CN105779135A - Sweet osmanthus fragrance substance extracting method - Google Patents
Sweet osmanthus fragrance substance extracting method Download PDFInfo
- Publication number
- CN105779135A CN105779135A CN201610360501.XA CN201610360501A CN105779135A CN 105779135 A CN105779135 A CN 105779135A CN 201610360501 A CN201610360501 A CN 201610360501A CN 105779135 A CN105779135 A CN 105779135A
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- CN
- China
- Prior art keywords
- fragrance
- adsorbent
- flos osmanthi
- osmanthi fragrantis
- liquid
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention relates to the technical field of extracting fragrance substances from flowers, in particular to a sweet osmanthus fragrance substance extracting method. The method includes the following steps of spraying liquid A in sweet osmanthus planting soil when sweet osmanthus buds are going to flower within 5-7 days, wherein the volume of liquid A sprayed on each sweet osmanthus plant is 20-30 ml; 120 hours later, putting sweet osmanthus in a fragrance collecting tower with Baijiu fragrance, wherein the temperature is controlled to be 25-50 DEG C, the humidity is controlled to be 50-95%, and light is controlled by a fluorescent lamp for flowering; after an adsorbent layer adsorbs all fragrance, taking out the adsorbent and putting the adsorbent into a container to be sealed and stored; extracting the fragrance adsorbed in the adsorbent through a carbon dioxide liquid supercritical or soaking method. Compared with the prior art, the method has the outstanding substantial advantages and remarkable progresses that flower fragrance collecting time is shortened, flower fragrance collecting amount is increased, flower fragrance collecting can reach 0.35%, and the fragrance collecting tower is simple in structure, reasonable in design and low in manufacturing cost.
Description
Technical field
The present invention relates to from spending the middle technical field extracting flower aroma substance, particularly to a kind of Flos Osmanthi Fragrantis aroma substance extracting method.
Background technology
Flos Osmanthi Fragrantis is one of big famous flower of Chinese tradition ten, integrate greening, beautify, sweetening treatment view and admire the excellent Landscape Tree Species having both with practicality, Flos Osmanthi Fragrantis clearly can dust-tight, dense can be far excessive, rate as an unsurpassed one.Especially time midautumn, Cong Gui is in full bloom, night is quiet take turns circle when, reward osmanthus of filling a wine cup for, CHENXIANG is assailed the nostrils, Bracing.Chanting in colored poem at ancient Chinese, the quantity chanting Gui Zhizuo is also rather considerable.Just deeply liked by Chinese from ancient times, be considered tradition famous flower.But for the collection never ripe perfect method of Flos Osmanthi Fragrantis fragrance, therefore it is necessary to provide a kind of method that can collect Flos Osmanthi Fragrantis fragrance.
Summary of the invention
Present invention aims to the defect of prior art and deficiency, it is provided that a kind of simple in construction, Flos Osmanthi Fragrantis aroma substance extracting method reasonable in design, easy to use.
For achieving the above object, the technical solution used in the present invention is:
A kind of Flos Osmanthi Fragrantis aroma substance extracting method of the present invention, a, when Flos Osmanthi Fragrantis alabastrum will 5～7 days will open time, spray wine A liquid in the soil planting this Flos Osmanthi Fragrantis, it is 20～30ml that every strain Flos Osmanthi Fragrantis sprays the amount of wine A liquid；
B, after 120 hours, this Flos Osmanthi Fragrantis is placed in the aroma collection tower of liquor flavor, temperature controls at 25～50 DEG C, control method is 25～30 DEG C and keeps 1～3 hour, 30～40 DEG C keep 1～2 hour, 40～45 DEG C keep 2～4 hours, and humid control is 50～95%, and the flowers are in blossom puts to utilize daylight lamp control light allow；
C, utilizing the adsorbent layer of aroma collection top of tower, per kilogram flower wants the adsorbent of 0.8～1.3 kilogram, 5～10 hours aromaadsorption time, substantially sucks after fragrance, takes out adsorbent and is put in container, airtight deposits, storage temperature 4～10 DEG C；
The fragrance of absorption in d, use carbon dioxide liquid supercritical or immersing extraction adsorbent.
Further, the adsorbent described in step c is any one in activated carbon, macroporous resin or degreasing cotton.
Further, described aroma collection tower is made up of Ta Gai and tower main body, and tower lid is arranged on the top of tower main body, Ta Gai and tower main body and both can adopt threaded, it would however also be possible to employ snapping, it is possible to ensure that tower lid will not fall down from tower main body top；The surface configuration of described tower lid has several air-vents；Flos Osmanthi Fragrantis and adsorbent layer are arranged in the inner chamber of described aroma collection tower,
The internal chamber wall of described tower main body is disposed radially multiple boss for placing adsorbent layer, the internal chamber wall of described tower main body is fixedly installed the web plate for placing Flos Osmanthi Fragrantis, adsorbent layer is positioned at the surface of web plate, described tower body lumen is additionally provided with the liquid storage cylinder for holding Chinese liquor, the outer wall of described tower main body is provided with the inlet for filling Chinese liquor, and the bottom of liquid storage cylinder is additionally provided with leakage fluid dram；The internal chamber wall of described tower main body is disposed radially multiple daylight lamp for providing light source, and daylight lamp is between adsorbent layer and web plate.
Further, the A liquid described in step a by 98% pure water, 0.1% hat toxin, 0.1% (-)-methyl cis-2-pent-2'-enyl-3-oxocyclopentylacetate, 0.3% ethylene and 1.5% nitrogen-phosphorus-potassium compound fertilizer form.
Compared with prior art, the substantive distinguishing features that the present invention highlights with significant progress is:
1, carry out catalysis the flowers are in blossom the emission efficiency of speed and the fragrance of a flower by A liquid, by the emission efficiency of the distilled spirit fragrance catalysis fragrance of a flower, both can shorten fragrance of a flower acquisition time, fragrance of a flower collecting amount can be improved again, the fragrance of a flower of the present invention is collected can reach 0.35%, compared with tradition, it is possible to improve tens times；
2, in collection process, reach environmentally safe, obtain the fragrance of a flower gas of nonhazardous；
3, the aroma collection tower structure of the present invention is simple, reasonable in design, low cost of manufacture.
Accompanying drawing explanation
Fig. 1 is the structural representation of aroma collection tower；
Description of reference numerals:
1, Ta Gai；1-1, air-vent；
2, tower main body；2-1, boss；2-2, web plate；2-3, inlet；2-4, liquid storage cylinder；
3, daylight lamp；4, Chinese liquor；5, Flos Osmanthi Fragrantis；6, adsorbent layer.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is further illustrated.
Example 1:
A kind of Flos Osmanthi Fragrantis aroma substance extracting method of the present invention, comprises the steps:
A, when Flos Osmanthi Fragrantis alabastrum will 5 days will open time, spray wine A liquid in the soil planting this Flos Osmanthi Fragrantis, the amount of every strain Flos Osmanthi Fragrantis spray wine A liquid is 20ml.
B, after 120 hours, this Flos Osmanthi Fragrantis 5(be it should be noted that: Flos Osmanthi Fragrantis, soil move together with flowerpot) it is placed in the aroma collection tower of liquor flavor, temperature controls at 25～50 DEG C, control method is 25 DEG C and keeps 1 hour, 30 DEG C keep 2 hours, 40 DEG C keep 4 hours, and humid control, 50%, utilizes daylight lamp 3 to control light and allows the flowers are in blossom puts；
C, utilizing the adsorbent layer 6 of aroma collection top of tower, per kilogram flower wants the adsorbent of 1 kilogram, 10 hours aromaadsorption time, substantially sucks after fragrance, takes out adsorbent and is put in container, airtight deposits, storage temperature 4 DEG C；Adsorbent layer 6 is made up of the adsorbent of some parts exactly.
The fragrance of absorption in d, use carbon dioxide liquid supercritical extraction adsorbent.
Further, the adsorbent described in step c is activated carbon；A liquid described in step a by 98% pure water, 0.1% hat toxin, 0.1% (-)-methyl cis-2-pent-2'-enyl-3-oxocyclopentylacetate, 0.3% ethylene and 1.5% nitrogen-phosphorus-potassium compound fertilizer form.
Example 2:
A kind of Flos Osmanthi Fragrantis aroma substance extracting method of the present invention, comprises the steps:
A, when Flos Osmanthi Fragrantis alabastrum will 6 days will open time, spray wine A liquid in the soil planting this Flos Osmanthi Fragrantis, the amount of every strain Flos Osmanthi Fragrantis spray wine A liquid is 25ml；
B, after 120 hours, this Flos Osmanthi Fragrantis 5(be it should be noted that: Flos Osmanthi Fragrantis, soil move together with flowerpot) it is placed in the aroma collection tower of liquor flavor, temperature controls at 25～50 DEG C, control method is 28 DEG C and keeps 3 hours, 35 DEG C keep 1.5 hours, 43 DEG C keep 3 hours, and humid control, 70%, utilizes daylight lamp 3 to control light and allows the flowers are in blossom puts；
C, utilizing the adsorbent layer 6 of aroma collection top of tower, per kilogram flower wants the adsorbent of 0.8 kilogram, 7.5 hours aromaadsorption time, substantially sucks after fragrance, takes out adsorbent and is put in container, airtight deposits, storage temperature 8 DEG C；Adsorbent layer 6 is made up of the adsorbent of some parts exactly；
The fragrance of absorption in d, use carbon dioxide liquid supercritical extraction adsorbent.
Further, the adsorbent described in step c is macroporous resin；A liquid described in step a by 98% pure water, 0.1% hat toxin, 0.1% (-)-methyl cis-2-pent-2'-enyl-3-oxocyclopentylacetate, 0.3% ethylene and 1.5% nitrogen-phosphorus-potassium compound fertilizer form.
Example 3:
A kind of Flos Osmanthi Fragrantis aroma substance extracting method of the present invention, comprises the steps:
A, when Flos Osmanthi Fragrantis alabastrum will 7 days will open time, spray wine A liquid in the soil planting this Flos Osmanthi Fragrantis, the amount of every strain Flos Osmanthi Fragrantis spray wine A liquid is 30ml.
B, after 120 hours, this Flos Osmanthi Fragrantis 5(be it should be noted that: Flos Osmanthi Fragrantis, soil move together with flowerpot) it is placed in the aroma collection tower of liquor flavor, temperature controls at 25～50 DEG C, control method is 30 DEG C and keeps 2 hours, 40 DEG C keep 1 hour, 45 DEG C keep 2 hours, and humid control, 95%, utilizes daylight lamp 3 to control light and allows the flowers are in blossom puts；
C, utilizing the adsorbent layer 6 of aroma collection top of tower, per kilogram flower wants the adsorbent of 1.3 kilograms, 5 hours aromaadsorption time, substantially sucks after fragrance, takes out adsorbent and is put in container, airtight deposits, storage temperature 10 DEG C；Adsorbent layer 6 is made up of the adsorbent of some parts exactly.
The fragrance of absorption in d, use immersing extraction adsorbent.
Further, the adsorbent described in step c is degreasing cotton；A liquid described in step a by 98% pure water, 0.1% hat toxin, 0.1% (-)-methyl cis-2-pent-2'-enyl-3-oxocyclopentylacetate, 0.3% ethylene and 1.5% nitrogen-phosphorus-potassium compound fertilizer form.
As it is shown in figure 1, described aroma collection tower is made up of tower lid 1 and tower main body 2, tower lid 1 is arranged on the top of tower main body 2, tower lid 1 and tower main body 2 and both can adopt threaded, it would however also be possible to employ snapping, it is possible to ensure that tower lid 1 will not fall down from tower main body 2 top；The surface configuration of described tower lid 1 has several air-vents 1-1；Flos Osmanthi Fragrantis 5 and adsorbent layer 6 are arranged in the inner chamber of described aroma collection tower；The internal chamber wall of described tower main body 2 is disposed radially multiple boss 2-1 for placing adsorbent layer 6, the internal chamber wall of described tower main body 2 is fixedly installed the web plate 2-2 for placing Flos Osmanthi Fragrantis 5, adsorbent layer 6 is positioned at the surface of web plate 2-2, described tower main body 2 inner chamber is additionally provided with the liquid storage cylinder 2-4 for holding Chinese liquor, the outer wall of described tower main body 2 is provided with the inlet 2-3 for filling Chinese liquor, and the bottom of liquid storage cylinder 2-4 is additionally provided with leakage fluid dram (not shown)；The internal chamber wall of described tower main body 2 is disposed radially multiple daylight lamp 3 for providing light source, and daylight lamp 3 is between adsorbent layer 6 and web plate 2-2.
Compared with prior art, the substantive distinguishing features that the present invention highlights with significant progress is:
1, carry out catalysis the flowers are in blossom the emission efficiency of speed and the fragrance of a flower by A liquid, by the emission efficiency of the distilled spirit fragrance catalysis fragrance of a flower, both can shorten fragrance of a flower acquisition time, fragrance of a flower collecting amount can be improved again, the fragrance of a flower of the present invention is collected can reach 0.35%, compared with tradition, it is possible to improve tens times；
2, in collection process, reach environmentally safe, obtain the fragrance of a flower gas of nonhazardous；
3, the aroma collection tower structure of the present invention is simple, reasonable in design, low cost of manufacture.
The above is only the better embodiment of the present invention, therefore all equivalences done according to the structure described in present patent application scope, feature and principle change or modify, and are all included within the scope of present patent application.
Claims (3)
1. a Flos Osmanthi Fragrantis aroma substance extracting method, it is characterised in that: comprise the steps:
A, when Flos Osmanthi Fragrantis alabastrum will 5～7 days will open time, spray wine A liquid in the soil planting this Flos Osmanthi Fragrantis, the amount of every strain Flos Osmanthi Fragrantis spray wine A liquid is 20～30ml；
B, after 120 hours, this Flos Osmanthi Fragrantis (5) is placed in the aroma collection tower of liquor flavor, temperature controls at 25～50 DEG C, control method is 25～30 DEG C and keeps 1～3 hour, 30～40 DEG C keep 1～2 hour, 40～45 DEG C keep 2～4 hours, and humid control is 50～95%, and the flowers are in blossom puts to utilize daylight lamp (3) control light allow；
C, utilizing the adsorbent layer (6) of aroma collection top of tower, per kilogram flower wants the adsorbent of 0.8～1.3 kilogram, 5～10 hours aromaadsorption time, substantially sucks after fragrance, takes out adsorbent and is put in container, airtight deposits, storage temperature 4～10 DEG C；
The fragrance of absorption in d, use carbon dioxide liquid supercritical or immersing extraction adsorbent.
2. a kind of Flos Osmanthi Fragrantis aroma substance extracting method according to claim 1, it is characterised in that the adsorbent described in step c is any one in activated carbon, macroporous resin or degreasing cotton.
3. a kind of Flos Osmanthi Fragrantis aroma substance extracting method according to claim 1, it is characterised in that the A liquid described in step a by 98% pure water, 0.1% be preced with toxin, 0.1% (-)-methyl cis-2-pent-2'-enyl-3-oxocyclopentylacetate, 0.3% ethylene and 1.5% nitrogen-phosphorus-potassium compound fertilizer form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610360501.XA CN105779135A (en) | 2016-05-28 | 2016-05-28 | Sweet osmanthus fragrance substance extracting method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610360501.XA CN105779135A (en) | 2016-05-28 | 2016-05-28 | Sweet osmanthus fragrance substance extracting method |
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| CN105779135A true CN105779135A (en) | 2016-07-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610360501.XA Pending CN105779135A (en) | 2016-05-28 | 2016-05-28 | Sweet osmanthus fragrance substance extracting method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107041446A (en) * | 2017-01-09 | 2017-08-15 | 南宁市化工研究设计院 | It is a kind of to improve the method that jasmine fresh flower tells fragrant amount |
| CN111378530A (en) * | 2020-04-28 | 2020-07-07 | 兰星平 | Extraction method of osmanthus fragrans fragrant substance and floral essence solution obtained by extraction method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN101705150A (en) * | 2009-11-30 | 2010-05-12 | 浙江科技学院 | Green preparation method of osmanthus spice |
| CN102604743A (en) * | 2012-04-14 | 2012-07-25 | 河南羚锐制药股份有限公司 | Method for extracting volatile substance from plant |
| CN103525555A (en) * | 2013-09-25 | 2014-01-22 | 广西芳香植物开发应用有限公司 | Ecological flower growing method before extracting of aroma substance of sweet osmanthus |
| CN104531358A (en) * | 2014-12-08 | 2015-04-22 | 福建春伦茶业集团有限公司 | Jasmine flower scented oil collection extraction device and process thereof |
-
2016
- 2016-05-28 CN CN201610360501.XA patent/CN105779135A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN101705150A (en) * | 2009-11-30 | 2010-05-12 | 浙江科技学院 | Green preparation method of osmanthus spice |
| CN102604743A (en) * | 2012-04-14 | 2012-07-25 | 河南羚锐制药股份有限公司 | Method for extracting volatile substance from plant |
| CN103525555A (en) * | 2013-09-25 | 2014-01-22 | 广西芳香植物开发应用有限公司 | Ecological flower growing method before extracting of aroma substance of sweet osmanthus |
| CN104531358A (en) * | 2014-12-08 | 2015-04-22 | 福建春伦茶业集团有限公司 | Jasmine flower scented oil collection extraction device and process thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107041446A (en) * | 2017-01-09 | 2017-08-15 | 南宁市化工研究设计院 | It is a kind of to improve the method that jasmine fresh flower tells fragrant amount |
| CN111378530A (en) * | 2020-04-28 | 2020-07-07 | 兰星平 | Extraction method of osmanthus fragrans fragrant substance and floral essence solution obtained by extraction method |
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Application publication date: 20160720 |