CN105778359A - High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof - Google Patents

High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof Download PDF

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Publication number
CN105778359A
CN105778359A CN201610164814.8A CN201610164814A CN105778359A CN 105778359 A CN105778359 A CN 105778359A CN 201610164814 A CN201610164814 A CN 201610164814A CN 105778359 A CN105778359 A CN 105778359A
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CN
China
Prior art keywords
parts
banburying
rubber
sealing member
age resistor
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Withdrawn
Application number
CN201610164814.8A
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Chinese (zh)
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不公告发明人
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Individual
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Individual
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Priority to CN201610164814.8A priority Critical patent/CN105778359A/en
Publication of CN105778359A publication Critical patent/CN105778359A/en
Withdrawn legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C08L27/02Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L27/12Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Sealing Material Composition (AREA)

Abstract

The invention relates to a sealing material and belongs to the technical field of shaft rod sealing materials for pumps, valves and speed reducers having rotary motion. The material is prepared from 75-95 parts of compound rubber, 1-2 parts of melamine, 1-2 parts of zinc oxide, 1-2 parts of molybdenum sulfide, 4-6 parts of di-tetradecanol ester, 6-8 parts of chlorinated paraffin, 4-5 parts of polyethylene wax micro powder, 1-2 parts of tetrabutylammonium bromide, 1-2 parts of isopropyl xanthogen disulfide, 1-2 parts of antiager, 2-3 parts of polybutyl acrylate, 5-7 parts of limestone and 1-2 parts of terpineol. The preparation method includes: blending, banburying, tabletting, extruding and vulcanizing. The material has the advantages of higher wear resistance, higher corrosion resistance and lower pollution.

Description

Corrosion resistance preferable mechanical seal auxiliary sealing member material and preparation method thereof
Technical field
The present invention relates to a kind of encapsulant, belong to and have the axostylus axostyle of rotary motion to seal for pump class, valve, decelerator etc. Field of material technology.
Background technology
The existing pump packing using sizing specification, is filled in the stuffing-box of pump more.Although the more letter of this sealing means Just, a certain degree of effect can be played, but between this type of packing and pump shaft, still there is a certain degree of friction, even if The packing that coefficient of friction is the least, it is also surprising with the caloric value of axle contact position, therefore generally requires cooperation cooling system Cooperation.Long-Time Service is also quite serious to bearing wear simultaneously, and bearing can be caused permanent injury by Long-Time Service.
Muddy packing------is also referred to as: " pouring-in soft packing " is equipped with special grease and profit by a new generation's high-performance fiber Sliding, refined senior " packing " soft packing, arbitrary dimension, arbitrary shape, easily install, by special High Pressure Gun Just can directly inject, it is not necessary to as traditional packing, need precut, the packing box seal of any size can be suitable for.
Mechanical seal is the most advanced compared with for first two bearing seal mode is the gland seal device of a kind of rotating machinery.Such as The equipment such as centrifugal pump, centrifuge, reactor and compressor.Owing to power transmission shaft is applied in inside and outside equipment, so, between axle and equipment There is a circumferential clearance, the medium in equipment by this gap to outward leakage, if pressure subatmospheric in equipment, then empty Gas is revealed in equipment, it is therefore necessary to have one to stop the gland seal device revealed.The kind of axle envelope is a lot, owing to mechanical seal has There is leakage rate few and the advantage such as life-span length, so mechanical seal is in the topmost sealing side of these equipment in the world today Formula.End face seal is named again in mechanical seal, is defined such that and is perpendicular to rotation by least one pair of in relative national standards End face keep under the cooperation of fluid pressure and the effect of compensation mechanism elastic force (or magnetic force) and auxiliary seal laminating and phase The device preventing fluid from leaking that slip is constituted.
Mechanical seal is by a pair or several to being perpendicular to the end face of axle work slip relatively at fluid pressure and compensation mechanism Elastic force (or magnetic force) effect is lower to keep laminating and is equipped with auxiliary seal and reaches the gland seal device of Drain Resistance.Conventional machinery seals structure By stationary ring (stationary ring), rotating ring (rotating ring), flexible member, spring base, holding screw, rotating ring auxiliary seal ring and static The element compositions such as ring auxiliary seal ring, stop pin is fixed on gland to prevent stationary ring from rotating.Rotating ring and stationary ring are often Also whether can have nose balance ability according to them and be referred to as compensating ring or uncompensated ring.Use middle rotating ring auxiliary seal ring Easily senile abrasion, loses effect.
Summary of the invention
The technical problem to be solved in the present invention is, not enough for prior art, propose a kind of resilience effect more, more resistant to mill, Pollute less mechanical seal auxiliary sealing member material.
The present invention solves that the technical scheme that above-mentioned technical problem proposes is: a kind of mechanical seal auxiliary sealing member material Proportioning number is as follows: mixed rubber 75-95, melamine 1-2, zinc oxide 1-2, molybdenum bisuphide 1-2, double ten four carbon alcohols ester 4-6, Chlorinated paraffin 6-8, polyethylene wax micro mist 4-5, TBAB 1-2, dithiodiisopropyl xanthate 1-2, age resistor 1-2, butyl polyacrylate 2-3, lime stone 5-7, terpinol 1-2.
Described mixed rubber is to be mixed by the Polyether urethane rubber that weight ratio is 1:9 and fluorubber.
Described lime stone is the white lime containing a small amount of quick lime impurity.
Described age resistor is poor efficiency age resistor, typically uses phenol antiager.
The preparation method of described mechanical seal auxiliary sealing member material is as follows:
(1) dispensing: weight portion as described in claim 1 weighs raw material, and mixes;
(2) banburying: the raw material that will mix, puts into rubber internal mixer banburying 10-20 minute, and banburying temperature is: 85-100 ℃ ;
(3) in blocks: the material through banburying to be taken out, puts into friction machine and be rolled into film;
(4) extrusion: by step (3) film, use extruder for shaping;
(5) sulfuration: step (4) moulding material being put into the mould of vulcanizer, molds, vulcanize 6-15 minute, pressure is 20Mpa, temperature is 120-150 DEG C, then opens mould, and get product material.
The present invention uses technique scheme to provide the benefit that: because selecting mixed rubber Oil repellent higher, therefore make Rubber is the most stable, the most oxidizable and the phenomenon of ageing of rubber occur, has more preferable resilience, corrosion resistance and wear-resisting Property, service life is longer, needn't often change, although use poor efficiency age resistor, but the more environmental protection that has fewer environmental impacts, Even if occurring that leakage situation also to causing significant damage, and will not select mixed rubber fluorine-containing religion height itself, the most more Stable, it is difficult to oxidized or displaces, thus without the normal use affecting product itself.
Detailed description of the invention
Embodiment
A kind of mechanical seal auxiliary sealing member material of the present embodiment, proportioning number is as follows: mixed rubber 75-95, melamine Amine 1-2, zinc oxide 1-2, molybdenum bisuphide 1-2, double ten four carbon alcohols ester 4-6, chlorinated paraffin 6-8, polyethylene wax micro mist 4-5, four fourths Base ammonium bromide 1-2, dithiodiisopropyl xanthate 1-2, age resistor 1-2, butyl polyacrylate 2-3, lime stone 5-7, pine Oleyl alcohol 1-2.
Wherein, mixed rubber is to be mixed by the Polyether urethane rubber that weight ratio is 1:9 and fluorubber, and lime stone is The quick lime that white lime containing a small amount of quick lime impurity or water suction are made moist.
Age resistor uses phenol antiager, owing to this case rubber is fluorine-containing higher, more stable for other rubber, because of This employing anti-aging effect is poor but the phenol antiager of less pollution uses, the most more Environmental Safety, and anti-aging effect The most unaffected.
The material of the present embodiment is adopted and is prepared with the following method:
(1) dispensing: weight portion as described in claim 1 weighs raw material, and mixes;
(2) banburying: the raw material that will mix, puts into rubber internal mixer banburying 10-20 minute, and banburying temperature is: 85-100 ℃ ;
(3) in blocks: the material through banburying to be taken out, puts into friction machine and be rolled into film;
(4) extrusion: by step (3) film, use extruder for shaping;
(5) sulfuration: step (4) moulding material being put into the mould of vulcanizer, molds, vulcanize 6-15 minute, pressure is 20Mpa, temperature is 120-150 DEG C, then opens mould, obtains sealing member material.
The present invention is not limited to above-described embodiment.The technical scheme that all employing equivalents are formed, all falls within the present invention and wants The protection domain asked.

Claims (1)

1. a mechanical seal auxiliary sealing member material, it is characterised in that this material mixture ratio number is as follows: mixed rubber 75- 95, melamine 1-2, zinc oxide 1-2, molybdenum bisuphide 1-2, double ten four carbon alcohols ester 4-6, chlorinated paraffin 6-8, polyethylene wax micro mist 4-5, TBAB 1-2, dithiodiisopropyl xanthate 1-2, age resistor 1-2, butyl polyacrylate 2-3, lime Stone 5-7, terpinol 1-2;
Described mixed rubber is to be mixed by the Polyether urethane rubber that weight ratio is 1:9 and fluorubber;
Described age resistor is poor efficiency age resistor;Lime stone is quick lime;
The preparation method of described mechanical seal auxiliary sealing member material is as follows:
(1) dispensing: weight portion as described in claim 1 weighs raw material, and mixes;
(2) banburying: the raw material that will mix, puts into rubber internal mixer banburying 10-20 minute, and banburying temperature is: 85-100 ℃ ;
(3) in blocks: the material through banburying to be taken out, puts into friction machine and be rolled into film;
(4) extrusion: by step (3) film, use extruder for shaping;
(5) sulfuration: step (4) moulding material being put into the mould of vulcanizer, molds, vulcanize 6-15 minute, pressure is 20Mpa, temperature is 120-150 DEG C, then opens mould, and get product material.
CN201610164814.8A 2014-07-30 2014-07-30 High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof Withdrawn CN105778359A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610164814.8A CN105778359A (en) 2014-07-30 2014-07-30 High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610164814.8A CN105778359A (en) 2014-07-30 2014-07-30 High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201410368469.0A Division CN104151750B (en) 2014-07-30 2014-07-30 Mechanical seal auxiliary sealing member material and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105778359A true CN105778359A (en) 2016-07-20

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Family Applications (1)

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CN201610164814.8A Withdrawn CN105778359A (en) 2014-07-30 2014-07-30 High-corrosion-resistance auxiliary sealing member material for mechanical sealing and preparation method thereof

Country Status (1)

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CN (1) CN105778359A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102757607A (en) * 2012-07-27 2012-10-31 山东凯特工业技术有限公司 Fluorine-containing sealing wadding and preparation method thereof
CN103724834A (en) * 2013-12-13 2014-04-16 芜湖佳诚电子科技有限公司 Electrical insulation sealing ring

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102757607A (en) * 2012-07-27 2012-10-31 山东凯特工业技术有限公司 Fluorine-containing sealing wadding and preparation method thereof
CN103724834A (en) * 2013-12-13 2014-04-16 芜湖佳诚电子科技有限公司 Electrical insulation sealing ring

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Application publication date: 20160720

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