CN105732083B - A method of with cow dung dry method baking ceramsite - Google Patents

A method of with cow dung dry method baking ceramsite Download PDF

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Publication number
CN105732083B
CN105732083B CN201610014497.1A CN201610014497A CN105732083B CN 105732083 B CN105732083 B CN 105732083B CN 201610014497 A CN201610014497 A CN 201610014497A CN 105732083 B CN105732083 B CN 105732083B
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cow dung
bentonite
temperature
dry method
baking ceramsite
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CN105732083A (en
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韩新宇
史建武
吴玉珍
刘树银
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/009Porous or hollow ceramic granular materials, e.g. microballoons

Abstract

The present invention relates to a kind of methods with cow dung dry method baking ceramsite, belong to haydite manufacture technology field.The present invention includes step:Batch mixing, granulation, pretreatment, high-temperature roasting, cooling.Haydite density that the present invention produces is small, portion's hole is more, form and ingredient are uniform, and intensity is high, wear-resistant, and has good corrosion resistance, freeze-proof, shock resistance and insulating, and heat preservation, heat-insulated, sound insulation, moisture resistance are suitable for the fields such as building trade.

Description

A method of with cow dung dry method baking ceramsite
Technical field
The present invention relates to a kind of methods with cow dung dry method baking ceramsite, belong to haydite manufacture technology field.
Background technology
Haydite density is small, portion's hole is more, form and ingredient are uniform, and intensity is high, wear-resistant, and with good anticorrosive Property, freeze-proof, shock resistance and insulating(Heat preservation, heat-insulated, sound insulation, moisture resistance), so be widely used in building materials, agricultural, Industry, gardening, fire-resistant heat insulating material, environmental project and other field.Currently, there are many method of production haydite, the use such as Zhu Xiang Sludge, cow dung wet method has burnt out Superlight ceramsites, but embryo material moisture content itself is high, has a large amount of vapor to go out in drying process It is existing, so that product is cracked, intensity is relatively low, and water absorption rate is higher, and technique is more complex;The flyash such as Du Xin, clay and sludge dry method Burn out high-strength ceramic granule, but cost is higher, and current clay has become China and needs resources to be protected.Therefore, existing The method for producing haydite is not ideal enough.
Invention content
The present invention provides a kind of method with cow dung dry method baking ceramsite, solve because occurring in the drying process big Amount vapor and make that haydite density is big, water absorption rate is higher, compression strength is relatively low, and preparation method is complicated, and cost is higher, with country The technical problems such as the clay resource of protection.And raw material is waste, it can be achieved that refuse reclamation, while being replaced with bentonite glutinous Soil has saved resource.
The technical scheme is that:A method of it is described to fire pottery with cow dung dry method with cow dung dry method baking ceramsite The method of grain is as follows:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, Bentonite, cow dung are 4 by weight:1 ratio is stirred;Cow dung used is the discarded cow dung in vaccary, and cow dung is existed It dries at 100~110 DEG C, is then crushed with pulverizer, then the cow dung that size is 80~120 mesh is filtered out with sieve;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure is 6.5~8.0Mpa, Dwell time is 20~35s, is pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, temperature be 300~ Puffing 10~30min is dried at 400 DEG C;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1180~1220 DEG C, by dry it is puffing after material constant temperature burn it is swollen 10~20min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
The beneficial effects of the invention are as follows:
Haydite density that the present invention burns out is small, portion's hole is more, form and ingredient are uniform, and intensity is high, wear-resistant, and has Good corrosion resistance, freeze-proof, shock resistance and insulating (heat preservation, heat-insulated, sound insulation, moisture resistance), density, resists water absorption rate Compressive Strength meets national standard.Preparation method is simple, at low cost, it is easy to accomplish continuous production, product quality are stablized, do not polluted It is environment, corrosion-free, and raw material is waste, it can be achieved that refuse reclamation, while clay is replaced with bentonite, save resource.
Specific implementation mode
Embodiment 1:A method of with cow dung dry method baking ceramsite, the tool of the method with cow dung dry method baking ceramsite Steps are as follows for body:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, Bentonite, cow dung are 4 by weight:1 ratio is stirred, you can 80 parts of bentonite of selection, 20 parts of cow dung are stirred; Cow dung used is the discarded cow dung in vaccary, and cow dung is dried at 100 DEG C, is then crushed with pulverizer, then sieved with sieve Select the cow dung that size is 80 mesh;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure 6.5Mpa, when pressurize Between be 35s, be pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, is 400 DEG C in temperature The lower puffing 20min of drying;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1180 DEG C, by dry it is puffing after material constant temperature burn swollen 20min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
Performance indicator such as table 1 after testing:
Table 1
It can be seen that from the performance of table 1:The haydite density burnt out with this condition is smaller, and internal void is more, water suction Rate is relatively low, and compression strength is higher, and form and ingredient are uniform.Since preheating time is moderate, Bear-grudge material, which are warmed, reaches best viscosity, Play foaming effect.
Embodiment 2:A method of with cow dung dry method baking ceramsite, the tool of the method with cow dung dry method baking ceramsite Steps are as follows for body:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, Bentonite, cow dung are 4 by weight:1 ratio is stirred, you can 80 parts of bentonite of selection, 20 parts of cow dung are stirred; Cow dung used is the discarded cow dung in vaccary, and cow dung is dried at 110 DEG C, is then crushed with pulverizer, then sieved with sieve Select the cow dung that size is 100 mesh;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure 7.5Mpa, when pressurize Between be 20s, be pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, is 350 DEG C in temperature The lower puffing 10min of drying;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1200 DEG C, by dry it is puffing after material constant temperature burn swollen 15min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
Performance indicator such as table 2 after testing:
Table 2
It can be seen that from the performance of table 2:The haydite density burnt out with this condition is smaller, and internal void is more, water suction Rate is relatively low, and compression strength is higher, and form and ingredient are uniform.Since sintering temperature is suitable, the gas of sufficient amount is generated in Bear-grudge bodies Make its dilatancy, Bear-grudge bodies melting amount of liquid phase is very big, and the effect of liquid phase surface tension is moderate, and solid particle is due to liquid phase surface Power and it is close to each other, liquid phase be filled into gas make Bear-grudge bodies be densified.
Embodiment 3:A method of with cow dung dry method baking ceramsite, the tool of the method with cow dung dry method baking ceramsite Steps are as follows for body:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, Bentonite, cow dung are 4 by weight:1 ratio is stirred, you can 80 parts of bentonite of selection, 20 parts of cow dung are stirred; Cow dung used is the discarded cow dung in vaccary, and cow dung is dried at 110 DEG C, is then crushed with pulverizer, then sieved with sieve Select the cow dung that size is 120 mesh;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure 8.0Mpa, when pressurize Between be 30s, be pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, is 300 DEG C in temperature The lower puffing 30min of drying;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1220 DEG C, by dry it is puffing after material constant temperature burn swollen 10min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
Performance indicator such as table 3 after testing:
Table 3
It can be seen that from the performance of table 3:The haydite density burnt out with this condition is smaller, and internal void is more, water suction Rate is relatively low, and compression strength is higher, and form and ingredient are uniform.Preheating temperature does not have much influence the firing of haydite.
Embodiment 4:A method of with cow dung dry method baking ceramsite, the tool of the method with cow dung dry method baking ceramsite Steps are as follows for body:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, Bentonite, cow dung are 4 by weight:1 ratio is stirred, that is, is selected 80 parts of bentonite, 20 parts of cow dung, be stirred;Institute Cow dung is the discarded cow dung in vaccary, and cow dung is dried at 105 DEG C, is then crushed with pulverizer, then screened with sieve Go out the cow dung that size is 100 mesh;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure 7.5Mpa, when pressurize Between be 30s, be pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, is 350 DEG C in temperature The lower puffing 20min of drying;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1200 DEG C, by dry it is puffing after material constant temperature burn swollen 15min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
Performance indicator such as table 4 after testing:
Table 4
It can be seen that from the performance of table 4:The haydite density burnt out with this condition is smaller, and internal void is more, water suction Rate is relatively low, and compression strength is higher, and form and ingredient are uniform.Since sintering time is excessively suitable, the micropore phase of not unicom will not be made It connects, to form big stomata, compression strength is made not reduce.
The specific implementation mode of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula can also be made without departing from the purpose of the present invention within the knowledge of a person skilled in the art Go out various change.

Claims (1)

1. a kind of method with cow dung dry method baking ceramsite, it is characterised in that:The method with cow dung dry method baking ceramsite It is as follows:
Step1, batch mixing;Auxiliary material cow dung is added in major ingredient bentonite, forms material, which includes bentonite, cow dung, swelling Soil, cow dung are 4 by weight:1 ratio is stirred;Cow dung used is the discarded cow dung in vaccary, by cow dung 100~ It dries at 110 DEG C, is then crushed with pulverizer, then the cow dung that size is 80~120 mesh is filtered out with sieve;
Step2, granulation;By the material mixed powder compressing machine compression moulding, briquetting pressure is 6.5~8.0MPa, pressurize Time is 20~35s, is pressed into a diameter of 30mm, the cylinder of a height of 10mm;
Step3, pretreatment;The material of compression moulding is placed in crucible, then is moved into Muffle furnace, is 300~400 DEG C in temperature The lower puffing 10~30min of drying;
Step4, high-temperature roasting;So that Muffle furnace is warming up to 1180~1220 DEG C, by dry it is puffing after material constant temperature burn it is swollen 10~ 20min;
Step5, cooling;By the material cooled to room temperature of high-temperature roasting, haydite finished product is obtained.
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Publication number Priority date Publication date Assignee Title
CN107311587B (en) * 2017-06-28 2019-11-08 昆明理工大学 A method of ceramsite board is made with ardealite and cow dung
CN109400108A (en) * 2018-11-06 2019-03-01 海安南京大学高新技术研究院 A kind of preparation method of light, and high-strength fly-ash haydite
CN111302762A (en) * 2020-03-09 2020-06-19 重庆财山建材有限公司合川分公司 Expanded ceramsite and manufacturing method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101613219A (en) * 2009-07-31 2009-12-30 柳树 A kind of method of utilizing mud and cow dung to make haydite
CN105130397A (en) * 2015-07-13 2015-12-09 昆明理工大学 Novel ceramisite and preparation method thereof

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JP2008266263A (en) * 2007-04-24 2008-11-06 N M G Environmental Development Co Ltd Method for treating livestock feces

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Publication number Priority date Publication date Assignee Title
CN101613219A (en) * 2009-07-31 2009-12-30 柳树 A kind of method of utilizing mud and cow dung to make haydite
CN105130397A (en) * 2015-07-13 2015-12-09 昆明理工大学 Novel ceramisite and preparation method thereof

Non-Patent Citations (1)

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