CN1057481A - The continuation method of preparation low density cake soap - Google Patents
The continuation method of preparation low density cake soap Download PDFInfo
- Publication number
- CN1057481A CN1057481A CN91101921.9A CN91101921A CN1057481A CN 1057481 A CN1057481 A CN 1057481A CN 91101921 A CN91101921 A CN 91101921A CN 1057481 A CN1057481 A CN 1057481A
- Authority
- CN
- China
- Prior art keywords
- soap
- pure
- added
- low density
- cake
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000344 soap Substances 0.000 title claims abstract description 107
- 238000000034 method Methods 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000003760 tallow Substances 0.000 claims abstract description 6
- 235000015278 beef Nutrition 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 9
- 235000013599 spices Nutrition 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000003755 preservative agent Substances 0.000 claims description 6
- 239000003963 antioxidant agent Substances 0.000 claims description 5
- 230000003078 antioxidant effect Effects 0.000 claims description 5
- 238000012856 packing Methods 0.000 claims description 5
- 238000005520 cutting process Methods 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims description 2
- 238000004806 packaging method and process Methods 0.000 claims description 2
- 238000005276 aerator Methods 0.000 claims 2
- 230000004927 fusion Effects 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 abstract description 6
- 238000005282 brightening Methods 0.000 abstract description 3
- 239000003337 fertilizer Substances 0.000 abstract description 3
- 230000002087 whitening effect Effects 0.000 abstract description 3
- 230000005484 gravity Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 description 13
- 238000002844 melting Methods 0.000 description 8
- 230000008018 melting Effects 0.000 description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 3
- 239000004408 titanium dioxide Substances 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 2
- 239000002738 chelating agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- MIJKYXHQIOTHGT-UHFFFAOYSA-N C(C)(C)(C)C=1C(=C(C=CC1)O)C(C)(C)C.CC1=CC=CC=C1 Chemical compound C(C)(C)(C)C=1C(=C(C=CC1)O)C(C)(C)C.CC1=CC=CC=C1 MIJKYXHQIOTHGT-UHFFFAOYSA-N 0.000 description 1
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 description 1
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- Detergent Compositions (AREA)
Abstract
The continuation method of a kind of preparation specific gravity control at 0.5-0.9 low density cake soap disclosed, institute's soap system consist of 10-50% Oleum Cocois and 50-90% Tallow, beef, moisture content is 28%-35%, does not use opalizer, whitening agent or brightening agent in this method and has increased admissible water-content in the finished product fertilizers soap blank.
Description
The present invention relates to prepare the continuation method that proportion can be controlled in the low density cake soap within 0.5 to 0.9 scope.The present invention be more particularly directed to not use opalizer, whitening agent or brightening agent and economically preparation have the method for white soap of washroom nature of soap matter; Increase the method for described soap-cake volume; And the method that increases admissible water-content in the finished product fertilizers soap blank.
The whole bag of tricks by the preparation of introducing air in soap composition inflation soap-cake is known.These methods need specific installation and need special formulation to have nothing in common with each other with the method for producing commercial acceptable product in some cases from simple and mechanical being stirred to of soap agitator.The typical prior art method comprises:
When 1, in agitator, stirring, air stirred in the molten soap bubble, for example by reverse rotation center whipping appts.
2,115 °F by improved soap extrusion machine introducing air in part exsiccant soap flakes, be disclosed in United States Patent (USP) 2,525 by Schulerud, in No. 081.
3, commercially available Mazzoni " Float-o-matic " screw extrusion press.
4, introduce gas and mix by the parichnos between two surfaces of replacing mutually and to inflate, be disclosed in No. 90648, the European patent.
5, make molten soap pass through heat exchanger, flashing chamber adds the continuous stirred tank reactor of air, is cooling/mixing tank then, is disclosed in United States Patent (USP) 2,295 by Mills, in No. 594.
Method 1,2,3 and 4 can not produce the soap-cake with desired uniform color, outward appearance or density.Method 3,4 and 5 needs special equipment.
Additive method is disclosed United States Patent (USP) 1,780,330(Blair); 2,210,924(Hood); 2,398,776(Bodmam); 2,494,891(Marshall); 4,311,604(Horning) and 4,680,132(Clark etc.) in.
A purpose of the inventive method is to inflate so that reduce soap blank density to cake soap, increases soap blank volume and floatability.
Another purpose of the inventive method is to increase admissible water-content in the cake soap.
The 3rd purpose of the present invention is by with in small, broken bits and equally distributed form air being added in the soap composition, to increase the light scattering effect of composition.
The 4th purpose of the present invention is the continuation method by the economy of having simplified common soap complete processing, produces with the cake soap of commercially available similar composition and compares the cake soap with advantageous characteristic.
In addition, the 5th purpose of the present invention is in the good control mode air to be added in the soap composition, so that the density of soap-cake has circulation ratio between 0.5 to 0.9 specific gravity range, and makes soap-cake have consistent quality and color.
This method has some advantages than prior art.
This method provides the density of the soap-cake that is easy to control, and promptly provides to have highly reproducible soap density, between 0.5 to 0.9.
This method has been improved the homogeneity of soap-cake composition, makes soap quality homogeneous.This method is convenient to air filled cavity and is dispersed in whole soap compositions, therefore the soap that obtains having good service performance and improved whiteness.Can make pure soap continuous charge with the inventive method, make finished product fertilizers soap blank water content in same range as at 28% and 35% common water composition.This method has shortened or has reduced drying and pressing steps that soap is produced, has therefore simplified the soap manufacture method, and the energy consumption in producing than common soap is low.This method has also been created condition for the adaptability that increases in the use of soap production unit.
Fig. 1 and 2 expresses the step of two kinds of schemes of this method.
With reference to Fig. 1 first method of the present invention is described. In the first step of the method, namely prepare the pure state soda soap with washroom soap character by method or the continuous processing of still according to common soap production method, so pure soap consists of 10% to 50% coconut oil and 90% to 50% tallow, moisture is 28% to 35% simultaneously.
Preservative agent and/or chelating agent include, but are not limited to tetrasodium ethylenediamine tetraacetate and Etidronic Acid, are sneaked into to maintain in 180 ℃ of pure soap of melting in the agitator to the temperature of 220 ℃ of F.
The soap material of melting is pumped in the melt mixer of water leg, is cooled to be higher than the mixture melting temperature. To include, but are not limited to the toluene di-tert-butyl phenol antioxidant and be dissolved in the spices, the antioxidant that will be dissolved in when the pure soap of above-mentioned melting is pumped into the feed hopper of Goodway charger in the spices adds in the pure soap of melting. This moment, pure soap preferably contained 30% moisture.
Make the blender continued operation, and with 90 pounds/cun2The air of pressure is introduced in the soap material, and high speed shear is mixed simultaneously. In according to the known method of the art that the soap injection soap making of inflation is framed.
With chilled soap cutting and with required mark impression, be transported to again in the packing machine (not shown) then.
With reference to Fig. 2 second method of the present invention described.
Preservative agent and/or chelating agent sneaked into maintain in 180 °F to the 220 °F pure soap of melting in the agitator under the temperature.
Antioxidant is dissolved in the spices, when the pure soap of above-mentioned melting is pumped into the feed hopper of Goodway charger, the above-mentioned antioxidant that is dissolved in the spices is added in the pure soap of melting.
Make the mixing tank operate continuously, and with 90 pounds/cun
2The air of pressure is introduced in the soap material, and high speed shear is mixed simultaneously.Then heat being inflated soap directly inserts in soap mould, tank therefor or other packing materials.After the soap cooling, packaging closures and notes are gone up mark.
According to method of the present invention, the density of product can be by regulating gas velocity, and the rate of pumping of blender end speed and Goodway mixing tank is controlled.Compare with 10% to 15% moisture content of general washroom soap obtain cake soap moisture up to 30%.
Because homodisperse bubble causes the light scattering effect that increases soap R-value (whiteness value) in bar soap, thus in this prescription, need not whitening agent, brightening agent or opalizer such as titanium dioxide, they are added into usually to improve the whiteness of washroom soap.
No matter be all can clearly observe intuitively or by MacBeth colorimeter reading, the whiteness of inflation soap-cake is equal to or greater than the whiteness of the washroom soap-cake of the made unaerated of the analogous composition that contains 0.5% titanium dioxide.(inflation soap R-value is 84.5, and the R-value that has the unaerated soap of 0.5% content of titanium dioxide in contrast to this is 79.2).
Owing to be dispersed in the characteristic of the high speed shear mixing that whole soap materials match with air filled cavity, improved the homogeneity of product greatly, the soap-cake of producing has commercial acceptable outward appearance aspect color and the surface texturisation.
Clearly, the used energy of the inventive method is lower than the energy of cake soap general under present manufacturing condition, and is convenient to reduce the preparation cost.
Another advantage of the inventive method is that it has saved and is generally used for extrusion machine and the moisture eliminator step of cake soap in producing.
The Goodway mixing tank is commercially available mixing tank, and by Goodway In-dustries, Inc, of Bohema, N, Y make and sell.
By following specific embodiment the present invention is described, but is not limited to these embodiment.
Embodiment 1
The pure soap that the preparation total amount is 30 pounds, it consists of 85% Tallow, beef and 15% Oleum Cocois, and moisture is 31.5%, and molten soap is moved in the Goodway mixing tank continuously, at this air is added in the soap, and high speed shear is mixed simultaneously.Heat inflation soap is made into big block and cooling, cuts into piece and packing.
Embodiment 2
The pure soap that the soda soap that the preparation total amount is 30 pounds is formed, it contains 70% Tallow, beef and 30% Oleum Cocois, and moisture is 30%.The preservatives that in molten soap, adds q.s.Add 1% to 1.4% soap scent, and this soap is moved on in the Goodway mixing tank immediately, at this air is added in the molten soap, high speed shear is mixed simultaneously.Inflation soap is continuously removed mixing tank, and moulding also makes it cooling.Refrigerative soap is cut into piece and packing.
Embodiment 3
The pure soap of 30 pounds of total amounts of preparation, it consists of 85% Tallow, beef and 15% Oleum Cocois, and moisture is 30%, makes the molten soap inflation according to the method for embodiment 1 and 2.Heat is inflated soap directly insert in the transparent container groove that has recessed icon indicia, cooling and encapsulation.
Has the character of washroom soap and the density that density is lower than water (density of the soap that can float) according to the prepared cake soap of aforesaid method.Soap-cake is very pure white, the general soap-cake big approximately 40% of its volume ratio identical weight.
The performance of the soap-cake that so obtains is better than having the washroom soap and the laundry soap-cake of similar composition, these performances are about improving the wearing quality of soap-cake, spending rate in the soap-cake use, the maintenance performance and the lathering power of soap blank shape and quality in the raising repeated use process.
Although invention has been described with regard to specific embodiments in an embodiment, but being to be understood that, the person skilled in the art under the situation that does not deviate from the spirit and scope of the invention, can make other changes and improvements of the present invention, as shown in the additional claim, these qualifications will be applied.
Claims (4)
1, a kind of preparation has the continuation method of the low density inflation soap of washroom soap character, and the step that this method comprises has:
A) preparation consists of 10-50% Oleum Cocois and 50-90% Tallow, beef, and moisture content is pure soap between 28% to 35%,
B) the molten soap material is added in the high speed shear mixing tank of operate continuously,
C) with 90 pounds/cun
2The continuous introducing air of pressure, make it to act on molten soap,
D) soap is put into soap make framed,
E) cooling, cutting, impression and package soap bars.
2, the process of claim 1 wherein the inflation before preservatives, spices and other ancillary components are added in the pure soap.
3, the process of claim 1 wherein:
A) preservatives is added in the pure soap,
B) in the melt mixer that is higher than the soap fusing point, soap is cooled off,
C) antioxidant and spices are added in the soap material,
D) above-mentioned material is added in the mixing tank aerator continuously,
E) while continuous introducing air in soap,
F) will inflate soap add soap make framed in,
G) cool off then, cut, impress and pack.
4, a kind of production has the continuation method of the low density inflation soap of washroom soap character, and the step that this method comprises has:
A) by the pure soap of claim 1 preparation,
B) the pure soap of fusion is pumped in the mixing tank aerator,
C) add preservatives simultaneously continuously, spices and other ancillary components,
D) with 90 pounds/cun
2The continuous introducing air of pressure and act on soap with it,
E) fusion is inflated soap and put into soap mould, ready-made plastic channel, or in other packing materials,
F) wrapper packaging container and marking.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US48680390A | 1990-03-01 | 1990-03-01 | |
| US486,803 | 1990-03-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1057481A true CN1057481A (en) | 1992-01-01 |
Family
ID=23933304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN91101921.9A Pending CN1057481A (en) | 1990-03-01 | 1991-02-28 | The continuation method of preparation low density cake soap |
Country Status (14)
| Country | Link |
|---|---|
| JP (1) | JPH04218599A (en) |
| CN (1) | CN1057481A (en) |
| AR (1) | AR245204A1 (en) |
| BG (1) | BG60595B1 (en) |
| BR (1) | BR9100796A (en) |
| CA (1) | CA2037310A1 (en) |
| CZ (1) | CZ280807B6 (en) |
| EG (1) | EG19135A (en) |
| HU (1) | HU210140B (en) |
| PL (1) | PL166591B1 (en) |
| RO (1) | RO106758B1 (en) |
| RU (1) | RU2039084C1 (en) |
| YU (1) | YU47164B (en) |
| ZA (1) | ZA911267B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7517843B2 (en) | 2000-09-22 | 2009-04-14 | Kao Corporation | Method for manufacturing soap products of a constant weight |
| CN103013722A (en) * | 2012-12-12 | 2013-04-03 | 合肥豪豪日化有限公司 | High water content compound laundry bar soap and preparation method thereof |
| CN103415607A (en) * | 2011-03-16 | 2013-11-27 | 荷兰联合利华有限公司 | Aerated soap bars |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN109234085A (en) * | 2018-08-16 | 2019-01-18 | 惠州兆婷化妆品有限公司 | A kind of floating soap and preparation method thereof |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE60115378T2 (en) * | 2000-09-22 | 2006-08-10 | Kao Corporation | PROCESS FOR THE PREPARATION OF SOAP CONTAINING AIR CONTAINERS |
| EP1239027B1 (en) | 2000-09-22 | 2006-01-25 | Kao Corporation | Method of manufacturing soap with air bubbles |
| GB0317257D0 (en) * | 2003-04-03 | 2003-08-27 | Unilever Plc | Improved detergent bar and process for manufacture |
| CN102459553A (en) * | 2009-06-04 | 2012-05-16 | 花王株式会社 | Framed soap composition |
| US9695388B2 (en) | 2012-03-04 | 2017-07-04 | Daniel H. Traynor | Soap with dispersed articles producing light and/or sound |
-
1991
- 1991-02-20 ZA ZA911267A patent/ZA911267B/en unknown
- 1991-02-27 RO RO147011A patent/RO106758B1/en unknown
- 1991-02-27 BG BG93938A patent/BG60595B1/en unknown
- 1991-02-27 BR BR919100796A patent/BR9100796A/en not_active Application Discontinuation
- 1991-02-28 AR AR91319136A patent/AR245204A1/en active
- 1991-02-28 EG EG12191A patent/EG19135A/en active
- 1991-02-28 PL PL91289238A patent/PL166591B1/en unknown
- 1991-02-28 HU HU91683A patent/HU210140B/en not_active IP Right Cessation
- 1991-02-28 CN CN91101921.9A patent/CN1057481A/en active Pending
- 1991-02-28 RU SU914894780A patent/RU2039084C1/en active
- 1991-02-28 CA CA002037310A patent/CA2037310A1/en not_active Abandoned
- 1991-02-28 YU YU35091A patent/YU47164B/en unknown
- 1991-03-01 CZ CS91548A patent/CZ280807B6/en unknown
- 1991-03-01 JP JP3035778A patent/JPH04218599A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7517843B2 (en) | 2000-09-22 | 2009-04-14 | Kao Corporation | Method for manufacturing soap products of a constant weight |
| CN103415607A (en) * | 2011-03-16 | 2013-11-27 | 荷兰联合利华有限公司 | Aerated soap bars |
| US8957004B2 (en) | 2011-03-16 | 2015-02-17 | Conopco, Inc. | Aerated soap bars |
| CN103415607B (en) * | 2011-03-16 | 2016-07-06 | 荷兰联合利华有限公司 | Inflation soap bar |
| CN103013722A (en) * | 2012-12-12 | 2013-04-03 | 合肥豪豪日化有限公司 | High water content compound laundry bar soap and preparation method thereof |
| CN103013722B (en) * | 2012-12-12 | 2015-01-21 | 合肥豪豪日化有限公司 | High water content compound laundry bar soap and preparation method thereof |
| CN105861202A (en) * | 2016-03-18 | 2016-08-17 | 杭州稞恩生物科技有限公司 | Floating soap and preparation method thereof |
| CN109234085A (en) * | 2018-08-16 | 2019-01-18 | 惠州兆婷化妆品有限公司 | A kind of floating soap and preparation method thereof |
| CN109234085B (en) * | 2018-08-16 | 2020-08-25 | 惠州兆婷化妆品有限公司 | Floating soap and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| YU47164B (en) | 1995-01-31 |
| JPH04218599A (en) | 1992-08-10 |
| PL166591B1 (en) | 1995-06-30 |
| HU210140B (en) | 1995-02-28 |
| BR9100796A (en) | 1991-11-05 |
| CA2037310A1 (en) | 1991-09-02 |
| YU35091A (en) | 1993-11-16 |
| CZ280807B6 (en) | 1996-04-17 |
| PL289238A1 (en) | 1991-11-04 |
| AR245204A1 (en) | 1993-12-30 |
| HU910683D0 (en) | 1991-09-30 |
| HUT57825A (en) | 1991-12-30 |
| CS9100548A2 (en) | 1991-09-15 |
| BG93938A (en) | 1993-12-24 |
| BG60595B1 (en) | 1995-09-29 |
| RU2039084C1 (en) | 1995-07-09 |
| RO106758B1 (en) | 1993-06-30 |
| EG19135A (en) | 1994-06-30 |
| ZA911267B (en) | 1992-10-28 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |