Rugosae.
The preparation method of a kind of long-acting slow-release fragrance fabric the most according to claim 1, its feature exists
In: the mass percent of described superfine powder accounts for the 10-20% of suspension slurry.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510024110.6A CN105839420A (en) | 2015-01-16 | 2015-01-16 | Preparation method of sustained-release fragrant fabric |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510024110.6A CN105839420A (en) | 2015-01-16 | 2015-01-16 | Preparation method of sustained-release fragrant fabric |
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| CN201510024110.6A Pending CN105839420A (en) | 2015-01-16 | 2015-01-16 | Preparation method of sustained-release fragrant fabric |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106637478A (en) * | 2016-10-20 | 2017-05-10 | 上海星松化纤股份有限公司 | Terylene-based intelligent temperature-adjusting fiber and manufacturing method thereof |
| CN107699977A (en) * | 2017-10-26 | 2018-02-16 | 浙江华峰氨纶股份有限公司 | A kind of polyurethane elastomeric fiber with permanent fragrance and preparation method thereof |
| CN109183184A (en) * | 2018-08-14 | 2019-01-11 | 北京麻世纪麻业科技发展有限公司 | A kind of preparation method and capsule fiber of capsule fiber |
| CN111021061A (en) * | 2019-12-24 | 2020-04-17 | 淄博大染坊丝绸集团有限公司 | After-finishing process of hyaluronic acid real silk fabric |
| CN111041841A (en) * | 2019-12-24 | 2020-04-21 | 淄博大染坊丝绸集团有限公司 | Finishing process of argan silk fabric |
| CN113802385A (en) * | 2021-09-23 | 2021-12-17 | 天津工业大学 | Preparation method of lasting fragrance-retaining knitted fabric capable of releasing fragrance substances in gradient manner |
| CN113832736A (en) * | 2021-09-23 | 2021-12-24 | 天津工业大学 | Preparation method of lasting fragrance-retaining knitted underpants capable of releasing fragrance substances in gradient manner |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106637478A (en) * | 2016-10-20 | 2017-05-10 | 上海星松化纤股份有限公司 | Terylene-based intelligent temperature-adjusting fiber and manufacturing method thereof |
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| CN107699977A (en) * | 2017-10-26 | 2018-02-16 | 浙江华峰氨纶股份有限公司 | A kind of polyurethane elastomeric fiber with permanent fragrance and preparation method thereof |
| CN109183184A (en) * | 2018-08-14 | 2019-01-11 | 北京麻世纪麻业科技发展有限公司 | A kind of preparation method and capsule fiber of capsule fiber |
| CN111021061A (en) * | 2019-12-24 | 2020-04-17 | 淄博大染坊丝绸集团有限公司 | After-finishing process of hyaluronic acid real silk fabric |
| CN111041841A (en) * | 2019-12-24 | 2020-04-21 | 淄博大染坊丝绸集团有限公司 | Finishing process of argan silk fabric |
| CN111041841B (en) * | 2019-12-24 | 2022-10-11 | 淄博大染坊丝绸集团有限公司 | Finishing process of argan silk fabric |
| CN111021061B (en) * | 2019-12-24 | 2022-10-11 | 淄博大染坊丝绸集团有限公司 | After-finishing process of hyaluronic acid real silk fabric |
| CN113802385A (en) * | 2021-09-23 | 2021-12-17 | 天津工业大学 | Preparation method of lasting fragrance-retaining knitted fabric capable of releasing fragrance substances in gradient manner |
| CN113832736A (en) * | 2021-09-23 | 2021-12-24 | 天津工业大学 | Preparation method of lasting fragrance-retaining knitted underpants capable of releasing fragrance substances in gradient manner |
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Application publication date: 20160810 |
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