CN105733412A - Epoxy polysiloxane anticorrosive paint - Google Patents
Epoxy polysiloxane anticorrosive paint Download PDFInfo
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- CN105733412A CN105733412A CN201610312685.2A CN201610312685A CN105733412A CN 105733412 A CN105733412 A CN 105733412A CN 201610312685 A CN201610312685 A CN 201610312685A CN 105733412 A CN105733412 A CN 105733412A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an epoxy polysiloxane anticorrosive paint, and belongs to the field of fine chemical paints. The epoxy polysiloxane anticorrosive paint comprises a component A and a component B in a mass ratio of 100:(13-16), wherein the component A is prepared from the following raw materials in parts by weight: 30-45 parts of epoxy resin, 5.0-10.0 parts of epoxy polysiloxane, 6.0-10.0 parts of a reactive diluent, 1.0-2.0 parts of a silane coupling agent, 0.3-0.5 part of a thickening agent, 0.4-0.6 part of a dispersing agent, 0.2-0.4 part of a flatting agent, 0.2-0.4 part of a defoaming agent, 0.4-0.6 part of a plasticizer, 1.0-3.0 parts of a diluent, 5.4-16.8 parts of pigments and 29-38 parts of a filler; the component B is a cashew nut shell oil-modified amine curing agent. The paint is greatly improved in corrosion resistance, acid resistance, alkali resistance, heat resistance, weather resistance and the like, and has excellent adhesion, flexibility, solution resistance, and the like.
Description
Technical field
The invention belongs to fine chemistry industry technical field of coatings, be specifically related to a kind of epoxy polysiloxane anticorrosive paint.
Background technology
For a long time, Chinese Enterprise it is difficult to find all the time at international Atwind electric protection coating, Heavy-duty Coatings In Ocean Chemical Industry
Figure, at sea wind-powered electricity generation heavy antisepsis field, China's coatings enterprises is the most in full retreat.In the face of harsh building ring
Border, develops the high-performance coating with good anticorrosion and anti-wear performance, is that solution marine material corrodes and abrasion is asked
Inscribe one of maximally effective approach.The most domestic, annual because metal material corrosion or local corrosion are destroyed, cause
Equipment pipe leak suddenly or lose intensity, cause substantial amounts of accident and economic loss.
The stable development of China's economic, brings extensively for industries such as transportation, petrochemical industry, the energy, machineries
Wealthy development space, thus driven the development of relevant auxiliary products.Account for the deputy protective coating of Coating Market
In national economy, have very important effect, especially have relatively high-tech require Marine Antifouling Paint,
Container anticorrosive paint and industrial antisepsis coating will have good development prospect.Due to anticorrosive paint application surface
Extensively, position in industry is of crucial importance, the most significant to energy-saving and emission-reduction, and country encourages and supports anticorrosive paint
Technical research, production, it is contemplated that future portion routine anticorrosive paint production capacity will turn to anticorrosive paint.
Anticorrosive paint epoxy resin is as its excellent anti-corrosion resin, but its resistance to ag(e)ing, humidity resistance etc.
The most poor;Domestic current outdoor anticorrosion epoxy paint development is slow, and formula is less;Organic-silicon-modified resin valency
Lattice differ, and performance difference is obvious, and matured product is less.
Summary of the invention
For solving the problem that above-mentioned prior art exists, the invention provides a kind of epoxy polysiloxane anticorrosion and be coated with
Material, this anticorrosive paint has good salt fog resistance, resistance to acids and bases, ageing-resistant time, resistance to water, resistance to gasoline
The performances such as property, hardness, adhesive force, impact resistance, pliability, wearability and thermostability.
For realizing object above: technical scheme is as follows:
A kind of epoxy polysiloxane anticorrosive paint, is made up of first component and second component, first component and the matter of second component
Amount ratio is 100:13-16, and described first component is made up of the raw material of following weight portion: epoxy resin 30-45 part,
Epoxy radicals polysiloxanes 5.0-10.0 part, reactive diluent 6.0-10.0 part, silane coupler 1.0-2.0 part, increasing
Thick dose of 0.3-0.5 part, dispersant 0.4-0.6 part, levelling agent 0.2-0.4 part, defoamer 0.2-0.4 part, plasticising
Agent 0.4-0.6 part, diluent 1.0-3.0 part, pigment 5.4-16.8 part, filler 29-38 part;Described second group
It is divided into cashew nut oil modified amine hardener.
The epoxide number of described epoxy resin is 0.30-0.0, and softening point is 20-35 DEG C.
Described epoxy resin is E-44 type epoxy bisphenol A type epoxy resin, E-51 type epoxy bisphenol A-type ring
One in epoxy resins, AL-3040 type bisphenol-A epoxy resin, C40 type cardanol epoxy resin or
The compositions of 2-4 kind.
Described epoxy radicals polysiloxanes is SMH-30 type epoxy radicals polysiloxanes.
Described reactive diluent is butyl glycidyl ether, phenyl glycidyl ether, tetramethylolmethane (+)-2,3-Epoxy-1-propanol
Ether, polyethyleneglycol diglycidylether, trihydroxymethylpropanyltri diglycidyl ether, polypropylene glycol diglycidyl
Ether or T 55 is a kind of or the compositions of 2-7 kind.
Described silane coupler is 3-glycydoxy trimethoxy silane or 3-glycidyl ether
One or both compositions in epoxide propyl-triethoxysilicane;
Described thickening agent is selected from aerosil or bentonite;
Described dispersant is BYK-P104 dispersant;
Described levelling agent is BYK-373 levelling agent;
Described defoamer is BYK-054 defoamer;
Described plasticizer is dibutyl phthalate;
Described diluent is a kind of or 2-3 kind in propylene glycol monomethyl ether, propandiol butyl ether or propylene glycol phenylate
Compositions;
Described filler is that glass flake, barium sulfate, mica powder, Pulvis Talci, graphite powder, zinc phosphate or silicon are micro-
A kind of or the mixture of 2-7 kind arbitrary proportion in powder.
Described pigment is the mixed of a kind of or 2-3 kind arbitrary proportion in titanium dioxide, aluminium triphosphate, iron oxide red
Compound.
Described cashew nut oil modified amine hardener is the cashew nut oil modified amine hardener of ZY-5010.
A kind of preparation method of epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 50-60 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, be sequentially added into silane coupler, pigment, filler, thickening agent, dispersant,
Levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, by activity
It is viscous that diluent carries out tune, after being cooled to room temperature, obtains first component;
(3) by cashew nut oil modified for second component amine hardener, with first constituent mass than 13:100-16:100, stirring is mixed
Close and use.
The technique effect that the present invention is useful: the present invention is a kind of epoxy polysiloxane anticorrosive paint, and it utilizes hydrogenation
The polysiloxane-modified coating of bisphenol A epoxide resin, epoxy radicals, can apply and the low paint of anticorrosion, intermediate coat, finish paint;
Improving a lot at corrosion-resistant, acidproof, alkaline-resisting, thermostability, weatherability etc. prepared by this formula;Have simultaneously
The aspects such as standby excellent adhesive force, pliability and endurance.
Detailed description of the invention:
Embodiment 1:
A kind of epoxy polysiloxane anticorrosive paint.It is made up of the raw material of following weight portion:
The preparation method of above-mentioned epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 60 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, it is sequentially added into silane coupler, pigment, filler, thickening agent, dispersion
Agent, levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, use
It is viscous that reactive diluent carries out tune, after being cooled to room temperature, obtains first component.
(3) by first component and the cashew nut oil modified amine hardener of second component, before using, mixing makes according to the above ratio
With.
Embodiment 2:
A kind of epoxy polysiloxane anticorrosive paint.It is made up of the raw material of following weight portion:
The preparation method of above-mentioned epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 60 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, it is sequentially added into silane coupler, pigment, filler, thickening agent, dispersion
Agent, levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, use
It is viscous that reactive diluent carries out tune, after being cooled to room temperature, obtains first component.
(3) by first component and the cashew nut oil modified amine hardener of second component, before using, mixing makes according to the above ratio
With.
Embodiment 3:
A kind of epoxy polysiloxane anticorrosive paint.It is made up of the raw material of following weight portion:
The preparation method of above-mentioned epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 55 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, it is sequentially added into silane coupler, pigment, filler, thickening agent, dispersion
Agent, levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, use
It is viscous that reactive diluent carries out tune, after being cooled to room temperature, obtains first component.
(3) by first component and the cashew nut oil modified amine hardener of second component, before using, mixing makes according to the above ratio
With.
Embodiment 4:
A kind of epoxy polysiloxane anticorrosive paint.It is made up of the raw material of following weight portion:
The preparation method of above-mentioned epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 55 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, it is sequentially added into silane coupler, pigment, filler, thickening agent, dispersion
Agent, levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, use
It is viscous that reactive diluent carries out tune, after being cooled to room temperature, obtains first component.
(3) by first component and the cashew nut oil modified amine hardener of second component, before using, mixing makes according to the above ratio
With.
Embodiment 5:
A kind of epoxy polysiloxane anticorrosive paint.It is made up of the raw material of following weight portion:
The preparation method of above-mentioned epoxy polysiloxane anticorrosive paint, its step is as follows:
(1) being mixed with epoxy radicals polysiloxanes by epoxy resin by proportioning, heating and temperature control is carried out at 50 DEG C
Dissolve;
(2) by above-mentioned hybrid resin, it is sequentially added into silane coupler, pigment, filler, thickening agent, dispersion
Agent, levelling agent, defoamer, plasticizer and diluent carry out high speed dispersion, are ground to particle diameter 50 microns, use
It is viscous that reactive diluent carries out tune, after being cooled to room temperature, obtains first component.
(3) by first component and the cashew nut oil modified amine hardener of second component, before using, mixing makes according to the above ratio
With.
Each embodiment and blank group are tested according to following standard: salt spray resistance testing standard: GB/T
The mensuration of 1771 2007 paint and varnish resistance to neutral salt spray performance;Acidproof, alkaline-resisting, toluene, acetone, second
The chemical reagent testing standard such as alcohol, methanol: the survey of GB/T11547-2008 plastics resistant to liquid chemical reagent performance
Fixed;Ageing-resistant time test standard: GB/T 1865-2009 paint and varnish artificial weathering aging and artificial spoke
Penetrate and expose to the open air;Water resistance test standard: GB/T 1,733 1993 paint film resistance to water algoscopy;Resistance to gasoline, resistance to bavin
Oil testing standard: GB-T 1734-1993 paint film petrol-resistance algoscopy;Hardness test standard: GB/T
6739 2006 paint and varnish pencil methods measure hardness of paint film;Adhesive force test testing standard: GB/T
6739-2006 " paint and varnish pencil method measures hardness of paint film ";Impact resistance testing standard: GB/T
1732 1993 paint film impact resistance algoscopys;Pliability testing standard: GB/T 1,731 1993 paint film is pliable and tough
Property algoscopy;The mensuration of wearability test standard: GB/T 1,768 2006 paint and varnish wearability rotates
Elastic grinding wheel method;Thermostability testing standard: GB/T 1735-1979 paint film Heat-tolerance Determination method;Its result is such as
Under:
Claims (9)
1. an epoxy polysiloxane anticorrosive paint, it is made up of first component and second component, it is characterized in that: first component is 100:13-16 with the mass ratio of second component, and described first component is made up of the raw material of following weight portion: epoxy resin 30-45 part, epoxy radicals polysiloxanes 5.0-10.0 part, reactive diluent 6.0-10.0 part, silane coupler 1.0-2.0 part, thickening agent 0.3-0.5 part, dispersant 0.4-0.6 part, levelling agent 0.2-0.4 part, defoamer 0.2-0.4 part, plasticizer 0.4-0.6 part, diluent 1.0-3.0 part, pigment 5.4-16.8 part, filler 29-38 part;Described second component is cashew nut oil modified amine hardener.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: the epoxide number of described epoxy resin is 0.30-0.0, and softening point is 20-35 DEG C;Epoxy resin is a kind of or compositions of 2-4 kind in E-44 type epoxy bisphenol A type epoxy resin, E-51 type epoxy bisphenol A type epoxy resin, AL-3040 type bisphenol-A epoxy resin, C40 type cardanol epoxy resin.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described epoxy radicals polysiloxanes is SMH-30 type epoxy radicals polysiloxanes.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described reactive diluent is butyl glycidyl ether, phenyl glycidyl ether, tetramethylolmethane glycidyl ether, polyethyleneglycol diglycidylether, trihydroxymethylpropanyltri diglycidyl ether, polypropylene glycol diglycidyl ether or T 55 is a kind of or the compositions of 2-7 kind.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described silane coupler is one or both the compositions in 3-glycydoxy trimethoxy silane or 3-glycydoxy triethoxysilane.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described thickening agent is selected from aerosil or bentonite;Described dispersant is BYK-P104 dispersant;Described levelling agent is BYK-373 levelling agent;Described defoamer is BYK-054 defoamer;Described plasticizer is dibutyl phthalate;Described diluent is a kind of or compositions of 2-3 kind in propylene glycol monomethyl ether, propandiol butyl ether or propylene glycol phenylate.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described filler is a kind of or mixture of 2-7 kind arbitrary proportion in glass flake, barium sulfate, mica powder, Pulvis Talci, graphite powder, zinc phosphate or silicon powder.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described pigment is a kind of or mixture of 2-3 kind arbitrary proportion in titanium dioxide, aluminium triphosphate, iron oxide red.
A kind of epoxy polysiloxane anticorrosive paint the most according to claim 1, it is characterised in that: described cashew nut oil modified amine hardener is the cashew nut oil modified amine hardener of ZY-5010.
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CN106237798A (en) * | 2016-08-31 | 2016-12-21 | 芜湖恒耀汽车零部件有限公司 | The inner wall anti-corrosive coating of boiler waste gas purification device water tank |
CN106349881A (en) * | 2016-08-31 | 2017-01-25 | 芜湖恒耀汽车零部件有限公司 | Preparation method of inner wall corrosion-resistant coating of water tank for boiler exhaust gas purification device |
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