CN105833939A - High-speed centrifugal film dispersion machine - Google Patents

High-speed centrifugal film dispersion machine Download PDF

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Publication number
CN105833939A
CN105833939A CN201610388795.7A CN201610388795A CN105833939A CN 105833939 A CN105833939 A CN 105833939A CN 201610388795 A CN201610388795 A CN 201610388795A CN 105833939 A CN105833939 A CN 105833939A
Authority
CN
China
Prior art keywords
grinding
dispersion machine
film dispersion
sensor
storage tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610388795.7A
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Chinese (zh)
Inventor
边浩光
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUXI XINGUANG POWDER PROCESS CO Ltd
Original Assignee
WUXI XINGUANG POWDER PROCESS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WUXI XINGUANG POWDER PROCESS CO Ltd filed Critical WUXI XINGUANG POWDER PROCESS CO Ltd
Priority to CN201610388795.7A priority Critical patent/CN105833939A/en
Publication of CN105833939A publication Critical patent/CN105833939A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C7/00Crushing or disintegrating by disc mills
    • B02C7/02Crushing or disintegrating by disc mills with coaxial discs
    • B02C7/04Crushing or disintegrating by disc mills with coaxial discs with concentric circles of intermeshing teeth
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/02Feeding devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C7/00Crushing or disintegrating by disc mills
    • B02C7/11Details
    • B02C7/14Adjusting, applying pressure to, or controlling distance between, discs

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  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Crushing And Grinding (AREA)

Abstract

The invention discloses a film dispersion machine. The film dispersion machine comprises a grinding cavity (18). A dynamic grinding disc (4) and a static grinding disc (5) are arranged in the grinding cavity (18). A material hole is formed in the middle of the static grinding disc (5) and communicates with the bottom of a storage tank (8) through a first circulating pipe (7). A circulating pump (6) is arranged on the first circulating pipe (7). The grinding cavity (18) communicates with the upper portion of the storage tank (8) through a second circulating pipe (11). The film dispersion machine is good in dispersion effect.

Description

A kind of high speed centrifugation film dispersion machine
Technical field
The present invention relates to the processing of nano material, particularly a kind of for CNT dispersion, Graphene machinery The film dispersion machine that the dispersion of the high viscosity nano materials such as stripping is peeled off.
Background technology
The dispersion of current CNT and the application diversification day by day of grapheme material, demand increases day by day.On market There is no suitable machine to complete this decentralized task.Existing way is to carry out sand milling with sand mill.Due to The viscosity of material to be processed is generally at 5000-10000CPS, and sand mill is owing to using abrading-ball, uses mill Ball exists for the problem that ball material separates, and ball material separates within most can only processing 2000CPS, and viscosity is high After, easily there is putty problem, existing way in machinery, and maximum disadvantage is just because the event that putty causes Barrier frequency of maintenance is too high.Maintenance cost high problem.
Summary of the invention
For the defect of prior art, the invention provides a kind of high speed centrifugation film dispersion machine.
A kind of film dispersion machine, including grinding chamber 18, is provided with movable grinding disc 4 and quiet mill in described grinding chamber 18 Dish 5, is provided with material hole in the middle of described static cutting disk 5, described material hole is by the first circulation pipe 7 and storage tank 8 Bottom connection, described first circulation pipe 7 is provided with circulating pump 6, and described grinding chamber 18 is by the second circulation Pipe 11 connects with the top of described storage tank 8.
Optionally, adjusted between described movable grinding disc 4 and described static cutting disk 5 by the described static cutting disk 5 of adjustment Grinding gap.Described movable grinding disc 4 is connected with the grinding motor 1 being arranged at outside grinding chamber 18 by rotating shaft, Sealing gland is carried out between described rotating shaft and grinding chamber 18.In described storage tank 8, agitator 13 is installed, described in stir Mix device 13 to be driven by the stirring motor 12 being arranged at storage tank 8 top.Described storage tank 8 is a hermetically sealed can. Also include controller 10 and sensor 9, controller 10 respectively with described grinding motor 1, circulating pump 6, quiet Mill 5 is connected with sensor 9.Described sensor 9 is particle size sensor, and described controller 10 is according to reception The particle size sensor signal arrived, adjusts the position of described static cutting disk 5.Described sensor 9 is flow sensor, Described controller 10, according to the detection signal of the flow sensor received, adjusts described grinding motor 1 or follows The rotating speed of ring pump 6.Being provided with agitator 13 in described storage tank 8, described agitator 13 is by being arranged at storing The stirring motor 12 on tank 8 top drives.The top of described storage tank 8 is provided with vacuum pumping pump 15;Described grind Mill chamber 18 is made up of upper shell 17 and lower shell 3, and described upper shell 17 and lower shell about 3 two parts are handed over Stack, form an airtight cavity, by adjust described lower shell 3 adjust described movable grinding disc 4 with Grinding gap between described static cutting disk 5;Controller 10, according to the load grinding motor 1 detected, is adjusted Grinding gap a between whole described movable grinding disc 4 and described static cutting disk 5.
The invention has the beneficial effects as follows: the present invention uses one to move quiet two mills, and material is in the middle of static cutting disk Input, by sound two abrasive disk space run up, by centrifugal mill of making every effort to defeat at a high speed, and plays dispersion The effect of material.Static cutting disk can be set to fluctuate in certain limit, with adaptation granularity in running Wide in range material.Obtain more preferable dispersion effect.
Accompanying drawing explanation
Fig. 1 is the structural representation of film dispersion machine of the present invention.
Detailed description of the invention
Understandable for enabling the above-mentioned purpose of the present invention, feature and advantage to become apparent from, the most right The detailed description of the invention of the present invention is described in detail, and makes the above and other purpose of the present invention, feature and excellent Will definitely become apparent from.The part that reference instruction identical in whole accompanying drawings is identical.The most deliberately by than Example draws accompanying drawing, it is preferred that emphasis is illustrate the purport of the present invention.
The film dispersion machine of the present invention substantially can be divided into grind section and Matter Transfer portion, and it is right that grind section is mainly responsible for CNT or the grinding of Graphene, circulation portions is then responsible for that Matter Transfer is sent into grind section thus can realize thing The grinding repeatedly of material, so that material reaches the particle diameter specified.
Refer to Fig. 1, a kind of film dispersion machine, including grinding chamber 18, be provided with dynamic in described grinding chamber 18 Mill 4 and static cutting disk 5, described movable grinding disc 4 is by rotating shaft and the grinding motor being arranged at outside grinding chamber 18 1 is connected, and carries out sealing gland between rotating shaft and grinding chamber 18, and sealing gland can use labyrinth air seal circle/pad existing, Being provided with material hole in the middle of described static cutting disk 5, described material hole is by the bottom of the first circulation pipe 7 with storage tank 8 Connection, described first circulation pipe 7 is provided with circulating pump 6, and described grinding chamber 18 is by the second circulation pipe 11 Connecting with the top of described storage tank 8, be provided with agitator 13 in described storage tank 8, agitator 13 is by setting The stirring motor 12 being placed in storage tank 8 top drives, and the top of described storage tank 8 is provided with hopper 14, treats Grinding material enters in storage tank 8 from hopper, and storage tank 8 is a hermetically sealed can, and top is provided with vacuum pumping pump 15, the air in storage tank 8 can be extracted out by vacuum pumping pump 15, permissible by gas atmosphere inlet 19 It is passed through protective gas, is so possible to prevent the oxidation of material in process of lapping.Further, also include controlling Device 10 and flow sensor 9, controller 10 respectively with described grinding motor 1, circulating pump 6, static cutting disk 5 It is connected with sensor 9.
Further, grinding chamber 18 is made up of upper shell 17 and lower shell 3, upper shell 17 and lower shell 3 Upper and lower two parts overlap on together, form an airtight cavity, when gap a changes up and down, by overlapping Part compensates, and upper shell 17 is fixed cylinder, and lower shell 3 can move up and down relative to upper shell 17, Described static cutting disk 5 is arranged in described lower shell 3, and lower shell 3 adjusts motor 16 with gap and is connected, and passes through Gap adjusts motor 16 and drives lower shell 3 to move up and down, thus adjusts between movable grinding disc 4 and static cutting disk 5 Gap.Adjust gap a by adjustment cylinder can farthest reduce grinding component (movable grinding disc 4 With static cutting disk 5) impact, owing to grinding component does not do movement relative to cylinder, such that it is able to prevent its machinery Abrasion, damage, increase service life.
In the present invention, treating material is deposited in storage tank 8, by circulating pump 6 by storage tank 8 Material is delivered to static cutting disk 5, enters from the material hole of static cutting disk 5 bottom two mill intermediate space a, static cutting disk 5 rotate in the middle part of process of lapping, but static cutting disk 5 can fluctuate, thus adjust gap a, due to Static cutting disk 5 does not rotates, and such static cutting disk 5 only moves up and down, and this regulative mode makes equipment not Easily be damaged (if adjusting movable grinding disc 4, the rotating shaft of movable grinding disc to move up and down, simultaneously need to rotate, this It is more complicated that sample allows for guiding mechanism, is susceptible to damage).Gap a is by can be by the journey in controller 10 Sequence makees fluctuating of respective range according to the granularity of material.Movable grinding disc 4, with the linear speed of 50-100m/s, is made Constant runs up, and material passes through two abrasive disk spaces, is sheared by the effect of high speed centrifugation power, grinds, Being back to after grinding in storage tank 8, after completing a cycle grinding, material is sent into and is ground by circulating pump 6 again In mill chamber 18, so go round and begin again, until reaching to set granularity.Agitator 13 in process of lapping For material stirring is mixed.
Controller 10 controls circulating pump 6 according to the signal gathered described in sensor 9, grinds motor 1 and quiet mill Dish 5.Specifically, sensor 9 can include that flow sensor and particle size sensor, controller 10 receive After raw meal particle size detected by particle size sensor, adjust the position of static cutting disk 5, Mei Yizhou according to detected value After phase is ground, raw meal particle size all can diminish, and controller 10 controls static cutting disk 5 and is gradually increasing, thus reduces Gap a so that material is by the most finely ground, and controller 10 can also receive the stream that flow sensor is sent here Amount signal, flow signal indicate entry into material in grinding chamber 18 number, the thing in entering grinding chamber 18 When material exceeds setting range or exceedes disposal ability, controller 10 reduces the rotating speed of circulating pump 6, thus reduces Enter the material in grinding chamber 18, or controller 10 is when detecting that flow increases, improve and grind motor 1 Rotating speed, such that it is able to process more material.May insure that entrance is ground by the above-mentioned adjustment of controller 10 Inventory in mill chamber 18 adapts with the disposal ability of grinding chamber 18, it is ensured that enter the thing in grinding chamber 18 Material is all fully ground, by constantly adjusting gap a, it is ensured that material to be ground reaches to set granularity.Enter One step, controller 10 can also detect the load (power output) grinding motor 1, and load can basis The voltage of motor is calculated with parameters such as electric currents, and these belong to prior art and repeat no more.When electricity being detected When the load of machine exceedes the threshold value of setting, at this moment indicating, enter the material between mill more, particle diameter is relatively big, Controller 10 increases gap a by adjusting motor 16, otherwise then reduces gap a.The present invention uses mill Grind, it is to avoid ball material separation problem, and the amount every time ground is the least, thus avoids putty.
Elaborate a lot of detail in the above description so that fully understanding the present invention.But more than retouch Stating is only presently preferred embodiments of the present invention, and the present invention can be to be much different from other side described here Formula is implemented, and therefore the present invention is not limited by disclosed above being embodied as.The most any it is familiar with this area Technical staff, without departing under technical solution of the present invention ambit, may utilize method and the skill of the disclosure above Technical solution of the present invention is made many possible variations and modification by art content, or be revised as equivalent variations etc. Effect embodiment.Every content without departing from technical solution of the present invention, according to the present invention technical spirit to more than Any simple modification, equivalent variations and the modification that embodiment is done, all still falls within technical solution of the present invention protection In the range of.

Claims (10)

1. a film dispersion machine, it is characterised in that include grinding chamber (18), described grinding chamber (18) Inside it is provided with in the middle of movable grinding disc (4) and static cutting disk (5), described static cutting disk (5) and is provided with material hole, described Material hole is connected with the bottom of storage tank (8), on described first circulation pipe (7) by the first circulation pipe (7) Being provided with circulating pump (6), described grinding chamber (18) is by the second circulation pipe (11) and described storage tank (8) Top connection.
Film dispersion machine the most according to claim 1, it is characterised in that by adjusting described static cutting disk (5) the grinding gap between described movable grinding disc (4) and described static cutting disk (5) is adjusted.
Film dispersion machine the most according to claim 1, it is characterised in that described movable grinding disc (4) leads to The grinding motor (1) crossing rotating shaft and be arranged at outside grinding chamber (18) is connected, described rotating shaft and grinding chamber (18) Between be hermetic.
Film dispersion machine the most according to claim 1, it is characterised in that in described storage tank (8) Being provided with agitator (13), described agitator (13) is by the stirring being arranged at described storage tank (8) top Motor (12) drives.
Film dispersion machine the most according to claim 1, it is characterised in that described grinding chamber (18) by Upper shell (17) and lower shell (3) composition, described upper shell (17) and upper and lower two of lower shell (3) Part overlaps on together, adjusts described movable grinding disc (4) and described quiet mill by adjusting described lower shell (3) Grinding gap between dish (5).
Film dispersion machine the most according to claim 1, it is characterised in that also include controller (10) With sensor (9), controller (10) respectively with grind motor (1), circulating pump (6), sensor (9), Gap adjusts motor (16) and is connected.
Film dispersion machine the most according to claim 6, it is characterised in that described sensor (9) is Particle size sensor, described controller (10), according to the particle size sensor signal received, adjusts described quiet mill The position of dish (5).
Film dispersion machine the most according to claim 6, it is characterised in that described sensor (9) is Flow sensor, described controller (10), according to the detection signal of the flow sensor received, adjusts institute State grinding motor (1) or the rotating speed of circulating pump (6), or regulation gap a.
Film dispersion machine the most according to claim 1, it is characterised in that described movable grinding disc (4) with The linear speed of 50-100m/s rotates.
Film dispersion machine the most according to claim 1, it is characterised in that described controller (10) According to the load of the grinding motor (1) detected, adjust described movable grinding disc (4) and described static cutting disk (5) Between grinding gap a.
CN201610388795.7A 2016-06-03 2016-06-03 High-speed centrifugal film dispersion machine Pending CN105833939A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Publications (1)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108175117A (en) * 2018-02-12 2018-06-19 费军 A kind of novel feed granules manufacture machinery
CN109382167A (en) * 2017-08-03 2019-02-26 中国石油化工股份有限公司 A kind of self-loopa millstone device under hyperbaric environment
CN110817853A (en) * 2018-08-07 2020-02-21 中国石油化工股份有限公司 Preparation method of edge carboxylated graphene
CN110947461A (en) * 2018-05-15 2020-04-03 安徽省华腾农业科技有限公司 Method for producing granules
CN111570024A (en) * 2020-05-26 2020-08-25 吕金坤 Be applied to grinding compounding equipment in straw class fodder preparation
CN115461155A (en) * 2020-04-23 2022-12-09 吉布尔法伊弗股份公司 Grinding method and installation with material input recognition

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CN1284409A (en) * 2000-04-24 2001-02-21 范继云 Down moving disc grinder with multi-stage serial pressure regulator
CN101797525A (en) * 2010-04-02 2010-08-11 陈佳明 Household stone milling machine
CN201644145U (en) * 2010-03-30 2010-11-24 威海恒邦化工有限公司 Ammonium phosphate tailing mill
CN202741192U (en) * 2012-06-05 2013-02-20 张万松 Pressure-adjustable electric stone mill
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CN204583182U (en) * 2015-02-16 2015-08-26 绍兴市辰星聚氨酯有限公司 For the special reactor of full water foamed polyurethane combined material synthesis insulation material
CN204768953U (en) * 2015-07-10 2015-11-18 东莞市琅菱机械有限公司 Self -circulation formula nanometer sand mill
CN105618190A (en) * 2016-01-30 2016-06-01 太仓液压元件有限公司 Low-energy-consumption colloid grinder type emulsifying machine
CN106076573A (en) * 2016-06-27 2016-11-09 安徽省思维新型建材有限公司 There is the water paint grinding system circulating the function that liquidates
CN205672986U (en) * 2016-06-03 2016-11-09 无锡新光粉体科技有限公司 A kind of high speed centrifugation thin film dispersion machine

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1284409A (en) * 2000-04-24 2001-02-21 范继云 Down moving disc grinder with multi-stage serial pressure regulator
CN201644145U (en) * 2010-03-30 2010-11-24 威海恒邦化工有限公司 Ammonium phosphate tailing mill
CN101797525A (en) * 2010-04-02 2010-08-11 陈佳明 Household stone milling machine
CN202741192U (en) * 2012-06-05 2013-02-20 张万松 Pressure-adjustable electric stone mill
CN204583182U (en) * 2015-02-16 2015-08-26 绍兴市辰星聚氨酯有限公司 For the special reactor of full water foamed polyurethane combined material synthesis insulation material
CN204564132U (en) * 2015-03-03 2015-08-19 徐挺 There is the reactor of bottom stirrer
CN204768953U (en) * 2015-07-10 2015-11-18 东莞市琅菱机械有限公司 Self -circulation formula nanometer sand mill
CN105618190A (en) * 2016-01-30 2016-06-01 太仓液压元件有限公司 Low-energy-consumption colloid grinder type emulsifying machine
CN205672986U (en) * 2016-06-03 2016-11-09 无锡新光粉体科技有限公司 A kind of high speed centrifugation thin film dispersion machine
CN106076573A (en) * 2016-06-27 2016-11-09 安徽省思维新型建材有限公司 There is the water paint grinding system circulating the function that liquidates

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109382167A (en) * 2017-08-03 2019-02-26 中国石油化工股份有限公司 A kind of self-loopa millstone device under hyperbaric environment
CN108175117A (en) * 2018-02-12 2018-06-19 费军 A kind of novel feed granules manufacture machinery
CN108175117B (en) * 2018-02-12 2020-10-23 嘉兴考普诺机械科技有限公司 Feed particle manufacturing machine
CN110947461A (en) * 2018-05-15 2020-04-03 安徽省华腾农业科技有限公司 Method for producing granules
CN110947461B (en) * 2018-05-15 2021-06-08 安徽省华腾农业科技有限公司 Method for producing granules
CN110817853A (en) * 2018-08-07 2020-02-21 中国石油化工股份有限公司 Preparation method of edge carboxylated graphene
CN110817853B (en) * 2018-08-07 2021-07-30 中国石油化工股份有限公司 Preparation method of edge carboxylated graphene
CN115461155A (en) * 2020-04-23 2022-12-09 吉布尔法伊弗股份公司 Grinding method and installation with material input recognition
CN115461155B (en) * 2020-04-23 2023-11-24 吉布尔法伊弗股份公司 Grinding method and installation with material input recognition
CN111570024A (en) * 2020-05-26 2020-08-25 吕金坤 Be applied to grinding compounding equipment in straw class fodder preparation

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Application publication date: 20160810

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